Loctite EA 9466™: Product Description Typical Curing Performance Fixture Time

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Technical Data Sheet

LOCTITE® EA 9466™
Known as LOCTITE® Hysol® 9466™
August-2019

PRODUCT DESCRIPTION TYPICAL CURING PERFORMANCE


LOCTITE® EA 9466™ provides the following product
characteristics:
Fixture Time
Technology Epoxy
Fixture time is defined as the time to develop a shear strength
Chemical Type Epoxy
of 0.1 N/mm².
Appearance (Resin) White opaque paste Fixture Time, ISO 4587, minutes:
Appearance (Hardener) White translucent liquid Steel (grit blasted) 180
Appearance (Mixture) Off-white opaque paste
Components Two components - requires mixing
Viscosity Medium
Mix Ratio, (by volume) 2 : 1
Cure Speed vs. Time, Temperature
Resin : Hardener
The rate of cure will depend on the ambient
Mix Ratio, (by weight) 100 : 50
temperature, elevated temperatures may be used to accelerate
Resin : Hardener
the cure. The graph below shows shear strength developed
Cure Room temperature cure after mixing with time at various temperatures on grit blasted steel lap
Application Bonding shears and tested according to ISO 4587.

LOCTITE® EA 9466™ is a toughened, industrial grade epoxy


adhesive with extended work life. Once mixed, the two 125
% of Full Strength on Steel

80 °/ 100 °C
component epoxy cures at room temperature to form a tough, 40 °C 22 °C
off-white bondline which provides high peel resistance and 100
high shear strengths. The fully cured epoxy is resistant to a
wide range of chemicals and solvents, and acts as an excellent 75
electrical insulator. LOCTITE® EA 9466™ provides excellent
bond strengths to a wide variety of plastics and metals. Typical 50
applications include general purpose industrial applications
requiring extended work life for adjusting parts during assembly 25
.
0
1min 5min 10min 30min 1h 3h 6h 24h 72h
TYPICAL PROPERTIES OF UNCURED MATERIAL Cure Time
Resin:
Specific Gravity @ 25 °C 1.0
Flash Point - See SDS
Viscosity, Brookfield - RVT,25°C,mPa·s (cP):
Spindle 6, speed 20 rpm 15,000 to 50,000

Hardener:
Specific Gravity @ 25 °C 1.0
Flash Point - See SDS
Viscosity, Brookfield - RVT,25°C,mPa·s (cP):
Spindle 5, speed 50 rpm 25,000 to 60,000
Mixed:
Working life, minutes 60
TDS LOCTITE® EA 9466™, August-2019

TYPICAL PROPERTIES OF CURED MATERIAL TYPICAL ENVIRONMENTAL RESISTANCE


Cured for 7 days @ 22 °C, 1.2 mm thick film Cured for 5 days @ 22 °C
Physical Properties: Lap Shear Strength, ISO 4587:
Glass Transition Temperature, ASTM E 1640, °C 62 Steel (grit blasted)
Shore Hardness, ISO 868, Durometer D 60
Elongation, ISO 527-3, % 3
Hot Strength
Tensile StrengthASTM D 882 N/mm² 32
Tested at temperature
(psi) (4,640)
100
Tensile Modulus, ISO 527-3 N/mm² 1,718
(psi) (249,110)

% Strength @ 22 °C
Electrical Properties: 75
Dielectric Breakdown Strength, 30
IEC 60243-1, kV/mm
50

25

0
TYPICAL PERFORMANCE OF CURED MATERIAL 0 20 40 60 80 100 120
Temperature, °C
Adhesive Properties

Cured for 5 days @ 22 °C Heat Aging


Lap Shear Strength, ISO 4587: Aged at temperature indicated and tested @ 22 °C
Steel (grit blasted) N/mm² 37.0 150

% Initial Strength @ 22 °C
(psi) (5,365)
Aluminum (abraded) N/mm² 26.0 125
(psi) (3,770) 150 °C
Aluminum (anodised) N/mm² 17.9 100
(psi) (2,595)
Galvanized Steel (Hot Dipped) N/mm² 8.5 180 °C
75 22 °C
(psi) (1,230)
Stainless steel N/mm² 23.0 50
(psi) (3,335)
Polycarbonate N/mm² 5.3 25
(psi) (765)
Nylon N/mm² 1.6 0
(psi) (230) 0 200 400 600 800 1000
Wood (Fir) N/mm² 11.3 Exposure Time, hours
(psi) (1,635)
GRP N/mm² 5.0
Chemical/Solvent Resistance
(psi) (725)
Aged under conditions indicated and tested @ 22 °C.
ABS N/mm² 4.7
(psi) (680) % of initial strength
180° Peel Strength, ISO 8510-2: Environment °C 500 h 1000 h
Steel (grit blasted) N/mm 8.0 Motor oil (10W30) 87 135 145
(lb/in) (45.5) Unleaded gasoline 22 95 125
Tensile Strength, ISO 6922:
Water/glycol 50/50 87 75 75
Steel pin (grit blasted) to Soda glass N/mm² 43.2
(psi) (6,260) Salt fog 22 --- 80
98% RH 40 85 90
Impact Strength, ISO 9653, J/m²:
Steel (grit blasted) 5.8 Condensing Humidity 49 --- 90
Water 22 --- 90
Acetone 22 75 90
Isopropanol 22 90 100

Tensile Strength, ISO 6992:


Steel pin (grit blasted) to Soda glass
% of initial strength
Environment °C 500 h 1000 h
98% RH 40 90 90

Henkel Americas Henkel Europe Henkel Asia Pacific


+860.571.5100 +49.89.320800.1800 +86.21.2891.8859
For the most direct access to local sales and technical support visit: www.henkel.com/industrial
TDS LOCTITE® EA 9466™, August-2019

GENERAL INFORMATION Storage


For safe handling information on this product, consult the Store product in the unopened container in a dry location.
Safety Data Sheet (SDS). Storage information may be indicated on the product container
labeling.
This product is not recommended for use in pure oxygen Optimal Storage: 8 °C to 21 °C. Storage below 8 °C or
and/or oxygen rich systems and should not be selected as greater than 28 °C can adversely affect product properties.
a sealant for chlorine or other strong oxidizing materials. Material removed from containers may be contaminated during
use. Do not return product to the original container. Henkel
Where aqueous washing systems are used to clean the Corporation cannot assume responsibility for product which
surfaces before bonding, it is important to check for has been contaminated or stored under conditions other than
compatibility of the washing solution with the adhesive. In those previously indicated. If additional information is required,
some cases these aqueous washes can affect the cure and please contact your local Technical Service Center or
performance of the adhesive. Customer Service Representative.

Directions for use: Conversions


1. For best performance part surfaces should be clean and (°C x 1.8) + 32 = °F
free of grease. kV/mm x 25.4 = V/mil
mm / 25.4 = inches
2. For high strength structural bonds, remove surface
µm / 25.4 = mil
contaminants such as paint, oxide films, oils, dust, mold
N x 0.225 = lb
release agents and all other surface contaminants.
N/mm x 5.71 = lb/in
3. Dual Cartridges: To use simply insert the cartridge into N/mm² x 145 = psi
the application gun and start the plunger into the cylinders MPa x 145 = psi
using light pressure on the trigger. Next, remove the N·m x 8.851 = lb·in
cartridge cap and expel a small amount of adhesive to be N·m x 0.738 = lb·ft
sure both sides are flowing evenly and freely. If automatic N·mm x 0.142 = oz·in
mixing of resin and hardener is desired, attach the mixing mPa·s = cP
nozzle to the end of the cartridge and begin dispensing
the adhesive. For hand mixing, expel the desired amount
Note:
of the adhesive and mix thoroughly. Mix for approximately
The information provided in this Technical Data Sheet (TDS) including
15 seconds after uniform color is obtained. the recommendations for use and application of the product are based
Bulk Containers: Mix thoroughly by weight or volume in on our knowledge and experience of the product as at the date of this
the proportions specified in Product Description section. TDS. The product can have a variety of different applications as well as
Mix vigorously, approximately 15 seconds after uniform differing application and working conditions in your environment that
color is obtained. are beyond our control. Henkel is, therefore, not liable for the suitability
4. Do not mix quantities greater than 4 kg as excessive heat of our product for the production processes and conditions in respect
build-up can occur. Mixing smaller quantities will minimise of which you use them, as well as the intended applications and
results. We strongly recommend that you carry out your own prior trials
the heat build-up. to confirm such suitability of our product.
5. Apply the adhesive as quickly as possible after mixing to Any liability in respect of the information in the Technical Data Sheet or
one surface to be joined. For maximum bond strength any other written or oral recommendation(s) regarding the concerned
apply adhesive evenly to both surfaces. Parts should be product is excluded, except if otherwise explicitly agreed and except in
assembled immediately after mixed adhesive has been relation to death or personal injury caused by our negligence and any
applied. liability under any applicable mandatory product liability law.
6. Keep assembled parts from moving during cure. The bond In case products are delivered by Henkel Belgium NV, Henkel
should be allowed to cure 24 hours before subjecting Electronic Materials NV, Henkel Nederland BV, Henkel
to any service loads. Technologies France SAS and Henkel France SA please
7. Excess uncured adhesive can be wiped away with organic additionally note the following:
solvent (e.g. Acetone). In case Henkel would be nevertheless held liable, on whatever legal
ground, Henkel’s liability will in no event exceed the amount of the
8. After use and before adhesive hardens mixing and concerned delivery.
dispensing equipment should be cleaned with hot soapy
water. In case products are delivered by Henkel Colombiana, S.A.S. the
following disclaimer is applicable:
The information provided in this Technical Data Sheet (TDS) including
Not for product specifications the recommendations for use and application of the product are based
The technical data contained herein are intended as reference on our knowledge and experience of the product as at the date of this
only and are not considered specifications for the product. TDS. Henkel is, therefore, not liable for the suitability of our product for
Product specifications are located on the Certificate of Analysis the production processes and conditions in respect of which you use
or please contact Henkel representative. them, as well as the intended applications and results. We strongly
recommend that you carry out your own prior trials to confirm such
suitability of our product.
Any liability in respect of the information in the Technical Data Sheet or
any other written or oral recommendation(s) regarding the concerned
product is excluded, except if otherwise explicitly agreed and except in
relation to death or personal injury caused by our negligence and any
liability under any applicable mandatory product liability law.

Henkel Americas Henkel Europe Henkel Asia Pacific


+860.571.5100 +49.89.320800.1800 +86.21.2891.8859
For the most direct access to local sales and technical support visit: www.henkel.com/industrial
TDS LOCTITE® EA 9466™, August-2019

In case products are delivered by Henkel Corporation, Resin


Technology Group, Inc., or Henkel Canada Corporation, the
following disclaimer is applicable:
The data contained herein are furnished for information only and are
believed to be reliable. We cannot assume responsibility for the results
obtained by others over whose methods we have no control. It is the
user's responsibility to determine suitability for the user's purpose of
any production methods mentioned herein and to adopt such
precautions as may be advisable for the protection of property and of
persons against any hazards that may be involved in the handling and
use thereof. In light of the foregoing, Henkel Corporation specifically
disclaims all warranties expressed or implied, including
warranties of merchantability or fitness for a particular purpose,
arising from sale or use of Henkel Corporation’s products. Henkel
Corporation specifically disclaims any liability for consequential
or incidental damages of any kind, including lost profits. The
discussion herein of various processes or compositions is not to be
interpreted as representation that they are free from domination of
patents owned by others or as a license under any Henkel Corporation
patents that may cover such processes or compositions. We
recommend that each prospective user test his proposed application
before repetitive use, using this data as a guide. This product may be
covered by one or more United States or foreign patents or patent
applications.

Trademark usage: [Except as otherwise noted] All trademarks in this


document are trademarks and/or registered trademarks of Henkel and
its affiliates in the U.S. and elsewhere.

Reference 1.4

Henkel Americas Henkel Europe Henkel Asia Pacific


+860.571.5100 +49.89.320800.1800 +86.21.2891.8859
For the most direct access to local sales and technical support visit: www.henkel.com/industrial

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