Designation: C658 − 98 (Reapproved 2012)

Standard Specification for

Chemical-Resistant Resin Grouts for Brick or Tile1
This standard is issued under the fixed designation C658; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.

1. Scope C723 Practice for Chemical-Resistant Resin Grouts for

1.1 This specification covers the requirements for chemical- Brick or Tile
resistant resin grouts for filling joints of chemical-resistant C904 Terminology Relating to Chemical-Resistant Nonme-
brick or tile units. For use of these materials, see Practice tallic Materials
C723. (For mortars, see Specification C395.) 3. Terminology
1.2 The values stated in inch-pound units are to be regarded 3.1 Definitions—For definitions of terms used in this
as standard. The values given in parentheses are mathematical specification, see Terminology C904.
conversions to SI units that are provided for information only
and are not considered standard. 4. Types of Resins, Fillers, and Setting Agents
NOTE 1—Resin grouts and mortars are differentiated as follows: Resin 4.1 The liquid resins may be furan, epoxy, vinyl ester, or
grouts are applied to the joints, generally 1⁄4 in. (6 mm) wide, after the others capable of forming chemical-resistant grout when mixed
brick or tile are set in place and the setting bed has hardened (grouting or with a suitable setting agent and filler.
tilesetter’s method). Resin mortars are trowelled onto the brick or tile in
sufficient quantity to achieve a 1⁄8-in. (3-mm) thick joint after the brick or 4.2 The fillers may be silica, carbon, or other chemical
resistant materials. Fillers may be supplied as a separate

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tile are laid in place (buttering or bricklayer’s method).
component or can be combined as a premix with the liquid
2. Referenced Documents resin and/or setting agent.
2.1 ASTM Standards:2 4.3 The setting agents may include amines, polyamides,
C307 Test Method for Tensile Strength of Chemical- peroxides, acids, or other reactants. Setting agents may be
Resistant Mortar, Grouts, and Monolithic Surfacings supplied as a separate component to be incorporated into the
C308 Test Methods for Working, Initial Setting, and Service resin and filler at the time of mixing or may be supplied as a
Strength Setting Times of Chemical-Resistant Resin Mor- constituent of the filler.
tars
C395 Specification for Chemical-Resistant Resin Mortars 5. General Requirements
C413 Test Method for Absorption of Chemical-Resistant 5.1 When these components are mixed at 65 to 85°F (18 to
Mortars, Grouts, Monolithic Surfacings, and Polymer 29°C) they form a uniform and flowable grout. The mixed
Concretes grout shall be of a viscosity such that it will readily flow to the
C531 Test Method for Linear Shrinkage and Coefficient of full depth of the open joint.
Thermal Expansion of Chemical-Resistant Mortars,
5.2 The filler shall have properly graded particles, not
Grouts, Monolithic Surfacings, and Polymer Concretes
exceeding 1⁄32 in. (1 mm), that will permit the filling of a
C579 Test Methods for Compressive Strength of Chemical-
minimum joint width of 3 ⁄16 in. (5 mm).
Resistant Mortars, Grouts, Monolithic Surfacings, and
Polymer Concretes 5.3 The service limitations of the grout shall be defined by
the manufacturer.
1
This specification is under the jurisdiction of ASTM Committee C03 on 6. Physical Requirements
Chemical-Resistant Nonmetallic Materialsand is the direct responsibility of Sub-
6.1 Chemical-resistant resin tile grouts prepared from these
committee C03.02 on Monolithics, Grouts and Polymer Concretes.
Current edition approved Aug. 1, 2012. Published September 2012. Originally materials shall conform to the physical requirements prescribed
approved in 1970. Last previous edition approved in 2008 as C658 – 98 (2008). in Table 1.
DOI: 10.1520/C0658-98R12.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or 7. Test Methods
contact ASTM Customer Service at [email protected]. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on 7.1 Determine the properties enumerated in this specifica-
the ASTM website. tion in accordance with the following methods:

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1
 C658 − 98 (2012)
TABLE 1 Physical Requirements at 73 ± 4°F (23 ± 2°C) 7.1.5 Linear Shrinkage— Test Method C531.
Furan Resin Epoxy Resin Vinyl Ester
Grout Grout Resin Grout 8. Rejection
Initial setting time, max, h 10 16 10 8.1 The grout may be rejected if it fails to meet any of the
Service strength setting time, 7 7 7
max, days requirements of this specification.
Compressive strength, 7 days, 4000 (28) 7500 (52) 7500 (52)
min, psi (MPa) 9. Packaging and Package Marking
Tensile strength, 7 days, min, 600 (4) 1200 (8) 1300 (9)
psi (MPa)
9.1 Each component shall be packaged to prevent deterio-
Water absorption, max,% 0.5 0.5 0.4 ration in storage and shall be labeled in such a manner to
Linear Shrinkage, 7 days, 1.0 0.4 1.0 indicate clearly the other components with which it is to be
max,%
used.
9.2 The supplier, at his discretion and responsibility, may
indicate on the package that the product contained therein
7.1.1 Setting Time— Test Method C308. meets the requirements of this specification.
7.1.2 Compressive Strength—Test Method C579.
7.1.3 Tensile Strength— Test Method C307. 10. Keywords
7.1.4 Water Absorption— Test Method C413. 10.1 brick; chemical-resistant; grout; tile

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