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IMA Question Paper Anna University

IMA Question Paper May/June 2022

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0% found this document useful (0 votes)
169 views2 pages

IMA Question Paper Anna University

IMA Question Paper May/June 2022

Uploaded by

rahul singh
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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la[zl zi sl2 Jo] 2[o| slo [sf] Rog. N Question Paper Code : 20373 B.B/1Tech, DEGREE EXAMINATIONS, APRILMAY 2022, Fourth/fth semester Chemical tingineering (CH 8191 — INSTRUMENTAL, METHODS OF ANALYSIS a] Engineering) (Common to Chemical and Blectroche! (Regulations 2017) Maximum : 100 marks Time : Three hours Answer ALL, questions. PART A — (10 « 2 = 20 marks) gant 2 Differentiate analytical and instrumental Distinguish between single and double beam spectrophotometer Differentiate calibration and standardization ‘The transmittance of 3x10™ M solution in a 1 cm cell is 19.2%. Calculate absorption and absorption co-efficient. What is turbidity? How it is expressed? Why water cannot be used as a medium to record IR spectra of samples? Whatis the significance of fingerprint region in IR spectroscopy? What is carrier gas? What is the use of gradient elution in column chromatography? PART B— (6 x L 65 marks) 11. (a) Explain the different types of radiation sources used in analytical 3) instruments. “ Or Concentration of sample is directly proportional to sworn Milica and derive an expression for the same. * a & te _ (b) sctrophotometer. 12, (a) Describe the working model of double beam visible 9 a3) or max rules and Wodward-Fieser rules for xima. aa) (b) Explain the Epsilon determining absorption 18. (a) Summarize any four quantitative applications of UV-Visible spectroscop (13) Or (b) What is calibration? Explain in detail the most calibration of instrumental methods. a3) 14. (a) Explain the principle, instrumentation, advantages and disadvantages of cay Infrared spectrophotometer. Or (b) Write briefly about the IR radiation sources. Describe the qualitative analysis of alkanes, alken?® and carbonyl compounds using IR spectroscopy. a3) 15. (a) Explain the working principl: (Gas chromatography and add a note on the applications of various columns and detectors used sy Or given in mMoles/litzes. Caleulate Risen My suValso determineMhich anelytolwilllhave'a loner time? 8) e - a, of analyte Cs Gm ne K rn M4 A Cee Cs [Co= elt AnalyteA 10 7 Analyte 7 10 L => nt ii) ‘The molar absorptive of a particular solute is 2x10". Calculate the SG [Cn transmittance through 2 curveted with a 5.00 em light path for a B= OS 210° ff) solution. @ => F/Io Ce (b) Explain the application of chromatography in complete demineralization Oy a of water. 7 (a5) \sRBe 0 mp s x

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