K46000, K46001

Cloud and Pour Point Chamber

Operation and Instruction Manual

REV A

Koehler Instrument Company, Inc.

1595 Sycamore Avenue • Bohemia, New York 11716-1796 • USA
Toll Free: 1-800-878-9070 (US only) • Tel: +1 631 589 3800 • Fax: +1 631 589 3815
http://www.koehlerinstrument.com • e-mail: [email protected]
Petroleum Testing & Analysis Instrumentation • Custom Design & Manufacturing
 CERTIFICATE OF CONFORMANCE

Cloud and Pour Point Chamber

K4600X

This certificate verifies that part number K4600X, Cloud and Pour Point
Chamber, was manufactured in conformance with the applicable standards
set forth in this certification.

Specifications: ASTM D97

ASTM D2500

This unit is tested before it leaves the factory, to ensure total functionality
and compliance to the above specifications and ASTM standards. Test and
inspection records are on file for verification.

Jesse Kelly
Application Engineer
Koehler Instrument Company
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Operation and Instruction Manual

WEEE Directive Compliance Statement

Background
The goal of the WEEE Directive is to encourage design of environment-friendly products that
increase reuse, recycling and other forms of recovery to reduce waste streams and applies to
listed Electronic and Electrical Equipment (EEE) and Koehler's equipment falls broadly into
Appendix 1A; Section 9 Monitoring and Control Equipment: Measuring, weighing or adjusting
appliances for household or as laboratory equipment.
Any associated non-embedded equipment such as Lighting (Saybolt Color) and PCs/Printers also
fall under WEEE. If provided with an order these ancillary items must be WEEE compliant. For
these and other reasons (printer cartridges are regionalized) the equipment must be supplied
through a third party supplier in Europe.
The WEEE Directive applies to electrical and electronic equipment falling under the categories
set out in Annex IA provided that the equipment concerned is not part of another type of
equipment that does not fall within the scope of this Directive. Annex IB contains a list of
products which fall under the categories set out in Annex IA.
http://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=OJ:L:2003:037:0024:0038:en:PDF
We do not qualify for any of the 10 exemption categories.
http://www.dpa-system.dk/en/WEEE/Products/Exemptions
Professional use
For equipment defined for ’professional use’ local authorities have no role to play. Producers and
importers are basically responsible for collection of WEEE recyclables from the professional user
and for subsequent management. A separate statement is given cataloging the items that
require separation from the equipment along with basic information on subsequent processing or
recycling prior to disposal of the equipment.
http://www.dpa-system.dk/en/WEEE/Products/Private-or-professional-use
Responsibility for Registration and Annual Reporting:
Koehler will not sell directly to end users in the EU and so has no responsibility to register within
each EU state and to make annual reports. Koehler declares that this responsibility is born by the
importer who is the first level of the distribution chain and is subject to producer responsibility.
We will communicate this in writing to our distributor/importers in the EU stating they are
responsible to satisfy WEEE registration and reporting requirements in the EU states where they
conduct sales activities.
It is illegal to market electrical and electronic equipment covered by producer responsibility
without being registered.
http://www.dpa-system.dk/en/WEEE/Producers/Whoissubjecttoproducerresponsibility
Product Design
Koehler's designs allow for complete disassembly to a modular level which usually allows for
standard recycling. A qualified refrigeration system technician must be consulted when
disassembling and de-commissioning any equipment with refrigeration systems.
Koehler's scientific testing equipment is robustly designed to function over a long service life and
are typically repaired many times over the course of years rather than being replaced. We
believe that re-use and refurbishment is the very best form of re-cycling.
All batteries must be readily removable not soldered in place.
Recycling instructions
In the event that replacement becomes necessary, we will include instructions, particularized to
each instrument that informs the customer of their recycling responsibilities and giving them
guidance in doing this. All Koehler equipment has been placed on the market since 13th August
2005 and so Koehler is defined as a "new WEEE producer". As such we must provide information
on refurbishment, treatment, and re-use.

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Our instrument manual will include this compliance statement and indicate that any collection of
materials will be handled by their authorized distributor. In the event that the distributor is
unreachable or is no longer a distributor for Koehler Instrument, Co., other arrangements may be
made including accepting the materials directly.

Recycling is free of charge. Shipping is the responsibility of the end users. Whether shipping to a
distributor or to Koehler directly, safe, properly declared, and labeled packaging and shipping
expenses are the sole responsibility of the end user.

WEEE Marking

Since Koehler products are subject to the WEEE Directive we must display the WEEE symbol
shown above in accordance with European Standard EN 50419 on the equipment. It must be
indelible, at least 5mm in height, and clearly legible. If the equipment is too small the mark must
be in the product literature, guarantee certificate, or on the packaging. Rules on marking are
established in section 49 of the WEEE Order.

Koehler Instrument Company, Inc.

c/o RECYCLING
1595 Sycamore, Ave.
Bohemia, NY 11716

As a minimum the following substances, preparations and components have to be removed from
any separately collected WEEE:
- Mercury containing components, such as switches or backlighting lamps (compact fluorescent
lamps, CFL),
- Batteries
- Printed circuit boards if the surface of the printed circuit board is greater than 10 square
centimeters (about 4 sq in.),
- Toner cartridges, liquid and pasty, as well as color toner,
- Chlorofluorocarbons (CFC), hydrochlorofluorocarbons (HCFC) or hydrofluorocarbons (HFC),
hydrocarbons (HC)
- Liquid crystal displays (together with their casing where appropriate) of a surface greater than
100 square centimeters and all those back-lighted with gas discharge lamps,
- External electric cables
- Components containing refractory ceramic fibers as described in Commission Directive
97/69/EC of 5 December 1997 adapting to technical progress Council Directive 67/548/EEC
relating to the classification, packaging and labeling of dangerous substances (2),
- Electrolyte capacitors containing substances of concern (height > 25 mm, diameter > 25 mm or
proportionately similar volume)

2. The following components of WEEE that is separately collected have to be treated as

indicated:
- Equipment containing gases that are ozone depleting or have a global warming potential (GWP)
above 15, such as those contained in foams and refrigeration circuits: the gases must be properly
extracted and properly treated. Ozone-depleting gases must be treated in accordance with
Regulation (EC) No 2037/2000 of the European Parliament and of the Council of 29 June 2000
on substances that deplete the ozone layer (4).

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Operation and Instruction Manual

Table of Contents

1 INTRODUCTION ........................................................................... 4
1.1 KOEHLER’S COMMITMENT TO OUR CUSTOMERS ........................................................4
1.2 RECOMMENDED RESOURCES AND PUBLICATIONS........................................................4
1.3 INSTRUMENT SPECIFICATIONS .................................................................................4
2 SAFETY INFORMATION AND WARNINGS.................................. 4
3 GETTING STARTED ..................................................................... 5
3.1 PACKING LIST ......................................................................................................5
3.2 UNPACKING ........................................................................................................5
3.3 INSTRUMENT INSTALLATION ...................................................................................6
3.4 ASSEMBLY INSTRUCTIONS ......................................................................................6
4 OPERATION.................................................................................. 6
5 MAINTENANCE ............................................................................ 6
5.1 ROUTINE MAINTENANCE .......................................................................................6
5.2 REPLACEMENT PARTS ............................................................................................6
6 SERVICE ....................................................................................... 7
7 STORAGE ..................................................................................... 7
8 WARRANTY .................................................................................. 7
9 RETURNED GOODS POLICY....................................................... 7
NOTES.................................................................................................. 8
NOTES.................................................................................................. 9

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Operation and Instruction Manual

1.2 Recommended Resources and

1 Introduction Publications

The Koehler K4600X Cloud and Pour Point 1. American Society for Testing and Materials
Chamber immerses four copper test jackets in (ASTM)
suitable freezing mixtures at the required depth 100 Barr Harbor Drive
as per ASTM specifications. West Conshohocken, Pennsylvania 19428-
2959, USA
Cloud point and pour point are indicators of Tel: +1 610 832 9500
the lowest temperature of utility for petroleum Fax: +1 610 832 9555
products. The sample is periodically examined http://www.astm.org
while it is being cooled in the cloud and pour email: [email protected]
point chamber. The highest temperature at
which haziness is observed (cloud point) or the ASTM Publication:
lowest temperature at which movement of the oil  ASTM D97: Pour Point of Petroleum
is observed (pour point) is reported as the test Products
result.  ASTM D2500: Cloud Point of Petroleum
Products
This manual provides important information
regarding safety, technical reference, installation
requirements, operating condition specifications, 1.3 Instrument Specifications
user facility resource requirements, and
operating instructions for the Cloud and Pour
Models: K46000
Point Chamber. This manual should also be
K46001
used in conjunction with applicable published
laboratory procedures. Information on these Ports: Four (4)
procedures is given in section 1.2.
Dimensions (dia.xh) 10.5 x 12in
1.1 Koehler’s Commitment to Our (27 x 30 cm)
Customers
Weight: 14lbs (6.3kg)
Providing quality testing instrumentation and
technical support services for research and
testing laboratories has been our specialty for
more than 50 years. At Koehler, the primary 2 Safety Information and Warnings
focus of our business is providing you with the
full support of your laboratory testing needs. Our Safety Considerations. The use of this
products are backed by our staff of technically equipment may involve hazardous materials and
knowledgeable, trained specialists who are operations. This manual does not purport to
experienced in both petroleum products testing address all of the safety problems associated
and instrument service to better understand your with the use of this equipment. It is the
requirements and provide you with the best responsibility of any user of this equipment to
solutions. You can depend on Koehler for a full investigate, research, and establish appropriate
range of accurate and reliable instrumentation safety and health practices and determine the
as well as support for your laboratory testing applicability of regulatory limitations prior to use.
programs. Please do not hesitate to contact us
at any time with your inquiries about equipment, Equipment Modifications and Replacement
tests, or technical support. Parts. Any modification or alteration of this
equipment from that of factory specifications is
not recommended voids the manufacturer
Toll Free: 1-800-878-9070 (US only) warranty, product safety, performance
Tel: +1 631 589 3800 specifications, and/or certifications whether
Fax: +1 631 589 3815 specified or implied, and may result in personal
injury and/or property loss. Replacement parts
Email: [email protected] must be O.E.M. exact replacement equipment.
http://www.koehlerinstrument.com

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Unit Design. This equipment is specifically 3.2 Unpacking

designed for use in accordance with the
applicable standard test methods listed in Carefully unpack and place the instrument and
section 1.2 of this manual. The use of this accessories in a secure location. Use extra care
equipment in accordance with any other test while unpacking the Borosilicate Glass
procedures, or for any other purpose, is not materials. Ensure that all parts listed on the
recommended and may be extremely packing list are present. Inspect the unit and all
hazardous. accessories for damage. If you find any damage,
keep all packing materials and immediately
This unit is NOT explosion-proof and proper report the damage to the carrier. We will assist
precautionary measures should be taken during you with your claim, if requested. When
operation. Avoid using this unit in an submitting a claim for shipping damage, request
environment with flammable or explosive that the carrier inspect the shipping container
vapors. and equipment. Do not return goods to Koehler
without written authorization.
Chemical Reagents Information. Chemicals
and reagents used in performing the test may WARNING: Be sure two or more
exhibit potential hazards. Any user must be individuals are available for extracting and
familiarized with the possible dangers before moving the instrument from box to the floor.
use. We also recommend consulting the Individuals must lift in accordance to proper
Material Data and Safety Sheet (MSDS) on each technique. See Figure below.
chemical reagent for additional information.
MSDS information can be easily located on the
internet at http://siri.uvm.edu or
http://www.sigma-aldrich.com.

3 Getting Started
The instructions for preparing the equipment
assume that the user is aware of the contents of
this document, which lists the warranty
conditions and important precautions.
Unwrap the unit and wipe the shell with a soft
3.1 Packing List cloth to remove smudges caused by wrapping
material.
 K46000/K46001 Cloud and Pour Point
Chamber Very high ambient temperatures would also
Including: affect the efficiency of the unit. It is advisable to
 Copper Jackets maintain the environment of the machine below
 Gaskets 22.78°C (73°F).
 Discs
 Thermometer Holders Carefully unpack and place the instrument and
accessories in a secure location. Ensure that all
Accessories (To be purchased separately) parts listed on the packing list are present.
Inspect the unit and all accessories for damage.
 332-004-001 Test Jar
If any damage is found, keep all packing
 250-000-05F ASTM 5F Thermometer
materials and immediately report the damage to
 250-000-05C ASTM 5C Thermometer
the carrier. We will assist you with your claim, if
 250-000-06F ASTM 6F Thermometer requested. When submitting a claim for shipping
 250-000-06C ASTM 6C Thermometer damage, request that the carrier inspect the
shipping container and equipment. Do not return
goods to Koehler without written authorization.

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3.3 Instrument Installation 5.2 Replacement Parts

1. Equipment Placement. Place the

Part Number Description
instrument on a firm, level table in an area
with adequate ventilation or in a hood. The K460-0-1 Copper Pot Assembly
unit may be leveled by making minor turning K460-0-4 Outer Shell Assembly
adjustments to the feet located at the base
K460-0-5 Bottom Plate
of the unit. Please note that Koehler does
not supply a level with this equipment. K460-1-6 Cover
K460-1-7B Copper Cups
2. Ventilation. A fume hood or exhaust system K460-0-8 Thermometer Holder
is recommended when operating the unit. A
canopy-style hood may be used if the height K46120 Disc (Cork) Bottom
from the top of the unit to the canopy is 5 AS568-219 O Ring
feet or less. The exhaust blower should AS568-131 O Ring
have a rating of 1000 C.F.M. or greater.

3.4 Assembly Instructions

The K46001 Cloud and Pour Point Chamber is

identical to the K46000 unit but includes an
additional cooling coil which allows refrigerated
coolant to be circulated through the chamber.
The inlet is located at the bottom of the chamber
and the outlet is located at the top.

4 Operation

The Koehler Cloud and Pour Point Chamber is

designed for acquiring test data in accordance
with the ASTM D97, ASTM D2500 and related
test procedures. Please be sure to read the
safety and hazard warnings, the installation
procedure, and the standard test method before
operating this instrument.

5 Maintenance

5.1 Routine Maintenance

The Koehler Cloud and Pour Point Chamber

requires little routine maintenance to provide
many years of continuous service. However,
over the course of time, some instrument parts
may need to be replaced. When ordering
replacement part(s), please provide the model
number, serial number, and product shipment
date of your equipment so that we can ensure
you will receive the proper replacement part(s).

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for any special, indirect, incidental,

6 Service consequential, or exemplary damages.
KOEHLER INSTRUMENT COMPANY, INC.
Under normal operating conditions and with
DISCLAIMS ALL OTHER WARRANTIES,
routine maintenance, the K4600X Cloud and
EXPRESSED OR IMPLIED, INCLUDING ANY
Pour Point Chamber should not require service.
IMPLIED WARRANTIES OF FITNESS FOR A
Any service problem can be quickly resolved by
PARTICULAR PURPOSE. Please save the
contacting Koehler’s technical service
shipping carton in the event the equipment
department either by letter, phone, fax, or email.
needs to be returned to the factory for warranty
In order to assure the fastest possible service,
repair. If the carton is discarded, it will be the
please provide us with the following information.
purchaser’s responsibility to provide an
appropriate shipping carton.
Model Number:
Serial Number: 9 Returned Goods Policy
Date of Shipment: To return products for credit or replacement,
please contact Koehler Customer Service with
your purchase order number, our packing
7 Storage list/invoice number, the item(s) to be returned
and the reason for the return. You will be issued
This laboratory test instrument is equipped
a Returned Authorization (RA) number, which
with electrical components. Storage facilities
must be prominently displayed on the shipping
should be consistent with an indoor laboratory
container when you return the material to our
environment. This testing equipment should not
plant. Shipping containers without an RA
be subjected to extremes of temperature and/or
number prominently displayed with will be
moisture.
returned to the sender. Goods must be returned
freight prepaid. Returns will be subject to a
This equipment was shipped from the factory
restocking charge, the application of which will
in a corrugated cardboard container. If long term
depend upon the circumstances necessitating
storage is anticipated, re-packing the instrument
the return. Some returns cannot be authorized,
in a water-resistant container is recommended
including certain products purchased from
to ensure equipment safety and longevity.
outside vendors for the convenience of the
customer, products manufactured on special
order, products shipped from the factory past
8 Warranty ninety (90) days, and products which have been
We, at Koehler, would like to thank you for used or modified in such a way that they cannot
your equipment purchase, which is protected by be returned to stock for future sale.
the following warranty. If within one (1) year from
the date of receipt, but no longer than fifteen
(15) months from the date of shipment, Koehler
equipment fails to perform properly because of
defects in materials or workmanship, Koehler
Instrument Company, Inc. will repair or, at its
sole discretion, replace the equipment without
charge F.O.B. its plant, provided the equipment
has been properly installed, operated, and
maintained. Koehler Instrument Company must
be advised in writing of the malfunction and
authorize the return of the product to the factory.
The sole responsibility of Koehler Instrument
Company and the purchaser’s exclusive remedy
for any claim arising out of the purchase of any
product is the repair or replacement of the
product. In no event shall the cost of the
purchaser’s remedy exceed the purchase price,
nor shall Koehler Instrument Company be liable

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Notes

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Notes

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Notes

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