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Gujarat Technological University

This document contains instructions for a Materials Characterization exam given at Gujarat Technological University. The exam contains 5 questions worth a total of 70 marks. Question 1 asks students to describe the importance of material characterization, define optical microscopy and its types, and explain the principle and instrumentation of a rotary pump. Question 2 asks students to classify material characterization techniques, define microscope resolution and explain a formula, and discuss the principle and instrumentation of a Pirani gauge or thermogravimetric analysis. Question 3 contains similar questions about vacuum ranges, differential scanning calorimetry, and the components and working of a scanning electron microscope. Question 4 asks about the differences between DSC and DTA, diffraction patterns in TEM,

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59 views1 page

Gujarat Technological University

This document contains instructions for a Materials Characterization exam given at Gujarat Technological University. The exam contains 5 questions worth a total of 70 marks. Question 1 asks students to describe the importance of material characterization, define optical microscopy and its types, and explain the principle and instrumentation of a rotary pump. Question 2 asks students to classify material characterization techniques, define microscope resolution and explain a formula, and discuss the principle and instrumentation of a Pirani gauge or thermogravimetric analysis. Question 3 contains similar questions about vacuum ranges, differential scanning calorimetry, and the components and working of a scanning electron microscope. Question 4 asks about the differences between DSC and DTA, diffraction patterns in TEM,

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Seat No.: ________ Enrolment No.

___________

GUJARAT TECHNOLOGICAL UNIVERSITY


BE - SEMESTER– VII (NEW) EXAMINATION – WINTER 2021
Subject Code:2172109 Date:03/12/2021
Subject Name:Materials Characterization
Time:02:30 PM TO 05:00 PM Total Marks: 70
Instructions:
1. Attempt all questions.
2. Make suitable assumptions wherever necessary.
3. Figures to the right indicate full marks.
4. Simple and non-programmable scientific calculators are allowed.

MARKS

Q.1 (a) Describe the importance of Material characterization. 03


(b) What is optical microscopy? List the types of microscopes. 04
(c) Explain the principle and instrumentation of rotary pump. 07
Q.2 (a) Classify Material characterization techniques. 03
(b) What is resolution of Microscope? Explain using the formula. 04
(c) Explain the principle and instrumentation of Pirani gauge with their merits, 07
limitations and applications.
OR
(c) Discuss thermogravimetric analysis technique. 07

Q.3 (a) Write different Vacuum range. 03


(b) Discuss applications of Differential scanning calorimetry. 04
(c) Draw schematic showing basic components of the scanning electron microscope. 07
Briefly explain each component and its working in SEM.
OR
Q.3 (a) What do you meant by thermal analysis? Give its significance. 03
(b) Explain Hot Stage Microscopy. 04
(c) Discussmicrostructural study by image analysis. What are its applications? 07

Q.4 (a) Give the difference between DSC and DTA. 03


(b) Discuss- Diffraction pattern in TEM. 04
(c) Explain the principle and working of Rutherford backscattering spectroscopy 07
(RBS). Write applications and limitations.
OR
Q.4 (a) What is electron microscopy? How it differs from optical microscopy? 03
(b) What is STEM? How it differs from conventional TEM? Write applications. 04
(c) What do you mean by AFM? Explain the principle and instrumentation. Give 07
merits, limitations and applications.

Q.5 (a) What is Spectroscopy? Write their classification. 03


(b) Derive Bragg’s law. How it is useful to study crystal structure? 04
(c) What do you mean by photoelectron spectroscopy? Explain the principle and 07
instrumentation of XPS.
OR
Q.5 (a) What is X-ray diffraction? How it is useful in material characterization? 03
(b) Explain briefly Laue method of diffraction. 04
(c) Discuss Electron Probe Mico Analysis (EPMA) in terms of instrumentation and 07
working principle using line diagram.
**************

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