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User Manual DTrite Version 4

This user manual provides instructions for unpacking, assembling, operating, and maintaining the dTrite Electronic Titrator. The dTrite is a digital titrating instrument that delivers accurate and precise bottle-top titration. It has a volume range of 0.01mL-99.99mL and includes components like the titrating pipe, controller, magnetic stirrer, and accessories. The manual describes the parts, provides assembly steps, and explains basic operation and function settings. It also covers calibration, cleaning, troubleshooting, storage, and warranty information.

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Edgardo Bonilla
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© © All Rights Reserved
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0% found this document useful (0 votes)
374 views45 pages

User Manual DTrite Version 4

This user manual provides instructions for unpacking, assembling, operating, and maintaining the dTrite Electronic Titrator. The dTrite is a digital titrating instrument that delivers accurate and precise bottle-top titration. It has a volume range of 0.01mL-99.99mL and includes components like the titrating pipe, controller, magnetic stirrer, and accessories. The manual describes the parts, provides assembly steps, and explains basic operation and function settings. It also covers calibration, cleaning, troubleshooting, storage, and warranty information.

Uploaded by

Edgardo Bonilla
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
You are on page 1/ 45

User Manual

dTrite Electronic Titrator


Content
1. Unpacking ............................................................1
2. Overview ..............................................................2
3. Parts Description ................................................3
4. Assembly Instruction ........................................10
5. Operation ...........................................................16
6. Function Setting ................................................21
7. Accessories .......................................................23
8. Calibration .........................................................29
9. Cleaning and Maintenance .............................30
10. Trouble Shooting ............................................35
11. Storage ............................................................. 37
12. Warranty ..........................................................38
13. Limitations and Compatibility ........................38
Safety Reminder
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CAUTION:Possible damage to instrument.


Caution notes indicate any condition or practice,
which if not strictly observed or remedied, could
result in damage or destruction of the instrument.
1. Unpacking

Apart from the user manual, the dTrite package


should contain the following items.

dTrite Electronic Titrator Include:


Titrating pipe X1
Titrating pipe cover X1
dTrite X1
AC Adapter X 1
Controller X 1
Controller cable USB X 2
Bottle Adapter X 5(GL32; GL38; GL28; GL25; S40)
Magnetic Stirrer X 1
 Remote Titrating pipe X 1
Remote Control Handle X 1
Stirrer Bar(20mm)X 1
Filling valve X 1
Dispensing valve X 1
Filling pipe X 2
Installation tools X 1
Stander

Please check that all the items are present and inform
your supplier immediately if any of the above is missing.

1
2. Overview

A digital titrating instrument, dTrite delivers accurate


and precise bottle-top titration.
Please refer to "Limitations and Compatibility" for liquid
compatibility prior to operation.

2.1 Specification
0.01mL-99.99mL
Volume Range
Increment 10μL
R= 0.2%
Precision
CV=0.07%
Velocity 16 Stages
Capacity:4000mA/h
Fully charged in 4 hours
Battery
(please use standard charger)
working time:about 5 hours

2.2 Limitations of Use

Temperature:15 ~ 40°C
Vapor pressure:<500mbar
Viscosity:<500mm²/s
Humidity:20~90%
2
3. Parts Description
3.1 dTrite

No. Description
Liquid Level
① ① Observation
② (in piston running state)

③ Return Valve
② (to adjust the liquid

direction of dispensing )

③ Titrating pipe

④ Titrating pipe cover

⑤ Titrating pipe Tip

⑥ Bottle Adapter
⑦ Filling pipe

3
No. Description
Controller Port

① (Micro USB)

② Main Body lock

② Air Admission
③ Cap
(pressure balance)

3.2 Remote Control Handle

Control Knob

Data
Connector

4
3.3 Controller

Allows for dTrite control and function setting.



② ⑤

③ ④

No. Description

① LCD Display(show dTrite running state)

② Filling(press and hold for filling,release it to stop)

③ Dispensing(press and hold for fast titration,release it to stop)

Setting/magnetic stirrer(short press switching magnetic stirrer



on/off; press and hold 2s into setting interface)
Pre-Filling(press and hold 2s for piston to complete a aspirating

and dispensing process)
Knob(Turn Knob for dropwise titrating, short press Knob for reset

the liquid volume record to zero)

5
Control Panel can be fully
adjustable up to an angle of 45°


① ④

No. Description

1 Magnetic Stirrer Data Port(USB)

2 Locating Slot(to ensure magnetic stirrer assembly in place)

3 Sensor Holder Assembly Slot

4 Magnetic Stirrer Fastening Slot(to fixation with controller)

6
① ⑤


③ ④

No. Description

1 Power Switch(symbol “O”indicates Off,”-” indicates On)

2 Remote control handle Port

3 Communication port(non-function)

4 Charging/Communication port

5 Main Instrument Port

7
3.4 Magnetic Stirrer



No. Description

1 Stirring Plate(Max. Bar 20mm)

2 Communication port

3 Fastening key

4 Location key(to ensure magnetic stirrer assembly in place)

8
3.5 Display

Magnetic Stirring Battery


Indication Indication

Indication Arrow Liquid Unit

(piston movement) Volume

9
4. Assembly Instruction

Step - 1: Turn the Main Instrument Lock clockwise to connect


titrating tip with Main Body.

Step - 2: Press the titrating pipe tail end into the location slot.

Location slot

10
Step - 3: Push the titration pipe tail end with a certain length.

Step - 4: Connect the titration pipe tail end with the Dispensing
valve.

11
Step - 5: locking the titration pipe.

CAUTION:Titrating pipe are made of FEP. Please

confirm compatibility prior to use(Refer to chapter12


“Limitations and Compatibility”).

12
Step - 6: Connect filling pipe with filling valve.

Step - 7: Choose a suitable bottle adapter, then connect it with


dTrite main body.

13
Step - 8: Turn bottle adapter to fasten main body and bottle.

CAUTION:

① Please enable that the adapter is fastened prior to


each use.
② For perfect titration, please do not move or touch
Main Instrument during operation to avoid physical
damage to your dTrite.

14
Step - 9: Use USB cable to connect Main Instrument with
Controller.

Step - 10: Turn Return Valve to direction ①


If liquid is needed to be emptied from the barrel, turn Return
Valve to direction ②.
dTrite basic system was assembled.

15
5. Operation

CAUTION: Do a complete process of aspirating and

dispensing before the first time work.

5.1 Titration

Step - 1: Power on.

Step - 2: Waiting self-check complete.

16
Step - 3: Long press Pre-filling button( ) 2 seconds to let
air out, leaving the piston at the bottom of the barrel finally.

Step - 4: Press and hold Filling button ( )to fill targeted


liquid until Indication Arrow showing that the piston is moving
downward.
Long press knob 2 seconds, do the same operation also.

17
Step - 5: Long press Dispensing button( )for fast titration.
Turn Knob for dropwise titrating.
The dispensing liquid volume will been continue recording
and the volume will be show on the screen.

NOTE:
When recorded volume reaches the maximum value of 99.99ml,
the instrument will stop.Please press the knob to reset Liquid
Volume to zero.

CAUTION: There will may be some air bubble in the

barrel during the operation. These bubble dose not effect


the actual use.
If the bubble is bigger to effect the actual use, please

18
running several times aspirating and dispensing. If this
solution not works, please contact with the dealer or
manufacturer.

5.2 Liquid Emptying


If liquid is needed to be emptied from the barrel.
Step - 1: Turn Return Valve to direction ②.

19
Step - 2: Long press Dispensing button ( ),until the
piston run to the bottom of the barrel, make the liquid had been
emptying.

Step - 3: Turn Return Valve to direction ①.


Emptying operation was completed.

20
6. Function Setting

Press Setting button( )for about 2 seconds to enter

Function Setting interface.

Press Setting button( )to flick through pages.

Long press Setting button( )for about 2 seconds on any

page to exit Function Setting interface.

Page I: Aspiration speed within a range of 1-16. Turn Knob to


adjust and press for confirmation.

21
Page II: Dispensing speed within a range of 1-16. Turn Knob to
adjust and press for confirmation.

Page III: Magnetic stirrer speed within a range of off-5. Turn


Knob to adjust and press for confirmation.

NOTE: This function is effective after connecting the magnetic


stirrer only.

22
7. Accessories
7.1 Remote Control Handle

The Control Handle is fully map the operation of Control Panel,


easy to operate over a long distance.

Turn Knob for dropwise titrating, short press for reset liquid
volume record to zero, long press 2 second for filling liquid.

MAX. Length:90 cm

7.2 Magnetic Stirrer


23
Magnetic stirrer convenient user for mixing during the titration
experiments.

Step - 1: Connect Control Panel Fastening Slot with Magnetic


Stirrer Fastening Slot.

Step - 2: Turn the Magnetic Stirrer into horizontal position until


the Location Hole into the Location Slot.

Step - 3: Connect the USB Port under the Magnetic Stirrer with
the Control Panel.
24
7.3 Assemble Sensor Holder.

Step - 1: Fasten the Holder into place.

Step - 2: Press black button of the clamp and release until


reaching the appropriate altitude.

25
Assembly diagram

7.4 Remote Titrating pipe

26
Remote titrating pipe can effectively extend the titration
distance.

MAX. Length 1.5m

CAUTION:

Titrating pipe are made of FEP. Please confirm


compatibility prior to use(Refer to chapter12“Limitations
andCompatibility”).

Step - 1: Connect the titration pipe tail end with the Dispensing
valve.

27
Step - 2: locking the titration pipe.

Step - 3: Follow the figure to assemble the adapter and remote


titrating pipe.

28
1

8. Calibration
Calibration should take place at 20-25℃, kept constant within

29
±0.5℃. A dedicated calibration software will write calibration
values in your dTrite, after the distilled water has been
repeatedly weighed up at least five times.

Hardware needed::
●Electronic balance with readability of 0.01 mg
●Distilled water
●X86-or X64-architectured PC with pre-loaded Windows
(XP/Vista / 7/8/10 )operating system

Software needed:
● Dedicated calibration software of dTrite
(For more information, please contact with your nearest
distributor.)

CAUTION:

If your dTrite can not work properly after calibration,


please contact your nearest distributor for assistance.

9. Cleaning and Maintenance

CAUTION: dTrite cannot be autoclaved.


30
9.1 Cleaning the Outer Surface

The outer surface of your dTrite is made of ABS, ideal for easy
cleaning with simply clean water.

9.2 Cleaning the Barrel

dTrite barrel cleaning is repeatedly inhale row clear water for


cleaning.
Aspiration and dispensing at least 5 times, according to user's
actual situation to increase or decrease.
To ensure emptying remained in the barrel, the operation
reference “liquid emptying”

Step - 1: Turn Return Valve to direction①, long press Pre-filling


button make the piston stop at the barrel bottom

31
1

2
Step - 2: Press Filling and Dispensing button to aspiration and
dispensing simply clean water at least 5 times.
Step - 3: long press Pre-filling button make the piston stop at
the barrel bottom.
Step - 4: Ensure that into the tube is not submerged in a
liquid, Press filling button make piston run to the top of the
barrel.
Step - 5: Turn Return Valve to direction②, press Dispensing
button make piston run to the bottom of the barrel.
Step - 6: Cleaning work is finish,Turn Return Valve to
direction①

CAUTION: User is not recommended to remove and

32
cleaning of dTrite barrel, if the barrel cleaning operation fail to
meet the cleaning requirements of users. please contact the
dealer or manufacturer professional services personnel for
cleaning.
Ensure dTrite empty without liquid residue before delivery to service
personnel and inform details of last liquid handling.

9.3 Filling and Dispensing valve Replacement

Use the Installation tools to disassemble the old valve, replace the

33
new valve to the same position.
Valve has no fixed replacement cycle, problems after the
replacement.
The issue that could be has involvement with valve, please checking
the “Trouble Shooting”

CAUTION: The following operation must to use

installing tools to do.


Before disassemble, ensure to remove the dispensing and
filling pipe.

Disassemble Dispensing valve

34
Disassemble Filling valve

10. Trouble Shooting


Issue Possible Cause Solution

35
Piston
Contact with
overflows with Piston wears out.
manufacturer
liquid

Piston or its parts are


① Do “Cleaning
contaminated or
Piston moves the Barrel”
damaged due to
with difficulty ② Contact with
crystallization and
manufacturer
sedimentation.

Failure to filling Filling valve is clogged.


① Replace
Failure to refill;
Dispensing valve is filling valve
refilling sucks
contaminated or ② Contact with
back into the
titration tip damaged. manufacturer
titration tip.

Bubbles in the Filling pipe is loose or Replace filling

instrument/ damaged. pipe

Dispensing Filling pipe is away from Chicking filling


volume is less the liquid. pipe
than the volume Return pipe is not Contact with
displayed. installed or wrongly manufacturer

36
installed.

The instrument is not Checking


fully refilled. Operation
Checking filling
Filling valve is clogged valve
or damaged. Replace filling
valve

Battery dead charging

USB cable
No display
Connection fail connection
checking

11. Storage
During storage periods at constant temperature and humidity,
37
the recommended temperature range is from 0-40℃ and
humidity no more than 80%.
Please every month to charging for dTrite if being unused in
long time , make sure there are 50% power in battery at least.

12. Warranty
dTrite electronic titrators are covered by one-year warranty
against defects in workmanship and materials. Please contact
us or your nearest distributor.
ANY WARRANTY WILL, HOWEVER, BE DEEMED AS VOID
WITH NORMAL WEAR AND TEAR OR FOR OPERATIONS
CONTRARY TO THE INSTRUCTIONS GIVEN IN THIS
MANUAL.
Each and every dTrite has been calibrated and tested in
compliance with ISO8655-6 / DIN12650 when manufactured,
ensuring safe and comfortable operation.

13. Limitations and Compatibility


It is recommended to confirm reagent’s compatibility with this

38
instrument when applied for special purposes, trace analysis for
example.

–The liquid-path construction of your dTrite is made of


borosilicate glass, FEP and PTFE. Do not apply it in handling
liquids like hydrofluoric acid.
– The instrument would be clogged or damaged by solid
particles in turbid liquid like activated carbon.
– The plastic parts of your dTrite would be in swelling condition if
concentrated acid and alkaline, and methylbenzene, benzene
and other nonpolar organic solvents are put into use.
– Keep your dTrite away from the highly combustible carbon
disulfide.
– dTrite cannot be autoclaved.
– Do not put your dTrite in contact with corrosive gas like HCL
smog.

Compatibility(Max. Conc. 1 mol/L)


Acetic acid

39
Alcoholic potassium hydroxide solution

Ammonium iron (II) sulfate solution

Ammonium thiocyanate solution

Barium chloride solution

Bromide bromate solution

Cerium (IV) sulfate solution

EDTA solution

Hydrochloric acid

Hydrochloric acid in Acetone

Iodine solution*

Iodide Iodate solution*

Iron (II) sulfate solution

Nitric acid

Oxalic acid solution

Perchloric acid

Perchloric acid in glacial acetic acid

40
Potassium bromate solution

Potassium bromate bromide solution

Potassium dichromate solution

Potassium hydroxide solution

Potassium iodate solution

Potassium permanganate solution*

Potassium thiocyanate solution

Silver nitrate solution*

Sodium arsenite solution

Sodium carbonate solution

Sodium chloride solution

Sodium hydroxide solution

Sodium nitrite solution

Sodium thiosulfate solution

Sulfuric acid

Tetra-n-butylammonium hydroxide sol.

41
Triethanolamine in Acetone*

Zinc sulfate solution

CAUTION: This compatibility is against parts

which are directly in contact with liquid, if any of


above solution needs to be applied, contact with
manufacturer for consultation.

42

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