228-30693

AUTO SAMPLER
SIL-HTA/HTC
FOR SHIMADZU HIGH PERFORMANCE
LIQUID CHROMATOGRAPH
SERVICE MANUAL

This manual is intended for the use of trained service engineers only .Unauthorized
personnel are advised not to attempt the procedures shown in this manual.

SHIMADZU CORPORATION
ANALITICAL &MEASURING INSTRUMENTS DIVISION
KYOTO , JAPAN
Blank Paper
 Contents

Chapter1 Introduction
Introduction •••••••••••••••••••••••••••••••••••••• P1-2
Chapter2 Safety Instructions P2-1
2.1 Precautions for Safe Operation ••••••••••••••••••••• P2-2
2.1.1 Application Precaution •••••••••••••••••••••••• P2-2
2.1.2 Installation Site Precautions •••••••••••••••••••• P2-3
2.1.3 Installation Precautions •••••••••••••••••••••••• P2-4
2.1.4 Operation Precaution ••••••••••••••••••••••••• P2-5
2.1.5 Precautions for Inspection, Maintenance Adjustment , P2-6
and Care of the Instrument •••••••••••••••••
2.2 Static Electricity Precautions •••••••••••••••••••••• P2-7
2.1.2 Typical Causes of Static Electricity Accidents•••••••• P2-7
2.2.2 Preventing Static Electricity Accidents •••••••••••• P2-8
2.3 Precautions for Mobile Phase Selection and Use •••••••• P2-11
2.4 Warning Labels •••••••••••••••••••••••••••••••• P2-14

Chapter3 Features and System Specifications P3-1

3.1 Setting and Operation ••••••••••••••••••••••••••• P3-2
3.1.1 Operation setting ••••••••••••••••••••••••••• P3-2
3.1.2 Unit Operation •••••••••••••••••••••••••••••• P3-3

Chapter4 Specifications P4-1

4.1 Sample Injection •••••••••••••••••••••••••••••••• P4-2
4.2 Others •••••••••••••••••••••••••••••••••••••••• P4-3

Chapter5 Component Description P5-1

5.1 Component Description ••••••••••••••••••••••••••• P5-2

Chapter6 Installation P6-1

6.1 List of Installation •••••••••••••••••••••••••••••• P6-2
6.2 Autosampler shipping screw ••••••••••••••••••••••• P6-3
6.3 Wiring (Connecting the fiber cable •••••••••••••••••• P6-4
6.4 Plumbing the inlet/outlet tubing •••••••••••••••••••• P6-4
6.5 Plumbing the rinse solvent drain tubing •••••••••••••• P6-6
(standard accessories )

Chapter7 Options
7.1 List of options •••••••••••••••••••••••••••••••••• P7-2
7.2 2-ml Sample loop ••••••••••••••••••••••••••••••• P7-3
<Procedure for Tubing Connection> •••••••••••••••• P7-4
<Procedure for changing the setting of tubing volume> • P7-5

7.3 4-channel OPT interface (PC-4) ••••••••••••••••••••• P7-7

7.4 SCSI board (option)•••••••••••••••••••••••••••••• P7-8
7.5 2-channel board •••••••••••••••••••••••••••••••• P7-9

SIL-HTA/HTC Service Manual

Chapter 8 FACTORY SCREENS (Adjustment) P8-1
8.1 Adjustment Screen list •••••••••••••••••••••••••• P8-2
8.2 How to Display the FACTORY Screen •••••••••••••••• P8-3
1.RACK TEACHING •••••••••••••••••••••••••••• P8-5
2.INJ.P TEACHING •••••••••••••••••••••••••••• P8-7
3.VALVE TEACHING••••••••••••••••••••••••••• P8-9
4.ERASE INJ.P-DATA••••••••••••••••••••••••••• P8-12
5.ERASE RACK-DATA••••••••••••••••••••••••••• P8-12
6.RETRY COUNT•••••••••••••••••••••••••••••• P8-13
7.ALL CLEAR •••••••••••••••••••••••••••• P8-13
8.MONIT DRY-PE TEMP••••••••••••••••••••••••• P8-14
8.3 Inputting the Serial Number ••••••••••••••••••••••• P8-14
8.4 Upgrading the SCL(Firmware) P8-15
(Upgrading from the floppy disk ••••••••
8.5 Upgrades the SIL (firmware) ••••••••••••••••••••••• P8-16
8.6 Operation check of the panel key •••••••••••••••••••• P8-18
8.7 LCD display check ••••••••••••••••••••••••••••••• P8-19
8.8 Initialization of the backup memory •••••••••••••••• P8-19

Chapter9 Electrical system P9-1

9.1 Electrical system ••••••••••••••••••••••••••••••• P9-2
9.2 Storage parameter •••••••••••••••••••••••••••••• P9-3
9.3 DIP switch setting ••••••••••••••••••••••••••••• P9-4
9.4 Replacement of Board ••••••••••••••••••••••••••• P9-4
9.4.1 Replacement of PBSCL-1A•••••••••••••••••••••• P9-4
<Removing the FLASH EEPROM>••••••••••••••••• P9-5
1.When the original EEPROM is mounted(PB-SCL1A)•• P9-5
2.To replace with new EEPROM•••••••••••••••••• P9-6

9.4.2 Replacement of PCB 10Avp CPU•••••••••••••••••• P9-7

<Removing the FLASH EEPROM>••••••••••••••••• P9-7
1.When the original EEPROM is mounted(PCB 10AVP CPU ASSY) • P9-7
2.To replace with new EEPROM•••••••••••••••••• P9-8

9.5 Diagram(Power unit) •••••••••••••••••••••••••••• P9-9

9.6 Diagram (SILHT main unit) ••••••••••••••••••••••• P9-10
9.7 Diagram (System controller) ••••••••••••••••••••••• P9-11

Chapter10 Maintenance 1 P10-1

10.1 Maintenance ••••••••••••••••••••••••••••••••• P10-3
<Consumable parts>•••••••••••••••••••••••••••• P10-3
<Maintenance List> •••••••••••••••••••••••••••• P10-3
10.2 Z mount •••••••••••••••••••••••••••••••••••••• P10-5
10.2.1 Removing Z mount••••••••••••••••••••••••••• P10-5
10.2.2 Removal of Z feed screw ••••••••••••••••••••••• P10-10
10.2.3 Z feed screw grease-up ••••••••••••••••••••••• P10-11
10.2.4 Z shaft oiling ••••••••••••••••••••••••••••••• P10-11

SIL-HTA/HTC Service Manual

 10.2.5 Z sensor replacement ••••••••••••••••••••••••• P10-12
10.3 Removing of XY arm ••••••••••••••••••••••••••••• P10-15

10.4 Belt Adjustment ••••••••••••••••••••••••••••••• P10-17

10.4.1 X belt Adjustment ••••••••••••••••••••••••••• P10-17
10.4.2 Y belt Adjustment ••••••••••••••••••••••••••• P10-18
10.4.3 Z belt Adjustment ••••••••••••••••••••••••••• P10-18
10.5 Valve mount •••••••••••••••••••••••••••••••••• P10-18
10.5.1 Removing valve mount ••••••••••••••••••••••• P10-19
10.5.2 Removing and mounting high-pressure valve ••••••• P10-20
10.5.3 Removing and mounting low-pressure valve •••••• P10-21
10.6 Measuring pump ••••••••••••••••••••••••••••••• P10-22
10.6.1 Structure of Measuring pump •••••••••••••••••• P10-22
10.6.2 Disassembling of Measuring pump ••••••••••••••• P10-23
10.6.3 Removing the measuring pump feed screw ••••••••• P10-24
10.6.4 Adjustment of slit disc position of the measuring pump P10-26
10.6.5 Replacement of valve mount sensor P10-27
(high-pressure valve , low-pressure valve , and measuring pump)
10.7 Replacement and Adjustment of X Encoder Sensor •••••• P10-29
10.8 Replacement of X PCB Sensor ••••••••••••••••••••• P10-30
10.9 Adjustment of Y Encoder •••••••••••••••••••••••• P10-30
10.10 Replacement of Y Sensor •••••••••••••••••••••••• P10-32
10.11 Replacement of the board(LC2K INJ2) •••••••••••••• P10-34
10.12 Replacement of Rack sensor ••••••••••••••••••••• P10-35
10.13 Replacement of Door sensor ••••••••••••••••••••• P10-35
10.14 Replacement of Cooling Rack Plate •••••••••••••••• P10-37
10.14.1 Dismantling procedure ••••••••••••••••••••••• P10-37
10.14.2 Assembly Procedure ••••••••••••••••••••••••• P10-40

Chapter11 Maintenance 2 P11-1

11.1 List of maintenance items •••••••••••••••••••••••• P11-2
11.2 Needle •••••••••••••••••••••••••••••••••••••• P11-4
11.3 Needle seal ••••••••••••••••••••••••••••••••••• P11-6
11.4 Piping (PEEK tubing) ••••••••••••••••••••••••••• P11-9
11.5 Removing the INJ port piping ••••••••••••••••••••• P11-10
11.6 Sample loop •••••••••••••••••••••••••••••••••• P11-11

Chapter12 Troubling shooting P12-1

12.1 Error Messages •••••••••••••••••••••••••••••••• P12-2
12.2 MAINTENANCE(Part Replacement)•••••••••••••••• P12-4

Chapter13 Circuit Diagram

PB SCL-1A•••••••••••••••••••••••••••••••••••••••• P13-2
PB SCL-4••••••••••••••••••••••••••••••••••••••••• P13-10
PCB 10AVP CPU ASSY•••••••••••••••••••••••••••••• P13-12
SIL MAIN•••••••••••••••••••••••••••••••••••••••• P13-15
LC2K-FILTER ASSY•••••••••••••••••••••••••••••••• P13-26
LC2K INJ2 ••••••••••••••••••••••••••••••••••••••• P13-27
PCBLC-2K COOL ASSY•••••••••••••••••••••••••••••• P13-29
PB SCL-2••••••••••••••••••••••••••••••••••••••••• P13-35

SIL-HTA/HTC Service Manual

 PB SCL-3••••••••••••••••••••••••••••••••••••••••• P13-37
PB SCL-5••••••••••••••••••••••••••••••••••••••••• P13-39

ChaPter14 Parts configuration and Parts Number P14-1

SIL-HT•••••••••••••••••••••••••••••••••••••••••• P14-2
Auto Sampler A ASSY••••••••••••••••••••••••••••••• P14-8
ASSY base ••••••••••••••••••••••••••••••••••••••• P14-12
XY ARMASSY••••••••••••••••••••••••••••••••••••• P14-15
ASSY Z•••••••••••••••••••••••••••••••••••••••••• P14-18
ASSY NEEDLE MOUNT••••••••••••••••••••••••••••• P14-21
ASSY V mount •••••••••••••••••••••••••••••••••••• P14-23
ASSY SIL pump ••••••••••••••••••••••••••••••••••• P14-27
Low Pressure Valve•••••••••••••••••••••••••••••••• P14-29
High Pressure Valve ••••••••••••••••••••••••••••••• P14-31
F Panel SCL•••••••••••••••••••••••••••••••••••••• P14-33
Electrical unit ASSY••••••••••••••••••••••••••••••••• P14-36
Rack Plate ASSY••••••••••••••••••••••••••••••••• P14-39
Consumable parts••••••••••••••••••••••••••••••••• P14-41
Repair Parts ••••••••••••••••••••••••••••••••• P14-42
<Electrical Parts>•••••••••••••••••••••••••••••• P14-42
<Valve assy>••••••••••••••••••••••••••••••• P14-44
<XY truck> •••••••••••••••••••••••••••••• P14-46
<Z truck> •••••••••••••••••••••••••••••• P14-47
<Auto Sampler Base Parts>••••••••••••••••••• P14-48
<Parts for SIL-HTc> •••••••••••••••••••••••• P14-49

SIL-HTA/HTC Service Manual

 Chapter 1 Introduction

CONTENTS

Chapter1 Introduction
Introduction •••••••••••••••••••••••••••••••••••••• P1-2

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1.Introduction

1.Introduction
<Characteristics of this Service Manual>
This Service Manual describes the maintenance procedures for the SIL-HTA and
SIL-HTC.
This manual is to be used by Shimadzu-certified service personnel.
Untrained personnel should not perform the maintenance procedures described in
this manual.

Information in the Instruction Manual is not duplicated in this manual.

This Service Manual is to be used in conjunction with the Instruction Manual.
New information required for maintenance is issued as Technical Information.
Insert Technical Information into this Service Manual and use the information in
conjunction with the main text of this Manual.

<Note>
Parts of the text or diagrams in this manual may differ due to improvements in
the instrument.
Shimadzu does not handle all of the parts listed in this manual as service parts.

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 Chapter2 Safety Instructions

CONTENTS

Chapter2 Safety Instructions P2-1

2.1 Precautions for Safe Operation ••••••••••••••••••••• P2-2
2.1.1 Application Precaution •••••••••••••••••••••••• P2-2
2.1.2 Installation Site Precautions •••••••••••••••••••• P2-3
2.1.3 Installation Precautions •••••••••••••••••••••••• P2-4
2.1.4 Operation Precaution ••••••••••••••••••••••••• P2-5
2.1.5 Precautions for Inspection, Maintenance Adjustment , P2-6
and Care of the Instrument •••••••••••••••••
2.2 Static Electricity Precautions •••••••••••••••••••••• P2-7
2.1.2 Typical Causes of Static Electricity Accidents•••••••• P2-7
2.2.2 Preventing Static Electricity Accidents •••••••••••• P2-8
2.3 Precautions for Mobile Phase Selection and Use •••••••• P2-11
2.4 Warning Labels •••••••••••••••••••••••••••••••• P2-14

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 Safety Instruction

2.Safety Instruction

2 . 1 P r ec a u t i o n f o r S a f e O p e r a t i o n s

• To ensure safe operation of the instrument, read these Safety Instructions carefully before use.
• Observe all of the WARNINGS and CAUTIONS described in this section. They are extremely important for
safety.
In this manual, warnings and cautions are indicated using the following conventions.

WARNING
Signifies danger of death, or serious injury, if the instructions given are not followed.

CAUTION
Signifies danger of minor injury, or of damage to objects, if the instructions given are not followed.
“Minor injury”: Injury not requiring hospitalization.
“Damage to objects”: Damage to other nearby objects.

2. 1 . 1 A p p l i c a t i o n P r e c a u t i o n s

WARNING
This instrument is an auto sampler for use with a high performance liquid chromatography system. Operate the
instrument for its intended purposes only. Using the instrument for any other purpose could cause accidents.

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12.
1. 2 I n s ta l l a t i o n S i t e P r e c a u t i o n s

WARNING
• The solvents used in high performance liquid chromatography are flammable and toxic.
The room where the equipment is installed should be well-ventilated, other-wise, solvent
vapors could cause poisoning or ignite and cause a fire.

• High performance liquid chromatography uses large amounts of flammable

organic solvents. Use of open flame in the vicinity of this unit must be strictly
prohibited. Do not install in the same room with equipment that emits or could
potentially emit sparks, since sparks could result in a fire. Provide fire extin-
guishers for use in case of fire.

• Provide protective equipment near the unit. If solvent gets into the eyes, or on
the skin, it must be flushed away immediately. Provide equipment, such as eye
wash stations and safety showers, as close to the unit as possible.

WARNING
• The lab table or other surface on which this instrument is installed should be level,
stable, sufficiently strong to support the units weight, and have a depth of at least
60cm. Otherwise, the instrument could tip over or fall off the surface.
• Avoid installation sites that are exposed to corrosive gases or are excessively dusty.
These adverse conditions may be detrimental to maintaining the instrument perfor-
mance and may shorten its service life. 60cm
• Do not hold the front panel when you carry this unit, and front panel could be dam-
aged or removed. Also, be sure to carry the unit with two or more people.

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2. 1 . 3 I n s t a l l a t i o n P r e c a u t i o n s 1
WARNING
• Take measures to prevent the instrument from falling in the event of an earthquake or other disaster. Strong
vibrations could cause the instrument to fall over, resulting in injury.
• The power supply voltages and power consumption of this instrument are listed below. The power supply volt-
age of the instrument is indicated by the voltage selector on its back, and on the label affixed to its right side.
Connect the unit only to a power supply of the voltage indicated, otherwise, fire or electric shock could result.
Check that the power supply voltage is stable and its current capacity is sufficient to operate all the components
of the system. If not, the unit will not operate at its rated performance.

SIL-HTA
Part Number Power Supply Voltage Power Consumption Frequency
228-41000-31 AC100V ± 10%
228-41000-32 AC110∼120V ± 10% 150VA 50/60Hz
228-41000-38 AC220∼240V ± 10%

SIL-HTC
Part Number Power Supply Voltage Power Consumption Frequency
228-41001-31 AC100V ± 10%
228-41001-32 AC110∼120V ± 10% 300VA 50/60Hz
228-41001-38 AC220∼240V ± 10%

• Ground the instrument. Grounding is necessary to prevent electrical shock in the event of an accidental electri-
cal discharge, and important for ensuring stable operation. See Section Instruction Manual
"5.3.1 Connecting to the power outlet”.

• Do not place heavy objects on the power cord, and keep any hot items away.
It could be damaged, resulting in fire, electric shock or malfunction, if the cord
becomes damaged, contact your Shimadzu representative immediately.

• Do not modify the cord in any way. Do not bend it excessively or pull on it. It could
become damaged, resulting in fire or electric shock. If the cord becomes damaged,
contact your Shimadzu representative.

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 CAUTION
When installing the instrument, be careful not to let your finger get caught in any
small openings, as this could result in injury.

2. 1 . 4 O p er a t i o n P r e c a u t i o n s

WARNING
• Take thorough measures to prevent buildup of static electricity. Section Instruction manual“1.2
Static Electricity Precautions”, p.6. Static buildup could result in fires or explo-
sions.

• Always wear goggles when handling solvents. If the solvent gets into the
eyes, blindness could result. Should solvent get into the eyes, flush immedi-
ately with large amount of water and get medical attention.

• Do not use flammable sprays (hair sprays, insecticide sprays, etc.) near this
instrument. They could ignite and cause a fire.

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2.1.5 Precautions for Inspection, Mainteance Adjustment, and Care of the Instrument 1
WARNING
• Unplug the instrument before performing inspection, maintenance, or parts replacement. Otherwise, electrical
shock or short circuit accidents could occur.

• Never remove the main cover. This may cause injury or malfunction of the instru-
ment. The main cover does not need to be removed for routine maintenance,
inspection and adjustment. Have your Shimadzu representative perform any
repairs requiring removal of the main cover.

• Replace fuses only with fuses of the proper type and capacity. Any other fuses
could cause a fire.
• If the power cord plug gets dusty, remove the plug from the power cord and wipe away the dust with a dry cloth.
If dust is allowed to accumulate, fire could result.
• Replacement parts must be of the specifications given Section 4.1 “Accessories”, 11.2 “Replacement Parts”. If
any other parts are used, they could become damaged and cause a malfunction.
• If any water gets into the instrument, wipe it away immediately to prevent rust. Never use alcohol or thinner sol-
vents for cleaning this instrument. They could cause discoloration.

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 Static Electricity Precautions

2. 2 S t a ti c El e c t r i c i t y P r e c a u t i o n s
1 WARNING
Liquid chromatography (LC) uses flammable organic solvent(s) as the mobile phase. LC systems are also
often used where large amount of flammable substances are present. Thus, an accident can produce large
scale damage. Operators must be constantly on guard against accidents involving fire or explosion.
The major cause of these accidents is static electricity. Devising preventative measures for static can be dif-
ficult, because the symptoms before an accident vary and can be hard to detect, since such accidents occur
as a result of several simultaneous coincidences. Recommended methods for preventing static electricity
accidents are provided below. Take thorough safety measures based on this information.

2. 2 . 1 T y p i c a l C a s u s e o f S t a t i c E l e c t r i c i t y A c c i d e n t s

Static electricity accidents are generally caused by this sequence of events:

Release of Energy Ignition of

Generation of Accumulation of
through Electrical Flammable
Static Electricity Static Electricity
Discharge Substances

When liquid is passed through thin tubing at Generation of Static Electricity

high flow rates, as in liquid chromatography, by a Liquid Flowing over a Solid A: Charges move with flow
the electrostatic charges of the flowing mat- Flowing liquid of liquid:
B: Immobile charges,
ter generate static electricity, as shown in A fixed to surface of solid
the figure below.

Solid
If electrostatically charged liquid is allowed
Potential Accident Situation
to accumulate in an electrically insulated Liquid flowing through thin
container, the charge will gradually tubing at high flow rates
*Air bubbles in liquid facilitate
increase, and can eventually reach several
generation of static electricity
thousand volts. If this happens and an elec-
trical conductor is brought within a certain Insulated containre of
polyethylene, etc.
distance of the container, electrical dis- Spark
Electrical
charge will occur, releasing thermal energy Discharge
Flammable gas present
which will ignite any flammable gas in the in container

vicinity. Dry Air

Spark
Electrical
Discharge
Flammable organic solvent
with large electro-static
charge

Floor covered with rubber, etc.,

cannot conduct electricity away

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2. 2 . 2 P r e v en t i n g S t a t i c E l e c t r i c i t y A c c i d e n t s
1
The best way to prevent static electricity accidents is simply to prevent the occurrence and accumulation of elec-
trostatic charges.

TIP
• Take two or more of the following preventative measures.
• If large amounts of flammable solvents are collected in a large container, implement preventative measures 1, 2,
and 3 below.

Preventative Measure 1

Use a metal container for the waste liquid, and ground the container. This will ensure that the electrical
charges of the container and liquid pass to the ground.

Accessories for this measure:

(1) Grounding wire with clip ........................... Part Number 228-21353-91
(2) 18 Liter metal container ............................ Part Number 038-00044
(3) 4 Liter metal container .............................. Part Number 038-00043-01

TIP
• Be sure to ground the metal waste container properly. If the grounding wire is not properly attached or con-
nected to the ground, static electricity can build up in the container.
• Some metal containers have surfaces that are laminated or oxidized, and therefore do not conduct electricity.
After grounding the metal container, use a tester to verify that electricity is conducted to the ground
• If the liquid to be drained into the waste container is virtually non-conductive (10-10 S/m or less), it will be neces-
sary to add properly conductive, and therefore safe, liquid to the tank. This conductive liquid may be added
beforehand.

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2-8
1 Preventative Measure 2

Cover the spaces between the tubing and the sides of the inlet and outlet openings of the waste container
with caps or other protective covering. This will prevent any sparks generated outside the container from
getting inside.

Accessories for this measure:

(1) Caps for 18 liter or 4 liter containers.......... Part Number 228-21354-91
(set of 3 caps covering 3mm diameter openings)

Preventative Measures for Static Connect clip to metal parts

Connect to ground terminal of

instrument or other grounding
point, to ground container

Reduce the opening

with a cap

1.8 Liter metal can

(preferably plated) Static of the liquid is
conducted through
container to ground

Preventative Measure 3

Keep electrostatically charged objects, including the human body, away from the waste container. To prevent
electrostatic charging of the human body, take the following precautions:
• Wear anti-static clothing and shoes.
• Ground the human body with anti-static wrist straps. For safety, the wrist strap should be connected to the
ground using an intervening resistor of about 1MΩ.
• Spread anti-static matting or the like on the floor, to make the floor conductive.

TIP
Persons who have not taken anti-static precautions should touch a grounded metal object before coming near the
waste container to drain static charges.

Preventative Measure 4

• Use tubing with an inner diameter of at least 2mm for drain lines with high flow rates.

TIP
Air bubbles in liquid can multiply the electrostatic charge by a factor of 20, 30 or more. Periodically check the tub-
ing connections for leaks.

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 Preventative Measure 5

If it is not possible to use a conductive waste container, take the following precautions:
1
• Ensure that the end of the inflow tubing is always submerged inside the container. Place some type of
grounded metal object, such as a ground wire connected to the instrument, into the liquid.

TIP
• The above precaution will be ineffective for low conductivity (less than 10-10 S/m) liquids.
• Use as small a container as possible to minimize damage in the event of fire.
• Ambient humidity exceeding 65% will prevent static. Keep the room at a proper humidity.

TIP
Anti-static equipment (anti-static clothing, shoes, and matting) and charge measurement equipment (potentiome-
ter) are sold by speciality manufacturers.

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 Precautions for Mobile Phase Selection and Use

2. 3 P r e c a u t i o n s f o r M o b i l e P h a s e S e l e c t i o n a n d U s e
1
CAUTION
PEEK resin possesses high mechanical strength, and among synthetic resins, it is the most suitable for use
in high performance chromatographs. The following are safety-related considerations which require certain
limitations in the use of PEEK, as follows.

The following mobile phases should not be used when PEEK resin parts are used in the plumbing.
• concentrated sulfuric acid
• concentrated nitric acid
• dichloroacetic acid
• acetone
• tetrahydrofuran (THF)
• dichloromethane
• chloroform
• dimethyl sulfoxide (DMSO)
These mobile phases weaken the PEEK resin, which could result in cracked plumbing and mobile phase
leaks.
NOTE: Briefly using a weak solution of no more than 0.5% acetone in water (e.g. to check gradient performance)
will present no problems.

PEEK Tubing
1. The resistance to pressure of PEEK tubing varies depending on the internal diameter, manufacturing pro-
cess and solvents used. For this instrument, be sure to use the PEEK tubing having an internal diameter
of 0.13mm, provided standard with this instrument. Be advised that Shimadzu will assume no responsibil-
ity for any mishaps associated with the use of PEEK tubing provided by another manufacturer.
For example, the PEEK tubing might rupture if acetonitrile is delivered at a pressure continuously exceeding
27.5MPa (280kgf/cm2), posing considerable danger.
2. If PEEK tubing is bent to a curvature with an excessively short radius, that portion of tubing will be weak-
ened. Be sure that the curvature radius of the PEEK tubing is no shorter than 10mm. Avoid forcibly bend-
ing and fixing the tubing, and strive to obtain as natural a curvature as possible.

Radius of 10mm or greater

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 TIP 1
• Use only HPLC grade or comparable mobile phase and filter with a filter of 0.45µm mesh or finer before use to
remove particulates and foreign matter.
• Halogen ions can corrode the stainless steel material (316SS) used in the plumbing, so avoid mobile phases
that contain halogen ions - such as KCl, NaCl, NH4Cl - mobile phases that generate halogen ions in certain
reactions. If such mobile phases must b used, clean all lines thoroughly with distilled water immediately after
analysis.
• Always degas the mobile phase, otherwise bubbles will form during mixing of solvents or when a change in tem-
perature or pressure occurs. Air bubbles can cause pump malfunctions and detector signal noise.
• For boiling points, viscosities, and other data relating to the mobile phases used, see Section Instruction Manyual
"11.2.3 MobilePhase Characteristics”.

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 Warning Labels

2. 4 W a r n i n g L a b e l s
1 To help users operate the unit safely, warning labels are affixed in places where special attention is required.
Should any of these labels peel off or become damaged, obtain replacements from Shimadzu.

Caution label (P/N 228-40357)


Warning label‫ޓ‬SIL-HTA㧦P/N 228-40955-01 
‫ޓޓޓޓޓޓޓ‬SIL-HT C㧦P/N 228-40955-02 

Caution/Warning label
(P/N 228-38924-02)

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Blank Paper
 Chapter3 Features and System
Specifications

CONTENTS

Chapter3 Features and System Specifications P3-1

3.1 Setting and Operation ••••••••••••••••••••••••••• P3-2
3.1.1 Operation setting ••••••••••••••••••••••••••• P3-2
3.1.2 Unit Operation •••••••••••••••••••••••••••••• P3-3

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 3.Features and System Specifications

3 Fe a tu r e s a n d S y s t e m S p e c i f i c a t i o n s
3. 1 S ett i n g s a n d O p e r a t i o n

3. 1. 1 O p e r a ti o n s e t t i n g s

2 Unit operation settings are made as follows:

<Standard injection mode>

This is the simplest mode for making a standard injection. In this mode, specify the sample vial number, number
of injections, injection volume and analysis time in the analytical sequence table setting screen(details are in Sec-
tion 6.2 “Setting Analytical sequence”). Also, set the needle stroke, the rinse volume, the rinsing speed, sampling
speed, etc. in the “A.INJ PARAMETER” screen.

<Repeat injection mode>

This mode can be used to inject a predetermined number of samples repeatedly, at periodic intervals. In this
mode, a special repeat injection table is prepared(in addition to the default analytical sequence table). Preparing
this repeat injection table allows insertion analysis to be performed at a certain cycle while sampling table for
standard injection is being executed.

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 3.Features and System Specifications

3. 1. 2 U n i t O p e r a t i o n

Sample injection
The sequence of operations involved when injecting samples is as shown in the flow and operation diagrams
below. Use these diagrams to become familiar with the operation of the unit.
2
<Flow line>
Sample loop

Rinsing port
Solvent delivery
Measuring pump pump

Low- High-
pressure pressure
valve valve
Sampling
needle
Mannual prime
Injection
port
Rinse solvent
Column

1. Standby (READY) Sample loop

Mobile phase from the reservoir is pumped, in
order, through the high-pressure valve, sam-
Measuring pump
ple loop, sampling needle, injection port and Rinsing port

back through high-pressure valve, before

reaching the analytical column. The low-pres-
1 Solvent
sure valve is connective at port 1 and 2. 2 1
Sampling delivery
needle 2 pump
Injection Low- High- 6
port pressure 5 pressure
valve 3 valve

3
4 4 5

Rinse
Mannual
solvent Column
prime

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 3.Features and System Specifications

2. Release of pressure in flow line Sample loop

The high-pressure valve rotates to the load
position (60° clockwise), releasing the pres-
Measuring pump
sure inside the sample loop. Rinsing port

2 Sampling
needle 2
1 2 1 Solvent
delivery
pump
Injection Low- High- 6
port pressure pressure
valve
5 valve
3
3
4 4 5
Rinse
Mannual
solvent Column
prime

3. Rinsing of sampling needle Sample loop

The sampling needle is inserted into the rins-
ing port, where its outer surfaces are rinsed Measuring pump
with the rinse solvent inside the port.
Rinsing
NOTE port
This rinsing function is enabled by setting 1 Solvent
2 1
RINSE MODE as follows : delivery
2 pump
0 : No rinsing (default) Low- High- 6
Injection pressure pressure
1 : Rinsing before sample aspiration port
5
valve 3 valve

2 : Rinsing after sample aspiration 3

4 4 5
3 : Rinsing before and after sample
Rinse
aspiration Mannual solvent Column
This function is recommended when analyz- prime

ing components which tend to adsorb to the

needle surface. See p.78, RINSE MODE, for
more details.

4. Sample aspiration Sample loop

The low-pressure valve rotates 30° clockwise,
and the sampling needle is inserted into the Measuring pump
sample vial. Then the measuring pump draws Rinsing port

the sample into the sampling needle.

1 2 1 Solvent
Sample delivery
2 pump
Low- High- 6
Injection pressure pressure
port valve
5 valve
3
3
4 4 5
Rinse
Mannual solvent Column
prime

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 3.Features and System Specifications

5. Start of analysis Sample loop

The sampling needle is inserted into the injec-
tion port, and the high-pressure valve rotates
Measuring pump
60° counterclockwise to the injection position. Rinsing port

The sample is injected into the flow lines and,

along with the mobile phase, passes through
the high-pressure valve and into the column, Sampling
2
1 2 1 Solvent
delivery
2
where analysis begins. needle pump
Injection Low- High- 6
port pressure 5 pressure
valve 3 valve

3
4 4 5

Rinse
Mannual
solvent Column
prime

6. Purge of measurement flow line Sample loop

(rinse solvent aspiration)
The low-pressure valve rotates 30° counter- Measuring pump
clockwise.(Port 1 and 2 are connective.) And Rinsing port

after the plunger of the measuring pump has

returned to the home position, the low-pres-
1 2 1 Solvent
sure valve rotate 60° clockwise.(Port 4 and 5 Sampling delivery
needle 2 pump
are connective.) and the plunger operates to
Injection Low- High- 6
aspirate rinse solvent. port pressure
valve
5 pressure
valve
3
3
4 4 5

Rinse
Mannual
solvent Column
prime

7. Purge of measurement flow line Sample loop

(rinse solvent dischargement)
The low-pressure valve rotates 60° counter- Measuring pump
clockwise. (Port 1 and 2 are connective.) Rinsing port

And measuring pump plunger operates to dis-

charge rinse solvent to rinsing port.
1 2 1 Solvent
Sampling delivery
needle 2 pump
Injection Low- High- 6
pressure pressure
port
valve
5 valve
3
3
4 4 5

Rinse
Mannual
solvent Column
prime

8. Standby (READY)

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Blank Paper
 Chapter4 Specifications

CONTENTS

Chapter4 Specifications P4-1

4.1 Sample Injection •••••••••••••••••••••••••••••••• P4-2
4.2 Others •••••••••••••••••••••••••••••••••••••••• P4-3

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4.Specification

4.Specifications

4.1 Sample Injection

Injection system Full volume sample injection, variable injection volume (zero sample loss
during injection)
Injection volume setting range 0.1 to 100µL (standard), 1 to 2000µL (optional)
(0.1 to 0.9µL in 0.1µL increments, 1 to 2000µL in 1µL increments)
Number of samples processed SIL-HTC: Sample cooler model
350 (w/1mL sample vials), 140 (w/1.5mL sample vials), 100 (w/4mL sam-
ple vials),
384 (w/4 micro titer plates each with 96 wells), 1536 (w/4 micro titer plates
each with 384 wells)
384 (w/4 Deep well MTP each with 96 wells)
SIL-HTA: Model without sample cooler
350 (w/1mL sample vials), 210 (w/1.5mL sample vials), 100 (w/4mL sam-
ple vials),
384 (w/4 micro titer plates each with 96 wells), 1536 (w/4 micro titer plates
each with 384 wells)
384 (w/4 Deep well MTP each with 96 wells)
Sample vials 1.5mL glass, 1.1mL glass, 4mL glass,
0.3mL glass (w/plastic spacers), 0.3mL glass (4mL vial storage type),
1mL plastic, 0.2mL plastic, 4mL plastic, 96-well micro titer plate, 384-well
micro titer plate, 96-deep well
Injection volume repeatability RSD < 0.3% (at 10µL injection)
Carryover Less than 0.01% (using naphthalene analysis conditions)
Injection volume accuracy +/- 1% (at 50µL injection, n = 10)
Number of repeat injections 1 - 30 times/sample
Analysis time setting 0.01 minute steps (< 1000 minutes), 0.1 minute steps (> 1000 minutes)
Number of injection parameter steps 102 steps max.
Sample aspiration rate 0.1 to 15µL/sec (0.1µL/sec increments, 1 to 15µL/sec 1µL/sec incre-
ments)
Rinse aspiration rate Variable (1 to 35µL/sec, 1µL/increments)
Applicable pressure 35.0MPa max., 20.0MPa max. with PEEK tubing
Sample cooler System Direct cooling system (environment conditions: room temperature below
(SIL-HTC only) 30°C with humidity less than 70% when the cooler temperature is set to
4°C), dehumidification function built-in
Temperature setting 4 to 40°C (can be cooled down to 4°C when the room temperature is
range below 30°C and the humidity is below 70%.)
Temperature accu- ±3°C
racy

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 4.Specification

4.2 Others

Items Specifications
Liquid contact materials Stainless (316 SS), ceramic, Teflon (R), FEP, GFP, sapphire, PEEK
Ambient temperature 4~35°C
Ambient humidity ~80%
pH range 1~14
Dimensions and weight W540 × H415 × D500 mm, 40 kg (SIL-HTC), 35 kg (SIL-HTA)
Power supply SIL-HTA

Power
Part No. Power supply voltage Frequency
consumption
228-41000-31 AC100V ± 10%
228-41000-32 AC110 ~ 120V ± 10% 150VA 50/60Hz
228-41000-38 AC220 ~ 240V ± 10%

SIL-HTC

Power
Part No. Power supply voltage Frequency
consumption
228-41001-31 AC100V ± 10%
228-41001-32 AC110 ~ 120V ± 10% 300VA 50/60Hz
228-41001-38 AC220 ~ 240V ± 10%

Error display Exists (Error display and stop at the time of malfunction)

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Blank Paper
 Chapter5 Component Description

CONTENTS

Chapter5 Component Description P5-1

5.1 Component Description ••••••••••••••••••••••••••• P5-2

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5.Componen Deacription

5.C ompo ne nt Descrip tio n

5.1 C ompo ne n t Descrip tio n

Rinsing port drain outlet Inlet tubing

Drain tubing is inserted here to drain The pump or mixer is connected here.
rinse solvent from the rinsing port to Blue cover is attached to the tubing
the waste container. end.

Keyboard/Display
Specifies operation parameters.
Displays operation parameter
settings.

S IL -H T C

Outlet tubing
The column is
Outlet for connected here.
dehumidity

Power Switch
Turns the power ON/OFF, Pressing once turns
the power on. Pressing a second time turns the
power offf.
Leakage drain port
If leak occurs inside this unit, the
leaked solvent is discharged from Power Switch Solvent filter
this hole into waste bottle. Filters solids from the rinse
solvent.
(Pore size: 10 microns)
POWE POWE
R㨪 R㨪
Button in Button out
(power ON) (power OFF)

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 5.Componen Deacription

Rack (Option) Z track

For holding sample vials reagent vials. Moves the needle vertically (Z direction) or
Can be moved forward/backward (in Y horizontally (X direction).
direction).

Sampling needle High-pressure valve

Draws sample/reagent from a Switch valve for sending sample or reagent
sample/reagent vial, and to the column along with the mobile phase.
delivers it to the injection port.
Measuring pump
Measures and pumps samples, reagent,
and rinse solvent.

Low-pressure valve
Switch valve for determing the direction of
aspiration/delivery of sample, reagent and
rinse solvent.

Rinsing port
Needle is inserted here to clean
its outer surfaces.

Leak sensor
For detecting leaks inside
Injection port the unit.
Samples delivered by the sampling
needle pass from this port through the
high pressure valve, and into the column.

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5.Componen Deacription

“REMOTE” connectors (ch.1 to ch.8) “OPT LINK” connector

These are connectors for each device of LC- This is a data sending/receiving connector
10A/10Avp series. (See Section 5.5 in the SCL- with Chromatopac. (See Section 5.15 in
10Avp Instruction Manual.) the SCL-10Avp Instruction Manual.)
Ch.1 connects to the “REMOTE” connector at
the lower right. See also “REMOTE” connector
for SIL-HT. “RS-232C” connector
This is a data sending/receiving connector with PC or
Chromatopac. This is used mainly for connection with
PC. (See Section 5.16 in the SCL-10Avp Instruction
Manual.)

External control connector

This is a connector with external
3
instruments.
(See Section 3.3 in the SCL-10Avp
Instruction Manual and Section 4.2.4
in the SIL-HTA/C Instruction Manual.)

Power supply
connector
For connection of
power cord.

Fuse holder (2 pcs.)

Fuses are inserted here.

“AC OUT” connector

This is a connector for AC power supply
“REMOTE” connector for SIL-HT output.
This connector connects to the “REMOTE” This connector connects the power
connector ch.1 in the upper right. supply cable of the fraction collector (or
sub-controller). And the power supply of
the connection device synchronizes with
the power supply switch of this unit.

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 Chapter6 Installation

CONTENTS

Chapter6 Installation P6-1

6.1 List of Installation •••••••••••••••••••••••••••••• P6-2
6.2 Autosampler shipping screw ••••••••••••••••••••••• P6-3
6.3 Wiring (Connecting the fiber cable •••••••••••••••••• P6-4
6.4 Plumbing the inlet/outlet tubing •••••••••••••••••••• P6-4
6.5 Plumbing the rinse solvent drain tubing •••••••••••••• P6-6
(standard accessories )

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6.Installation

6.Installation

6.1 List of Installation

Service Instruction
Item Contents Manual Manual
Installation site Suitable sites ,and site preparation - P39
Example system configurations - P40
Shipping Screw Removing Autosampler P6-3 P41
shipping screw
Installation Installation - P42
Stacking brackets - P43
Connecting the Power Connecting to the outlet - P45
supply Grounding - P46
Plumbing preparation Types of tubing and connectors - P47
used - P47
Cutting the tubing - P48
Connecting the tubing - P49
Removing the protective plugs P50
Plumbing Rinse solvent and waste container - P50
preparation
Rinse solvent selection - P51
Plumbing the inlet/outlet tubing P6-4 P52
Plumbing the rinse solvent drain P6-6 P54
tubing
Wiring Connectors - P55
Connecting the fiber optic cable P6-4 P56
Connection to system controller P6-4 P57
Optional Equipment Sample vial Racks,and sample vial - P26
Sample loop 2ml P7-3 -
PC-4(4-channel) OPT interface P7-7 -
SCSI board(PB-SCSI) P7-8 -
2ch board(PC-55N) P7-9 -
Micro plates Micro titer racks - P27
Using the Micro titer Plate - P69
MTP adjust - P87
Transporting the Unit Transporting the unit - P59
Rinsing Rinsing the flow lines - P61
Cleaning the exterior - P62
When the unit is inactive for a long - P62
period
Reverse Cleaning of the Reverse Cleaning of the Flow Lines - P63
Flow Lines

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 6.Installation

SILHT SCL10Avp
Items Contents IM IM
External control Event cable - P5-29
connectors External control connectors - P3-6
(System controller) Connections - P5-30
Soft switching settings - P6-77,78
External control Event cable P31 -
connection Connecting the event cable P32 -

6.2 Autosampler shipping screw

<Removing the autosampler shipping screw>
A shipping screw is attached to the Z-mount unit to prevent damage during
transport.
To avoid damage, remove the shipping screw before turning on power
to the instrument.

Z-Mount Shipping Screw

Rubber Spacer

Removing Procedure
(1) Temporarily remove the transparent front cover (only on models with a cooler).
(2) Use a hex wrench to remove the Z-mount shipping screw.
(3) Carefully lift and remove the rubber spacer used to secure the needle during s
hipment.
(4) Re-attach the front cover (only on models with a cooler).

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6.Installation

Caution
To avoid damage to the sample loop, be sure that the customer fully understands t
he following caution.
The drive mechanism of the autosampler moves freely after the shipping screw is r
emoved. The actions listed below can deform the sample loop, which in the worst c
ase may cause tangling or damage to the loop during subsequent injections. These
actions must be avoided once the shipping screw is removed.
- Do not move the XY arm backward or forward while the Z-mount is
in the right most position.
- Do not move the Z-mount too far to the back and right.
- Do not leave the Z-mount at the back for more than 5 minutes.
- Do not apply sufficient force to distort the sample loop.

6.3 Wiring(Connecting the fiber cable)

<Connecting the fiber cable>

Referring to instruction manual “5.6.2

Connecting the fiber optic cable” , use the fiber
fiber optic cable to connect the autosampler
REMOTE terminal to the system contoroller’s
Channel1(SIL) REMOTE terminal.

Tip
Channel 1(SIL) on the system controller is
reserved for SIL.

6.4 Plumbing the inlet/outlet tubing

<the inlet /outlet tubing>

Inlet tubing : connected to pump or mixer
The inlet tubing is added the blue cover of the tubing
It is possible to make plumbing of inlet tubing
through the front-low panel
Outlet tubing : connected to column
Tubing for rinsing solvent is connected to port4 of low-pressure valve.

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 6.Installation

Tubing for rinsing solvent

Inlet tubing

Outlet tubing

< Procedure of plumbing "Pipe, IN" and "Suction filter pipe of RINSE liquid"

from left side of front under panel ("F PANEL B")>

(1) Remove rubber plugs from "F PANEL B (228-48093)".

(2) Loosen the screws in the holes for about 10mm out ( about 10 turns ).

Loosen the screws in the

holes
(3) Remove bottom fix of "F PANEL B" by pulling ahead the bottom side of the panel. And
pull down it and remove it from the screws.

pulling ahead the

bottom side of the
panel

Screw Screw

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6.Installation

(4) Fix the plumbings onto the left clamp and draw out from instrument as photo.

(5) Mount the "F PANEL B" by the opposite procedure of 3)

(6) Tighten the screws and put the rubber plugs on.

6.5 Plumbing the rinse solvent drain tubing(standard

accessories )

CAUTION
The volume of waste liquid produced pre analysis is about 200uL ,under default
conditions(default values). If a large number of sampler is analyzed continuously,
provide a larger waste container . If the container is too small, it will overflow.

<Drain outlet>

Outlet for
dehumidity
Rinsing port drain
outlet

Leakage drain port

The pipe is mounted with some inclination .
so as to make the liquid run smoothly.
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 6.Installation

Assemble the drain tube by the use of the teflon tube in the standard accessory refering
to photo.

Assembling the
drain tube (unit 60 35
mm)
35

40
35

10
100

note) Cut the offcut tube

40
from L shaped tube to
10mm length and insert it
to the end of tube.

40

Plumbing the drain tube

to SIL-HTC
Caution
Be careful not to bent the Teflon tubing
If the Teflon tubing is bent ,liquid leak from the
rinsing port may occur

Cut the other end of the drain tubing so that it will penetrate a short distance into the
waste cntainer

Caution
The end of the drain tubing must not be submerged into the waste liquid .
Waste liquid will leak from the rinsing port .
If necessary , tape the tubing to the container’s rim to prevent submersion.

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Blank Paper
 Chapter7 Options

CONTENTS

Chapter7 Options
7.1 List of options •••••••••••••••••••••••••••••••••• P7-2
7.2 2-ml Sample loop ••••••••••••••••••••••••••••••• P7-3
<Procedure for Tubing Connection> •••••••••••••••• P7-4
<Procedure for changing the setting of tubing volume> • P7-5

7.3 4-channel OPT interface (PC-4) ••••••••••••••••••••• P7-7

7.4 SCSI board (option)•••••••••••••••••••••••••••••• P7-8
7.5 2-channel board •••••••••••••••••••••••••••••••• P7-9

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7.Options

7.Options

7.1 List of options

Service SILHT
Item Contents Manual Instruction
Manual
Installation Rack and Vials - P58
Sample loop 2ml P7-3 -
4-channel Optlink interface(PC-4) P7-7 -
SCSI board(PB-SCSI) P7-8 -
2-channel board(PC-55N) P7-9 -

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 7.Options

7.2 2-ml Sample loop

<Parts list>
2-ml sample loop kit(P/N228-37548-93) ASSY OP loop(P/N228-37552-91)
No. P/N Q’ty No. P/N Q’ty
Parts name Parts name
16 228-30668 1 10 018-26020-03 200MM
Instruction Manual 2ml Spiral tube KS series
10 228-37552-91 1 11 018-26020-03 200MM
ASSY OP loop Spiral tube KS series
11 228-16000 1 12 011-30791-03 4MT
ferule 1.6F SUS316 1.6x1.0
12 228-16001-03 1 13 011-30791-03 1MT
male nut 1.6MN W6 SUS316 1.6x1.0
13 228-30496 1 21 228-16001 5PCS
Instruction Manual OP loop 2ML Male nut 1.6MN
22 228-16000 5PCS
ferule 1.6F
23 228-16004-01 3PCS
coupling 1.6C-0.8
26 072-60310-03 1PC
Wire bandTY-53M
27 228-33817-03 1PC
Label FOR 2ML

ASSY OP loop(P/N228-37552-91)

Loop volume
-91: 3927 +403ul
-383ul

7-3
7.Options

<Procedure for Tubing Connection>

Open the controller panel and the auto-sampler’s door.
(1)Remove the upper panel of instruments
(2)Mount the 2-mL sanple loop as the shape shown in following figure
Place the ring part (A) of 2-ml sample loop (a coupling is connected with its end) onto the
measuring pump , and insert the other ring part (B) behind the side wall of the pump
head.

Ring part A
Ring part B

Ring part A Ring part B

the front view of instrument

the top view of instrument

(3)Handle the tubing as shown with a thick line in

figure
(4)Disconnect the standard sample loop from the Port of
the high-pressure valve and connect it with the coupling
that is connected with one end of ring A
(5)Connect the other end of 2-ml sample loop to the Port
1 of the high-pressure valve using the male nut and
ferrule .
(6)Mount the upper panel of instrument removed in
procedure (1) as before

Port 1 ofhigh-pressure valve

Caution
Insert the pipe until it hits the bottom of the connection hole. If the pipe dose not reach

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 7.Options

the bottom, dead volume will occur and cause a peak to spread out.

<Procedure for changing the setting of tubing volume>

To change the sample loop volume from the standard volume to 2mL to the standard
volume , it is necessary to select the sample loop type by changing the setting in the main
unit.
Following the procedure below to change the sample loop volume, select a standard loop
or option loop.
If the setting of loop volume is not changed, a proper analysis result may not be obtained
in a usual analysis work.
In addition , don’t change the setting of loop volume without exchanging the loop. A
proper analysis result may not be obtained

(1)Turn on the power and operate the keys on the controller panel as below.
f5 key(menu)/5(maintenance)/func key/f3 key(SIL)/4(CALIBRATION),enter key
(2)Inputting five-digit password at this time displays “f2 OK”. Press the [f2]key on that
occasion. The password set at delivery is[00000].

(3)Press the 4(SAMPLE-LOOP-SETTING) and the [enter] key in the CALIBRATION

function menu

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7.Options

(4)Set the sample-loop capacity in the following scxreen.

When a standard sample loop is used , press [f2] key . If it is expanded to a 2ml
sample-loop , press the [f5] key.
Setting is stored and the display returns to the CALIBRATION function menu
pop-up screen.

(5) Setting is stored and the display returns to the CALIBRATION function menu pop-up
screen. Operate the keys on the controller panel as below
8(EXIT),[enter]/5(EXIT),[enter]/f5(MENU)

Caution
The inner volume of this loop is approx.4mL.
After the installation, replace the inside of sample loop with the mobile phase sufficiently
before injecting a sample.

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 7.Options

7.3 4-channel OPT interface(PC-4)

<Construction of the 4-channel OPT interface>

4-channel OPT interface (P/N228-23517-91) consist of a PC-4 board , a instruction
manual (P/N228-10756) and a cable OPT ASSY(P/N228-25268-91).

4ch OPT interface

<Installation of 4-ch OPT interface>

(1) Remove the 3 screws (back side) of the SIL-HT to remove the top board.
(2) Remove the 2 screws to remove the side panel R.
Remove the 2 screws to remove one blind panel from the rear panel.
(3) Mount the 4-channel OPT interface from within the inside of the rear panel and fix it
with 2 screws.
(4) Connect the OPT ASSY to the connect of PC-4 and PB-SCL1A.
Align the mark on the connector of the flat cable and that
on the PC-4 and PB-SCL1A connector for the flat cable
(5) Remount the cover (top board and the side panel R), and fix with the screws.

4ch OPT interface

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7.Options

7.4 SCSI board (option)

<Construction of SCSI board>

SCSI board (P/N228-345359-91) consists of a PB-SCSI(P/N228-34372-91).

SCSI board

<Installation of SCSI board>

(1) Remove the 3 screws (back side) of the SIL-HT to remove the top board.
Remove the 2 screws to remove the side panel R.
(2) Remove the 2 screws to remove one blind panel from the rear panel.
(3) Mount the SCSI board ,and fix it with 2 screws.
(4)Connect the cable (accessory of SCL-10Avp) to the connector of SCSI board and
PB-SCL1A.
Align the mark on the connector of the flat cable and that on the SCSI board and
PB-SCL1A connector for the flat cable.
(5) Remount the cover (top board and the side panel R), and fix with the screws.

SCSI board

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 7.Options

7.5 2-channel board

<Construction of the 2-channel board>

2-channel board (P/N223-03507-91) consist of a PC board( PC-55N) (P/N223-02740-90) , a
cable for analog signal input (P/N221-25536-90) and a terminal board(P/N071-33102)

2-channel board

<Installation of 2-channel board>

(1) Remove the 3 screws (back side) of the SIL-HT to remove the top boad.
(2) Remove the 2 screws to remove the side panel R
(3) Mount the 2-channel board from the exterior of the rear panel and fix it with 2 screws.
(4 )Connect the cable(accessory of SIL-HT(SCL) to the connect of PB-SCL1A and PC-55N.
Align the mark on the connector of the flat cable and that on the PC-55N and
PB-SCL1A connector for the flat cable
(5) Remount the cover (top board and the side panel R), and fix with the screws.

Note
Both of DIP switch (SW1) should be set “ON” on the 1 st board and “OFF” on the
2 nd board.

2 channel board

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7.Options

<Input connector specifications>

The analog signal output by the chromatograph should be connected to analog input
+ ,-and , E. Shield cable must be used for connecting the cables
It is possible to input START and STOP signals from a auto injector via this connector.

Input connector

1 6

F A/D1 Input Terminals

A

No. Terminal Input/ Function

Name Output
1 F.G Frame ground
2 - Input Analog input(Negative)
3 E Input Analog input(earth)
4 5V Output Digital 5V
5 START Input Terminal are reserved for future use
6 GND Output Digital ground
A N.C. Unused
B + Input Analog input (positive)
C AUX_OUT Output Terminal are reserved for future use
D AUX_IN Input
E STOP Input
F RUN Input

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 Chapter 8 Factory Screeens
(Adjustment)

CONTENTS

Chapter 8 FACTORY SCREENS (Adjustment) P8-1

8.1 Adjustment Screen list •••••••••••••••••••••••••• P8-2
8.2 How to Display the FACTORY Screen •••••••••••••••• P8-3
1.RACK TEACHING •••••••••••••••••••••••••••• P8-5
2.INJ.P TEACHING •••••••••••••••••••••••••••• P8-7
3.VALVE TEACHING••••••••••••••••••••••••••• P8-9
4.ERASE INJ.P-DATA••••••••••••••••••••••••••• P8-12
5.ERASE RACK-DATA••••••••••••••••••••••••••• P8-12
6.RETRY COUNT•••••••••••••••••••••••••••••• P8-13
7.ALL CLEAR •••••••••••••••••••••••••••• P8-13
8.MONIT DRY-PE TEMP••••••••••••••••••••••••• P8-14
8.3 Inputting the Serial Number ••••••••••••••••••••••• P8-14
8.4 Upgrading the SCL(Firmware) P8-15
(Upgrading from the floppy disk ••••••••
8.5 Upgrades the SIL (firmware) ••••••••••••••••••••••• P8-16
8.6 Operation check of the panel key •••••••••••••••••••• P8-18
8.7 LCD display check ••••••••••••••••••••••••••••••• P8-19
8.8 Initialization of the backup memory •••••••••••••••• P8-19

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 8.FACTORY SCREEN

8 . FACTORY SCREENS (Adjustment)

8.1 Adjustment Screen List

Commands Functions Starting methods Pages

1. RACK TEACHING Adjusts the vial position on the rack. - Supply power with the f1 P8-5
2. INJ.P TEACHING Adjusts the injection port. key held down and release P8-7
3. VALVE TEACHING Adjusts the (high pressure/low the f1 key while the LED P8-9
pressure) valves. for run and the LED for act
4. ERASE INJ.P-DATA Deletes the injection port teaching data. are blinking alternately. P8-12
5. ERASE RACK-DATA Deletes the vial position data on the rack - Press the func key in the P8-12
6. RETRY COUNT Displays the retry counts of the X, 5. MAINTENANCE screen P8-13
Y, and Z pumps. to enter the SIL screen (f3
7. ALL CLEAR Performs initialization. key). P8-13
8. MONIT DRY-PE TEMP Displays the humidity of - Enter the 5 FACTORY P8-14
dehumidifier peltier. screen.
S/N Allows you to input the serial No. - Supply power with the f1 P8-14
key held down and release
the f1 key while the LED
for run and the LED for act
are blinking alternately.
- Press the func key on the
5. MAINTENANCE screen
to enter the SIL screen (the
f1 key).
- Enter the S/N (f1 key)
screen.
Ver UP Upgrades the SCL (firmware). - Supply power with the f1 P8-15
key held down and release
the f1 key while the LED
for run and the LED for act
are blinking alternately.
- Enter the VerUp screen
(the f5 key) on the 5.
MAINTENANCE screen.

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 8.FACTORY SCREEN

Commands Functions Starting methods Pages

Upgrading Upgrades the SIL (firmware). - Short-circuit the EVENT P8-16
cable (black/gray) and
supply the power.
- Upgrade the version using
the version upgrade kit and
a PC.
Operation check of the panel When you press the panel key Supply power with the f3 P8-18
key (except f1 and f2 keys), the pressed key held down and release
key appears in the center of the the f3 key while the LED
screen, allowing you to check the for run and the LED for act
operation of the panel key. are blinking alternately;
LCD display check Every time the f1 key is pressed, start up the system in this P8-19
all the area of LDC is made blank, way.
allowing you to check the LCD
display.
Initialization of the backup Pressing the f2 key performs P8-19
memory backup memory check. When PASS
is displayed, initialization of the
backup memory is performed.

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 8.FACTORY SCREEN

8.2 How to Display the FACTORY Screen

(1) Supply power with the f1 key held down and release the f1 key while the LED for
run and the LED for act are blinking alternately. The FACTORY screen starts in
this way.
(2) When the FACTORY screen appears, SILHT/Ver/SN is displayed in the upper right
of the LCD.

SILHTA/C
Ver
SN

(3) Enter the 5. MAINTENANCE screen in the MENU screen. Press the func key
once. Press the f3 key (SIL) to enter the SIL screen.

SIL screen

(4) Press the 5 key, and then press the enter key to enter the FACTORY screen.

FACTORY SCREEN

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 8.FACTORY SCREEN

1. Position adjustment of the rack vial (RACK TEACHING)

<Required Parts>
- Fixture (for 1.5 ml vial rack) P/N228-39802-02
- Fixture (INJ PORT teaching) P/N228-34416 one piece
- Right/left rack for 1.5 ml vials (standard accessories)

Jig
INJ PORT Teaching

Jig
For Rack Via
l.5ML

Type C Rack for 1.5 ml vials Type A Rack for 1.5 ml vials

<Adjustment Method>
(1) Set the racks for 1.5 ml vials (right/left) to the unit.
(2) Enter 1. RACK TEACHING screen in the FACTORY screen.
(Press the 1 key, enter key, and the f2 key in this order in the FACTORY screen to enter
the RACK TEACHING screen.)

(3) Adjust the rack vial according to the Teaching screen.

Teaching is performed on the vial positions (CORNER1 AND CORNER2) on the left
rack (Rack-L) and right rack (Rack-R) respectively.

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8.FACTORY SCREEN

CORNER 1 (RACK-L) Rack 1 vial No. 1

CORNER 2 (RACK-L) Rack 1 vial No. 10 (Type C) and vial No. 15 (Type A)
CORNER 1 (RACK-R) Rack 2 vial No. 1
CORNER 2 (RACK-R) Rack 2 vial No. 10 (Type C) and vial No. 15 (Type A)

CORNER 2 CORNER 2

CORNER 1 CORNER 1
C Type Rack A Type Rack

The teaching data is stored in Rack L (CORNER 1 and 2) and RACK R

(CORNER 1 and 2) respectively in one set.
For this reason, teaching cannot be performed for CORNER 1 only.
However, teaching for RACK-L only or RACK-R only is possible.
Vial rack teaching is normally performed on both RACK-L and RACK-R.

(4) Mount the fixture (for 1.5 ml vial rack, INJ PORT teaching) on CORNER 1
(RACK-L) shown in the screen.

(5) Perform the position adjustment of the rack vial needle.

X direction: key and key

Y direction: key and key
Z direction: 0 key: up and CE key down

Adjustment standard
(Front/Rear/Right/Left) direction: Within 0.2 mm from the center of the Jig
(Up/Down): Within 0.3 mm from the end of the Jig

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 8.FACTORY SCREEN

(6) Press the enter key after adjustment. The needle mount (Z mount) moves to
CORNER 2 (RACK-L).
(7) Mount the Jig (1.5 ml vial hook, INJ PORT teaching) on CORNER 2 (RACK-L) and
perform the adjustment in the same way.

(8) As above, perform the adjustments on CORNER 1 (RACK-R) and CORNER 2

(RACK-R).

Note 1.
Regarding the func key in the screen

f1 f3 f5

- As the f5 key (SHIFT) is not functioning, do not press the f5 key.

- The f3 key changes the adjustment position from CORNER 1 (RACK-L) to
CORNER 1 (RACK-R). This function can be used when performing teaching on
RACK-L or RACK-R only.
Note that using this function for the teaching performed on both the right/left
racks does not update the skipped teaching information and the data returns to
the state before teaching is performed.

Note 2.
Teaching can be performed with 1.5 ml vial racks only.

2. Position adjustment of the injection port (INJ. P TEACHING)

<Required Parts>
- JIG (INJ PORT teaching) P/N228-36837

<How to make the adjustment>

(1) Enter the 2. INJ. P TEACHING screen in the FACTORY screen.
Press the 2 key, enter key, and the f2 key in this order in the FACTORY screen to enter
the INJ. P TEACHING screen.)

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 8.FACTORY SCREEN

(2) A message saying "set adjustment tool" appears.

Mount the tool on the injection port and press the f2 key.
The needle mount moves to the injection port. The screen changes to the INJ. P
TEACHING screen.

(3) Perform the teaching on the injection port according to the teaching screen.

X direction: key and key

Y direction: key and key
Z direction: 0 key: up and CE key down

Adjustment standard
(Up/Down): Within 0.3 mm from the end of the JIG
(Front/Rear/Right/Left) direction: Should be in the center of the JIG

Within 0.3 mm

(4) Press the ENTER key after adjustment.

(5) Pull out the fixture.

Note 1. Regarding the func key in the screen

- The f5 key (SHIFT) is not functioning. Do not press the f5 key.
- Be sure to perform teaching with the vial detector board attached.

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 8.FACTORY SCREEN

- Using the Z-HOME function after adjustment,

check how the needle goes down to the INJ port.
- Check if the needle goes down straight into the center of the needle seal hole.
- Even when the needle is set in the center of fixture,
due to looseness and the like of the bearing portion of the Z mount,
the needle may sometimes not to fall straight in the center of the seal.
In such a case, deviating the needle slightly toward the back of the instrument
(for 1 to 2 pulses) may produce good result.

3. Position adjustmentof the valve (high pressure/low pressure) (VALVE TEACHING)

Perform slit position adjustment of the high pressure/low pressure valve.
Adjustment is required when the valve assembly is removed
and/or the sensor is removed.

(1) So that the valve slit can be seen

Remove the top plate, side plate R, and the inner plate of the main unit.
To adjust the low pressure valve, remove the floppy disk drive.

Floppy disk drive

Inner panel

Liquid leak tray

Remove the liquid leak tray of

the valve that you wish to
adjust.

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8.FACTORY SCREEN

(2) Enter the 3. VALVE TEACHING screen in the FACTORY screen.

Press the 3 key and then press the enter key in the FACTORY screen.

Press the f2 key (6V) for the high pressure valve adjustment.
Press the f5 key (LPV) for the low pressure valve adjustment.

(3) Perform the UP-SIDE and DOWN-SIDE adjustment of the valve slit according to
the screen instruction.

High pressure valve (6V) teaching screen. LPV teaching screen

Operation direction of the valve

key: Lowers the slit. key: Rises the slit.
After adjustment ends, press the enter key to complete the adjustment.

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 8.FACTORY SCREEN

Low pressure valve

Valve slit mark

High pressure valve
Good

Bad

Rotor

Schematic view of the slit front

When the slit portion is viewed from the front, it looks as shown in the diagram.
Be sure to place your line of vision at the extension of the slit edge.
This is because the rotor adjustment position varies depending on your visual
line.
Pass standard: The deviation of the rotor slit and the valve must be within +- 0.2 mm.

High pressure valve <6V> UP-SIDE High pressure valve <6V> DOWN-SIDE

Low pressure valve <LPV> UP-SIDE Low pressure valve <LPV> DOWN-SIDE

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8.FACTORY SCREEN

4. Deleting the teaching data of the injection port (ERASE INJ P-DATA)
Enter the 4. ERASE INJ. P-DATA screen in the FACTORY screen.
(Press the 4 key, and then press the enter key in the FACTORY screen.)

When replacing the needle, delete the

injection port teaching data using this
command, and then replace the needle.
This is to prevent the needle seal from
being damaged as the result of the changed
needle position before/after mounting.

Press the f2 key and delete the teaching data of the injection port.
When the injection port is stored in abnormal position, execute this command and
delete the teaching data to perform the position adjustment again.

5. Deleting the teaching data of the rack vial position (ERASE RACK-DATA)
Enter 5. ERASE RACK-DATA screen in the FACTORY screen.
(Press the 5 key, and then press the enter key in the FACTORY screen.)

Press the f2 key and delete the rack vial teaching data.
(When the adjustment data of the vial position on the rack is stored in the abnormal
position, execute this command and delete the teaching data to perform position
adjustment again.)

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 8.FACTORY SCREEN

6.Display of the retry times (RETRY COUNT)

Enter the RETRY COUNT screen in the FACTORY screen.
(Press the 6 key, and then press the enter key in the FACTORY screen.)
Retry times of the X direction, Y direction, Z direction, and measurement pump are
displayed.

7. Initialization of the memory (ALL CLEAR)

Enter the 7. ALL CLEAR screen in the factory WINDOW.
(Press the 7 key, and then press the enter key in the FACTORY screen.)
Memory initialization (ALL CLEAR) is executed by pressing the f2 key.
Initialization of TOTAL OP TIME and others are performed.
This is performed at the shipment from factory.
Note:
Do not execute this command normally as it deletes all the logs.

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 8.FACTORY SCREEN

8. Temperature display of the dehumidifier peltier (MONIT DRY-PE TEMP)

Enter the 8. MONIT DRY-PE TEMP screen in the FACTORY screen.
(Press the 8 key, and then press the enter key in the FACTORY screen.)
Temperature of the dehumidifier peltier is displayed.
Depending on the sample work, it operates when the temperature setting is lower than
the room temperature. It is fixed at 2 degree (+/- 3 degree).

8.3 Inputting the Serial Number

(1) Supply power with the f1 key held down and release the f1 key while the LED for
run and the LED for act are blinking alternately, so as to start up in the
maintenance screen.
(2) Enter 5. MAINTENANCE screen in the MENU screen. Press the f1 (SCL) key to
enter the SCL screen.
(3) Press the S/N (f1 key) to enter the serial number input screen. Register it by the f2
key.

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 8.FACTORY SCREEN

8.4 Upgrading the SCL (Firmware)

(Upgrading from the floppy disk)

Note:
Firmware is loaded on the controller unit (SCL) and the sampler unit (SIL) of this
instrument. Upgrading must be conducted respectively.

<How to upgrade>
(1) Supply power with the f1 key held down and release the f1 key while the LED for
run and the LED for act are blinking alternately, so as to start up in the
maintenance screen.
Note:
Upgrade the version with the power connected to the main unit SILHTA/C being
OFF (disconnected).

(2) Enter the 5. MAINTENANCE screen in the MENU screen. Press the func key once.

(3) Insert the floppy disk for upgrading into the drive. Press the Ver up (f5 key) to
enter the version up screen.

f1 f2 f3 f4 f5 func

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 8.FACTORY SCREEN

(4) Select the program (SCLxxx.BNL) for upgrading, press SEL (f5 key) to start
upgrading.

func key functions:

- f1 key (PAGE UP) --- Switches the file pages (go UP).
- f2 key (BACKWRD) --- Performs selected movement of the execution file (go UP).
- f3 key (FORWARD) --- Performs selected movement of the execution file (go DOWN).
- f4 key (PAGE.DN) --- Selects the file page (go DOWN).
- f5 key (SEL) --- Executes upgrading of the selected file.

(5) After the end of upgrading, the screen goes off. Turn off the power of the main unit
SILHTA/C, and then supply the power again.

Note:
- Do not turn OFF the power during upgrading. When the power is turned OFF
during upgrading. Turning OFF the power during upgrading not only fails
upgrading, but may damage ROM (SCL), requiring ROM replacement.

8.5 Upgrading the SIL (Firmware)

<Required parts>
- Event cable (P/N 228-39249)
- Upgrading VP kit
228-35530-91 (for 100V))-38 (for 200V), one set
Event cable
- PC for upgrading use, Upgrading software

Upgrading VP kit

<Upgrading procedure>
To execute upgrading, refer to the ROM Version Upgrading Kit Instruction Manual
P/N228-30305 of the LC-10Avp series.
(1) Connect the RS-232C cable of the upgrading fixture to the serial port of the PC. (If
there are two or more ports, either one will do.)
(2) Optical link REMOTE terminal of the unit SILHT and the fixture optical port for
upgrading are connected. Connect the power supply to the upgrading fixture using
the power supply adapter attached to the upgrading kit.
Connect the RS-232C
cable to the serial port of
the PC
Connect the optical link
REMOTE terminal of SILHT.

Connect the power supply to the

upgrading fixture using the power
supply adapter.

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(3) <How to start the upgrading unit>

(3-1) Short-circuit the EVENT cable (black/gray) and connect it to the EXTcontrol
terminal at the lower rear surface of the main unit.
(3-2) Turn ON the power of the instrument and connect the event cable in (3-1) to
automatically start up the instrument in upgrading mode. When upgrading starts in
the screen, the auto-sampler does not perform initialization.
For the VP series, power is supplied while holding down the VP key.
As this instrument does not have the VP key, supply power with the above procedure.

Short-circuit the
EVENT cable
(black and gray).

Connect to the
EXTcontrol
terminal.

Starting up the SILHT upgrading mode

(4) Start up the upgrading program update.exe installed by the

Operate the upgrading programs as follows:

1. When starting up the upgrading program, perform configuration setting in the
communication/Settings menu. Once performed, settings are stored in the PC,
eliminating the need to make the settings again in the next startup or after.
- Port: Set to the port No. to which the RS-232C cable is connected at the rear surface
of the PC.
- Baud Rate: 19200 bps (other values not permitted)
- Time: Around 20000
- Retry count: Around 10

2. Press the "Connect" button to link to the unit.

- It is OK when " Succeeded to connect to the
instrument!" appears.
- When "Communication Time Out! " appears, it
indicates linking failure. Check if there is any defective connection of the cables or
incorrect configuration settings (such as Baud Rate and Port) of the upgrading

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 8.FACTORY SCREEN

program.
3. Set the floppy disk containing the upgrading data to the PC.
4. Specify the directory (normally A:¥) containing the upgrade file of the floppy in
"File/Change Directory", and press OK. (File name is not displayed until OK is
pressed.)
5. Upgrade file list appears in the "Files" box. Click on and select the target file.
6. Pressing the "Update" button starts upgrading. The total amount of byte and the
amount of the transferred byte are displayed below the dialog box.
7. Finally, a message dialog box that notifies the end of upgrading appears.

Note:
Do not turn OFF the power of the main unit SILHT right after the dialog box notifying
the completion of upgrading appears. When power supply is turned OFF right after
upgrading, ROM contents may be damaged. Turn OFF the power after 30 seconds or
more from the appearance of the dialog box showing upgrading completion.

8.6 Operation Check of Panel Key

(1) Supply the power of the main unit with the f3 key held down and release the f3 key
while the LED for run and the LED for act are blinking alternately, so as to start up.
(2) When any key except the f1 key and the f2 key are pressed, the pressed key appears
in the center of the screen, enabling you to check the panel key operation.

DIAG_F3_Mode(check KEY input)

SLEEP

The screen that appears when you press The screen that appears when
the f3 key to start up the system. the SLEEP key is pressed.

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8.7 LCD Check

(1) Supply the power of the main unit with the f3 key held down and release the f3 key
while the LED for run and the LED for act are blinking alternately, so as to start up.
(2) Every time the f1 key is pressed, LCD display changes to whole area blank or
marked out whole area, enabling you to check the LCD.
Note: The area for func in the lower right is not marked out.

Whole area blank Whole area marked out

8.8 Checking the Backup Memory (Initialization)

(1) Supply the power of the main unit with the f3 key held down and release the f3 key
while the LED for run and the LED for act are blinking alternately, so as to start
up.
(2) When the f2 key is pressed, backup memory check is performed. When PASS is
appears, initialization of the backup memory automatically starts.

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Blank Paper
 Chapter9 Electrical system

CONTENTS

Chapter9 Electrical system P9-1

9.1 Electrical system ••••••••••••••••••••••••••••••• P9-2
9.2 Storage parameter •••••••••••••••••••••••••••••• P9-3
9.3 DIP switch setting ••••••••••••••••••••••••••••• P9-4
9.4 Replacement of Board ••••••••••••••••••••••••••• P9-4
9.4.1 Replacement of PBSCL-1A•••••••••••••••••••••• P9-4
<Removing the FLASH EEPROM>••••••••••••••••• P9-5
1.When the original EEPROM is mounted(PB-SCL1A)•• P9-5
2.To replace with new EEPROM•••••••••••••••••• P9-6

9.4.2 Replacement of PCB 10Avp CPU•••••••••••••••••• P9-7

<Removing the FLASH EEPROM>••••••••••••••••• P9-7
1.When the original EEPROM is mounted(PCB 10AVP CPU ASSY) • P9-7
2.To replace with new EEPROM•••••••••••••••••• P9-8

9.5 Diagram(Power unit) •••••••••••••••••••••••••••• P9-9

9.6 Diagram (SILHT main unit) ••••••••••••••••••••••• P9-10
9.7 Diagram (System controller) ••••••••••••••••••••••• P9-11

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9.Electrical system

9.Electrical system

9.1 Electrical system

Storage parameter
board Items Page
PB-SCL1A Storage parameter in FLASH EEPROM P9-3
Storage memory in SRAM P9-3
PCB 10AVP CPU ASSY Storage parameter in FLASH EEPROM P9-3
Storage memory in SRAM P9-3

DIP switch setting

board Items Page
PB-SCL1A SIL-HTA(DIP switch setting) P9-4
SIL-HTC(DIP switch setting) P9-4

Board replacement
board Items Page
PB-SCL1A When the original FLASH P9-5
EEPROM(M9,M10) is mounted
To replace new FLASH P9-6
EEPROM(M9,M10)
PCB 10AVP CPU ASSY When the original FLASH P9-7
EEPROM(M3) is mounted
To replace new FLASH P9-8
EEPROM(M3)

Electrical system diagram

unit name Page
Power supply unit P9-9
SILHT main unit P9-10
SILHT System controller P9-11

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 9.Electrical system

9.2 Storage parameter

back up
SCL memory
board Storage information INI ALL
Initializ
I.M CLEAR ation
P207 P8-13 P8-19
PB-SCL1A FLASH EEPROM Serial Number - - -
(M9,M10) VP Log(maintenance ,error operation) - - o
OP TIME - - o
SRAM All parameters and time program o - o
of analysis file (file0 to file9)
Auto injector analysis table o - o
All of auto injector control parameters o - o
Setting by System menu o - o
System Configuration o - o
PCB 10AVP CPU ASSY FLASH EEPROM System serial number - - -
(M3) INJ port teaching information - - -
Valve (high-pressure, low-pressure) - - -
teaching
Rack teaching information - - -
(including MTP)
INJ COMP FACTOR - - -
Leak sensor level - - -
Retry count (X, Y, Z, measuring pump) - - -
Frequency of needle seal used - o -
6V ROTATION - o -
LPV ROTATION - o -
VP Log(maintenance ,error operation) - o -
OP TIME - o -
SRAM
Use frequency of needle seal (as - o -
temporary storage)
6 V ROTATION (as temporary storage) - o -
LPV ROTATION (as temporary storage) - o -
(o:Initiallization)
Note
When PCB 10AVP CPU ASSY and PB-SCL1A are replaced, normally mount the original
EEPROM.
When replacing EEPROM, system information must be set and adjusted again. For
replacing method, refer to the "Replacement of Board(9.4.1 9.4.2) .

SRAM memory is backed up by the power supplied by the backup battery.

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9.Electrical system

9.3 DIP switch setting

For PB-SCL1A, DIP switch must be set by SILHTA and SILHTC.
Remove the top board and right side plate R.

<Dip switching setting >

In the case of SILHTA ,set No.2 of DIP SW on the PB-SCL1A to ON ,
and No.1 and No.3-No.6 to OFF.
In the case of SILHTC ,set No.3 of DIP SW on the PB-SCL1A to ON , andNo.1-No.2 and
No.4-No.6 to OFF.

right side

PB-SCL1A DIP SWITCH

DIP switch setting

1 2 3 4 5 6
SILHTA OFF ON OFF OFF OFF OFF
SILHTC OFF OFF ON OFF OFF OFF

Note: When replacing the board, setting of the board is required.

9.4 Replacement of Board

9.4.1 Replacement of PB-SCL1A
CAUTION:
Before starting work, turn OFF the power and disconnect the power cable.

CAUTION:
When replacing PB-SCL1A , normally mount the original EEPROM (M9, M10). After

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 9.Electrical system

EEPROM is replaced, system information must be set again. (Refer to 9.2 Strage parameter)

< Removing of the FLASH EEPROM>

(1) Remove the top board and side panel R

PB-SCL1A

(2) Remove the connector on PB-SCL1A. Loosen the screw and remove PB-SCL1A
(3) Remove the FLASH EEPROM with special tool.

FLASH EEPROM ROM2P/N228-34650-93

ROM1 P/N228-34650-92

exclusive-use tool

1. When the original EEPROM (M9, M10) is mounted (PB-SCL1A)

Removal and mounting of Using the exclusive use tool, remove two EEPROM
EEPROM (ROM1 M9) (ROM1 M9, ROM2 M10) of the board installed in the
(ROM2 M10) system and mount them to new board.

Mounting backup battery Before mounting the backup battery, check the voltage of
it. (New battery has voltage of 3.0 V or more.)
If the battery has been exhausted, replacement is
required.

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9.Electrical system

Mounting the board Mount A new board to the system.

Date and time setting Set the date using SET.D.T (f2 key) on the System screen.

Initialization Display the Calibration menu of SCL (f1 key) of

MAINTENANCE menu (MENU 5) and perform
initialization (Init).

Parameter setting Set the system, analysis parameter, SIL parameter (needle
stroke etc.) etc.

Operation check Check the operation.

Note: When the power is turned OFF, SRAM memory is backed up by the power
supplied by the backup battery.
When the backup battery and the board are replaced, make setting again or load the file
saved in the floppy disk.

2. To replace with new EEPROM (M9, M10) (PB SCL-1A)

Mounting backup battery Before mounting the backup battery, check the voltage of
it. (New battery has voltage of 3.0 V or more.)

Mounting new board Mount a new board (new EEPROM (ROM1 M9, ROM2
(Setting DIP SW) M10) to the main unit.

Setting the date and time Set the date with SET.D.T (f2 key) in the system menu.

Initialization (Press f3 key With pressing f3 key, turn ON the power. While LED is
and turn ON the power, blinking, release f3 key and start with the check program
initialize with f2 key.) menu.
Press f2 key to check the memory and perform
initialization.

Input of serial number Start the factory menu. (With pressing f1 key, turn ON
the power, and release f1 key while LED is blinking.)
Input the serial number with S/N(f1 key) menu of SCL(f1
key) menu in MAINTENANCE screen (MENU 5).

Parameter setting Set the date and time, system, analysis parameter, and SIL
parameter (needle stroke etc.)

Operation check Perform operation check.

Note: When the power is turned OFF, SRAM memory is backed up by the power
supplied by the backup battery.
When the backup battery is replaced and when the board is replaced, make setting again

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 9.Electrical system

or load the file saved in the floppy disk.

9.4.2 Replacement of PCB 10Avp CPU

CAUTION:
Before starting work, turn OFF the power and disconnect the power cable.

CAUTION:
When replacing the PCB10AVPCPU (SIL-CPU board), normally mount the original
EEPROM (M3). After EEPROM is replaced, system information must be set again and
adjusted.

<Removing of FLASH EEPROM>

(1) Remove the top plate and right side plate R
(2) Remove the connector on PCB 10AVP CPU ASSY. Loosen the screw and remove
the PCB 10AVP CPU ASSY.

PCB 10AVP CPU ASSY

(3) Remove the FLASH EEPROM with special tool.

FLASH EEPROM

PCB 10AVP CPU ASSY

1.When the original EEPROM (M3) is mounted (PCB 10AVP CPU ASSY)

Removal and mounting of Using the exclusive-use tool, remove EEPROM M3 of the
EEPROM (ROM M3) board installed in the system and mount it to a new board.

Mounting backup battery Before mounting the backup battery, check the voltage of
it. (New battery has voltage of 3.0 V or more.)

If the battery has been exhausted, replacement is required

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9.Electrical system

Mounting new board Mount a new board to the system.

(Initialization)

Parameter check Check SIL parameter (needle stroke etc.)

Operation check Perform operation check.

Note: When the power is turned OFF, SRAM memory is backed up by the power
supplied by the backup battery. SRAM memory is initialized at replacement of backup
battery or board (Retry count number)

2.To replace with new EEPROM (M3) PCB 10AvpCPU

Mounting backup battery Before mounting the backup battery, check the voltage of
it. (New battery has voltage of 3.0 V or more.)
If the battery has been exhausted, replacement is
required.

Mounting new board Fix new EEPROM (M3) to a new board, and mount it to
the main unit
When ROM type is “MONITOR VP ROM”,
SIL(ROM)version upgrading is required
Initialization (ALLCLEAR) With pressing f1 key, turn ON the power. While LED is
(with pressing f1 key and blinking, release f1 key and start with the factory menu.
turn ON the power.
Execute FACTORY menu 7 ALL CLEAR of SIL menu
Initialize with FACTORY
(func f3 key)
menu.)

(Input of serial number) Start the factory menu. (With pressing f1 key, turn ON
the power, and release f1 key while LED is blinking.)
Input the serial number with S/N (f1 key) menu of SCL (f1
key) menu in MAINTENANCE screen (MENU 5).

Adjustment Perform adjustment.

Injection port teaching
Rack teaching
Valve (high-pressure, low-pressure) teaching
Leak sensor
Correct injection volume (INJ COMPFACTOR)

Operation check Perform operation check.

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9.5 Diagram (Power unit )

SCHEMATIC FOR SILHT ELECTORICAL UNIT ASSY

W:WHITE
B:BLACK

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9.6 Diagram (SILHT main unit)

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 9.Electrical system

9.7 Diagram (System controller)

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Blank Paper
 Chapter10 Maintenance 1

CONTENTS

Chapter10 Maintenance 1 P10-1

10.1 Maintenance ••••••••••••••••••••••••••••••••• P10-3
<Consumable parts>•••••••••••••••••••••••••••• P10-3
<Maintenance List> •••••••••••••••••••••••••••• P10-3
10.2 Z mount •••••••••••••••••••••••••••••••••••••• P10-5
10.2.1 Removing Z mount••••••••••••••••••••••••••• P10-5
10.2.2 Removal of Z feed screw ••••••••••••••••••••••• P10-10
10.2.3 Z feed screw grease-up ••••••••••••••••••••••• P10-11
10.2.4 Z shaft oiling ••••••••••••••••••••••••••••••• P10-11
10.2.5 Z sensor replacement ••••••••••••••••••••••••• P10-12
10.3 Removing of XY arm ••••••••••••••••••••••••••••• P10-15

10.4 Belt Adjustment ••••••••••••••••••••••••••••••• P10-17

10.4.1 X belt Adjustment ••••••••••••••••••••••••••• P10-17
10.4.2 Y belt Adjustment ••••••••••••••••••••••••••• P10-18
10.4.3 Z belt Adjustment ••••••••••••••••••••••••••• P10-18
10.5 Valve mount •••••••••••••••••••••••••••••••••• P10-18
10.5.1 Removing valve mount ••••••••••••••••••••••• P10-19
10.5.2 Removing and mounting high-pressure valve ••••••• P10-20
10.5.3 Removing and mounting low-pressure valve •••••• P10-21
10.6 Measuring pump ••••••••••••••••••••••••••••••• P10-22
10.6.1 Structure of Measuring pump •••••••••••••••••• P10-22
10.6.2 Disassembling of Measuring pump ••••••••••••••• P10-23
10.6.3 Removing the measuring pump feed screw ••••••••• P10-24
10.6.4 Adjustment of slit disc position of the measuring pump P10-26
10.6.5 Replacement of valve mount sensor P10-27
(high-pressure valve , low-pressure valve , and measuring pump)
10.7 Replacement and Adjustment of X Encoder Sensor •••••• P10-29
10.8 Replacement of X PCB Sensor ••••••••••••••••••••• P10-30
10.9 Adjustment of Y Encoder •••••••••••••••••••••••• P10-30
10.10 Replacement of Y Sensor •••••••••••••••••••••••• P10-32
10.11 Replacement of the board(LC2K INJ2) •••••••••••••• P10-34
10.12 Replacement of Rack sensor ••••••••••••••••••••• P10-35
10.13 Replacement of Door sensor ••••••••••••••••••••• P10-35

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 10.14 Replacement of Cooling Rack Plate •••••••••••••••• P10-37
10.14.1 Dismantling procedure ••••••••••••••••••••••• P10-37
10.14.2 Assembly Procedure ••••••••••••••••••••••••• P10-40

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 10.MAINTENANCE1

10.MAINTENANCE1

10.1 MAINTENANCE
<Consumable parts>
Service SILHT
Parts Name Maintenance Item Manual Instruction
Page (Page)
Needle Seal Replacement P11-6 P132
Measuring pump Seal Replacement - P135
Measuring pump Plunger Replacement - P139
LPV rotor and stator Replacement - P141
HPV rotor and stator Replacement - P145
Needle Replacement P11-4 P149
Fuse Replacement - P151
Panel Replacement - P152

Service SILHT
Maintenance Item Manual Instruction
Page (Page)
Piping(PEEK tube) P11-9 -
Sample loop P11-11 -
Removing the INJ port piping P11-10 -

<Maintenance List>
Parts Name Maintenance Item Service
Manual
Page
Z mount Removing Z mount P10-5
Removal of Z feed screw P10-10
Z feed screw grease-up P10-11
Z shaft oiling P10-11
Z sensor replacement P10-12
XY ARM Removing XY ARM P10-15
Teaching Injection Port P8-7
Rack Vial P8-5
Belt Adjustment X belt adjustment P10-17
Y belt adjustment P10-18
Z belt adjustment P10-18
Valve Mount Removal of valve mount P10-19
Removing and mounting the high-pressure valve P10-20
Adjustment of the high-pressure valve P8-9
Removing and mounting the low-pressure valve P10-21
Adjustment of the low-pressure valve P8-9
Disassembling the measuring pump (plunger, P10-23
spring, and bearing)

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10.MAINTENANCE1

Removing the measuring pump feed screw P10-24

Adjustment of slit disc position of the measuring P10-26
pump
Replacement of valve mount sensor P10-27
(high-pressure valve, low-pressure valve, and
measuring pump)
X Encoder Sensor Replacement and Adjustment of X Encoder Sensor P10-29
X PCB Sensor Replacement of X PCB Sensor P10-30
Y Encoder Slit Adjustment of Y Encoder Slit P10-30
Y Sensor Replacement of Y Sensor P10-32
Board (LC2K Replacement of Relay Board (LC2K INJ2) P10-34
INJ2)
Rack Sensor Replacement of Rack Sensor P10-35
Door Sensor Replacement of Door Sensor P10-35
Cooler Unit Replacement of Sample Cooler Unit P10-37

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 10.MAINTENANCE1

10.2 Z mount

10.2.1 Removing Z mount

Remove the needle from INJ port in the Z-Home state.
Turn OFF the power and disconnect the power cable.

1) Remove the top board ASSY (P/N228-40880).

Loosen three screws M3x6 on the back, slide the top board backward and remove it.
Top board

Frame bar
Frame stay ASSY

2) Remove the frame stay ASSY (P/N228-41010-91) and frame bar (P/N228-37036).
Remove two flat head screws M3x4.

Frame bar

Frame stay ASSY

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3)In the SIL-HTC, Remove the front panel F ASSY (P/N228-37512-91).

Front panel F

4) Remove the upper panel .

Removing the Upper panel

5) Remove the side panel L (P/N228-40882) M3x6 screws 2 pcs

Side panel L

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 10.MAINTENANCE1

6) Remove the panel

L1 (P/N228-40025), L2 (P/N228-40026) and L3 (P/N228-37573-91)

Panel L
Panel L2 Panel L3 Panel L1

Panel L

Screw sems M4x8 5pcs Screw M3x6 2pcs

This item is not specially required for removal of Z mount.

To remove Z cover, rotate Z motor with hand and lower the needle approx 25 to 28 mm
Remove three M3x6 screws and the spring.

rotate Z motor with

hand
Remove the spring

Z cover

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7) Remove the sample loop from Z mount (Remove the male nut bind fixing screw).
8) With pushing up the white connector, draw out the cable FPC-Z (P/N228-37541-91).

FPC-Z
White connector

Remove from the white connector

9) Peel off the cable FPC-Z from the fence XY (P/N228-37516-91).

10) Remove the screw that fixes Z mount and X belt. (Screw sems M3x10 2 pcs)

the fence XY

Screw sems M3x10 2 pcs

11) Hold down X belt with your finger and remember the degree of tension.
12) Loosen X mount pulley screw located under the encoder cover of X arm.

Encorder cover on X arm

X mount pulley screw

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13) Loosen four setscrews and pull out the shaft X (P/N 228-36363) to the right, and
remove Z mount (P/N228-37502-92). Setscrew M3x4 4 pcs

set screws
set screws

shaft Main unit front

Apply sampler oil (P/N228-40593-91) to the Y shaft.

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10.2.2 Removal of Z feed screw

1) Remove Z cover .
2) Remove the needle.
3) Memorize the degree of tension of Z belt by your finger.
4) Loosen Z motor fixing screws (sems M3x8 4 pcs). Remove Z belt
5) Remove Z feed screw E type stop ring (E-ring) (P/N026-66204) under Z mount.

E type stop ring (E-ring)

Flat tip screwdriver

Z mount

6) Rotate Z feed screw pulley (counterclockwise viewed from above) and remove it.

Rotate Z feed screw pulley

Setscrew M3x4 P/N021-04919-02 2 pcs

Pulley Z P/N228-36690 1 pc
Bearing (BRG DDLF-1260ZZ) P/N031-22615 2 pcs
Z feed screw P/N228-36684 1 pc

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10.2.3 Z feed screw grease-up

Remove the needle from INJ port in Z-Home state.
Turn OFF the power and disconnect the power cable.
Remove Z cover (P/N228-40232-91) of Z mount.
1) With rotating Z feed screw, wipe out stain and grease stuck to the feed screw.
(If the stain cannot be removed completely, remove Z feed screw.)
2) Apply the grease (P/N228-40638-91) of approx. 10g thoroughly to Z feed screw.
Rotate Z motor by hand to make the grease stick to the feed screw.
(At adjustment in the factory, grease of approx. 10g has been applied thoroughly.)

P/N228-40638-91 grease consists of following parts

P/N Parts name remarks
017-30829-01
grease POLYREX#2
038-00196-02
Vial glass010205
228-40839-01
Lavel,2010grease

10.2.4 Z shaft oiling shaft

Remove the needle from INJ port in Z-Home state. Z feed screw
Turn OFF the power and disconnect the power cable.
Remove Z mount front Z cover.
1) Rotate Z motor by hand, move the needle mount vertically,
and wipe out the stain stuck to the shaft.
(If the stain cannot be removed, loosen one setscrew M3x4 (P/N021-04919-02), peel off
FPC cable stuck above the Z mount shaft hole, and remove the shaft to wipe out the
stain.)
2)Apply the oil (P/N228-40593-91) thoroughly to the shaft.
Apply approx. 1 ml oil (P/N228-40593-91) evenly and thinly to the shaft.
Be sure to remove the excess oil that stays in a portion.

P/N228-40593-91 oil consists of following parts

P/N Part Name Remarks
017-30305-04
Oil daphnymultiway
C220
038-00196-02
Vial , glass 010205
228-40839-02
Label,2010 Oil

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10.2.5 Z sensor replacement

To replace photo sensor of Z mount, use three parts attached to the three photo sensors
with the cable of FPC-Z ASSY (P/N228-37541-91).
Remove the needle from INJ port in Z-Home state.
Turn OFF the power and disconnect the power cable.
Remove the top board, frame bar, frame stay, and panel T (type C).

1) Remove Z feed screw.

Remove Z feed screw.

2) Remove the sensor attached to the vial guide shaft.

the vial guide shaft

the sensor
3) By pushing up the white connector from the board LC-2K INJ2, disconnect the cable
(FPC-Z).
4) Remove the cable (FPC-Z) from the fence XY. Remove the fence XY.
Remove the cable (FPC-Z)
from the fence XY

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5) Remove Z home position sensor by loosening the

fixing screw.

fixing screw

6) Peel off FPC cable of the removed sensor

Peel off FPC cable

7) Remove the remained needle Z sensor and peel off FPC cable.

8) Remove FPC cable from Z mount.

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9) Mount a new sensor cable (FPC-Z).

With referring to the figure, align the mark of FPC cable to Z mount and mount the
new sensor.
Note:
Sensor positioning is performed using the partition
plate. Position alignment of sensor mounting is not
necessary.
Adjustment is performed with teaching.

PCB INJ2

FPC-Z

upside of Z mount

FPC-Z

FPC-Z

side of Z mount

10) After having mounted the sensor, mount the feed screw, belt, Z motor, XY fence, and
cover.

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10.3 Removing of XY arm

Remove the needle from INJ port in Z-Home state.
Turn OFF the power and disconnect the power cable.
Remove the top board, frame bar, frame stay, panel T (type C) .

1) Remove the front panel F (type C) and inner panel (type A).
(To perform the work with ease, remove the side plate L and
panels L1, L2, and L3

2) Remove two screws that fix Y belt and base ASSY.

two screws

3) Remove the sample loop from Z mount.

4) Remove the flat cable of connector CN1 of board PCBINJ2.
Shift the connector and disconnect the cable PCBINJ2

Remove the flat cable of connector CN1

the flat cable
of board PCBINJ2.

5) Loosen two screws sems M3x6, pull forward the shaft Y (P/N 228-36354) and remove
the ASSY base (SIL).
Screw sems M3x6 2 pcs

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pull forward the shaft Y

Remove the XY arm

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10.4 Belt Adjustment

X belt

Z belt

Y belt

10.4.1 X belt Adjustment

Adjustment of X belt tension at the factory is performed using a sonic type belt tension
meter in the range between 77 Hz and 100 Hz.
(Standard of X belt tension is 1 mm to 1.5 mm when X belt is pressed slightly by
finger.)
Adjust X belt tension by loosening X mount pulley screw located under X arm encoder
cover

X arm encoder cover

X mount pulley screw

X belt

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10.4.2 Y belt Adjustment

Adjustment of Y belt tension at the factory is performed using a sonic type belt tension
meter in the range between 60 Hz and 81 Hz.
(Standard of Y belt tension is 1.5 mm to 2.5 mm when Y belt is pressed slightly by
finger.)

Adjust Y belt tension using Y motor fixing screw (sems M4x16 4 pcs).
1) To loosen Y motor fixing screw
Remove the valve mount.
Remove the board (SIL-MAIN LC2K-COOL).
Panel R (228-37511-91) (screw truss M4x10 5 pcs) should be removed.

2) Adjust Y belt tension using four Y motor fixing screws.

Y motor fixing screw 4 pcs

Y belt

10.4.3 Z belt Adjustment

Adjustment of Z belt tension at the factory is performed using a sonic type belt tension
meter in the range between 386 Hz and 518 Hz.
(Standard of Z belt tension is 0.5 mm to 1 mm when Z belt is pressed slightly by finger.)
Adjust Z belt tension using four Z motor fixing screws M3x8 sems.

Z motor fixing
Z belt screws

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10.5 Valve mount

10.5.1 Removing valve mount
Turn OFF the power and disconnect the power cable.

1) Remove the following valve tubing.

Low-pressure valve No.2 (to rinse port)
No.4 (rinsing liquid)
High-pressure valve No.1 (to sample loop)
No.4 (from INJ port)
No.5 (to column)
No.6 (from pump)

2) Remove the top board (P/N228-40880)

3) Remove the side panel R (P/N228-40880).
Remove the connector from SIL-MAIN board.
Connector CN21 (measuring pump motor)
Connector CN19 (low-pressure valve)
Connector CN18 (high-pressure valve)
Connector CN5 (V sensor)

Remove the side panel R

4) Loosen the screw and remove the leak sensor tray.

5) Loosen four cap bolts M4x10 fixing the valve mount,
Pull out the valve mount toward you.
At this occasion, be very careful not to damage the flexible print board (FPC) at the left
side of the valve mount by getting it caught by the removed pipes in step 1).

pull out the valve mount forward.

Loosen four cap bolts M4x10 fixing the valve mount

Valve mount

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10.5 Valve mount

10.5.2 Removing and mounting high-pressure valve

< Removi ng high-pressure valve>

1) Remove the tubing mounted to the high-pressure valve.
2) Take out the valve mount.(refer to 10.5.1)
3) Loosen one screw (bind M3x6) and remove the sheet metal valve sensor holder
(P/N228-35981).
4) Remove three valve fixing screws (sems M4x12),
Pull the valve slightly toward you and deviate it to the left to remove it .

Valve fixing screw (sems

Sensor holder M4x12) 3 pcs
fixing screw high-pressure valve

valve mount

<Mounting>
1) Mount the valve from left side and fix it with screw. As the position is decided by the
pin, adjustment is not necessary.
2 )Mount the valve sensor holder (P/N 228-35981).
Take care so that the sensor may not get contact with the valve disc.
3) Apply the grease white (P/N017-30829-01 polirex #2 400G) thinly to whole
circumference of motor side gear. (At adjustment in the factory, 2 g of grease has been
applied.)
(Grease should not stick out from the gear so that the grease may not stick to the
sensor disc.)
Set the valve mount to the main unit and conduct teaching.(refer to 8.3)

gear(high-pressure valve)

high-pressure valve motor

high-pressure valve

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10.5.3 Removing and mounting low-pressure valve

<Removing low-pressure valve>
1) Remove the tubing mounted to the low-pressure valve.
2) Take out the valve mount. (refer to 10.5.1)
3) Loosen one screw (bind M3x6) and remove the sheet metal valve sensor holder
(P/N228-35981).

low-pressure valve

Sensor holder fixing screw

Valve fixing screw (sems

M4x12) 3 pcs

valve mount

<Mounting>
1) Mount the valve from left side and fix it with screw. As the position is decided by the
pin, adjustment is not necessary.
2) Mount the valve sensor holder (P/N 228-35981). Take care so that the sensor may
not get contact with the valve disc.
3) Apply the grease white (P/N017-30829-01 polirex #2 400G) thinly to whole
circumference of motor side gear. (At adjustment in the factory, 2 g of grease has been
applied.)
(Grease should not stick out from the gear so that the grease may not stick to the
sensor disc.)
Set the valve mount to the main unit and conduct teaching. (refer to 8.3)

gear (low-pressure valve)

low-pressure valve

low-pressure valve motor

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10.6 Measuring pump

10.6.1 Structure of Measuring pump

Side that has mark on the

bearing (sheet)

Disc with smaller inside diamete

Disc with larger inside diameter
Side that has mark on the
Mount the retainer in the
bearing (sheet)
direction illustrated

Whether the assembly plunger moves freely must be checked after head holder (14) is
installed. (Push the lower part of the assembly plunger SIL to check.)

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10.6.2 Disassembling of Measuring pump

1) Remove the tubing connected to the measuring pump, then
remove the measuring pump head.

seal holder

remove the measuring pump head

2) Draw out the seal holder (P/N228-37530-91), and then remove the plunger SIL
(sapphire) (P/N228-37531-91) with the plunger removing tool.

two cap
plunger SIL bolts
(sapphire)

3) To remove the head holder (P/N228-36335-01), loosen two cap bolts M4x30
alternately and remove the head holder with taking care so that the spring
(P/N228-36387-01) may not protrude.
Bearing is pushed and mounted with the head holder spring ring. When mounting
the bearing, pay attention to the direction of it.
When mounting the head holder, screw hole for mounting the plunger should come to
the center.

Bearing viewed from this side

Valve mount (measuring body)
Disc with larger inside diameter

Disc with smaller inside diameter

Disc with smaller inside diameter

pump spring Mount the retainer in the

direction illustrated Disc with larger inside diameter
Bearing viewed from this side
head holder

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10.6.3 Removing the measuring pump feed screw

1) Remove the measuring pump head, head holder, plunger, and the return spring.
2) Remove the valve mount.

3)Loosen the four screws fixing of

the measring pump motor, and remove the measuring pump.
4) Remove the horizontal direction partition panel of measuring pump.
Loosen two setscrews for slit disc and remove the slit disc with pulley.

groove

Two setscrews for slit disc

the horizontal direction partition panel of measuring pump
Clean the dirt on the surface as well as
the groove surface of the valve mount at disassembly.

slit disc

5) Extract the cross head.

Extract the cross head.

Apply sampler oil (P/N228-40593-91)

thinly on the cross head.

cross head the measuring pump feed screw

After cleaning, thickly apply sampler grease

(P/N228-40638-91) on the screw portion of the feed screw. bearing

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Note: Direction of bearing

Groove side

Side that has mark on the

bearing (sheet)
(Inside diameter is small.)

Side that has mark on the

bearing (sheet)
(Inside diameter is small.)

The bearing for assembly does not have

front or back.

Apply sampler grease (P/N228-40638-91)

Groove side at the three spots between the poles.

Note:
After disassembling, adjust the position of slit disc.
Refer to the position adjustment of measuring pump slit disc

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10.6.4 Adjustment of slit disc position of the measuring pump

Adjustment of measuring pump slit (disc of measuring pump back) becomes necessary
after having replaced the sensor and having performed maintenance of measuring
pump feed screw.
There are two items of criteria of slit disc position

Initial operation of measuring pump

When the power is turned ON, the measuring pump performs the following operation
during initialization.
1. Detects the sensor in linear direction.
2. Stops for two seconds.
3. Detects the sensor in rotating direction.

[Adjustment]
Turn ON the power. Then, turn OFF the power in the stop state of above 2 of
initialization.

[Criteria] 117degrees
Slit disc position should be in the range 72 to 117 degrees in 72 degrees
clockwise direction when viewed the measuring pump slit disc
from the back.
If the slit disc position is not in this range, remove the disc fixing
screw, rotate the disc so that it comes within the range and fix it
again with the fixing screw.
(Fixing hole of disc is set in the interval of 45 degrees.)
If the slit position is near 72 degrees and it is difficult to judge the above mentioned
range, fix the disc on the 117 degrees side.

[Criteria] 24 degrees
disc slit
(Turn ON the power and on the READY state of completion of
initialization (on the notch of slit disc), turn OFF the power.
Rotate the slit disc by hand counterclockwise until it
mechanically stops. At this time, viewed from the rear of the
system, the slit of measuring pump should be in the range 24 to 360 degrees
360 degrees after passing the sensor position in the rotating
direction.

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10.6.5 Replacement of valve mount sensor (high-pressure

valve, low-pressure valve, and measuring pump)

As soldering is usually difficult, the photosensor (high pressure valve, low pressure
valve, and measurement pump) attached to the valve mount is replaced by the set of
the sensor (FPC-Z) assembly.
Sensor replacement of the part having the following part number is also possible.
Photo interpreter: GP1S94 P/N061-7557-01

Note: After replacement of the sensor, it is required to perform the valve teaching for
high-pressure, low-pressure and adjust the measuring pump slit disc.

1) Pull out the valve mount.

the fixing screw of measuring
pump slit sensor

Valve mount left side Valve mount right side

Valve mount front

2) Remove the fixing screw of measuring pump slit sensor and remove the sensor.

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3) Fix a new sensor with the screw. Next, remove the horizontal direction detecting
sensor of the measuring pump and mount the new sensor. Mount the measuring
pump motor.
With referring to the figure, remove the sensor in the order.

4)After having mounted the valve mount to the main unit, mount the following
connectors to SILMAIN board.
Connector CN21 Measuring pump
Connector CN19 Low-pressure valve motor
Connector CN18 High-pressure valve motor
Connector CN5 V sensor
5)Perform teaching for high-pressure valve and low-pressure valve and adjust the
position of slit disc of measuring pump

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10.7 Replacement and Adjustment of X Encoder Sensor

1) Remove the top board, frame stay ASSY, frame bar, and panel T (type C).
2) Loosen X encoder cover fixing screw (sems M3x16) and remove the sensor cover X
(P/N228-36378-01)

In this occasion, as the clearance between the cover and the slit is small, slide the cover
straight toward the rear of the unit and then remove it.

X encoder cover

3) Remove X encoder sensor (PCB, LC2K-XENC ASSY P/N228-37355-91) and replace

it.
The clearance adjustment between the sensor and the slit is 0.3 +/- 0.2 mm. However,
adjustment is usually unnecessary as it is so designed as to satisfy this dimension
when the slit holder is mounted on the slit without looseness.
Move Z mount by hand in X horizontal direction to check that the slit does not touch the sensor.

When mounting and removing, take care not to touch the slit and bend it.

slit holder

0.3+/-0.2mm

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10.8 Replacement of X PCB Sensor

Remove the top board, frame stay ASSY, frame bar, and panel T (type C).
Remove X PCB sensor (P/N228-37365-91) by removing one screw (truss M3x8).

photo interrupter
P/N061-7155-01

X PCB sensor

10.9 Adjustment of Y Encoder Slit

1) Remove the top board, frame stay ASSY, frame bar, and panel T (type C).
2) Remove the side panel R, and remove the valve mount.
3) Pull out the Fan connector from PCB and remove
the rear panel.
4) Remove the board PBSCL-1 A,SIL-MAIN,and
LC2KCOOLASSY.

SIL-MAIN
LC2KCOOLASSY

PBSCL-1A
the rear panel

5) To remove the board, loosen five fixing screw (truss M4x10) of panel R
(P/N228-37511-91) and one screw (sems M3x6) of sensor cover XY (P/N228-36378-01).
panel R

five fixing screw (truss M4x10)

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6) Loosen the sems screw M3 and remove the sensor cover XY(P/N228-36378-01).

the sems screw M3

7) Loosen two setscrews of slit holder to adjust the slit position.

Move the mount in Y direction by hand to check that the slit does not touch the sensor.

0.3+/-0.2mm

Adjust clearance between the sensor and the slit to the position 0.3 +/-0.2 mm from
the right of sensor viewed from the main unit front.

8) Panel R has two positioning pins. Pay attention to those positions.

two positioning pins

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10.10 Replacement of Y Sensor

Replacement of sensor (FPC-Y) (P/N228-37540-91)
Remove the panel R (228-37511-91). (Refer to Section 12.7 Y Encoder Slit)
Loosen the screws fixing Y sensor and encoder sensor and remove the sensor.
Mount a new sensor referring to the following diagram and the mounting dimensions
in the next page.

P/N228-37540-91 FPC-Y

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The mounting dimensions of Y sensor

photo interrupter
P/N061-7155-01

photo interrupter
P/N061-7155-01

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10.11 Replacement of the board (LC2K INJ2)

LC2K INJ2

CAUTION:
On the SIL-HT, the SIL adjustment parameter is not written in the EEPROM of LC2K INJ2.
Even if the board is replaced, it is not necessary to change the adjustment parameter.

Remarks:
On the LC2010. the SIL parameter is written in the EEPROM of LC2K INJ2.
When replacing the board, the information "Load and Save" for the parameter is
necessary. Refer to LC2010 Service Manual.

Disconnect the connector and remove the board fixing screw from the front side then
replace the board.

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10.12 Replacement of Rack sensor

Remove the front panel F (type C).
Loosen two rack sensor fixing screws (sems, M3x6) and remove the rack sensor.
Remove the rack sensor from the cable and replace it.

rack sensor

rack sensor

10.13 Replacement of Door Sensor

To replace the door sensor, remove the sensor fixing screw.
<Removing the sensor fixing screw >
1) Remove PEEK tubing (No. 4) of high-pressure valve and PEEK tubing (No. 2) of
low-pressure valve .
2) Loosen the fixing screw of INJ port ASSY and remove INJ port ASSY.
Drain pipe is mounted to INJ port ASSY. Hold the pipe using flat tip screwdriver, lift
up INJ port ASSY and remove it.

Inj port assy

flat tip screw

drain pipe

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3) Insert the Philips screwdriver into the portion from which INJ port ASSY was
removed, loosen the sensor fixing screw, then remove the sensor. (Philips screwdriver
of 150 mm length is necessary)

screwdriver of 150 mm length

is necessary

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10.14 Replacement of Cooling Rack Plate and peltier

10.14.1 Dismantling procedure

1) Remove the device’s top plate and right-side plates and sampler’s rear panel.
2) Remove panel F (sampler’s transparent front plate), the two stays of sampler’s upper
section and the Autosampler unit’s top plate.
3) Remove the Z mount fixing screw and needle’s septum.
4) Remove the single rack sensor fixing screw.
5) Remove the rack plate cover (semitransparent
cover surrounding the rack plate).

6) Remove the two fan fixing screws on rear of

sampler unit and remove the fan together with
sheet metal stays from duct.

7) Remove the dehumidifying Peltier power connector and thermistor connector from
PCB. Work is made easier if the flat cable also is removed at this time.

8) Remove dehumidifying Peltier from duct.

flat cable

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Remove the sponge caps from the four corners

and loosen screws. Proceed carefully because the
dehumidifying Peltier is tightly packed into the
duct. In particular, care should be taken because
the harness connection unit catches between the
duct and base when the dehumidifying Peltier is
removed from the base.
Tighten the three main base fixing screws while
pressing the main base toward the back of the
device.
9) Remove duct.

Remove duct.

10) Loosen main base fixing screws (two at the front and one at the back).
11) Release the harness via the two Peltier harness fixing clamps of the rack plate.
12) Remove the Peltier power supply connector of the rack plate from the PCB.

V mount

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13) Lift up the base slightly and pull out the rack plate Peltier harness in a straight
line in the direction of the rear of the device.

14) Slide the Z mount to the left side of the device, now move it to the back and remove
the four rack plate fixing screws.

15) Place a hand under the Autosampler and push up the radiation fan of the rack
plate Peltier to be able to pull out the rack plate ASSY. The whole unit can be removed
if it is pulled upwards at an angle, but be careful not to hit the needle when doing so.

16) Degrease the area surrounding the main base Peltier mounting hole with acetone
and then coat the area with water repellent.
If white rust has already appeared on the base, wipe away the rust with a commercial
rust remover before commencing work. At this time, be careful not to scatter the
removed rust specks
17) Remove the 12 M4 truss screws on the rack plate to enable separation of the Peltier
unit. A slight amount of force is required in the separation task because the Peltier
unit is adhered to the rack plate with thermal compound.

thermistor transistor

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10.14.2 Assembly Procedure

1) A thin insulation sheet is sandwiched between the
transistor and rack plate.

2) Coat the thermistor with silicon compound before securing. Follow assembly procedure 1
to secure the transistor with the recovered insulation sheet sandwiched between the
transistor and rack plate. After securing is complete, coat the entire indentation with
silicon bond (do not leave any part uncoated).

3) Gather the thermistor and the harness of the transistor to the center rear and
bundle them there.

4) Fit the rack peltier heat insulator (P/N228-38662) to the square holes of the rack
plate. Have the thermistor and transistor gathered in 3) come out from the center.

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5) Apply the thermal compound to the peltier and then mount it to a new rack plate.
Be sure to fully tighten the screw marked by an arrow mark first.

6) Semi-tighten all of the Peltier fixing screws and then fully tighten the screws marked by
arrows in following fig. (This is to prevent the thermal compound from rising up.)
Mount the cooling racks on both sides and set a vial in each #40. Push the vials down to
set them in place and make sure that the rise between rack and rack plate at the front end
of the rack plate is <…
0.8mm.
7) Stick heat insulation material to both ends of the rack plate in alignment with the rack
plate and front end.

Insulation
material

Insulation
material

8) Insert the long convex section of the pin recovered in assembly procedure 1 into the
rack plate hole. (Insert pin from the rear of the area shown)
9) Mount the rack plate ASSY to the main base. Be sure to pass the harness through the
convex hole at the rear of the rectangular hole of the main base when mounting. Place
Teflon washers on the three screws outside of the area marked by an arrow. Evenly tighten
the screws in the four corners.

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10) In reverse order to item 13 of the dismantling procedure, pass the harness through the
notch of the main base. Also make sure that the sponge and Peltier fin marked by arrows
do not interfere with each other.
11) Secure the harness to the wiring fixing material removed in item 11 of the dismantling
procedure
12) Connect the rack plate power supply and thermistor connector in their original
positions.
13) Affix the packing seal around the rack plate so that the rack plate is covered.
14) Mount the rack sensor ASSY.
15) Mount the duct.

16) Insert the dehumidifying Peltier into the duct. And pass the harness between the base
and duct.

17) Connect the harness of the dehumidifying Peltier in its original position.
18) Secure the dehumidifying Peltier with the screws in the four corners and imbed sponge
caps in the screw holes.
19) Mount the fan on rear of sampler unit.

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Take the connector section of the fan on the right side (when viewed from the rear of the
device) and trap it in the notch at the bottom left of the duct. Now pass the black covering
of the left-side fan’s connector through the notch.

20) Mount the sampler’s rear plate. Be sure to connect the fan.

21) Mount panel F (sampler’s transparent front plate), the two upper stays of the sampler
and the top plate of the Autosampler unit.
22) Mount the devices top plate and right side plate.

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 Chapter11 Maintenance 2

CONTENTS

Chapter11 Maintenance 2 P11-1

11.1 List of maintenance items •••••••••••••••••••••••• P11-2
11.2 Needle •••••••••••••••••••••••••••••••••••••• P11-4
11.3 Needle seal ••••••••••••••••••••••••••••••••••• P11-6
11.4 Piping (PEEK tubing) ••••••••••••••••••••••••••• P11-9
11.5 Removing the INJ port piping ••••••••••••••••••••• P11-10
11.6 Sample loop •••••••••••••••••••••••••••••••••• P11-11

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11-1
11.MAINTENANCE2

11.Maintenace 2

11.1 List of maintenance items

<Replacement of consumable part>
Service SILHT
Parts Name Maintenance Item Manual Instruction
Page (Page)
Needle Seal Replacement P11-6 P132
Measuring pump Seal Replacement - P135
Measuring pump Plunger Replacement - P139
LPV rotor and stator Replacement - P141
HPV rotor and stator Replacement - P145
Needle Replacement P11-4 P149
Fuse Replacement - P151
Panel Replacement - P152

Service SILHT
Maintenance Item Manual Instruction
Page (Page)
Piping(PEEK tube) P11-9 -
Sample loop P11-11 -
Removing the INJ port piping P11-10 -

<Removing and assembling>

Parts Name Maintenance Item Service
Manual
Page
Z mount Removing Z mount P10-5
Removal of Z feed screw P10-10
Z feed screw grease-up P10-11
Z shaft oiling P10-11
Z sensor replacement P10-12
XY ARM Removing XY ARM P10-15
Teaching Injection Port P8-7
Rack Vial P8-5
Belt Adjustment X belt adjustment P10-17
Y belt adjustment P10-18
Z belt adjustment P10-18
Valve Mount Removal of valve mount P10-19
Removing and mounting the high-pressure valve P10-20
Adjustment of the high-pressure valve P8-9
Removing and mounting the low-pressure valve P10-21
Adjustment of the low-pressure valve P8-9

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11-2
 11.MAINTENANCE2

Disassembling the measuring pump (plunger, P10-23

spring, and bearing)
Removing the measuring pump feed screw P10-24
Adjustment of slit disc position of the measuring P10-26
pump
Replacement of valve mount sensor P10-27
(high-pressure valve, low-pressure valve, and
measuring pump)
X Encoder Sensor Replacement and Adjustment of X Encoder Sensor P10-29
X PCB Sensor Replacement of X PCB Sensor P10-30
Y Encoder Slit Adjustment of Y Encoder Slit P10-30
Y Sensor Replacement of Y Sensor P10-32
Board (LC2K Replacement of Relay Board (LC2K INJ2) P10-34
INJ2)
Rack Sensor Replacement of Rack Sensor P10-35
Door Sensor Replacement of Door Sensor P10-35
Rack Plate Rack plate and peltier unit P10-37

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11.MAINTENANCE2

11.2 Needle

<Repair part>
Contents of Needle assembly (P/N228-41024-92)
P/N Q’ty remarks
Part name
228-40817-04 1 length
needle 93mm
228-28430 1
ferule1.2F
228-36689 1
male nut needle

<Removing Needle>
For needle replacement, refer to Section 10.1.7 in the instruction manual.
This section describes supplementary contents.

1) Remove the rack.

2) Execute NEEDLE-REPLACEMENT of MAINTENANCE menu
Press the [5] key with the “MENU” screen displayed the” MAINTENANCE” screen
Press the [FUNC] key for once to proceeded the func key column by one and press the
[SIL] key.

MENU “5 MAINTENANCE” SCREEN

“SIL” SCREEN

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11-4
 11.MAINTENANCE2

3) Pressing the [2] key and the [Enter] key in the ”MAINTENANCE” screen displays the
following “SYSTEM CHECK” screen.
Select “4.NEEDLE REPLACEMENT “,and the pop-up menu “REPLACE THE NEEDLE
f2 OK” appears.

4)Press the [f2] key. The needle move to the pre-detemined position and the following
pop-up menu appears.
Turn off the power.

“Turn off the power , and replace the needle”

5) Open the door.

In the SIL-HTC, detach the panel.

Panel F ASSY

Loosen the panel screw with a Phillips head screwdriver , and pull out the panel,
slightly shifting it downward.

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11.MAINTENANCE2

6) Loosen three fixing screws and remove the Z-truck cover

screw

screw

screw

the Z-truck cover

7)Loosen and remove the male nut of the needle assembly with a spanner .

male nut

needle

11.3 Needle seal

<Consumable Part>
Needle seal (P/N228-33355-01)
P/N Q’ty Remarks
Part Name
228-33355-01 1 Material
Needle seal,PEEK 10XL :PEEK

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11-6
 11.MAINTENANCE2

<Replacing the Needle Seal>

For needle replacement, refer to Section 10.1.2 in the instruction manual.
This section describes supplementary contents.

1) Remove the needle from Injection Port in the Z-HOME state.

Pressing the [0] key with the “MENU” screen displayed shows “ANALYTICAL
SEQUENCE” screen. Pressing the [func] key twice and the [f1] key (Z-HOME) once
moves the Z-truck to home position.

“ANALYTICAL SEQUENCE” screen

f1 key(Z-HOME) Z-HOME State

2) Turn off the power

3) Open the door, and remove the sample racks
4) In the SIL-HTC, detach the panel

Panel F ASSY

5) Remove the injection port nut with the spanner14mm

nut

the spanner14mm
Tip the spanner14mm is not provided.

6) Remove the injection port sleeve.

7) Use a toothpick or similar tool to push the needle seal from the sleeve.
8) Insert a new needle seal into the sleeve
9) Insert the new needle seal and the sleeve into the housing with the needle seal facing
down. First , tighten the nut by hand , then the 14 spanner to tighten it an additional 90
degree.

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11.MAINTENANCE2

Tip
When tightening the cap of new needle seal, tighten it manually up to hard to
move and then use the wrench with 90 degrees. Since the PEEK needle seal is
used, tightening angle of wrench is 90 degrees. If using Vespel needle seal
(LC2010), its angle is 45 degrees. So be careful that the tightening angle varies
depending on the material of needle seal.

10) Turn on the instrument.

11) Reset the Needle seal counter.
Press the [5] key with the “MENU” screen displayed the” MAINTENANCE” screen
Press the [FUNC] key for once to proceeded the func key column by one and press the
[SIL] key.

“SIL” screen
Press the [4] key and the [enter] key in
the “SIL” screen.

Press the [6] key and the [enter] key in

the
CALIBRATION function menu pop-up
to display the
“6:CONSUMABLES-SETTIN” screen
Press [1] key and the [enter] key

Pressing th

Press the [f2] key changes the screen

12) In the SIL-HTc, attach the panel

13)Close the door
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11-8
 11.MAINTENANCE2

11.4 Piping(PEEK tubing)

Piping(high pressure valve-preheat block)

Piping(Inj Port-high pressure valve)

The PEEK tubings are used for the piping (between INJ port and high-pressure valve;
and between high-pressure valve and column).

CAUTION
Since there are unusable solvent and pressure range for PEEK tube, refer to "Safety
Precautions" in the instruction manual.

P/N PEEK tubing FEP tubing

IDxLength Length
Inj Port-high pressure valve 228-41380-91 0.25IDx200 140MM
high pressure valve-preheat block 228-41380-92 0.25IDx600 540MM

Piping(high pressure valve-preheat block)

Ferrule(SUS)

Piping(Inj Port-high pressure valve) Ferrule(SUS)

Note
Ferrule and male nut for PEEK tube are made of SUS.

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11-9
 11.MAINTENANCE2

11.5 Removing the INJ port piping

<Procedure of removing the injection port piping>

1) Loosen and remove the malenut(No. 4) of
high-pressure valve and the malenut(No.2) of low
pressure valve

2) Loosen the fixing screw of INJ port ASSY, and remove INJ port ASSY.
Drain pipe is attached to INJ port ASSY. Hold down the drain pipe fixed to INJ port
ASSY using the flat tip screwdriver and lift up INJ port ASSY and remove it.

the flat tip screwdriver

Drain pipe

lift up INJ port ASSY and remove it

Injection Port Piping(PEEK)

3) Loosen the male nut of Injection piping and remove it.

Note: When connecting the PEEK pipe using SUS ferrules and male nuts.
Tighten the male nut with a spanner referring to the amount described as follows:
Male nut with the outer diameter of 6 mm: Manually tighten the nut until it is hard
enough, then tighten for about 120 degrees further using a spanner.
Male nut with the outer diameter of 8 mm: Manually tighten the nut until it is hard
enough, then tighten for about 90 degrees further using a spanner.

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 11.MAINTENANCE2

11.6 Sample loop

<Sample loop parts list>

The Sample loop ASSY (P/N228-41370-91) consists of the following parts.
P/N Q’ty Remarks
Part Name
228-37549-91 1
sample loop
228-16001 1
male nut,1.6MN
228-16001-03 1
male nut,1.6MN W3
228-16000 2
ferule,1.6F
Instruction Manual 1
228-30364

<Removing and installing the sample loop in the unit>

For sample loop replacement, refer t the instruction manual.
This section describes supplementary contents.

<Removing the sample loop in the unit>

1) Pressing the [0] key with the “MENU” screen displayed shows “ANALYTICAL
SEQUENCE” screen. Pressing the [func] key twice and the [f1] key (Z-HOME) once
moves the Z-truck to home position.

f1 key(Z-HOME) Z-HOME state

2) Turn off the power

3) Open the Door and remove the rack

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11-11
11.MAINTENANCE2

4) In the SIL-HTC, remove the F panel

F panel assy

5) Remove the male nut of No.1 on high pressure valve

6) Remove the sample loop from the needle drive unit.

Remove the screw from the band which fixes the loop
Loosen the piping part (male nut ), and remove the
loop.
Fixing band

Male nut

7)Loosen the screw of holder. Remove the sample loop from the groove on the holder

screw

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 11.MAINTENANCE2

<Attaching a new sample loop>

Sample mounting specifications.
Sample mounting specifications are shown in the following figures 1, 2, 3 and 4.

The outer diameter of each loop must be

between the two coaxial cylindrical surfaces
that are separated for 5 mm.
Top plate side:
Z mount The rear end of the loop
Panel R must not protrude from the
Z mount end surface.
teflon tube
The clearance between
the sample loop the front end portion of
of the loop and the end
the sample loop holder
surface of the protrusion of
the main base must be 17mm or more.

When fixing the sample loop in the panel R, The needle must be located The upper end of the loop
the loop must pass above the sample at the inj port and the Z mount must satisfy the above
loop holder fixing screws as shown in Fig. 1. and the sample loop are The upper end of the loop
The position relation of the Teflon tube end satisfying the three-position relation.
surface and the holder end surface should -mentioned dimension
satisfy the above mentioned dimensions. Must be 15 mm or less against the Z mount top
surface shown in the figure.

The needle must not interfere with the bush when the needle is down.

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11.MAINTENANCE2

<Attaching a new sample loop>

1) Take the sample loop out of the box carefully not to deform it.
2) As shown in the following fig , attach the male nut and the ferrule to the pipe at the
end on the side marked by an arrow of the sample loop. Insert them to the former piping
port shown in following figure and tighten the male nut .

3) Put the tube on the groove on the holder, then tighten the screw to fix the sample loop.
Mathc the end of the Teflon tube (outer diameter: 3mm) covering the sample loop with the
end of the holder ,then fix the sample loop so that its rightmost loop portion becomes
parallel to the panel.
the groove on the holder
rightmost loop portion

holder

the groove on the panel

5) Insert the sample loop into the groove on the panel

If the sample loop is bent tightly into an acute angle , the inside of the piping may be
damaged. Be careful.
6)Attach the male nut and ferrule to the pipe at the other end of the sample loop , insert
them into the port No.1 of the high pressure valve and tighten the male nut
6)In the SIL-HTC , attach the F panel which has been removed to the former status.
7) Turn on the power ,and confirm that the sample loop is not interfering with other
parts.

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 11.MAINTENANCE2

<Checking Sample loop >

1)Mount a 1.5 mL rack (the resin rack or cooling rack) on the right side of the
instrument.
2) Place a vial at the first vial position from the front (resin rack: #91, cooling rack: #61),
and start injection.
3)Check that the first turn of the loop on the Z-mount side does not interfere with the black bush on
the front side of the Z-mount .

Z mount
First turn of the loop

Black bush

Front view of the Z-mount (Correct status)

4) Manually turn the Z-mount pulley to lower the sample

loop to the height indicated .

5) Check that the distance from the pipe center of the loop’s first turn on the Z-mount side and the
Z-mount is properly maintained, as shown i.

3-7mm

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11-15
11.MAINTENANCE2

6) Perform the Z-HOME operation and then turn off the power supply.
Pressing the [0] key with the “MENU” screen displayed shows “ANALYTICAL
SEQUENCE” screen. Pressing the [func] key twice and the [f1] key (Z-HOME) once
moves the Z-truck to home position.

“ANALYTICAL SEQUENCE” screen

f1 key(Z-HOME) Z-HOME State

7) Check that the loop dimensions are proper, as shown .

38+/-3mm
First turn only
Sample loop shape checking

95-100mm
8) Measure the difference in height between the upper part of the loop’s first turn and the
Z-mount, to check if the requirement shown following fig is satisfied.

19+/-2mm

Dimensional check in the height

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 11.MAINTENANCE2

9) Move the loop on the side of panel R, so that the amount of the deviation between the
loop on panel R and that on the Z-mount falls within 5 mm.

the amount of the deviation between

the loop on panel R and that on the
Z-mount falls within 5 mm.

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11-17
Blank Paper
 Chapter12 Trouble shooting

CONTENTS

Chapter12 Troubling shooting P12-1

12.1 Error Messages •••••••••••••••••••••••••••••••• P12-2
12.2 MAINTENANCE(Part Replacement) •••••••••••••••• P12-4

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12-1
12.Trouble shooting

12.Trouble shooting

12.1 Error Messages

This unit has several diagnostic functions. Upon detection of an abnormality , an alarm
sounds and an error message appears on the display .
The error messages are listed below , along with possible causes and corrective action.

TIP
Each message falls into one of the following three categories. The category is shown the “Type”
column.
Fatal : The unit stops operation.
Alarm : Press CE to clear the error message.
Warning : An error message is displayed, and alarm sounds . Unit operation continues .

Error message Classification Cause and measure

ROM FAILURE Fatal Cause: Displayed as ROM abnormal.

Board failure or ROM may be defective.
Measure: Check and replace board, or ROM.

RAM FAILURE Fatal Cause: Displayed as RAM abnormal. Board may be

failed.
Measure: Check and replace board.

NO NEEDLE HOME X Fatal Cause: Operation of needle X (horizontal) direction

is defective.
Measure: Load of mechanical unit may be large and
electrical unit (sensor, motor) may be defective. Check
the cause of error and replace.

NO NEEDLE HOME Y Fatal Cause: Operation error of needle Y (forward and

backward) direction.
Measure: Load of mechanical unit may be large and
electrical unit (sensor, motor) may be defective. Check
error cause and take measure.

NO NEEDLE HOME Z Fatal Cause: Operation error of needle Z (forward and

backward) direction.
Measure: Load of mechanical unit may be large and
electrical unit (sensor, motor) may be defective. Check
error cause and take measure.

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 12.Trouble shooting

NO 6-PORT VALVE Fatal Cause: Rotating position of high-pressure valve is

HOME defective.
Measure: Load of mechanical unit may be large and
electrical unit (sensor, motor) may be defective. Check
error cause and take measure.

NO LPV HOME Fatal Cause: Rotating position of low-pressure valve is

defective.
Measure: Load of mechanical unit may be large and
electrical unit (sensor, motor) may be defective. Check
error cause and take measure.

NO PUMP HOME Fatal Cause: Operation of measuring pump is defective.

Measure: Load of mechanical unit of measuring pump
may be large, or adjustment may be defective, or
electric unit (sensor, motor) may be defective.
Check cause of error and take measure.

NO VIAL DETECTED Alarm Cause: This message is displayed as sample vial is

not set to the set vial number.
Measure: In continuous analysis, analysis that has
not been set is not executed, but next analysis is
executed.

ERR LEAK DETECT Alarm Cause: This message is displayed if detection value of
leak sensor is exceeded. Liquid leak may have
occurred, leak sensor may not be sufficiently
adjusted, or leak sensor may be defective.
Measures: Check liquid leakage.
Check cause of error message and take measure.

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12-3
12.Trouble shooting

12.2 MAINTENANCE(Part Replacement)

<Consumable parts>
Service SILHT
Parts Name Maintenance Item Manual Instruction
Page (Page)
Needle Seal Replacement P11-6 P132
Measuring pump Seal Replacement - P135
Measuring pump Plunger Replacement - P139
LPV rotor and stator Replacement - P141
HPV rotor and stator Replacement - P145
Needle Replacement P11-4 P149
Fuse Replacement - P151
Panel Replacement - P152

Service SILHT
Maintenance Item Manual Instruction
Page (Page)
Piping(PEEK tube) P11-9 -
Sample loop P11-10 -
Removing the INJ port piping P11-9 -

<Maintenance List>
Parts Name Maintenance Item Service
Manual
Page
Z mount Removing Z mount P10-5
Removal of Z feed screw P10-10
Z feed screw grease-up P10-11
Z shaft oiling P10-11
Z sensor replacement P10-12
XY ARM Removing XY ARM P10-15
Teaching Injection Port P8-7
Rack Vial P8-5
Belt Adjustment X belt adjustment P10-17
Y belt adjustment P10-18
Z belt adjustment P10-18
Valve Mount Removal of valve mount P10-19
Removing and mounting the high-pressure valve P10-20
Adjustment of the high-pressure valve P8-9
Removing and mounting the low-pressure valve P10-21
Adjustment of the low-pressure valve P8-9
Disassembling the measuring pump (plunger, P10-23
spring, and bearing)
Removing the measuring pump feed screw P10-24

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12-4
 12.Trouble shooting

Adjustment of slit disc position of the measuring P10-26

pump
Replacement of valve mount sensor P10-27
(high-pressure valve, low-pressure valve, and
measuring pump)
X Encoder Sensor Replacement and Adjustment of X Encoder Sensor P10-29
X PCB Sensor Replacement of X PCB Sensor P10-30
Y Encoder Slit Adjustment of Y Encoder Slit P10-32
Y Sensor Replacement of Y Sensor P10-32
Board (LC2K Replacement of Relay Board (LC2K INJ2) P10-34
INJ2)
Rack Sensor Replacement of Rack Sensor P10-35
Door Sensor Replacement of Door Sensor P10-35
Rack Plate Replacement of Sample Cooler Unit and pertier unitP10-37

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12-5
Blank Paper
 Chapter 13 Circuit Diagram

CONTENTS

ChaPter13 Circuit Diagram

PB SCL-1A•••••••••••••••••••••••••••••••••••••••• P13-2
PB SCL-4••••••••••••••••••••••••••••••••••••••••• P13-10
PCB 10AVP CPU ASSY•••••••••••••••••••••••••••••• P13-12
SIL MAIN•••••••••••••••••••••••••••••••••••••••• P13-15
LC2K-FILTER ASSY•••••••••••••••••••••••••••••••• P13-26
LC2K INJ2••••••••••••••••••••••••••••••••••••••• P13-27
PCBLC-2K COOL ASSY•••••••••••••••••••••••••••••• P13-29
PB SCL-2••••••••••••••••••••••••••••••••••••••••• P13-35
PB SCL-3••••••••••••••••••••••••••••••••••••••••• P13-37
PB SCL-5••••••••••••••••••••••••••••••••••••••••• P13-39

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13-1
13.Circuit Diagram

PB SCL-1A ASSY P/N228-35224-93

Fig. PB SCL-1A ASSY

SIL-HTA/HTC Service Manual

13-2
 SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PB SCL-1A 1/7

13-3
13-4
SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PB SCL-1A 2/7
 SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PB SCL-1A 3/7

13-5
13-6
SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PB SCL-1A 4/7
 SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PB SCL-1A 5/7

13-7
13-8
SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PB SCL-1A 6/7
 SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PB SCL-1A 7/7

13-9
13.Circuit Diagram

PB SCL-4 P/N228-34369-91

Fig. PB SCL-4

SIL-HTA/HTC Service Manual

13-10
 SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PB SCL-4 1/1

13-11
13.Circuit Diagram

PCB 10AVP CPU ASSY P/N228-34259-93

Fig. PCB 10AVP CPU ASSY

SIL-HTA/HTC Service Manual

13-12
 SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB 10AVP CPU 1/2

13-13
13-14
SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB 10AVP CPU 2/2
 13.Circuit Diagram

PCB SIL MAIN P/N228-40900-91

Fig. PCB SIL MAIN

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13-15
13-16
SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB SIL MAIN 1/10
 SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB SIL MAIN 2/10

13-17
13-18
SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB SIL MAIN 3/10
 SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB SIL MAIN 4/10

13-19
13-20
SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB SIL MAIN 5/10
 SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB SIL MAIN 6/10

13-21
13-22
SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB SIL MAIN 7/10
 SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB SIL MAIN 8/10

13-23
13-24
SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB SIL MAIN 9/10
 SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB SIL MAIN 10/10

13-25
13.Circuit Diagram

PCB LC2K-FILTER ASSY P/N228-37270-92

Fig. PCB LC2K-FILTER ASSY

Fig. CIRCUIT DIAGRAM PCB LC2K-FILTER ASSY 1/1

SIL-HTA/HTC Service Manual

13-26
 13.Circuit Diagram

PCB LC2K-INJ2 ASSY P/N228-37320-91

Fig.PCB LC2K-INJ2 ASSY

SIL-HTA/HTC Service Manual

13-27
13-28
Fig. CIRCUIT DIAGRAM PCB LC2K-Inj2 ASSY 1/1

SIL-HTA/HTC Service Manual

 13.Circuit Diagram

PCB LC-2K COOL ASSY P/N228-37330-91

Fig. PCB LC-2K COOL ASSY

SIL-HTA/HTC Service Manual

13-29
13-30
Fig. CIRCUIT DIAGRAM PCB LC2K-COOL ASSY 1/5

SIL-HTA/HTC Service Manual

 SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB LC2K-COOL ASSY 2/5

13-31
13-32
SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB LC2K-COOL ASSY 3/5
 SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB LC2K-COOL ASSY 4/5

13-33
13-34
SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB LC2K-COOL ASSY 5/5
 13.Circuit Diagram

PCB PB-SCL2 P/N228-34363-92

Fig. PCB PB-SCL2

SIL-HTA/HTC Service Manual

13-35
13-36
SIL-HTA/HTC Service Manual
Fig. CIRCUIT DIAGRAM PCB PB-SCL2 1/1
 13.Circuit Diagram

PCB PB-SCL3 P/N228-34366-91

Fig. PCB PB-SCL3

SIL-HTA/HTC Service Manual

13-37
13-38
Fig. CIRCUIT DIAGRAM PCB PB-SCL3 1/1

SIL-HTA/HTC Service Manual

 13.Circuit Diagram

PCB PB-SCL5 P/N228-34505-91

Fig. PCB PB-SCL5

SIL-HTA/HTC Service Manual

13-39
13-40
Fig. CIRCUIT DIAGRAM PCB PB-SCL5 1/1

SIL-HTA/HTC Service Manual

 Chapter14 Parts configuration
and Parts Number

CONTENTS

ChaPter14 Parts configuration and Parts Number P14-1

SIL-HT•••••••••••••••••••••••••••••••••••••••••• P14-2
Auto Sampler A ASSY••••••••••••••••••••••••••••••• P14-8
ASSY base ••••••••••••••••••••••••••••••••••••••• P14-12
XY ARMASSY••••••••••••••••••••••••••••••••••••• P14-15
ASSY Z•••••••••••••••••••••••••••••••••••••••••• P14-18
ASSY NEEDLE MOUNT••••••••••••••••••••••••••••• P14-21
ASSY V mount •••••••••••••••••••••••••••••••••••• P14-23
ASSY SIL pump ••••••••••••••••••••••••••••••••••• P14-27
Low Pressure Valve•••••••••••••••••••••••••••••••• P14-29
High Pressure Valve ••••••••••••••••••••••••••••••• P14-31
F Panel SCL•••••••••••••••••••••••••••••••••••••• P14-33
Electrical unit ASSY••••••••••••••••••••••••••••••••• P14-36
Rack Plate ASSY••••••••••••••••••••••••••••••••• P14-39
Consumable parts••••••••••••••••••••••••••••••••• P14-41
Repair Parts ••••••••••••••••••••••••••••••••• P14-42
<Electrical Parts>•••••••••••••••••••••••••••••• P14-42
<Valve assy>••••••••••••••••••••••••••••••• P14-44
<XY truck> •••••••••••••••••••••••••••••• P14-46
<Z truck> •••••••••••••••••••••••••••••• P14-47
<Auto Sampler Base Parts>••••••••••••••••••• P14-48
<Parts for SIL-HTc> •••••••••••••••••••••••• P14-49

SIL-HTA/HTC Service Manual

14-1
14.Parts Configuration and Parts Number

228-41001-31 SIL-HTC100V 1/6

14-2
14.Parts Configuration and Parts Number

228-41001-31 SIL-HTC100V 2/6

14-3
14.Parts Configuration and Parts Number

228-41001-31 SIL-HTC100V 3/6

14-4
 14.Parts Configuration and Parts Number

228-41001-31 SIL-HTC100V 4/6

14-5
14.Parts Configuration and Parts Number

228-41001-31 SIL-HTC100V

No. P/N Q’ty 38 228-41249-92 1

PART NAME SAMPLER DOOR ASSY C
11 228-37012-94 1 42 228-39674-02 1
AUTO SAMPLER ASSY LABEL-02
12 228-37503-92 1 43 228-41247-91 1
ASSY,VMOUNT PEEK6V E-BOX HOLDER ASSY
13 228-41011-91 1 44 228-40886 1
F PANEL SCL ASSY SWGUIDE HOLDER 1
14 228-41010-92 1 45 228-40887 1
ELECTRIC UNIT ASSY C SW GUIDE HOLDER 2
15 228-41016-91 1 48 228-37099-01 1
FRAME STAYASSY DOOR HINGE
16 228-37538-92 1 49 228-37099-02 1
ASSY,PANEL SIL DOOR HINGE
17 228-41017-91 1 50 228-37076 1
INNER PANEL ASSY FRAME BAR
18 228-41018-01 1 51 228-37078 1
FDD ASSY BRACKET FOR SIL BOARD
19 228-41013-91 1 53 037-30031-12 1
PANEL SCL ASSY PAD RK-30
20 228-34744-92 1 54 037-51311-02 1
CABLE,FDD ASSY CATCH,MAGNET TL-229S
21 228-34747-92 1 56 201-47435 1
CABLE R-SCL1 200V RUBBER PLUG,PORT,SILLICONE
22 228-37581 1 58 228-38924-01 1
SUS PYPE RINSE-LV#2 LABEL Z MOUNT COVER
24 228-37549-91 1 59 228-37601-01 1
ASSY SAMPLE-LOOP LABEL DEW
25 228-41380-91 1 60 228-40666-01 1
PEEKTUBE 0.25ID LABEL NEEDLE
27 228-40878 1 61 228-37513-91 1
CHASSIS ASSY,SAMPLE COOLER FAN
28 228-40879 1 61 228-37513-92 1
bottom plate ASSY,SAMPLE COOLER FAN
29 228-40880 1 62 228-37512-91 1
top plate ASSYPANEL F
30 228-40881 1 64 228-40521 1
side plate R TAPE 10x10
31 228-40882 1 65 228-37330-91 1
side plate L PCB,LC2K-COOL ASSY
32 228-40892 1 66 228-41065-91 1
TUBE HOLDER PCB,LC-2K INJDOORASSY
33 228-40893 1 67 228-34259-93 1
F PANEL B PCB,10AVP CPU ASSY
34 228-36580 1 68 228-40900-91 1
HOLDER SWTOP PCB,SILX-MAIN ASSY
35 228-40954 1 69 228-34661-91 1
LABEL FRONT PANEL CABLE,OPBOX
36 228-40946 1 70 228-37297-91 1
SPACER SW CABLE,POWER UNIT FAN
37 228-40357 1 71 228-40911-91 1
LABEL SIGNAL CABLE,SR-MAIN

14-6 228-41001-31 SIL-HTC100V 5/6

 14.Parts Configuration and Parts Number

129 228-16004-03 1
72 228-40915-91 1 1.6C
CABLE,DOOR-INJ1 130 228-18565 1
74 228-23013-01 1 MALE NUT PEEK
KEY 132 03738881-51 2
75 228-34553 1 SPACER,CL-305N
ROD SW 133 228-37280-91 1
76 037-50493-01 2 HARNESS INJ1-COOL
BUSHING,BS-1PK 134 228-38936-91 1
77 228-36809 2 CABLE PEL-POWER
TUBE JOINT 135 228-41212 2
78 228-39621 5 FILTER,K5BRC26-30-13MG
PYPE HOLDER 136 07473307-01 1
79 228-37285-91 1 BATTERY,CR2032
CABLE,SR-COOL 137 228-40923-91 1
80 075-08032-03 1 ROM,SIL-HT
CORE,EMI FILTER SFC-6 138 072-60334-01 1
107 037-38860-33 2 CLAMP,LFC-16N-0
SPACER C305 139 072-60324-02 2
110 016-43201 20MM CLIP MFC-3000
PE TUBE 7x1 140 018-17101-03 0.19
111 016-43201 330 SHIELD,FINGER 97-540-02
PE TUBE 7x1 MM 141 072-60306 1
112 035-61561-11 1 CABLE TIE,TY-33M
FITTING L 1252 145 072-60093-01 2
113 228-16000 10 GROMMET,BLANK 11
FERRULE 1.6F 146 228-39789-01 1
114 228-16001-03 6 KNURLED KNOB,M4X10
MALE NUT 1.6MN,W6 148 023-92054-01 1
115 228-16001 4 WASHER,SST WAVE #4
MALE NUT 1.6MN 149 228-41033 1
116 228-41030 1 DOOR SENSOR HOLDER
PYPE ,DGU-LV#4
117 228-41380-92 1
PYPE,P-HV#6
118 22841380-92 1
PEEK TUBE0.25ID
119 228-40526-01 3
SPECER,SAMPLER DOOR(1.0)
119 228-40526-02 2
SPACER SAMPLER DOOR(1.5)
119 228-40526-03 2
SPACER SAMPLER DOOR(2.0)
121 072-60333-02 3
CLIP,WIRE SD-10
123 016-31385-05 15MM
VINYL-T 1.5x0.4 BLUE
125 228-41076 1
INNNER PANEL SIDE
128 228-28413 1
CONNECTOR 1.6/3.0

228-41001-31 SIL-HTC100V 6/6

14-7
14.Parts Configuration and Parts Number

228-37012-93 Auto Sampler A ASSY -94Auto Sampler C ASSY 1/4

14-8
 14.Parts Configuration and Parts Number

228-37012-93 Auto Sampler A ASSY -94Auto Sampler C ASSY 2/4

14-9
14.Parts Configuration and Parts Number

228-37012-93 Auto Sampler A ASSY -94Auto Sampler C ASSY 3/4

14-10
 14.Parts Configuration and Parts Number

228-37012-93 AUTO SAMPLER A ASSY,

-94 AUTO SAMPLER C ASSY 4/4
No. P/N Q’ty
PARTS NAME
11 228-37500-93 1
-93 ASSY BASE
11 228-37500-94 1
-94 ASSY BASE
12 228-37501-92 1
ASSY,XYARM
30 228-37511-91 1
ASSY,PANEL R
31 228-37572-91 1
-94 ASSY,PANEL B
32 228-37571-91 1
-94 ASSY,PANEL T
41 228-40528-91 1
ASSY,INJ1-INJ2
43 228-41118 1
-94 PANEL L
50 228-40474 1
-94 SEAL,FRONT
52 228-40516 2
-94 TAPE,50x100
53 228-40517 1
-94 TAPE,42x42
54 228-40518 2
-94 TAPE,6x35
55 228-40519 1
-94 PACKING PANEL R2
56 228-40520 1
-94 PACKING PANEL R3

14-11
14.Parts Configuration and Parts Number

228-37500-93 ASSY,Base(A type) -94 ASSY,Base(C type)1/3

14-12
 14.Parts Configuration and Parts Number

228-37500-93 ASSY,Base(A type) -94 ASSY,Base(C type) 2/3

14-13
 14.Parts Configuration and Parts Number

228-37500-93 ASSY,BASE(A TYPE) -94 ASSY,BASE(C TYPE) 3/3

No. P/N Q’ty 90 228-37508-91 1

PART NAME -93 RACK-PLATE ASSY
11 228-34836-02 1 90 228-37508-92 1
MAIN BASE -94 RACK-PLATE ASSY (COOLER)
12 228-41239 1 91 228-37507-93 1
COVER-Y ASSY,INJPORT
13 228-38087 1 95 228-28094 2
PULLY-Y -94 L-TYPE DRAIN TUBE
14 228-41134-02 1 98 021-04919-04 4
SHAFT-PULLEY-Y SET SCREW,STEEL M3X5 CUP
16 228-41175 1 POINT
SLIT-2 99 228-41133 1
17 228-36354 1 HOLDER-SLIT 2
SHAFT-Y 100 228-37510-91 1
18 228-36373 1 ASSY,RACK SENSOR
HOLDER,Y SHAFT 104 228-36753-02 3
19 228-36355-01 1 SPACER RACK
MOTOR Y 105 026-11049-02 2
20 228-38148 1 PARALLEL PIN,SST A-TYPE 3X6
Y MOTOR,NUTPLATE 111 228-37537-92 1
21 228-36358 1 -94 ASSY,DEHYUMI PELTIE
BELT Y 112 228-37540-91 1
22 228-41145 1 ASSY,FPC-Y
GUIDE-Y 2 113 228-37591 1
23 228-36650 3 TUBE L (RINSE)
PIN,RACK-PLATE 114 228-37592 1
24 228-37597 1 -94 TUBE L (COOLER)
PIN,RACK PLATE2 115 072-60314-02 2
25 228-36808 1 -94 CABLE CLAMP,UL-18G
INJ LEAK TRAY 119 020-37053 1
26 228-36809 1 -94 SCREW,SST TRUSS HEAD M4X6
TUBE JOINT 120 228-37600 1
30 228-38088 4 -94 PACKING,BASE L
-94 PIN,DEW PLATE 123 016-37507 30MM
32 228-38090 1 -94 TUBE,#9003-6.0X7.0-WH
-94 DEW TRAY 126 228-40119 1
34 031-22608 2 HARNESS CLAMP
BRG,DDLF-950ZZ 130 228-40495 1
41 228-38139 1 FLUORINE,HOSE
-94 DUCT R 140 037-38860-55 1
78 022-27618 3 SPACER,C403
BOLT HEXSOCH SEMS M4X10 141 228-40515 1
80 026-66203 1 -94 PACKING,INJ TRAY
SNAPRING,SST E 3
81 020-46650 4
-94 SCREW,SST SEMS P4 M4X8
88 020-37054 4
-94 SCREW,SST TRUSS HEAD M4X8
89 020-01523 2
SCREW,SUS M2.5x6

14-14
 14.Parts Configuration and Parts Number

228-37501-92 ASSY,XY ARM ASSY 1/3

14-15
14.Parts Configuration and Parts Number

228-37501-92 ASSY,XY ARM ASSY 2/3

14-16
 14.Parts Configuration and Parts Number

228-37501-92 ASSY,XY ARM 3/3

No. P/N Q’ty
PART NAME
11 228-37502-92 1
ASSY,Z
11 228-37500-94 1
-94 ASSY BASE
12 228-41175 1
SLIT-2
13 228-41238 1
SENSOR COVER X
14 228-36363 2
SHAFT X
35 228-37514-91 1
ASSY ,XYARM SUB
36 228-37515-92 1
ASSY,PULLY X
38 228-41143 1
FENCE XYARM
39 020-46536 2
SCREW,SST SEMS P3 M3X10
40 021-04919-04 4
SET SCREW,STEEL M3X5
41 228-37355-91 1
PCB,LC2K-XENC ASSY
42 228-37365-91 1
PCB,LC2K-XHP ASSY
43 228-37294-91 1
CABLE,SIL-XHP
44 017-30305-04 -
LUBRICATING OIL,DAPHNE 220C
46 072-60306 1
CABLE TIE,TY-33M
51 228-40773-07 2
SNAP RETEINER
60 228-37320-91 1
PCB,LC2K-INJ2 ASSY

14-17
14.Parts Configuration and Parts Number

228-37502-92 ASSY Z 1/3

14-18
14.Parts Configuration and Parts Number

228-37502-92 ASSY Z 2/3

14-19
 14.Parts Configuration and Parts Number

228-37502-92 ASSY Z 3/3

No. P/N Q’ty 61 228-40501 1
PART NAME LABEL
14 034-01603-51 1 62 023-66030 2
SPRING COMPRESSION UL10-50 WASHAR
15 228-36684 1
Z SCREW
17 228-36690 1
PULLY Z
24 228-36697 1
COLLAR
25 228-36607-01 1
MOTOR Z
26 228-40817-04 1
NEEDLE SILHT
29 228-36689 1
MALE NUT NEEDLE
31 228-36792-09 1
BELT Z
32 228-40232-91 1
ASSY Z COVER
35 031-22615 2
BRG DDLF-1260ZZ
38 228-36691 1
SHAFT Z
41 021-04919-04 3
SET SCREWM3x5
42 026-66204 1
SNAP RING SST E 4
43 020-46539 1
SCREW M3X16
44 228-37541-91 1
ASSY FPC-Z
45 228-37517-91 1
ASSY, ZMOUNT SUB
46 228-37518-92 1
ASSY NEEDLEMOUNT
47 228-37520-91 1
ASSY BUSH NEEDLE
48 020-46135 4
SCREW M3X8
49 020-46535 4
SCREW M3X8
50 020-46534 4
SCREW M3X6
51 020-46634 5
SCREW M3X6
54 228-28430 1
FERRULE 1.2F
55 020-37043 1
SCREW M3X6
60 021-61122 2
SCREW P-TIGHT STEEL 3X6

14-20
 14.Parts Configuration and Parts Number

228-37518-92 ASSY NEEDLE MOUNT 1/2

14-21
 14.Parts Configuration and Parts Number

228-37518-92 ASSY NEEDLE MOUNT 2/2

No. P/N Q’ty

PART NAME
11 228-37536-91 1
ASSY NEEDLE MOUNT SUB
12 034-01612-02 1
SPRING COMPRESSION UH16-20
13 228-497429-91 1
Z NUT/SCREW
17 026-63112 1
RETAINING RING C HOLE
18 228-36693 1
SENSOR PLATE ZHP
19 228-36694 1
SENSOR PLATE Z
20 020-46534 2
SCREW M3x6
21 228-37519-92 1
ASSY HT
22 228-41262-01 1
VIAL DETECT 2
23 022-27703 1
BOLT SST HEXSOCH M4
017-30305-04
LUBRICATING OIL DAPHNE C220
017-30829-01
GREASE,DAPHNE POLYLEX#2
400G

14-22
 14.Parts Configuration and Parts Number

228-37503-92 ASSY V MOUNT 1/4

14-23
14.Parts Configuration and Parts Number

228-37503-92 ASSY V MOUNT 2/4

14-24
 14.Parts Configuration and Parts Number

228-37503-92 ASSY V MOUNT 3/4

14-25
14.Parts Configuration and Parts Number

228-37500-93 ASSY V MOUNT 4/4

No. P/N Q’ty
PART NAME
11 228-3504-91 1
ASSY,SILPUMP
12 228-40177-92 1
LEAK TRAY ASSY,HT
13 228-36807 2
COVER VALVE SENSOR
14 228-35981 2
VALVE SENSOR HOLDER
17 228-41020-91 1
ASSY,6V PEEK
18 228-37506-91 1
ASSY,LV
20 228-37542-91 1
ASSY,FPC-V
21 228-37521-91 1
ASSY,MOTOR 6V
22 228-37521-92 1
ASSY ,MOTOR 5PV
31 228-37575 1
PYPE,LV#5-HV#3
32 228-37576 1
PYPE,P#IN-HV#2
33 228-37577 1
PYPE,P#OUT-LV#1
34 228-16000 6
FERRULE 1.6F
35 228-16001 2
MALE NUT 1.6MN
36 228-16001-03 4
MALE NUT 1.6MN,W6
37 228-18565 1
MALE NUT PEEK
38 228-18495-03 220
ETFE TUBE 1.6x1.0 MM
41 018-26020-02 180
SPIRAL TUBE,KS-4 MM

14-26
14.Parts Configuration and Parts Number

228-37504-91 ASSY SIL PUMP 1/2

14-27
14.Parts Configuration and Parts Number

228-37504-91 ASSY SIL PUMP

No. P/N Q’ty No. P/N Q’ty
PART NAME PART NAME
11 228-35749-01 1 46 020-46637 1
MOUNT VALVE SCREW M3X12
12 228-36288-01 1 60 020-46534 1
SCREW PUMP SCREW M3X6
13 228-36444-01 1 70 026-11049-02 1
MOTOR P APARALLEL SUS A 3X6
14 228-36335-01 1 80 020-46634 1
HEAD HOLDER SIL SCREW SUS M3X6
15 228-36290-01 1
PUMP HEAD SIL
16 228-36792-10 1
BELT STS40S2M166UG
19 228-36344 1
PULLY PUMP
20 228-36336-01 1
SENNSOR BLOCK
21 228-41422 1
PUMP SENSOR 2
22 228-36386 1
SLIT PUMP
23 228-36387-01 1
SPRING PUMP
24 037-38714-19 1
SPACER,SPC3X7
25 031-23719-06 2
BRG DDSST-168DSG
26 228-35008 1
BEARING CRT9-17
27 031-40390-26 1
BRG,54B-202820
28 031-40390-65 1
BRG,54F-0808
30 026-55302-01 1
KEY KESS2-10
32 022-27053 2
BOLT SUSM4X30
33 023-77040 4
WASHER SUS SUPRING M4
35 021-04919-04 2
SET SCREW M3X5
36 020-46535 4
SCREW SEMS M3X8
37 022-27054 2
BOLT SUS M4X35
39 228-37529-91 1
CROSS HEAD ASSY
40 228-37530-91 1
ASSY SEAL HOLDER
42 228-35145 1
SEAL 42429

14-28
 14.Parts Configuration and Parts Number

228-37506-91 LOW PRESSURE VALVE 1/2

14-29
 14.Parts Configuration and Parts Number

228-37506-91 LOW PRESSURE VALVE

No. P/N Q’ty

PART NAME
14 228-35998 1
SLIT VALVE
15 228-36917-01 1
STATOR 5PV
19 031-23003 1
BEARING A-2216
20 228-41285 1
VALVE BEARING
22 228-38654 1
PACKING 5PV
24 034-00037 6
SARABANE,H#7
27 022-27049 3
BOLT SUS M4X20
28 023-77040 3
WASHER
33 228-36923 1
ROTOR PV PEEK WIDE
36 020-46505 1
SCREW M2X8
37 021-04919-06 2
SET SCREW
38 228-41137 1
GEAR VALVE
39 228-38418 1

40 228-38419 1
BEARING
41 228-38421 1
NUT
43 228-40166-91 1
MACHING PART
70 228-41075-05 1
LABEL

14-30
 14.Parts Configuration and Parts Number

228-41020-91 High Pressure Valve 1/2

14-31
14.Parts Configuration and Parts Number

228-41020-91 HIGH PRESSURE VALVE 2/2

No. P/N Q’ty

PART NAME]
14 228-35998 1
SLIT VALVE
18 228-40259-01 1
STATOR HV3 R
21 031-23003 1
BEARING A-2216
22 228-41285 1
VALVE BEARING
25 034-00007 6
SARABANE,H#1
28 022-27049 3
BOLT SUS M4X20
29 023-77040 3
WASHER
41 021-04919-06 2
SET SCREW
42 020-46505 1
SCREW M2X8
52 228-40750-02 1
ROTOR,6V-3
55 228-40257 1
FLAT PACKING HV3
57 228-41137-01 1
GEAR VALVE
58 228-40829 1

59 228-38419 1
BEARIN
60 228-38421 1
NUT
62 228-40165-92 1
MACHING PARTS

14-32
 14.Parts Configuration and Parts Number

228-41011-91 F PANEL SCL ASSY 1/3

14-33
14.Parts Configuration and Parts Number

228-41011-91F PANEL SCL ASSY 2/3

14-34
 14.Parts Configuration and Parts Number

228-41011-91 F PANEL SCL ASSY

No. P/N Q’ty 42 228-41092 1

PART NEME COVER,LCD VOLUME
11 228-40899 1 43 037-38737-04 2
F PANEL ,SCL SPACER PC3x6
12 228-40899 1 45 072-60276-05 100
INNER PANEL SCL SHIELD COVER DK-534 MM
13 228-40926 1
SPACER 10 KEY
14 228-38940 1
LABEL FLOW LINE
16 228-38928 1
LABEL,FDD
17 208-94869-03 1
CABLE LCD(SCL)
18 228-34675-02 1
LCD COVER
20 037-51311-01 2
CATCH,MAGNET TL-229
21 228-34363-92 1
PB-SCL2 ASSY
22 228-34366-91 1
PB-SCL3 ASSY
22 228-34366 1
PB-SCL3 ASSY
23 228-34566 1
KEY TOP 2 SCL
24 228-34565 1
KEY TOP1 SCL
25 228-34505-91 1
PB-SCL5 ASSY
26 078-12114-11 1
LCD,DMF-5017NF-FW7
27 228-40905-91 1
PCB,LCD-VR ASSY
28 228-41078 2
SPACER B,SCL
29 228-41077 2
SPACER A SCL
30 072-60323-04 2
CLIP B-4T
31 037-50413-03 2
HINGE,B-1100-3
32 228-34742-92 1
CABLE SCL1-SCL2 ASSY
34 228-34536 3
FILTER LED
35 037-38743-08 4
SUPPORT,TA-312
39 037-38881-52 1
SPACER CL-310N
41 228-37392-91 1
EARTH,CONTROL PANEL

14-35
14.Parts Configuration and Parts Number

228-41010-91 ELECTRICAL UNITA(ATYPE)

14-36 -92 ELECTRICAL UNIT ASSY A(C TYPE) 1/3
 14.Parts Configuration and Parts Number

228-41010-91 ELECTRICAL UNITA(ATYPE)

-92 ELECTRICAL UNIT ASSY A(C TYPE) 2/3

14-37
14.Parts Configuration and Parts Number

228-41010-91 ELECTRICAL UNITA(ATYPE)

-92 ELECTRICAL UNIT ASSY A(C TYPE) 3/3
No. P/N Q’ty
PART NAME
11 228-40884 1
ELECTRICAL CHASI
12 037-38881-51 12
SPACER CL-305N
13 228-25246-94 1
FAN,POWER SUPPLY UNIT
14 072-05669-02 2
FUSE HOLDER,FH-B02
15 075-00152-01 1
FILTER,FN9222-10/06
16 228-37270-92 1
PCB,LC2K-FILTERASSY
17 072-02004-21 2
-91 FUSE,218 315
17 072-02004-23 2
-92 FUSE,218 005
18 078-80429-35 1
POWER SUPPLY, ZWS75AF-24/J
19 078-80429-75 1
-92 POWER SUPPLY, ZWS150AF-24/J
20 071-60122-01 1
RECEPTACLE,AC-F01FB01
21 228-40910-91 1
HARNESS,INLET-FUZE
22 228-37290-91 1
WIRE,EARTH-INLET
23 228-37290-92 1
WIRE,EARTH-INLET
24 228-40912-91 1
SWITCH ASSY
25 228-37286-91 1
CABLE FIL-SR
26 228-40913-91 1
CABKLE,OUTLET
27 228-40955-01 1
-92 LABEL VOLTAGE
27 228-40955-02 1
-93 LABEL VOLTAGE
28 037-70832-03 1
LABEL CE-22x16
29 072-60314-02 1
CABLE CLAMP,UL-18G

14-38
14.Parts Configuration and Parts Number

228-37508-92 Rack Plate ASSY

14-39
 14.Parts Configuration and Parts Number

228-37508-92 Rack Plate ASSY

No. P/N Q’ty
PartName
11 228-36609-02 1
Rack Plate
12 228-36651 1
Block , Rack hold
13 228-36753-02 12
Spacer , Rack
14 228-36608 1
Cover, Rack Plate
15 228-36652 1
Rack guide
16 228-36653 2
Pin Rack hold
17 020-46507 4
Screw,SUSsemsP3 M2X12
18 228-38980-01 2
SHIELD RACK PLATE
19 228-38980-02 1
SHIELD RACK PLATE
20 228-38656 1
RACK PLATE SHIELD
21 228-38677-91 1
THERMISTOR SIL ASSY
22 228-37389-91 1
ASSY,AUX HEATER-COOL
23 020-37501 2
SCREW, BINDING HEAD M3X6
25 228-38662 1
SHIELD RACK
26 228-38716 1
SHIELD FIN
27 228-38718 2
PELTIER UNIT
29 060-49902 -
HEAT SINK,HSC-100
30 026-11021-02 1
PARALLEL PIN, A-TYPE 1.6X10
31 031-40528-02 2
THRUST WASHER,STW-FT20
32 060-49780-03 1
INSULATOR,BFG-20 D-1

14-40
Consumable parts

P/N228-33355-01
NEEDLE SEAL PEEK
P/N228-35145
GFP,SEAL,42429

Fig.1 Fig.2

P/N228-36923 Fig.3 P/N228-41310-92 Fig.4

ROTOR,LPV,PEEK ROTOR,HPV,PEEK

COATED NEEDLE

FERRULE 1.2F
P/N228-21984-01
SUCTION FILTER NEW Fig.6
Fig.5
MALE NUT NEEDLE
P/N228-41024-92 COATED NEEDEL ASSY

14-41
14.Parts Configuration and Parts Number

Repair Parts
<Electrical Parts>

P/N228-35224-93 P/N228-34259-93 Fig.8

Fig.7
PB SCL-1A ASSY PCB 10AVP CPU ASSY

P/N228-34369-91 Fig.10
PB SCL-4

P/N228-40900-91
PCB SIL MAIN Fig.9

P/N228-34505-91
PB SCL-5 Fig.11
P/N228-34366-91 Fig.12
PB SCL-3

14-42
 14.Parts Configuration and Parts Number

P/N228-34363-92
PB SCL-2 Fig.13 Fig.14
P/N208-94869-03
Cable, LCD

P/N228-40905-91
PCB CONTRAST
P/N228-34565 Fig.16
Fig.15 Key Top 1, SCL

P/N228-34566
KEY TOP 2, SCL Fig.17

P/N078-12114-11 Fig.18
LCD,DMF50174NB-FW6

14-43
14.Parts Configuration and Parts Number

<Valve assy>

P/N228-35010-91
PLUNGER,SIL ASSY

Fig.19 Fig.20
P/N228-36445-01
MOTOR,HPV

P/N228-36917-01 Fig.22
P/N228-36446-01 STATOR 5PV
MOTOR LPV

Fig.21

Fig.23
Fig.24
P/N228-41020-91
P/N228-37506-91 HPV VALVE ASSY
LPV VALVE ASSY

14-44
 14.Parts Configuration and Parts Number

P/N228-37542-91
FPC-V ASSY
P/N228-38654 Fig.26
Fig.25
STATOR PACKING,LPV

P/N228-37530-91 Fig.28
ASSY SEAL HOLDER
P/N228-39247-92
LEAK SENSOR ASSY , 700MM

Fig.27

P/N228-36444-01 Fig.29
MOTOR MEASURING PUMP

14-45
14.Parts Configuration and Parts Number

<XY truck>

P/N228-36376
P/N228-36362-02 SLIT
Fig.30 Fig.31
MOTOR X

Fig.33

P/N228-37355-91
P/N228-37320-91 PCB LC2K-XENC ASSY
PCB LC2K-INJ2 ASSY
Fig.32

P/N228-37365-91
PCB LC2K-XHP ASSY
(X PCB sensor)
Fig.34
Fig.35
P/N228-37509-91
SLIT HOLDER ASSY

14-46
 14.Parts Configuration and Parts Number
<Z truck>

P/N228-36607-01
MOTOR Z Fig.37
Fig.36
P/N228-37541-91
FPC-Z ASSY

14-47
14.Parts Configuration and Parts Number

<Auto Sampler Base Part>

P/N228-36355-01 P/N228-37360-91
MOTOR Y PCB,RACK ASSY
Fig.39 Fig.40

P/N228-37508-92
RACK PLATE ASSY(C-TYPE)
P/N228-37508-91 Fig.42
RACK PLATE ASSY(A-TYPE)
Fig.41

P/N228-40528-91
Fig.43 HARNESS INJ1-INJ2 Fig.44
P/N228-37540-91
FPC-Y ASSY

14-48
 14.Parts Configuration and Parts Number
<Parts for SIL-HTc>

Fig.45 Fig.46
P/N228-37389-91 P/N228-38718
AUX HEATER-COOL ASSY PELTIER UNIT

P/N228-38677-91 Fig.48
THERMISTOR SIL ASSY
P/N228-37537-91 Fig.47 (For Rack plate assy of SIL-HTc)
Dehumidifier , Peltier ASSY

P/N228-38677-92
P/N228-37330-91 THERMISTOR ,SIL ASSY
PCB LC2K-COOL ASSY Fig.49 (For dehumidifier of SIL-HTc) Fig.50

14-49
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