DigiPREP

KeyPad Controller
Service Manual

www.scpscience.com

Providing Innovative Solutions to Analytical Chemists

 Providing Innovative Solutions to Analytical Chemists

Canada / International Europe

21800, Avenue Clark-Graham, 12, Avenue du Québec, Bâtiment I-2, Silic 642
Baie d’Urfé, QC H9X 4B6 91965 Courtaboeuf CEDEX, France
Tel: +1 (514) 457-0701 Tel: +33 (0) 1 69 18 71 17
Fax: +1 (514) 457-4499 Fax: +33 (0) 1 60 92 05 67

USA China
348 Route 11, C1102 Room, Chengming Building, No.2
Champlain, NY Xizhimen Nandajie,
12919-4816 Xicheng District, Beijing, China 100025
Tel: 1-800-361-6820 Tel: +86 (10) 51905671
Fax: 1-800-253-5549 (North America only) Fax: +86 (10) 51905672

Disclaimer: Products are supplied for laboratory use only and should not be used for any household, medical or therapeutic application. SCP SCIENCE presumes
that only trained and qualified individuals, familiar with procedures suitable for the safe operation of these instruments, will handle them. Our customers are solely
responsible for the safe operation, handling and use of these products.

CERTIFIED to comply with the following EMC and safety requirements standards:
EN 55022 (1998), EN 61000-4-3 (1996), ENV 50204 (1995), EN 61000-4-6 (1996), EN 61000-4-2 (1995), EN 61000-4-4 (1995), EN 61000-4-5 (1995),
and EN 61000-4-11 (1994). IEC 61010-1 and the IEC 61010-2-010, 2nd edition, 2001-02

MANUFACTURED IN CANADA

EU Users:
Contact your local
distributor for disposal
instructions.

Copyright by SCP SCIENCE

All Rights Reserved
This manual contains proprietary information, which shall not be reproduced or transferred to other documents
or disclosed to others without prior written permission from SCP SCIENCE.

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 TABLE OF CONTENTS
INTRODUCTION .................................................................................................................................... 7
WARRANTY .......................................................................................................................................... 7
BASIC VERIFICATION LIST ..................................................................................................................... 8
KEYPAD INSTRUCTION MANUAL
CAUTIONS, NOTES, SYMBOLS, SAFETY INFORMATION,WARRANTY ................................................. 10
COMPONENTS AND INSTRUMENT DESCRIPTION .............................................................................. 11
Unpacking ................................................................................................................................... 11
INSTRUMENT OPERATION .................................................................................................................. 12
KeyPad icons .............................................................................................................................. 12
SCREENS ........................................................................................................................................... 13
Banner screen ............................................................................................................................. 13
Menu screen ............................................................................................................................... 13
Utilities screen.............................................................................................................................. 13
Language screen ......................................................................................................................... 13
System screen............................................................................................................................. 13
OPERATING PARAMETERS ................................................................................................................. 14
Run screen .................................................................................................................................. 14
Calibration screen ........................................................................................................................ 14
SAFETY MESSAGES ........................................................................................................................... 15
Possible Safety Messages............................................................................................................ 15
Preventing Safety Messages ........................................................................................................ 16
Disabling Safety Messages........................................................................................................... 16
DigiPROBE ERROR MESSAGES........................................................................................................ 17
DIAGNOSTIC TEST PROCEDURE........................................................................................................ 17
CLEANING .......................................................................................................................................... 17
SPECIFICATIONS KEYPAD .................................................................................................................. 18
Electrical ...................................................................................................................................... 18
Environmental .............................................................................................................................. 18
KEYPAD SERVICE MANUAL
KEYPAD GENERAL DESCRIPTION ....................................................................................................... 20
LIGHT EMITTING DIODE & LCD ........................................................................................................... 21
KEYPAD MALFUNCTION ..................................................................................................................... 22
FAILED KEYPAD BUTTONS ................................................................................................................. 23
KEYPAD DIAGNOSTIC SECTION ......................................................................................................... 23
UIPS POWER SUPPLY SECTION ......................................................................................................... 24
HEATER DRIVE SECTION .................................................................................................................... 27
THE BLOCK IS NOT HEATING UP ....................................................................................................... 28

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 A/D CONVERTER ................................................................................................................................ 30
Possible A/D Problem .................................................................................................................. 31
RTD input connection................................................................................................................... 31
CPU SECTION .................................................................................................................................... 32
LCD display problem .................................................................................................................... 32
DigiPREP DIGESTION BLOCKS JR, MS, LS, HP INSTRUCTION MANUAL
INTRODUCTION .................................................................................................................................. 35
CAUTIONS AND NOTES ..................................................................................................................... 36
WARRANTY ........................................................................................................................................ 36
SYMBOLS .......................................................................................................................................... 36
OPERATIONAL PRECAUTIONS ............................................................................................................ 37
SAFETY INFORMATION ....................................................................................................................... 37
INSTALLATION .................................................................................................................................... 38
Unpacking ................................................................................................................................... 38
SETTING UP ....................................................................................................................................... 38
OPERATION WITH PROBES ............................................................................................................... 39
DigiPROBE ................................................................................................................................ 39
DigiSET ...................................................................................................................................... 39
BLOCK DESCRIPTION ........................................................................................................................ 40
CLEANING .......................................................................................................................................... 41
Cleaning of Minor Surface Spills ................................................................................................... 41
Cleaning of Digestion Wells .......................................................................................................... 41
Cleaning Melted Plastic from Wells ............................................................................................... 41
Cleaning of a Major Spill ............................................................................................................... 41
SPECIFICATIONS ................................................................................................................................ 42
Environmental .............................................................................................................................. 42
Electrical ...................................................................................................................................... 42
ACCESSORIES ................................................................................................................................... 43
OPTIONS ............................................................................................................................................ 44
ELECTRICAL SCHEMATIC ................................................................................................................... 45
DigiPREP HT INSTRUCTION MANUAL
INTRODUCTION .................................................................................................................................. 47
CAUTIONS AND NOTES ..................................................................................................................... 48
WARRANTY ........................................................................................................................................ 48
SYMBOLS .......................................................................................................................................... 48

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OPERATIONAL PRECAUTIONS ............................................................................................................ 49
SAFETY INFORMATION ....................................................................................................................... 49
BLOCK DESCRIPTION ........................................................................................................................ 50
Unpacking ................................................................................................................................... 50
ASSEMBLY ......................................................................................................................................... 51
DUAL PROBE OPTION....................................................................................................................... 53
HEAT DEFLECTOR ASSEMBLY............................................................................................................ 54
REFERENCE DATA .............................................................................................................................. 55
TYPICAL HEATING RATES ................................................................................................................... 56
METHOD DEVELOPMENT FOR DIGESTING SAMPLES ........................................................................ 57
CLEANING .......................................................................................................................................... 58
Cleaning of Minor Surface Spills ................................................................................................... 58
Cleaning of Digestion Wells .......................................................................................................... 58
Cleaning of a Major Spill ............................................................................................................... 58
SPECIFICATIONS ................................................................................................................................ 59
Environmental .............................................................................................................................. 59
Electrical ...................................................................................................................................... 59
ACCESORIES AND OPTIONS.............................................................................................................. 60
ELECTRICAL SCHEMATIC ................................................................................................................... 61
JR, MS, HP, HT SERVICE MANUAL
DigiPREP JR BLOCK DESCRIPTION .................................................................................................. 62
DigiPREP JR Spare Part List....................................................................................................... 63
DigiPREP MS BLOCK DESCRIPTION ................................................................................................. 65
DigiPREP MS Spare Part List ...................................................................................................... 66
DigiPREP HP BLOCK DESCRIPTION ................................................................................................. 67
DigiPREP HT BLOCK DESCRIPTION.................................................................................................. 69
DigiPREP HT Spare Part List ...................................................................................................... 70
DigiPREP LS BLOCK DESCRIPTION .................................................................................................. 71
MISCELLANEOUS PART LIST .............................................................................................................. 72
ELECTRICAL SCHEMATICS KEYPAD ................................................................................................... 73
DigiPREP DISMANTLING PROCEDURES ........................................................................................... 74
Removing the Corian Ring ............................................................................................................ 74
Removing the Graphite Block ....................................................................................................... 75
DigiPREP TESTS AND REPLACEMENT PROCEDURES ...................................................................... 75
Voltage Selector Switch, E239 ...................................................................................................... 75
Over-Temperature Protection Devices ........................................................................................... 76

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 Umbilical Cords..................................................................................................................... 77
Internal RTD, C176................................................................................................................ 78
Heating Pad Procedures .............................................................................................................. 78
Heating Pad Inspection Procedures .............................................................................................. 79
Heater Replacement Procedures .................................................................................................. 79
DigiPREP Dongle Testing Procedures .......................................................................................... 81
DigiPROBE Testing Procedures .................................................................................................. 81
DigiPREP TROUBLESHOOTING ......................................................................................................... 81
DigiPROBE Error Displaying on Controller .................................................................................... 81
System Functional with Dongle but not with DigiPROBE............................................................... 81
Heater Does Not Heat Up, Temperature Displays but Does Not Change......................................... 81
Heater Cannot Achieve Desired Temperature, But ContinuouslyTries to Ramp ................................ 81
Heater Cannot Achieve Desired Temperature, Stops Heating Too Early .......................................... 82
Heater is Overshooting Temperature ............................................................................................. 82
Controller Temperature Fluctuates Between Impossible Values ....................................................... 82
Controller Temperature Fluctuates Around Set Point....................................................................... 82
Breaker Switch On Controller Trips on the Start of Digestion ........................................................... 82
ELECTRICAL SCHEMATICS............................................................................................................ 83-85
SERVICE DEPARTMENT INFORMATION ............................................................................................... 88

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INTRODUCTION repairs will be chargeable to the distributor
at SCP SCIENCE’s current rates. Parts
This manual is to be used by distributors and required in the post warranty period will be
employees of SCP SCIENCE only. The DigiPREP charged according to the prevailing Service
KeyPad Controller is used to control the DigiPREP Parts Price List less distributor’s discount.
Digestion Systems (Jr, MS, LS, HP, HT). Transport charges for the instrument to be
returned are the responsibility of the
distributor.
WARRANTY c. Post Warranty Period: SCP SCIENCE
SCP SCIENCE warrants this product free from agrees to supply required service parts at
defect in workmanship and materials for one (1) prices according to the prevailing Service
year from date of purchase. SCP SCIENCE agrees Parts Price List less distributor’s discount.
to make every effort to supply products in The distributor agrees to pay freight charges
merchantable condition and free from defects. for service parts purchased after the warranty
period.
1. The warranty period for DigiPREP digestion
4. SCP SCIENCE reserves the right to request
systems is 12 months from the date of shipment
that failed parts be returned to a location
from SCP SCIENCE.
specified by SCP SCIENCE, in which case freight
charges shall be borne by the distributor. This
2. DigiPROBE and DigiSET Probe are
clause shall apply irrespective of whether the
consumable products and carry a warranty
unit is under warranty or not.
only to the extent that they are functional on
receipt. 5. A DigiPREP digestion system that does not
operate upon receipt (‘out-of-box failure’) may be
3. As part of the Agreement between SCP returned to SCP SCIENCE with transport charges
SCIENCE and the Distributor, the distributor to the account of SCP SCIENCE. Note that the
agrees to assume the responsibility to provide distributor must obtain a Return Material
service for any DigiPREP digestion system sold Authorization (RMA) number from SCP SCIENCE
by the distributor in the territory. before shipping the instrument. SCP SCIENCE
reserves the right to select the method of transport.
a. Warranty Period: Service parts required
during the warranty period shall be provided 6. The distributor agrees to cooperate in all respects
to the distributor at no charge. Freight costs for with SCP SCIENCE and will provide SCP
the service parts shipped to the distributor SCIENCE with service failure information, serial
will be borne by SCP SCIENCE. numbers of the digestion block and/or controller,
Transportation costs for returned instruments and any other service related information
and parts are the responsibility of the determined by SCP SCIENCE as being relevant to
distributor. Labour for repairs during the the repair of an instrument and to the improvement
warranty period or post warranty period of the product.
are the responsibility of the Distributor.
7. An RMA # is required prior to returning any item
b. Alternative Service: In the event that the to SCP SCIENCE.
distributor wishes SCP SCIENCE to perform
8. SCP SCIENCE shall not be responsible for any
repair service on their behalf, the distributor
damage or losses however caused, which may
shall return the instrument prepaid to the
be experienced as a result of the installation or use
designated SCP SCIENCE Service Center.
of this product.
Charges for labour required to complete the

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 BASIC VERIFICATION LIST 3. Power Supply
□ The Fuses are fine
1. Visual and physical inspection
□ Power cables are correctly inserted (see page 26)
□ All parts are included.
Comments and observations:
□ Power cord is fully inserted ___________________________________________
___________________________________________
□ All connectors and cables are inserted accordingly ___________________________________________
___________________________________________
□ The system powers up correctly ___________________________________________
___________________________________________
□ Cable connector looks fine (not bent)

Comments and observations: 4. Heater Drive Circuit

___________________________________________
___________________________________________ □ DigiPREP block is connected to the controller
___________________________________________
___________________________________________ □ DigiPREP block is heating accordingly
___________________________________________
___________________________________________ □ 'COM2' dongle is correctly inserted and passes
ohmic check

2. Display □ DigiPROBE is correctly inserted into its socket

(N/A for HT)
□ Touch Screen and LCD Backlight are working
Comments and observations:
□ Banner Screen is appearing ___________________________________________
___________________________________________
□ Main menu screen is appearing ___________________________________________
___________________________________________
□ Fonts and video color are correct ___________________________________________
___________________________________________
□ The touch Screen is sensing finger pressing.

□ The touch screen has been calibrated (from the

calibration screen)

Comments and observations:

___________________________________________
___________________________________________
___________________________________________
___________________________________________
___________________________________________
___________________________________________

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5. CPU and general component verification 3. The block is heating very slowly;

□ Software runs accordingly • Ensure that the voltage selector switch of

the heating block is at the correct position.
• Software version _________
• Ensure correct block has been selected.
□ Fan is fixed accordingly

• Controller serial number _________ 4. No display and no back light;

• Check fuse F1.

SYMPTOMS
• Check the 2 15A fuses inside the TS
The following symptoms must be verified before
housing.
going into more detail.

1. The block is over shooting the set point Symptoms Reference

temperature, and the temperature keeps Operation LED not illuminated Page 26, 28,
climbing; when power is on 36
Digital screen (LCD) is
• Check the Heater Drive Circuit Page 36
malfunctioning
LCD shows "DigiPROBE
• Ensure correct block has been selected. page 28
error"
The voltage selector switch of the heating
block is in the correct position. KeyPad buttons are not
Page 34, 78
functioning correctly
The controller is not functioning Page 31
2. The block is not heating; when power switch is on
The DigiPREP block is not
• Ensure the DigiSET dongle is installed. heating up
The heating block is not
• The power cable is connected.
reaching its temperature or vary
FIGURE 1: SYMPTONS VS. DOCUMENT REFERENCES
• Ensure the Voltage Selector Switch of the
heating block is at the appropriate voltage.

• Verify that the 180oC NC Thermal Switch

is closed.

• Check resistance of heater according to

the DigiBLOCK size.

• Verify the 450oC Thermostat is closed for

HT.

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 CAUTIONS & NOTES • Do not place the DigiPREP controller on a
surface containing flammable material.
Cautions, warnings, and notes are
included throughout this manual. • DigiPREP block should be operated in a fume
hood.
CAUTION
A caution is used to emphasize • DigiPREP controller must be plugged into a
information pertaining to procedures three-prong grounded outlet.
that, if not strictly followed, may result in
CAUTION
damage or destruction to the instrument WARRANTY
or improper instrument operation.
SCP SCIENCE warrants this product free
WARNING from defect in workmanship and materials
A warning is used to emphasize for one (1) year from date of purchase.
information about dangerous or
• Should the unit malfunction, call SCP
WARNING hazardous conditions relating to the SCIENCE's service department (see page 88),
operation, cleaning, or maintenance
or your local distributor. and a service
of the instrument that may result
representative will instruct you on how to
in personal injury.
proceed.
NOTE • There are no user-serviceable parts in this unit.
A note is used to emphasize procedures The warranty is void if the unit shows evidence
NOTE
or conditions that may be misinterpreted of being tampered with, of being subjected to
or overlooked, and to clarify potentially excessive moisture, heat or corrosion, or of
confusing situations. other misuse.

SAFETY INFORMATION • SCP SCIENCE shall not be responsible

for any damage or losses however caused
A minimum of safety considerations must be
which may be experienced as a result of the
followed when working with the DigiPREP system
installation or use of this product.
in order to maintain good laboratory practice:
• This product is not warranted for, nor has
• Do not place DigiPREP controller in a fume it been tested for, use with perchloric
hood. acid. The user accepts all responsibility if
this product is used with perchloric acid.
Symbol Description Symbol Description

V Voltage l Mains on

~ Alternating current 0 Mains off

Attention, consult
A Current
accompanying documents

Hz Frequency Caution, hot surfaces

Protective conductor terminal

F Fast-acting fuse

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COMPONENTS AND INSTRUMENT DESCRIPTION

1
2

3 4
7

1. Power light (LED) 5.

5 Power cord receptacle
2. LCD screen 6. Power Switch
3. KeyPad 7. DigiSET connection port
4. Connection port for umbilical cord (to block) 8. Detachable Power Cord

UNPACKING
Inspect the products for any shipping damage.
Retain all packing material in case
NOTE
If the instrument has been damaged in shipping,
you need to return the instrument to
contact the freight carrier to report damage and to
the manufacturer for service.
file a damage report. Also contact the SCP
SCIENCE service department to report damage
1. Verify that all components listed have been
and to request service information (see page 88 for
included:
contact information).
• DigiPREP keypad controller
If damage is noted, do not attempt
• Power cord WARNING to operate the instrument.
• DigiSET dongle

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 KEYPAD ICONS
Alarm Key: Press to toggle audible alarm on/off. LED flashes when alarm is set to on.

Target Temperature Key: Press to modify target temperature.

Target time Key: Press to modify or reinstate target time.

Enter key: Press to accept value(s)

Left Arrow Key: Press to move the cursor to the left.

Right Arrow Key: Press to move the cursor to the right.

INSTRUMENT OPERATION
The keypad controller uses different screens to
access dfferent functions.

Use the arrow keys to move the cursor on the

screen, and press enter to accept your selection.

A "<" or ">" symbol displayed next to an item

indicates that the current screen contains more
items than can be shown. Use the arrow keys to
move to the next item.

The system powers up on the Banner Screen.

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SCREENS LANGUAGE SCREEN

BANNER SCREEN LANGUAGE

EN FR DE IT ES NL >
SCP SCIENCE
DigiPREP KeyPad X.X LANGUAGE
<JP
The banner screen is displayed during power-up,
it will change to the menu screen after a short delay. The language screen lets you select the display
language.

MENU SCREEN Be careful not to select an unfamiliar

NOTE
language as it may be difficult to
MENU change back.
OPERATION UTILITIES
En- English
From the menu screen, you can select either the FR- French
'OPERATION' screen or the 'UTILITIES' screen. From DE- German
the 'UTILITIES' screen you can change the language, IT - Italian
select the block model, and calibrate the system. ES- Spanish
The 'OPERATION' screen lets you set the block tem- NL - Dutch
perature and target time. JP- Japanese (romanized)

Next, select which DigiPREP system you are

using. Your selection determines the correct set
UTILITIES SCREEN
of PID values that the controller will use to ensure
precise control of the temperature of the block:
UTILITIES
LANGUAGE SYSTEM
SYSTEM SCREEN
UTILITIES SYSTEM
< CALIBRATE JR MS LS HP HT

There are three options: LANGUAGE, SYSTEM, JR- DigiPREP JR. (24 position- ambient to 180oC)
and CALIBRATE. MS- DigiPREP MS (48 position- ambient to 180oC)
LS- DigiPREPLS 72 position- ambient to 180oC)
The calibration screen will be HP- DigiPREP HP (hot plate- ambient to 180oC)
NOTE explained in the last point of this HT- DigiPREP HT (all HT models- ambient to
section. 450oC)

NOTE
The system will perform properly
only if the correct block is selected.

The selection you make will be stored in the

memory of the controller, so there is no need to visit
this screen every time you use the system.

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 OPERATION PARAMETERS RUN SCREEN

Return to the menu screen. Select OPERATION Once you are finished entering the operation
and press enter. parameters, the run screen will be displayed:
TEMPERATURE 95.0oC
MENU TIME 120:23 AL
OPERATION UTILITIES

The run screen displays the current temperature

The next screen will prompt you to enter the target and time remaining. The temperature is displayed
temperature: to the nearest 0.1 of a degree, and the time is
displayed in minutes and seconds.
TARGET TEMPERATURE?
25 TO 180oC XXX.X An asterisk will appear occasionally in the upper
right corner of the display. This indicates that the
Using the number keys, enter the desired operating heating element is firing.
temperature. Press enter.
If "AL" is displayed in the bottom right corner of the
The next screen will prompt you to enter the target screen, the alarm is set to sound when the remaining
time: time runs out. Pressing the alarm key will toggle the
alarm off. You can also use the alarm key to silence
TARGET TIME? the alarm.
0 TO 999 XXX
To reset the timer, press the target time key to
The target time is the duration for which you want return to the target time screen.
the system to hold the target temperature. If the
alarm is activated, it will also use this time. The alarm
will sound at the end of the time sequence. Enter CALIBRATION SCREEN
the desired target time (in minutes) using the number
keys and press enter to accept the selection. CALIBRATION
#POINTS 0 (0-5)
From the next screen, you can choose whether or
not you want the heater to remain on at the end of Selecting CALIBRATE from the utilities screen will
the target time. bring you to the calibration screen, which is used to
enter calibration infromation for the DigiPROBE.
END OF TIME?
Calibration is done by comparing the keypad
HEATER OFF ON
display temperature to an NIST-calibrated (or similar)
Select OFF to turn the heater off at the end of the thermometer. The difference between the reading
target time, and ON if you want the block to remain from the calibrated device and the keypad display
at the target temperature indefinitely. (Press enter to temperature will be entered into the system.
accept the selection)
Not all thermometers have the same
NOTE
response time.

Run the system using a DigiPROBE inserted

in a DigiTUBE filled with water. On the keypad,
press the target temperature key and set the target

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temperature to the temperature you wish to use as SAFETY MESSAGES
your setpoint.
During operation, the keypad controller monitors
Once the setpoint temperature is reached and the system to detect potential problems.
both the keypad value and the reference value (from
the calibrated thermometer) are stable, measure and If there is a problem, the alarm will sound and
record the reference temperature and the keypad the controller will display a safety message. The
display temperature. (Better accuracy is achieved if controller will also suspend control of the block and
the values are taken from the same tube at the same the block will begin to cool down. To resume control
time.) The difference between the two values will be of the block, press any key on the keypad.
entered into the system. Calculate the input value as
follows: The timer will continue to count
Treference - T keypad = input value NOTE
down during this time.

Repeat for up to five reference temperatures.

POSSIBLE SAFETY MESSAGES
Next, re-access the calibration screen. (You may
have to turn off and back on to access the utilities Overtemp. Protection – Check Block Temp.
screen.) The calibration screen will prompt you to
enter the number of calibration point measured: This message will be displayed if the block or
sample temperature overshoots the target
CALIBRATION temperature significantly.
#POINTS 0 (0-5)
Possible Causes:
Using the number keys, enter a vlue between 0
and 5. (Choosing "0" will clear all calibration data • Samples were placed in a block that is too hot.
from the system.) Press enter. The number of points Try allowing the block to cool to near-ambient
you select will appear as the title of the next screen. temperature before beginning the next
(This example will use a 1 calibration point.) digestion.

1 POINT • The voltage switch on the back of the block is

SPT 0.0 DIFF +0.0 set to the wrong position.

Using the numeric keypad, enter the first • An exothermic reaction occured.
calibration set point value ("SPT") and press enter.
Next, enter the calculated error ("DIFF"): for a positive
Temperature Dropping – Check DigiPROBE
value, hold down the right-arrow key until the correct
value is reached. For a negative value, hold down
This message will be displayed if the sample block
the left-arrow key until the correct value is reached.
temperature is falling despite the controller attempt-
Press enter to save the values and exit the screen.
ing to heat it.
To return to the factory calibration or
Possible Causes:
to clear all data from the keypad,
NOTE
choose the number of calibration
• The sample has evaporated.
points as "0" and press enter to
make the selection.
• DigiPROBE is not submerged into the sample
sufficiently.
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 • DigiPROBE is not in use but was not returned Possible Causes:
to its well.
• The DigiPROBE is being moved in and out of
• An endothermic reaction occurred. the sample repeatedly.

• The DigiPROBE is being moved in and out of

Check DigiPROBE or DigiSET Dongle the holding well repeatedly.

This message occurs when the temperature is not • The sample has evaporated.
changing and has not reached the set point.

Possible Causes: PREVENTING SAFETY MESSAGES

• The DigiPROBE is not in the sample.
To avoid receiving safety messages, keep the
following tips in mind:
• The DigiSET dongle is not connected.
• When using the DigiPROBE, place the tip of the
• The DigiSET PROBE is connected but not in
PROBE about 1 mm from the bottom of the
a sample.
digestion vessel.

• Use watch glasses whenever possible.

Set point Exceeds Sample Boiling Point
• Use DigiTUBE racks whenever possible, as
These messages occur when the temperature
they will help insulate the block against
has not reached the target temperature for an
unnecessary heat loss.
extended period of time.
• Ensure that all samples are positioned correctly
Possible Causes:
in the block before leaving the DigiPREP
unattended.
• The target temperature entered is greater than
the boiling point of the sample.
• Do not remove the rack while the DigiPROBE
is in the sample. Remove the PROBE first, then
• The rate of evaporation of the sample is too
the rack of samples.
high, causing evaporative cooling.
• Return the DigiPROBE back to its storage well
If you wish to boil your samples
when not in use.
at a high rate, control the block
temperature instead of the sample
NOTE
temperature. Remove the DISABLING SAFETY MESSAGES
DigiPROBE and install the
DigiPROBE dongle. If you wish to operate the controller without
safety messages, you can disable them by
holding down the enter key while powering up
Temperature Unsteady – Check DigiPROBE
the controller. To re-enable the safety messages,
This message occurs when the temperature turn off the controller and then turn the power
varies too quickly. back on. Some methodologies have not been
considered in creating safety messages, so it
may be necessary to suspend the safety messages.

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 the appearance of the LCD after booting:
Disabling the safety messages is FAINT SQUARES BLANK
NOTE
not recommended.
Please phone your SCP service department
(see page 85) and report this information
DigiPROBE ERROR MESSAGES before returning the product. This will help our
technicians determine the cause of the malfunction
Error messages pertaining to the DigiPROBE are more quickly.
displayed on the run screen in the Temp field. If the
field displays “ERROR” during a run, the system will
stop heating. Power down the controller, check the CLEANING
connections, turn the power back on. (Remember
that if you are not using the DigiPROBE, the The keypad may be cleaned using a mild soap,
DigiPROBE dongle must be connected.) If problem water, and a clean cloth. Ensure that the controller
persists, consult the service department (see page is disconnected from the power supply. No organic
85). solvents should be used as it may destroy the finish
on the keypad mask. The system should not be
Disconnecting or reconnecting the immersed in any liquid.
umbilical cable while the system is
NOTE turned on, especially while the run
screen is displayed, will likely result
in permanent damage to the
instrument.

DIAGNOSTICS TEST PROCEDURE

If you are having trouble with the DigiPREP

controller, follow the steps below and contact the
service department.

1. Shut off power to DigiPREP keypad.

2. Ensure that DigiPROBE is installed and

inserted into either the holding well or the
sample. If you are not using DigiPROBE,
ensure that the dongle is connected.

3. Ensure that the umbilical cable is connected

properly to the block and the controller.

4. Turn the power back on.

5. Is the blue LED light on? YES NO

6. Is the LCD backlight lit up? YES NO

7. If there is a problem with the LCD, describe

KeyPad 17
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 SPECIFICATIONS DigiPREP KEYPAD
ENVIRONMENTAL
Relative humidity 30% to 80% ELECTRICAL
Altitude Up to 2000m Model Keypad
Installation Category ll Voltage 115/230V ±10%
Pollution Degree 2 Amperage 13 A
Ambient operating -5 °C to 40 °C Frequency 50/60 Hz
temp. Maximum operating
85 °C
temp.

Line voltage fluctuations greater

NOTE than 10% will affect instrument
performance.

RoHs

Toxic or hazardous substances and elements

Hexavalent Polybrominated Polybrominated
Lead Mercury Cadmium Chromium
Part name Biphenyle Diphenyl Ether
(Pb) (Hg) (Cd)
(Cr6+) (PBB) (PBDE)
Housing o o o o o o
Electronics o o o o o o
Display o o o o o o
Wiring Harness o o o o o o
Fasteners o o o o o o

O: Indicates that the toxic or hazardous substance X: Indicates that the toxic or hazardous substance
contained in all the homogenous materials for this contained in all the homogenous materials for this
part, according to EIP-A, EIP-B, EIP-C, is below the part, according to EIP-A, EIP-B, EIP-C, is above the
limit requirement in SJ/T11363-2006. limit requirement in SJ/T11363-2006.

18 KeyPad
SCP SCIENCE
Version 1.0
Legend:
1. Rounded-Head Nylon Screw #6-32 x 1” 11. Nylon Nut #6-32
2. On/Off Switch 12. Stud #6-32
3. Dongle 2-Pin Female 13. Brass Insert #6 Screw
4. Panel Lock Nut 14. LCD
5. Panel Mount Connector 7-Pin Male 15. Fish Paper
6. Panel Mount Connector 2-Pin Male 16. Nylon Stand-off #6-32 x ¼”
7. Flat Head Nylon Screw #6-32 X 1 “ 17. Bottom Kydex ¼”
8. Voltage Selector Switch 18. Feet
9. Flat Washer, Nylon #6 Screw 19. Pan Phillips Head Tapping Screw #8 x ¾”
10. LED
KeyPad 19
SCP SCIENCE
Version 1.0
 CONTROLLER GENERAL DESCRIPTION

The following figure shows a general block diagram The KeyPad controller system is composed of
of the KeyPad controller and all the interaction a keypad to enter information regarding set point
between components. Each part will be explained temperature and controlling time to a CPU, which
in details in a different section of the document. controls the DigiPREP block (Jr, MS, LS, HP or HT).

(100- 260Vac)
115/230 Vac +5V digital
UIPS +12Vdc Regulators and
Module Voltage Reference +5V analog (AVCC)

Heater Drive Heating

Module Block

RTD sensor RTD Input LCD Display

Circuit
A/D
Host CPU
Module
PC DTE (RS 232 COM)
Debug/Update

Selector /
Signal_Out

(optional)
KEYPAD Buzzer/
Accessories Connector
(I/O, PWM and ADC) Alarm

FIGURE 5: GENERAL KEYPAD BLOCK DIAGRAM

20 KeyPad
SCP SCIENCE
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LIGHT EMITTING DIODE (LED) & LCD DIGITAL SCREEN (LED) IS MALFUNCTIONING

OPERATION LED NOT ILLUMINATED (BLUE) WHEN • With the system powered up, verify that the
POWER IS ON. following message is appearing for 5 seconds on
the LCD screen.
• Ensure the power cord is fully inserted into its
socket (see figure 2).
SCP SCIENCE
• Verify that the power switch is in the ON position.
DigiPREP KEYPAD 10.0

• Remove the bottom plate by removing the four

feet and verify that the front LED is connected to • If the startup message is not appearing or strange
connector "J6" (see figure 6 for details). characters are displayed replace the LCD
monitor.

• After 5 seconds, the user should see the

following

MENU
OPERATION UTILITIES

• If not, remove the bottom plate by removing the

4 screws holding the feet in place and verify that
the LCD ribbon cable is fully inserted into the J2
connector (see figure 7 for details).
FIGURE 6: LED CABLE POSITION

If the LED is not lit, please refer to the Power

Circuit section before changing the LED.

Ensure hat the LED has not been

NOTE connected in reverse, positive to
negative.

FIGURE 7: LCD DISPLAY RIBBON CABLE POSITION

Legend
1. J2, LCD ribbon cable

If the LCD display is still not working, please

refer to the CPU section before changing the Digital
screen.

KeyPad 21
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 KEYPAD MALFUNCTION

The KeyPad is made of 16 independant

switches. The information of a pressed button is
sent to the CPU with help of a row and
column detector. One should feel a "soft click" upon
pressing a button.

5Vdc

R52 R51 R50 R49

RJ7 10K RJ6 RJ5 10K RJ4
10K 10K
ROW4 ROW3 ROW2 ROW1

C31 R20 C30

R23 C33 R22 C32 R21 1nF
1nF 100
100 1nF 100 1nF 100
GND GND GND GND

1 4 7 Shift Left
COL1

R16
C26
100 1nF
GND
2 5 8 0
COL2

R17 C27
100 1nF
GND

Alarm Temperature Time Enter

COL3

R18 C28
100 1nF
GND

3 6 9 Shift Right
COL4

R19 C29
100 1nF

GND

FIGURE 8: KEYPAD ELECTRONIC DIAGRAM

22 KeyPad
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FAILED KEYPAD BUTTONS KEYPAD DIAGNOSTIC SECTION

Please write down each failed To identify if the trouble is caused due to the
button number in order to see keypad buttons or a faulty circuit, verify the
NOTE if the problem is for a complete impedance of the buttons that do not respond to the
row or column or if it is for commands by measuring between the following pins
different row and column buttons of J8 (see figure 9):

• In order to verify the buttons please reset the Pin 1 and pin 5 .............. Button #3
KeyPad controller (ON/OFF) and select the Pin 1 and pin 6 .............. Alarm Button
Operation section in the main menu. Pin 1 and pin 7 .............. Button #2
Pin 1 and pin 8 .............. Button #1
•A target temperature is now asked. Pin 2 and pin 5 .............. Button #6
Pin 2 and pin 6 .............. Temperature setting button
•First, verify all Digits. Every time you press a Pin 2 and pin 7 .............. Button #5
button, you should see the corresponding Pin 2 and pin 8 .............. Button #4
number under the cursor. Pin 3 and pin 5 .............. Button #9
Pin 3 and pin 6 .............. Time setting button
• When it is done and all Digits are fine, enter 25. Pin 3 and pin 7 .............. Button #8
and press the ENTER key. Pin 3 and pin 8 .............. Button #7
Pin 4 and pin 5 .............. Right shift button (>)
•Enter "1" in the "Target Time" menu and Pin 4 and pin 6 .............. ENTER button
press the ENTER key. Pin 4 and pin 7 .............. Button #0
Pin 4 and pin 8 .............. Left shift button (<)
•Now it is time to verify the ARROW keys.
• Press the left and right arrow key a couple If the buttons are OK:
of times and see if the cursor switched •Pushed : Less than 200 ohms.
from ON to OFF and so on. •Not pushed: less than 30 Mohms.

• Select HEATER OFF and press ENTER (make If all the values are correct, the circuit is faulty.
sure DigiPREP is connected). Change the KeyPad PCB.

•Enter a time scale of 1 minute and press enter.

• Press the ALARM, TARGET TEMPERATURE and

TARGET TIME button one at a time and verify
if they execute correctly the commands below:

ALARM
A small "AL" should appear on the
LCD display.

TARGET TEMPERATURE
The target temperature menu should FIGURE 9 : PUsH BUTTON MEASURING LOCATION
appear.
TARGET TIME Legend
The target time menu should appear. 1. J8 (pins 1 to 8)

KeyPad 23
SCP SCIENCE
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 UIPS POWER SUPPLY SECTION
The power section is rectifying and regulating
power for different parts of the KeyPad controller.
It is designated as a Universal Input Power Supply
(UIPS) since it can operate within 100 - 260 VAC to
output +12Vdc/0.8A. No selector switch is needed
for 115 VAC or 230 VAC input supply. The +12Vdc
voltage is then regulated to supply 5.0Vdc Digital
and 50Vdc(AVCC) analog to the main circuits of the
system.

FIGURE 10: AC/DC CONVERTER

24 KeyPad
SCP SCIENCE
Version 1.0
THE CONTROLLER IS NOT FUNCTIONING • Place the negative lead of the multimeter on
TP2, which is the ground test point. Place the
WHEN THE POWER SWITCH IS ON
positive lead of the multimeter on TP3, which is
the +12V test point. You should measure
• Ensure the power cord is fully inserted into its between 11.8 Vdc and 12.2 Vdc. If not, meausre
socket (see Figure 2). the voltage across U1-1 and U1-2, and U1-4
and U1-3, you should read respectively 1.2V
• Unscrew the bottom plate by removing the 4 and 0.2 V. If not, replace U1.
screws holding the feet in place.
• Measure the voltage across U3-1 and GND. You
• Verify that the F1 Fuse is ok. (see figure 11 and 12 should read about 2.5 Vdc. If not replace U3.
for part location.)
• Place the negative lead of the multimeter on TP2
•Replace by a 0.75A if necessary and the positive lead on TP4, which is the +5.0V
test point. You should measure between 4.9 Vdc
•Verify the 2 fuses along the KeyPad housing are and 5.2 Vdc. If not replace U4.
ok.
• Place the negative lead of the multimeter on TP6,
•Replace them by a 15A if necessary. which is the analog ground test point. Place the
positive lead of the multimeter on TP5, which is
•Verify all the power cable connections. the AVCC test point. You should measure
between 4.9 Vdc and 5..2 Vdc. If not, replace
•Green wire is connected with "Earth GND" U5.

• Black wire of the filter is connected with the 15A

fuse holder; the black wire from the fuse holder,
with the power switch; the black wire of the
power switch, to "HOT" pin.

• White wire of the filter is connected with the 15A

use holder; the white wire from the fuse holder,
with the power switch; the white wire of the
power switch, to the "NEUTRAL" pin.

•Use a multimeter to measure the following

voltages (see figure 13):
FIGURE 11: AC POWER CONNECTORS & FUSE F1 LOCATION
•Place the negative lead of the multimeter on
TP1GND. Place the positive lead of the multimeter Legend
on TP1. You should measure about 160 Vdc 1. Fuse F1 (0.75A)
for 120 Vac input supply or 300 Vdc for 2. EARTH GND connector
240 Vac input supply. If the voltage is much 3. NEUTRAL connector
lower, measure the voltage across the cathode 4. HOT connector
and anode of diodes D3, D4, D5 and D6. You
should read about 63Vdc for 120 Vac and
125 Vdc for 240 Vac. If not, replace the
faulty diodes.

KeyPad 25
SCP SCIENCE
Version 1.0
 Legend
1. Fuse 15A
2. Fuse 15A
3. AC Filter

FIGURE 12: AC FILTER AND 15A FUSES LOCATION

5
4

10

6
7
8
FIGURE 13: DC POWER AND REGULATORS
Legend
1. Test point TP1
2. Diodes: D3, D4, D5 and D6
9
3. Test point TP1GND
4. U1
5. U3 pin 1
6. Test point TP4 (5.0Vdc supply)
7. Test point TP2 (Digital ground testpoint)
8. Test point TP3 (12Vdc supply)

26 KeyPad
SCP SCIENCE
Version 1.0
HEATER DRIVE SECTION

This circuit controls the heater inside all types of

DigiPREP blocks. It consists of an opto-isolated
triac driven circuit.

FIGURE 14: HEATER DRIVE CIRCUIT

KeyPad 27
SCP SCIENCE
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 THE DigiPREP BLOCK IS NOT HEATING UP

DigiPREP connection verification

• Ensure that the cable between the KeyPad

controller and the heating block is correctly
inserted on both sides.

• Verify that the voltage selector of the heating

block is properly set.

COM2 dongle verification FIGURE 15: DIGISET CONNECTOR LOCATION

When the COM2 of the KeyPad Legend

NOTE
controller is not connected to a DigiSET connector
DigiSET system, the port must be
shorted.

• Make sure that sections 1 and 2 have been verified

INTERNAL WIRING CONNECTION VERIFICATION
before continuing.
• After removing the bottom plate, verify the
• Ensure that the DigiSET dongle is fully inserted connectivity between the heating block external
into COM2 port (see figure 2) connector and the PCB (see figure 16).

• If so, before opening the bottom plate, verify with

a multimeter that the COM2 dongle is shorted. If
not, replace the part with a new one.

• If the dongle is ok, remove the bottom by

removing the 4 screws that hold the feet in place.
Check if the DigiSET cable (see figure 15 for
position) is fully inserted.

FIGURE 16: HEATING BLOCK CONNECTOR LOCATION

Legend
1. Heater connector (Hot heating block)
2. Neutral connector (Neutral heating block)
3. Earth Ground

DIGISET VERIFICATION (ONLY IF APPLICABLE)

Make sure that the DigiSET is fully fonctional (see

28 KeyPad
SCP SCIENCE
Version 1.0
DigiSET operation and service manual). Be very careful not to touch any
NOTE components inside the KeyPad as it
is running.
Opto-isolated Triac Driven circuit verification
The block temperature must be
Fan verification NOTE
lower than the set point temperature
• The fan should turn on at power-up. If it does for the LED to flash.
not or if it does slowly, replace the fan and
the triac. In both cases, it will cause the triac • If the LED is not on, if possible, use and
to be overheated and destroyed. oscilloscope and verify if there is a
pulsing signal on the trigger input
• To remove the fan, unscrew the 2 screws as (TP8), coming from the CPU. If there
shown in figure 17. is no signal on TP8, please refer to the
CPU section for more details.
Otherwise, check the integrity of the LED
and the transistor Q2 (see below).

• If there is a signal on TP8, the block

temperature is below set point temperature,
the DigiSET dongle and cable are
installed correctly and the LED is ON
or flashing, measure the voltage at TP9. It
should be maximum 3Vdc. If it is higher or
close to 0Vdc, change the opto-coupler
U8.

IGURE 17: FAN SCREWS LOCATION

Legend
1. Fan screws

Opto-isolator section verification

This test will confirm if the CPU is

operating correctly.

• Remove the bottom plate

FIGURE 18: OPTO-ISOLATOR U8, TEST POINTS AND LED D9
• Set the target temperature to 35oC and
target time to 1 minute. Legend
1. Test Point TP8
• After starting the system, turn the module 2. D9 SMT LED (green)
upside down and see if the LED D9 (see 3. Test point TP9
figure 18 for position) is flashing. 4. U8

KeyPad 29
SCP SCIENCE
Version 1.0
 Q2 SWITCH (NPN BIPOLAR TRANSISTOR)
VERIFICATION

• If the signal on TP8 coming from the CPU is

on, the problem could be the bipolar
transistor Q2.

•Measure with a multimeter the voltage

between Q2 collector pin 3 and GND. If the
signal on TP8 is pulsing, Q2 should switch
between 0.3V and a maximum of 4.7V. If
TP8 is high, Q2 should be steady at 0.3V. If FIGURE 19: HEATER DRIVE TEST PINS AND
Q2 is OK in either case, the problem is COMPONENTS LOCATION
probably the triac (see below)
Legend
• If the signal on TP8 is low and the LED is ON, 1. Q2 pin 3 (collector)
then Q2 is defective. 2. HEATER pin (Hot)
3. NEUTRAL pin
4. T1, Triac
D9 LED verification

If Q2 is good and the signal on TP8 is high or

pulsing and the LED lights up or pulsing, the
LED is OK. If not, D9 is defective.

TRIAC T1 verification

•The only way to see if the Triac is behaving

correctly is by measuring between " HEATER
connector" pin and "NEUTRAL" ( see figure
FIGURE 20: TRIAC OUTPUT WHEN HEATING
19). Make sure that there is 120V/230V AC
SECTION IS FIRING
(toggling or not). Also refer to figure 20 for
an example of what an be seen on a scope if
the control is toggling. If all of those tests are correct, please
refer to the DigiPREP block service
• Make sure that the heating block page 62 for more details.
temperature is lower than the set point
temperature if you want the Triac to toggle.
A/D CONVERTER
• If the triac output remains low while it should
toggle as shown in figure 20, replace the
triac. The analog to Digital conversion is the feed back
information coming from the block temperature
If you're using a scope, it must be sensor or from a DigiPROBE. The CPU section
NOTE handles this information in order to monitor and con-
isolated from the wall outlet.
trol the block temperature.

30 KeyPad
SCP SCIENCE
Version 1.0
POSSIBLE A/D PROBLEM ANALOG CIRCUIT MEASUREMENTS WITH
100 OHMS RESISTOR BETWEEN PINS 3
If the DigiPROBE is reading the AND 4 OF J9
wrong temperature, make sure that
Test Point Required Value
the DigiPROBE itself is functional
before looking at the converter TP7 5V
NOTE
circuit. This can be accomplished by TP11 5V
measuring the resistance across pin TP10 1V
1 and 2 of the DigiPROBE connec-
tor. TP14 1.95V
Typical 25oC = 108 ohms. TP13 0.95V
TP12 2.60V

RTD INPUT CONNECTION If you fail to get those values, the analog section is
faulty; the KeyPad PCB must be replaced.
• Visually inspect the external connection of the
DigiPROBE.

• Unscrew the bottom plate by removing the 4

screws that are holding the feet in place. Make
sure that the J9 connector is fullt connected with
the header (see figure 21 for location). If it is, then
start investigating the circuit as explained below.

A/D POWER AND CONNECTIONS

• Disconnect J9 from the board, then power up the
FIGURE 21: J9 CONNECTOR LOCATION
controller. With the negative lead of a multimeter
on TP6 and its positive lead on the test points
Legend
below (see figure 22), you should read the
1. J9 header with RTD cable connection
following measurements:

ANALOG CIRCUIT MEASUREMENTS

WITH J9 OPEN
Test Point Required Value
TP7 5V
TP11 5V
TP10 1V
TP12 0V

• Now on J9, short pins 2 and 3, short pins 4 and 5

and insert a 200 ohms 1% precision resistor
between pins 3 and 4, you should read the
following measurements:

KeyPad 31
SCP SCIENCE
Version 1.0
 CPU SECTION

The CPU section is basically the microcontroler

PIC18F8722, U6 (see figure 23 for location)

FIGURE 22: A/D CIRCUIT TEST POINTS AND J9 LOCATION

Legend
1.
2. TP12 (Analog input to CPU)
FIGURE 23: CPU AND REFERENCE VOLTAGES LOCATION
3. TP13 (Differential voltage)
4. TP7 (5Vdc analog voltage)
Legend
5. TP6 (GND analog voltage)
1. Pin 3 of J1
6. TP10 (1Vdc reference voltage)
2. Pin 1 of J1
7. TP11 (RTD supply voltage)
3. Via to pin 27 of U6
8. TP14 (RTD signal voltage)
4. Via to pin 26 of U6
9. J9 header with RTD cable disconnected
5. Via to pin 25 of U6
(pins 1 to 5)
6. U6, CPU

If anyof the sections 1 to 5 has been verified and

A/D CONVERSION BEHAVIOR a CPU problem is suspecgted then try the following
sections.
• If all the previous measurements are correct, make
sure that all the external components or
instruments (snesors, PROBE, DigiSET, etc) and
LCD DISPLAY PROBLEM
interconnection cables are properly connected.
If the section 1 has been fully investigated and the
• Reconnect cable J9 to its header and verify if the
system is always returning to the default setup (EN
system is heating up accordingly and the block
language, default heating block type etc.), replae the
temperature feedback is correct.
KeyPad PCB.

32 KeyPad
SCP SCIENCE
Version 1.0
A/D CONVERSION PROBLEM

If the section 5 has been fully investigated and

the system does not provide the right temperature
readings, verify the analog supply and the analog ref-
erence voltage of the microcontroller U6.

• With the negative lead of a multimeter on the via

connected to pad C25-1 and its possible lead on
the via connected to pd C25-2, you should read
5Vdc.

• With the negative lead of a multimeter on the via

connected to pad C25-1 and its positive lead on
the via connected to pin U6-27, you should read
5Vdc.

If those values are less than 4.8V, replace the

KeyPad PCB.

CPU UNSTABLE

If CPU is resetting by itself, check pin 9 of U6.

WIth the negative lead of a multimeter on pin 3 of J1
and its positive lead on pin 1 of J1, you should read
a steady voltage value of at least 3.7 Vdc. If not, re-
place the KeyPad PCB.

KeyPad 33
SCP SCIENCE
Version 1.0
DIGESTION BLOCKS
DigiPREP
(Jr, MS, LS, HP)
IInstruction
i Manual
M l

www.scpscience.com

Providing Innovative Solutions to Analytical Chemists

INTRODUCTION
DigiPREP digestion blocks are designed for laboratory use in the digestion and evaporation of a variety of
samples, primarily water, wastewater, soil, and sludge samples. DigiPREP Jr, MS, LS, and HP blocks have
a temperature range of ambient to 180°C.

DigiPREP blocks require a DigiPREP controller (keypad, colour touch screen, or PC Classic – sold sepa-
rately) for operation.

DigiPREP blocks are designed to hold DigiTUBE sample digestion vessels. Optional accessories
include DigiPROBE (used to monitor sample and/or block temperature) and DigiSET PROBE (used to
monitor and shut off the heating system at a set sample volume level).

They are available in 50ml & 100ml format.

KeyPad 35
SCP SCIENCE
Version 1.0
 CAUTIONS AND NOTES WARRANTY
Cautions, warnings, and notes are included SCP SCIENCE warrants this product free
throughout this manual. from defect in workmanship and materials
for one (1) year from date of purchase.
CAUTION
A caution is used to emphasize • Should the unit malfunction, call SCP
CAUTION information pertaining to procedures SCIENCES's service department (see page
that, if not strictly followed, may result in 92), or your local distributor. and a service
damage or destruction to the instrument representative will instruct you on how to
or improper instrument operation. proceed.

WARNING • There are no user-serviceable parts in this unit. The

A warning is used to emphasize warranty is void if the unit shows evidence of being
WARNING information about dangerous or tampered with, of being subjected to excessive
hazardous conditions relating to the moisture, heat or corrosion, or of other misuse.
operation, cleaning, or maintenance of the
instrument that may result in personal injury. • SCP SCIENCE shall not be responsible
for any damage or losses however caused
NOTE which may be experienced as a result of
A note is used to emphasize procedures the installation or use of this product.
NOTE or conditions that may be misinterpreted
or overlooked, and to clarify potentially • This product is not warranted for, nor has
confusing situations. it been tested for, use with perchloric acid.
The user accepts all responsibility if this
product is used with perchloric acid.

Symbol Description Symbol Description

V Voltage l Mains on

~ Alternating current 0 Mains off

Attention, consult
A Current accompanying documents

Hz Frequency Caution, hot surfaces

Protective conductor terminal

F Fast-acting fuse

36 KeyPad
SCP SCIENCE
Version 1.0
OPERATIONAL PRECAUTIONS SAFETY INFORMATION
DigiPREP block must be connected to a A minimum of safety considerations must be
controller that is properly grounded. In the event followed when working with DigiPREP low
of an electrical short circuit, grounding reduces temperature blocks in order to maintain good
the risk of electrical shock by providing an escape laboratory practice:
wire for electrical current. DigiPREP controllers are
supplied with an electrical cord that has a grounding • Do not place the DigiPREP blocks on a surface
wire with a grounding plug. Ensure that the plug containing flammable material.
is plugged into an outlet that has been properly
installed and grounded. Consult a qualified • DigiPREP block requires a clearance of three
electrician if there is any doubt about the existence inches (7.5cm) on all sides.
of proper grounding at the outlet.
• DigiPREP block should be operated in a fume
DigiPREP block is designed to be lifted from hood.
the bottom only. Ensure that the controller is
disconnected prior to moving the block. Do not • Do not place the DigiPREP controller in a fume
attempt to lift the block by the top white trim hood.
as damage may result.
• DigiPREP system must be plugged into a
DigiPREP blocks are elevated-temperature three-prong grounded outlet
digestion systems with exposed hot surfaces. Be
careful around the instrument when it is in operation.

KeyPad 37
SCP SCIENCE
Version 1.0
 INSTALLATION SETTING UP

UNPACKING Place the DigiPREP block in a fume hood. The

controller must not be placed in the fume hood.
Retain all packing material in case With the controller’s power switch in the “off”
NOTE you need to return the instrument position, do the following:
to the manufacturer for service. • Verify that the voltage selector at the back of the
DigiPREP block is properly set.(Typically 115 for
1. Verify that all components listed have been North America, and 230 for Europe.)
included: • Connect the block’s umbilical cable to the
• DigiPREP block controller.
• Operation manual
• DigiPROBE dongle Disconnecting or reconnecting the
• DigiTUBE rack umbilical cable while the controller is
•Jr: 1 rack WARNING turned on, especially while it is on the
•MS: 2 racks RUN screen, will likely result in
•LS: 3 racks permanent damage to the instrument.
•HP: 0 racks
• Connect the power cord to the back of the
Optional items, such as glass, quartz, controller .
calibrated or non-calibrated digestion • Connect the DigiSET (or DigiSET dongle)
tubes may have been included in the to the back of the controller.
shipment. Carefully check the packing • Connect DigiPROBE (or DigiPROBE dongle)
list(s) and the contents of shipping to the back of the block.
NOTE
cartons to verify that all items
listed are included. Please notify SCP If you are not using the DigiPROBEor
SCIENCE or your local distributor of NOTE DigiSET, the dongles must be
any discrepancies. connected; otherwise, an error message
may be displayed.
Inspect the products for any shipping damage.
If the instrument has been damaged in shipping, • Insert the glass well liner into the DigiPROBE well.
contact the freight carrier to report damage and (Small hole near right of block)
to file a damage report. Also contact the SCP • If you are using DigiPROBE, insert the PROBE
SCIENCE service department to report damage into the well liner.
and to request service information (see page 88
for contact information). The system is now ready to be plugged in
and turned on. Please see your controller
If you find evidence of damage, do manual for operation instructions.
WARNING not attempt to operate the instrument.

38 KeyPad
SCP SCIENCE
Version 1.0
OPERATION WITH PROBES
DigiPROBE can be calibrated with DigiPREP
DigiPROBE controllers or the PC Classic controller (with
Go2Temp software). Please see your controller
DigiPROBE (optional) may manual for calibration instructions.
be used with DigiPREP
system to monitor and control
the sample temperature (when DigiSET
placed in the sample) or the
block temperature (when DigiSET (optional) can be used with all DigiPREP
placed in the storage well low temperature systems to monitor and suspend
located on the block). the heating cycle at a pre-set sample volume level.

DigiSET PROBE is connected to the DigiSET unit

When using the DigiPROBE with the and 'COM 2' from DigiSET unit is connected
NOTE DigiPREP HP, a flat-bottomed, conical to the 'COM 2' of the controller with the supplied
flask is recommended for best results. cable. Please consult the DigiPREP controller manual
for more detailed instructions.
Install the PROBE in the port marked 'DigiPROBE'
on the back of the DigiPREP block. If using to
monitor and control the heating of the block via the
sample temperature, insert the PROBE end into a
control sample with the PROBE holder supporting
the DigiPROBE. (The 010-500-036 PROBE holder
is used with 50ml DigiTUBEs and 010-501-036
is used with 100ml DigiTUBEs and a 6"(15 cm)
PROBE. The 010-500-037 PROBE holder is used
with glass digestion tubes and a 10" (25 cm) PROBE.)

If using to monitor & control the block

temperature, place the DigiPROBE in the storage
well, located at the rear right corner of the graphite
block. Ensure that there is a glass liner (catalogue
number 010-500-041) in the well.

The control sample should be a typical

NOTE digestion sample. The tip of the
DigiPROBE should be approximately
1 mm from the bottom of the digestion
vessel.

Serious temperature overrun may

occur during digestion if the DigiPROBE
CAUTION is not in an appropriate sample or
the storage well. Always place the
DigiPROBE in the storage well when
not in use.

KeyPad 39
SCP SCIENCE
Version 1.0
 DigiPREP JR, MS, LS, HP BLOCK DESCRIPTION

DigiPREP Jr

4 2

DigiPREP MS
1

DigiPREP LS 6

1. DigiPROBE 4. Voltage selector

connection port switch (115V or 230V)

DigiPREP HP 2. Umbilical cable 5. DigiPROBE dongle

connects to controller (4 pin male)

3. DigiPROBE 6. 24-position
storage well DigiTUBE rack
(MS:2, LS:3, JR:1)

40 KeyPad
SCP SCIENCE
Version 1.0
CLEANING the model of your block, first turn the unit onto its
side and check the bottom for an aluminium key.
If the surface is still hot, contact with liquid
may create steam that can scald you. 1. If your DigiPREP block has an aluminium key:
WARNING
It is important to allow the instrument
to cool before cleaning. Insert the aluminium key into one of the slots
located on the bottom of the unit beside the rubber
CLEANING OF MINOR SURFACE SPILLS feet. Gently push the aluminium key into the slot
Turn off the system and disconnect the block from until the white top ring begins to lift. Repeat the
the DigiPREP controller. Allow the block to cool. process for the three remaining slots, and
Sponge up any excess liquid, dilute the area with return the aluminium key to the base of the unit.
clean water, and wipe dry with a paper towel. (If the aluminium key is missing, a substitution
such as a flat-head screwdriver may also work.)
CLEANING OF DIGESTION WELLS
Turn off the system and disconnect the system 2. If your DigiPREP block does not have an
from the block controller. Allow the block to cool aluminium key:
before proceeding further.
Suction the solution out of the well(s) with an The white top ring is held in place by plastic spring
eye dropper, squeeze bottle, or pipette. Dilute any clips inside the housing at all four corners. Release
remaining spillage with water, two or three times, the clips by gently lifting the corners of the white top
and suction as much solution out as possible. ring until it becomes free. If it does not remove easily,
Sponge the remaining residue with a paper towel. insert a flat-blade screwdriver between the white
Allow the system to dry completely before top ring and the outer Kydex skin. Gently twist the
plugging into a power outlet. Observe good labatory screwdriver to pry the white top ring off at all
practices by wearing gloves to preform the above four corners.
task. Next, use tweezers or pliers to gently remove
the insulation from the sides of the block. (If
CLEANING MELTED PLASTIC FROM WELLS a replacement set of insulation is required,
Heat the block to 160°C. Using a pair of contact the service department.)
needle-nose pliers, carefully pinch and gently The graphite block is held into place by four
pull the softened plastic residue from inside the mounting bolts located on the bottom of the unit.
well. If it is difficult to remove the melted plastic Turn the unit upside-down onto a soft surface, being
increase the block temperature by 5°C. careful not to scratch the Teflon coating on the
graphiteblock. Using a flat-blade screwdriver, remove
CLEANING OF A MAJOR SPILL the plastic cover plates. Next, using an Allen wrench
If a solution has run down below the white top (6mm or ¼ inch), remove the mounting bolts. Finally,
ring and under the block, turn off the system and lift the housing up from around the graphite block. (Lift
unplug the block from the power source. Allow gently as there is wiring attached to the graphite block.)
the block to cool before proceeding further. You may now clean any affected parts with
The block must be disassembled, cleaned, and a damp cloth. Gloves and a lab coat are strongly
thoroughly dried prior to running again. recommended. (Be careful not to pinch the wires
between the graphite block and other components.)
NOTE Please consult the service
To assemble repeat in reverse order.
department for help if required.
Before reassembling, make sure that the Teflon
sheet is adhered to the block, that the heater is
In order to access the block, you must first remove
secured in place, and that the aluminium plate
the white top ring. This step will be different depending
is placed over the insulation. Also ensure that all
on the model of your DigiPREP block. To determine
components are dry prior to reassembling.
KeyPad 41
SCP SCIENCE
Version 1.0
 SPECIFICATIONS DigiPREP HP, MS, JR, LS
Environmental
The main supply cord is constructed
Relative humidity 30% to 80%
NOTE
of heat-resistant material and should
Altitude Up to 2000m only be replaced by an equivalent or
Installation Category ll better cord.
Pollution Degree 2
Line voltage fluctuations greater than
Ambient operating -5°C to 40°C
NOTE 10% will affect instrument
temp.
performance.

Electrical
Model DigiPREP HP / MS DigiPREP Jr DigiPREP LS
Voltage 115/230V ±10% 115/230V ±10% 230V ±10%
Power 925W 725W 2665W
Frequency 50/60 Hz 50/60 Hz 50/60 Hz
Ambient operating temp. Ambient to 180°C Ambient to 180°C Ambient to 180°C

RoHs

Toxic or hazardous substances and elements

Hexava- Polybromi-
Mer- Cadmi- lent Chro- Polybrominat-
Lead nated Diphenyl
Part name cury um mium ed Biphenyle
(Pb) Ether
(Hg) (Cd) (PBB)
(Cr6+) (PBDE)
Housing o o o o o o
Graphite Block o o o o o o
RTD probe o o o o o o
Over temperature sen-
o o o o o o
sor
Heater o o o o o o
Umbilical Cord & wiring o o o o o o
Voltage Selector o o o o o o
Fasteners o o o o o o

O: Indicates that the toxic or hazardous substance X: Indicates that the toxic or hazardous substance
contained in all the homogenous materials for this contained in all the homogenous materials for this
part, according to EIP-A, EIP-B, EIP-C, is below part, according to EIP-A, EIP-B, EIP-C, is above
the limit requirement in SJ/T11363-2006.

42 KeyPad
SCP SCIENCE
Version 1.0
OPTIONS
Catalogue Number Description
010-500-014 DigiSET (115V/230 V)
010-500-031 DigiVAC top
010-500-033 DigiVAC blower unit
010-500-035 DigiPROBE holder for DigiTUBEs
010-500-039 DigiPREP Fume Hood
010-500-049 DigiPREP Fume Hood II
010-500-051 Dongle for DigiSET port (2-pin female)
010-500-059 DigiPREP Fume Hood to fit LS
010-500-205 DigiPREP MS, 50ml 115V/230V
010-500-210 DigiPREP LS, 50ml
010-505-052 Dongle for DigiPROBE port (4-pin male)
010-505-015 DigiPROBE for use with DigiTUBEs (6inch/15cm)
010-505-016 DigiPROBE for use with 100 ml glass tubes (10 inch / 25cm)
010-505-041 DigiPROBE storage wells for HP
010-505-205 DigiPREP Jr, 50ml, 24 pos. 115V/230V
010-505-230 DigiPREP HP, 50ml, 115V/230V

ACCESSORIES 50ML
Catalogue Number Description
010-500-019 DigiPROBE watch glasses (25)
010-500-023 24-position rack (for MS, LS), 50ml
010-500-026 DigiTUBE storage rack , 50ml (5/pk)
010-500-041 Glass storage well (10/pk)
010-500-066 Teflon digestion tubes, 65 ml (6/pk)
010-500-068 Borosilicate glass tubes, 225 mm, 100 ml (6/pk)
010-500-069 DigiPREP LS start-up kit, 50ml
010-500-081 Disposable watch glasses (1000/pk)
010-500-224 Umbilical Cord Extension, 2 meter
010-500-227 Umbilical Cord Extension, 1 meter
010-500-230 DigiFILTER manifold
010-500-261 DigiTUBEs with RackLock feature, 50 ml (750/pk)
010-500-262 DigiTUBEs with RackLock feature, shrink-wrapped (30x25)
010-505-021 24-position rack (for DigiPREP Jr), 50ml
010-505-023 24-position 2-tier rack for 100 ml borosilicate glass tubes
010-505-052 DigiPREP MS start-up kit
010-505-066 DigiPREP Jr start-up kit

KeyPad 43
SCP SCIENCE
Version 1.0
 ACCESSORIES 100ML
Catalogue Number Description
010-501-010 DigiPROBE Holder, for 100ml tubes
010-501-014 DigiSET for DigiPREP 100ml (115V/230V)
010-501-020 DigiSET PROBE Holder
010-501-028 Foam Storage Rack 100 ml (pk/5)
010-501-060 Caps, Blue for 100ml DigiTUBEs (pk/100)
010-501-081 Disposable Watch Glass, 100ml (p500)
010-501-115 DigiPROBE, 6" for 100ml
010-501-210 DigiPREP Jr, 100ml, 12 Pos (115V/230V)
010-501-215 Start up Kit for 100ml DigiPREP Jr
010-501-230 DigiPREP MS, 100ml, 30 Pos (115V/230V)
010-501-235 Start up Kit for 100ml DigiPREP MS
010-501-250 DigiPREP LS, 100ml (230v)
010-501-255 Start up Kit for 100ml DigiPREP LS
010-501-261 DigiTUBE, 100ml,with RackLock (pk300)
010-501-262 DigiTUBE, 100ml, with RackLock/No Caps (pk300)
010-501-263 DigiTUBE, 100ml, with no RackLock (pk300)
010-501-264 DigiTUBE, 100ml, with no RackLock, No Caps (pk300)
010-501-510 Rack for DigiPREP Jr, 100ml
010-501-530 Rack for DigiPREP MS, 100ml
010-501-550 Rack for DigiPREP LS, 100ml

44 KeyPad
SCP SCIENCE
Version 1.0
 *QG
([    0

([    0
1RW8VHG

/    /
([([ 0 0 / /
1RW8VHG

&RQWUROOHU *QG
&RQWUROOHU&RQQHFWRU
      
*1'($57+ 6WUDLQ5HOLHI

57 *URXSHG
*URXSHG
57' %ODFN 5HG
([ ([
W
'LJL352%('RQJOH
ELECTRICAL SCHEMATIC – DigiPREP

0 0
5HG :KLWH  




SCP SCIENCE
'LJL352%(&RQQHFWRU    

5HG
DIGIPREP HTJr, MS, LS, HP

(;
(; %ODFN
0 5HG
0 %ODFN
(DUWK*URXQG
%ODFN
7R0HWDO6XSSRUW3ODWH *UDSKLWH%ORFN 5HG

7+(50$/6ZLWFK#&-506+3/6
6WUDLQ5HOLHI

Notes:
127(6
*LS Heater 230 VAC 50/60 HZ 2655W
W
,QWHUQDO57' selector switch for LS models
** No voltage /6+HDWHU9$&+=:
*** DigiPROBE Dongle is used only when no DigiPROBE is connected
1R9ROWDJH6HOHFWRU6ZLWFKIRU/6PRGHO
9DF9ROWDJH6HOHFWRU6ZLWFK

Version 1.0
KeyPad
'LJL352%('RQJOHLVXVHGRQO\ZKHQQR'LJL352

45
SAMPLE DIGESTION SYSTEMS

DigiPREP HT
Instruction Manual

www.scpscience.com

Providing Innovative Solutions to Analytical Chemists

INTRODUCTION
DigiPREP HT is a high temperature digestion block capable of heating to 450oC. DigiPREP HT
is available in four styles; DigiPREP HT 250 with 10 or 20 positions which are used with 250ml
digestion tubes; DigiPREP HT 100 with 10 or 40 positions which are used with 100ml tubes.
Digestion tubes are also available calibrated. They may be made of borosilicate glass or made of quartz. The
assembly, installation and operation of each of these blocks is quite similar; the main difference is the number
and volume of digestion tubes they hold.

The heating cycle is controlled by a Colour Touch Screen or KeyPad controller. One should refer to the
controller manual for the correct setup and its operations. It is important that the controller be set to the 'HT' block
setting from the 'UTILITIES' screen of the controller in use. This will ensure optimal heating control of the
block.

DigiPREP HT typically comes with a manifold, insert rack, and related accessories for performing high
temperature digestions (up to 4500C). The SiC coated graphite block,and Teflon coated components, are
meant to handle the harsh environment of the laboratory. The system should provide many years of continued
service with minimal maintenance.

It is understood that the operator of this equipment is qualified to do so. If training is required please contact
your local distributer or the main office of SCP SCIENCE.

KeyPad 47
SCP SCIENCE
Version 1.0
 CAUTIONS AND NOTES WARRANTY
Cautions, warnings, and notes are included SCP SCIENCE warrants this product free
throughoutthis manual. from defect in workmanship and materials
for one (1) year from date of purchase.
CAUTION
A caution is used to emphasize information
• Should the unit malfunction, call SCP
pertaining to procedures that, if not
SCIENCES's service department (see page
CAUTION strictly followed, may result in damage
92), or your local distributor. and a service
or destruction to the instrument or
representative will instruct you on how to
improper instrument operation.
proceed.
WARNING
• There are no user-serviceable parts in this unit.
A warning is used to emphasize information
The warranty is void if the unit shows evidence
about dangerous or hazardous conditions
of being tampered with, of being subjected to
WARNING relating to the operation, cleaning, or
excessive moisture, heat or corrosion, or of other
maintenance of the instrument that may
misuse.
result in personal injury.
• SCP SCIENCE shall not be responsible for
NOTE
any damage or losses however caused which
A note is used to emphasize procedures
may be experienced as a result of the installation
NOTE or conditions that may be misinterpreted
or use of this product.
or overlooked, and to clarify potentially
confusing situations.
• This product is not warranted for, nor has it
been tested for, use with perchloric acid.
The user accepts all responsibility if this product
is used with perchloric acid.

• The controller must be placed outside the fume

hood.
Symbol Description Symbol Description

V Voltage l Mains on

~ Alternating current 0 Mains off

Attention, consult
A Current accompanying documents

Hz Frequency Caution, hot surfaces

Protective conductor terminal

F Fast-acting fuse

48 KeyPad
SCP SCIENCE
Version 1.0
OPERATIONAL PRECAUTIONS SAFETY INFORMATION
DigiPREP HT must be grounded. In the event A minimum of safety considerations must be
of an electrical short circuit, grounding reduces the followed when working with the DigiPREP HT in
risk of electrical shock by providing an escape wire order to maintain good laboratory practice:
for electrical current. DigiPREP HT is supplied with
an umbilical cord that has a ground wire that is • Do not place the DigiPREP HT on a surface
connected through the controller to earth ground. containing flammable material.
Ensure that the plug is plugged into an outlet that
has been properly installed and grounded. Consult • DigiPREP HT requires a clearance of 3 inches
a qualified electrician if there is any doubt about the on all sides.
existence of proper grounding at the outlet.
• DigiPREP HT must be operated in a fume hood.
DigiPREP HT is designed to be lifted from
the bottom only. Ensure that the controller is • Do not place the DigiPREP controller in a fume
disconnected prior to moving the system. Do not at- hood.
tempt to lift the system by the top white trim or the ‘U’
channel as damage may result. • DigiPREP HT is connected to a DigiPREP
controller.
DigiPREP HT is an elevated-temperature
digestion system with exposed hot surfaces. Be • DigiPREP HT requires 230V ± 10% three-prong
careful around the instrument when it is in operation. grounded outlet.

DigiPREP HT digestion block should be

operated in a fully functional fume hood.

KeyPad 49
SCP SCIENCE
Version 1.0
 DigiPREP HT BLOCK DESCRIPTION

1
5 8

6
7
3
Boiling Rods
Heat Shield (optional) (pack of 40)

1. Exhaust manifold module 5. Drip Tray

2. Dual-zone Tube Rack 6. Thumb Screws (6)
3. Umbilical cable (to connect to controller) 7. Dual PROBE Connection (option)
4. Digestion Tubes 8. Glass Water Jet

Unpacking
Optional items, such as glass,
Retain all packing material in case you quartz, calibrated or non-calibrated
NOTE need to return the instrument to the digestion tubes may have been
manufacturer for service. included in the shipment. Carefully
NOTE check the packing list(s) and the
1. Verify that all components listed have been contents of shipping cartons to
included: verify that all items listed are included.
Please notify SCP SCIENCE or
• DigiPREP HT system your local distributor of any
• Operation manual discrepancies.
• Exhaust Manifold
• Dual-Zone Tube Rack Inspect the products for any shipping damage.
• Rack and Manifold support If the instrument has been damaged in shipping,
• Thumb screws (6pc) contact the freight carrier to report damage and
• Drip tray to file a damage report. Also contact the SCP
• Exhaust connection hose SCIENCE service department to report damage
• Water Jet and to request service information (see page 88 for
• Boiling Rods contact information).

WARNING If damage is noted, do not attempt to

operate the instrument.

50 KeyPad
SCP SCIENCE
Version 1.0
ASSEMBLY
Assemble the DigiPREP HT system following the step listed below.

Set the block proportion of the DigiPREP HT with

the back sitting towards the front edge of a lab bench.

Insert the aluminum ‘U’ support into the 2 square

holes found in the top white ring, with thread holes facing
towards back

Insert and tighten two thumb screws through the

skin, and into the thread holes of the aluminum ‘U’
support.

Insert the right and left rack support panels. The short
90 degree bend goes toward the back of the system.
The cut outs should be placed facing up as shown in
the picture. Use 2 thumb screws to hold each of the
panels in place.

KeyPad 51
SCP SCIENCE
Version 1.0
 The Dual-Zone Tube Rack may be placed on the system. The first
set of cut outs is to support the Dual-Zone Tube Rack when it is in
the cooling position. The second set supports the Exhaust Manifold
module. The manifold may be placed on the top two upper cut outs;
this is the resting place of the manifold when not in use.

The drip tray is shown in place. It may be stored on top of the Teflon
manifold when not in use.

Connect the black tubing to the Teflon drain tubes of each of the
manifold drains from the top part of the ‘Y’ connectors.

The long black tubing is connected to the bottom of the last ‘Y’
connector. One ‘Y’ is supplied for the HT 250-20 and 3 ‘Y’ are
supplied for the HT 100-40 position. (As shown in picture). The HT
100-10 and HT 250-10 position Teflon manifolds are connected
directly to the black exhaust tubing . The Teflon manifold may
have 1, 2, or 4 drain tube connections. The end of the long black
drain tube connects to the water jet (supplied with system) or the
Universal Fume Scrubber (UFS option)

DigiPREP HT system may now be placed in the fume hood.

The picture shown on the left shows a typical digestion set up, the insert
rack with digestion tubes in place, lowered onto the graphite heating block,
the Teflon manifold has been lowered onto the tubes, the exhaust tube is
connected to a vacuum system for the removal of the unwanted fumes.

52 KeyPad
SCP SCIENCE
Version 1.0
 Next, ensure that DigiPREP controller is set temperature. The second RTD PROBE is connected
to the correct settings for controlling DigiPREP to the 2 pin connector on the back of the DigiPREP
block in use. (HT for all of DigiPREP HT high HT system to allow for the monitoring of
temperature digestion blocks) With the controller’s the precision of block controller display temperature.
power switch in the “off” position, verify the following: (Or the correct size hole may be made to house the
panel mount connector for field installation). The 2 pin
• Voltage selector switch on the back of the female connector on the back of the DigiPREP HT
controller is properly set to 230 volts.(The Colour system is supplied with a mating cable with
Touch Screen & KeyPad do not have a voltage two bare ends. This cable is to facilitate the
selector connection of the second PROBE sensor to an
) instrument capable of reading a 100 RTD. If
• Connect the blocks umbilical cord to the an Ohm meter is being used, the typical value at
controller. 100°C is 138.5, and for 380°C the resistance
value is 240.13 (see table page 61.) It is
Disconnecting or reconnecting the recommended to use a certified controller capable
umbilical cable while the controller is of measuring a temperature from 100 ohms platinum
WARNING turned on, especially while it is RTD. (0.00385 factor)
on the RUN screen, will likely result The tolerance of the temperature PROBEs used
in permanent damage to the on the DigiPREP HT systems is of a ‘Class A’
instrument. specifications. A typical variation at 100°C is ±
0.15°C and at 400°C is ± 0.95oC.

• Connect the power cord to the back of the

controller. Parts for the Dual PROBE Option (field installation)
complete with mating cable.
• Connect the DigiSET dongle to the back of
thecontroller.

DigiSET is not typically used with

NOTE
the DigiPREP HT Digestion blocks.
The system is now ready to be
plugged in and turned on. Consult Mating Cable
the controller manual for
programming and operation Field installation kit
instructions.

DUAL PROBE OPTION

The dual PROBE may be retrofitted in the field
or may have come factory installed. This option
allows the lab to verify the DigiPREP HT block
temperature independently of the DigiPREP
Controller used. The dual PROBE contains two
separate RTDs in one sheath; one sensor is
connected through the umbilical cord to the
DigiPREP controller to monitor and control the block

KeyPad 53
SCP SCIENCE
Version 1.0
 HEAT DEFLECTOR ASSEMBLY

1) If evaporation times are too long, Heat

Deflector shields may be installed (option
product number 010-520-032) They push
into place as shown in the following
instructions.

2) Install heat deflector as shown. Lips on

side & bottom.

3) Push heat deflector in and flush at bottom.

4) Use fingers to push top snug to lip on

Dual-Zone insert rack.

5) Place fingers through holes in top of rack to

reach heat deflector.

54 KeyPad
SCP SCIENCE
Version 1.0
REFERENCE DATA
RTD Resistance vs. temperature tables for IEC 60751 100 Ohm Platinum RTDs with temperature Coef-
ficient of 0.00385-Ref. 54
(°C) 0 1 2 3 4 5 6 7 8 9
(0) 100.00 100.39 100.78 101.17 101.56 101.95 102.34 102.73 103.12 103.51
(10) 103.90 104.29 104.68 105.07 105.46 105.85 106.24 106.63 107.02 107.40
(20) 107.79 108.18 108.57 108.96 109.35 109.73 110.12 110.51 110.90 111.28
(30) 111.67 112.06 112.45 112.83 113.22 113.61 113.99 114.38 114.77 115.15
(40) 115.54 115.93 116.31 116.70 117.08 117.47 117.85 118.24 118.62 119.01
(50) 119.40 119.78 120.16 120.55 120.93 121.32 121.70 122.09 122.47 122.86
(60) 123.24 123.62 124.01 124.39 124.77 125.16 125.54 125.92 126.31 126.69
(70) 127.07 127.45 127.84 128.22 128.60 128.98 129.37 129.75 130.13 130.51
(80) 130.89 131.27 131.66 132.04 132.42 132.80 133.18 133.56 133.94 134.32
(90) 134.70 135.08 135.46 135.84 136.22 136.60 136.98 137.36 137.74 138.12
(100) 138.50 138.88 139.26 139.64 140.02 140.39 140.77 141.15 141.53 141.91
(110) 142.29 142.66 143.04 143.42 143.80 144.17 144.55 144.93 145.31 145.68
(120) 146.06 146.44 147.19 147.57 147.94 148.32 148.32 148.70 149.07 149.45
(130) 149.82 150.20 150.57 150.95 151.33 151.70 152.08 152.45 152.83 153.20
(140) 153.58 153.95 154.32 154.70 155.07 155.45 155.82 156.19 156.57 156.94
(150) 157.31 157.69 158.06 158.43 158.81 159.19 159.55 159.93 160.30 160.67
(160) 161.04 161.42 161.79 162.16 162.53 162.90 163.27 163.65 164.02 164.39
(170) 164.76 165.13 165.50 165.87 166.24 166.61 166.98 167.35 167.72 168.09
(180) 168.46 168.83 169.20 169.57 169.94 170.31 170.68 171.05 171.42 171.79
(190) 172.16 172.53 172.90 173.26 173.63 174.00 174.37 174.74 175.10 175.47
(200) 175.84 176.21 176.57 176.94 177.31 177.68 178.04 178.41 178.78 179.14
(210) 179.51 179.88 180.24 180.61 180.94 181.34 181.71 182.07 182.44 182.80
(220) 183.17 183.53 183.90 184.26 184.63 184.99 185.36 185.72 186.09 186.45
(230) 186.82 187.18 187.54 187.91 188.28 188.63 189.00 189.36 189.72 190.09
(240) 190.45 190.81 191.18 191.54 191.90 192.26 192.63 192.99 193.35 193.71
(250) 194.07 194.44 194.80 192.16 192.52 195.88 196.24 196.60 196.96 197.33
(260) 197.69 198.05 198.41 198.77 199.13 199.49 199.95 200.21 200.57 200.93
(270) 201.29 201.65 202.01 202.36 202.72 203.09 203.44 203.80 204.16 204.52
(280) 204.88 205.23 205.59 205.95 206.31 206.67 207.02 207.38 207.74 208.10
(290) 208.45 208.81 209.17 209.52 209.88 210.24 210.59 210.98 211.31 211.66
(300) 212.02 212.37 212.73 213.09 213.44 213.80 214.15 214.51 214.86 215.22
(310) 215.57 215.93 216.28 216.64 216.99 217.35 217.70 218.05 218.41 218.76
(320) 219.12 219.47 219.82 220.18 220.53 220.88 221.24 221.59 221.94 222.29
(330) 222.65 223.00 223.35 223.70 224.06 224.41 224.76 225.11 225.46 225.81
(340) 226.17 226.52 226.87 227.22 227.57 227.92 228.27 228.62 228.97 229.32
(350) 229.67 230.02 230.37 230.72 231.07 231.42 231.77 232.12 232.47 232.82
(360) 233.17 233.52 233.87 234.22 234.56 234.91 235.26 235.61 235.96 236.31
(370) 236.65 237.00 237.35 237.70 238.04 238.39 238.74 239.09 239.43 239.78
(380) 240.13 240.47 240.82 241.17 241.51 241.86 242.20 242.55 242.90 243.24
(390) 243.59 243.93 244.28 244.62 244.97 245.31 245.66 246.00 246.35 246.69

KeyPad 55
SCP SCIENCE
Version 1.0
 TYPICAL HEATING RATES FOR DigiPREP HT

1st Step 2nd Step

When programming the first 'time to temperature' When programming the additional ramp and
and the 'time at temperature' cycle, it is assumed that soak cycles, the Time to Temperature will depend
the DigiPREP HT will begin the cycle from ambient on the last temperature reached – i.e. the previous
temperature. To enter the 'Time to Temperature' for setpoint. This becomes more complex, as the
the first step is a simple matter of using the graph heating rates for the DigiPREP HT depend on
below. both the Setpoint temperature and the ΔT. Two
equations are needed:
Example: Equation 1: ΔT = Tfinal – Tinitial
Heat a DigiPREP HT block from 25oC (ambient) Equation 2: Time to Temperature = ΔT / rate
to 300oC.
HT Typical Heating Rates (°C/min) vs
Solution: Setpoint temperature and ΔT
From the graph, draw a line from 300oC across Δ T (°C) Setpoint Temperature
to the curve representing the voltage that the 25-50 50-225 225-350 350 +
DigiPREP HT is connected to. (208 V is typical 0-25 1 3 2 2
in North America, 230 V in typical Europe). Draw
25-200 - 20 min 4 3
a line down from this point to the Time Scale.
Time to Temperature = at least 25 minutes. 200-325 - - 8 4
325-425 - - - 5

HT - Typical Time to Temperature

HT- Typical Time to Temperature
(deg C)

500
450
Temperature (°C)

400
SetpointTemperature

350
300
250
200
150 208 Volts
208 Volts
Setpoint

100 230 Volts

230 Volts
50
0
0 20 40 60 80 100
Time
TimetotoTemperature (minutes)
Temperature (minutes)
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Example: METHOD DEVELOPMENT
On the second ramp and soak cycle, heat the
FOR DIGESTING SAMPLES
DigiPREP HT to 300oC, assuming that the first
Setpoint temperature was 200oC. A typical H2SO4 digestion program is as follows.
Suitable boiling chips or the supplied boiling rods
Solution: should be used to prevent bumping during the
Calculate ΔT. digestion procedure.
ΔT=Tfinal-Tinitial
=second set point - first set point Step 1
=300oC - 200oC=100oC Set point Temperature is 150oC
To determine the rate from the HT Typical Heating Time to Temperature 45 minutes
Rates chart, use the '25 to 200' row because ΔT is Time at Temperature is 60 minutes.
within this range. Use the '225-350' column since Step 2
the second set poitn is 300oC. Set Point Temperature is 380oC
Time to temperature is 45 minutes
The table recommends a heating rate of at least Time at Temperature is 30 minutes
o
4 C/min.
Time to Temperature =ΔT ÷ rate If the sample contains water, the water must be
=100 / 4 = 25 min evaporated off prior to proceeding to Step 2. If this is
Therefore, a minimum of 25 minutes is required. not done then severe bumping may occur.

The amount of vacuum pulled on the manifold

3rd Step should be sufficient to prevent fume from escaping
Example:
from the tube. The incoming air will promote reflux,
On the third ramp and soak cycle, heat the
as this is a necessary step to wash down the walls
DigiPREP HT to 380oC. The second Setpoint of the tubes to ensure complete digestion of the
temperature was 300oC (from the previous example) sample.

Solution: If bumping occures at the set point temperature

Calculate ΔT. then the temperature should be lowered by 5oC.
ΔT=Tfinal-Tinitial If bumping does not occur at set point
=third set point - second set point temperature then the temperature may be raised by
=380oC - 300oC=80oC 5oC to help speed up the rate of evaporation.
To determine the rate from the ‘HT Heating Rates’ The amount of TKN digestion reagent in the sample
chart, use the ‘25 to 200’ row because ΔT will have an impact on the boiling point of the
is within this range. Use the ‘350+’ column sample. Blank samples will not evaporate at the
since the second setpoint is 380oC. same rate as sample with solids.

The table recommends a heating rate of 3oC/min At the end of Step 1 the sample should resemble
Time to Temperature =ΔT ÷ rate a black liquid. It should contain about 10-15% of the
=80 / 3 = 26.6 min volume of the starting sample if it was a liquid sample
to start with.
Therefore, use a 'time to temperature' of 27 minutes.
If the sample is dry at this step. More sulphuric acid
needs to be added to the TKN digestion reagent.

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 Step 2 is the digestion step that completes the Allow the system to cool before proceeding
destruction of organic nitrogen bonds. The solution at further. DigiPREP HT must be disassembled,
the end of this step should be a clear coloured liquid. cleaned,and thoroughly dried prior to running again.
If black spots remain in thesolution then the
digestion time needs to be extended. If the solution in Please consult the service
NOTE
the tube turns to a solid at room temperature more departmentfor help if required.
sulphuric acid needs to be added to the TKN diges-
tion reagent. In order to access under the block, first remove
the exhaust manifold and the insert rack from the
The Dual-Zone tube rack two-tier upright. Then remove the ‘U’ channel and
should be lifted at the end of the white top ring. To do so, remove the two thumb
the digestion step to allow screws from the back of the system that holds the ‘U’
the tubes to cool as shown support with the two side panels connected. Lift the
in the picture (right). ‘U’ channel straight up and set off to the side.
It is not necessary to place
tubes in all positions during To remove the block and inner heater pan, turn
a digestion. the unit upside-down onto a soft surface, a piece
of cardboard is fine to do this on. Remove the four
locking nuts from the bottom of the support pan and
CLEANING lift up on the outer housing. Lift gently as the over
temperature protection device and temperature
If the surface is still hot, contact with sensor are attached to the graphite block through
a liquid may create steam that can the side of the inner heater pan. The RTD probe and
WARNING scald you. It is important to allow the over temperature bulb may be gently removed from
instrument to cool before cleaning. the graphite block. Caution should be exercised so
not to pinch the over temperature gas line. Access
Cleaning of minor surface spills is now available for cleaning the inner pan and other
Turn off the system and unplug the DigiPREP affected areas.
HT from the power source. Allow the system to cool.
Sponge up any excess liquid, dilute the area with The coated block surface may be cleaned with a
clean water, and wipe dry with a paper towel. mixture of 100ml HNO3 and 25ml HF in a litre of DI
water.
Cleaning of digestion wells
Turn off the system and unplug the DigiPREP The Teflon Exhaust manifold may be rinsed with
HT from the power source. Allow the system to cool tap or DI water after each run. Place the manifold,
before proceeding further. tube adapter side down to drain and dry. It is
Suction the solution out of the well with an eye fine to run water through the manifold without
dropper, squeeze bottle, or pipette. Dilute any disassembling for cleaning purposes.
remaining spillage with water, two or three times, and
suction as much solution out as possible. Sponge
the remaining residue with a paper towel. Allow the
system to dry completely before powering up.

Cleaning of a major spill

If a solution has run down around and below
the graphite digestion block, turn off the system
and unplug DigiPREP HT from the power source.

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SPECIFICATIONS DigiPREP HT
ENVIRONMENTAL ELECTRICAL
Relative humidity 30% to 80% Model DigiPREP HT
Altitude Up to 200m Voltage 230V ±5%
Installation Category ll Power 3362W 40 and 20 posi-
Pollution Degree 2 tion
Ambient operating -5°C to 40°C Power 3000W / 10 position
temp. Internal thermal fuse Manual reset above
450°C
Frequency 50/60 Hz
Ambient operating Ambient to 450°C
temp.

The main supply cord is constructed Line voltage fluctuations greater

NOTE
NOTE of heat-resistant material and should than 10% will affect instrument
only be replaced by an equivalent or performance.
better cord.

RoHs

Toxic or hazardous substances and elements

Mer- Hexavalent Polybrominat- Polybrominated
Lead Cadmium Chromium
Part name cury ed Biphenyle Diphenyl Ether
(Pb) (Cd)
(Hg) (Cr6+) (PBB) (PBDE)
Housing o o o o o o
SiC Block o o o o o o
RTD probe o o o o o o
Over temperature
o o o o o o
sensor

O: Indicates that the toxic or hazardous substance X: Indicates that the toxic or hazardous substance
contained in all the homogenous materials for this contained in all the homogenous materials for this
part, according to EIP-A, EIP-B, EIP-C, is below the part, according to EIP-A, EIP-B, EIP-C, is above the
limit requirement in SJ/T11363-2006. limit requirement in SJ/T11363-2006.

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 ACCESSORIES and OPTIONS
DigiPREP HT 100 10 OR 40 POSITION

Catalogue Number Description

010-520-010 DigiPREP HT 100-40 Teflon coated Insert Rack
010-520-011 Digestion tubes (100 ml), borosilicate uncalibrated
010-520-032 Heat Deflector for HT Insert Rack
010-520-039 Cooling Finger for HT 100 600mm long
010-520-085 Digestion tube Quartz uncalibrated
010-520-111 Digestion Tube, Calibrated at 25ml and 50ml
010-520-115 Digestion Tube, Calibrated at 25ml and 75 ml
010-520-211 Insert Rack HT100-10, Teflon Coated
010-520-215 Manifold HT 100-10 position
010-520-310 Dual Probe for HT field installable
010-520-318 DigiPREP HT Ball-Glass Condensor for 100ml Digestion Tubes
010-520-322 DigiPREP Quartz Ball Condensor for 100ml Digestion tubes

DigiPREP HT 250 10 OR 20 POSITION

Catalogue Number Description
010-520-030 DigiPREP HT 250 Teflon coated Insert Rack
010-520-031 Digestion Tube, borosilicate uncalibrated
010-520-032 Heat Deflector for DigiPREP HT Insert Rack
010-520-087 Digestion Tube, Quartz, uncalibrated
010-520-131 DigestionTube, Calibrated at 50ml and 100ml
010-520-133 Digestion tube, borosilicate Calibrated at 25ml and 50ml
010-520-250 Exhaust Manifold Rack, DigiPREP HT 250-20 position
010-520-253 Exhaust Mainfold, DigiPREP HT 250-10 position
010-520-312 DigiPREP HT 250 Ball Glass Condensor
010-520-316 Cooling Finger for DigiPREP HT 250 (100mm long) for use with 010-520-320
010-520-320 DigiPREP HT Digestion tube, 250ml, with Socket Joint Tube

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ELECTRICAL SCHEMATIC – DigiPREP HT

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 DigiPREP JR BLOCK DESCRIPTION

1. DigiPROBE Connector-Connection port sample volume is reached. DigiSET

for DigiPROBE. DigiPROBE will allow dongle must be installed to run DigiPREP
direct monitoring and control based on Jr without the DigiSET option.
actual sample temperature. DigiPROBE
Dongle must be installed to run the 5. DigiPREP Controller – DigiPREP Jr is
DigiPREP Jr without the DigiPROBE designed to be used with DigiPREP
option. KeyPad* or Touch Screen* controller
(*Sold separately)
2. Cable Connector – Connection port for the
DigiPREP Jr umbilical cable to the 6. DigiPROBE (Option) – To monitor and
controller. control sample or block temperature.

3. Power Switch/ Power Cord Receptacle – 7. DigiPROBE Storage Well – Use with
On/Off switch – contains circuit breaker replaceable glass liner.
and receives the female end of the power
cord. 8. Voltage Selector Switch - Select appropriate
voltage. If 115 V is showing, system is
4. DigiSET Connector – Connection port running at 115 volts.
for DigiSET. DigiSET will automatically
shut off the digestion block when a pre-set

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DigiPREP SPARE PARTS LIST
1
6
DigiPREP JR(010-505-205)

1. P200 CPVC Corian top support

2. C403 Label: DigiPREP Jr 2 5

3. C401 Label: SCP SCIENCE

3
4. S129 Housing for DigiPREP Jr

5. M113 Screw for CPVC Corian top support

6. S104 Harness, umbilical cord (Jr, HP, MS, HT) 4

BOTTOM OF DigiPREP JR
2
6
1. M180 Screws to secure feet (all DigiPREP
systems)

2. M173 Rubber feet (all DigiPREP systems) 5

3. C584 Label: DigiPROBE 1 4

4. E346 RTD panel connector

5. S104 Harness, umbilical cord (Jr, HP, MS, HT)

6. M109 Teflon hole plugs 3

1
TOP VIEW: EXPOSED
3
1. P200 CPVC Corian top support

2. C176 RTD 4
2
3. S129 Housing for Jr unit 5

4. E346 RTD panel connector

5. S104 Harness, umbilical cord (Jr, HP, MS, HT)

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 SIDE VIEW: EXPOSED

1. W137 Old-style thermal switch 180C

2. E239 Voltage selector switch

3. E353 Heater pad

4. G103 Graphite block (coated)

5. C176 RTD thermal sensor

6. J111 Insulation, Jr, 10-pc. set

Other miscellaneous parts

A352 Aluminium plate-Secures bottom insulation

C161 Hot label for Corian top-possible hot sur-

faces
1
P340 White Corian top 2

S121 HEATER HARNESS JR

3
1 E353 Heater 115V/230V 48” Lead UL (Jr)

2 E106 Thermal protection relay

3 E239 Voltage selector 4

4 P149 Teflon tape 0.003 x 7.5 x 11

5 G103 Graphite block grade HLM (Jr), coated

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DigiPREP MS BLOCK DESCRIPTION

1. DigiPROBE Connector – Connection port shut off the digestion block when a
for DigiPROBE. DigiPROBE will allow pre-set sample volume is reached.
direct monitoring and control based on DigiSET dongle must be installed to run
actual sample temperature. DigiPROBE DigiPREP MS without the DigiSET
Dongle must be installed to run the option.
DigiPREP MS without the DigiPROBE
option. 5. DigiPREP Controller – DigiPREP MS is
designed to be used with DigiPREP
2. Cable Connector – Connection port for KeyPad* or Touch Screen* controller
the DigiPREP MS umbilical cable to (*Sold separately).
controller.
6. DigiPROBE well – Use with replaceable
3. Power Switch/ Power Cord Receptacle – glass liner.
On/Off switch – contains circuit breaker
and receives the female end of the power 7. Voltage Selector Switch-Select appropriate
cord. voltage. If 115 V is showing, system is
running at 115 volts.
4. DigiSET Connector – Connection port
for DigiSET. DigiSET will automatically

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 DigiPREP MS (010-500-205)
1
6
1 P200 CPVC Corian top support

2 C632 Label: DigiPREP MS

2 5
3 C401 Label: SCP SCIENCE
3
4 S124 Housing for DigiPREP MS

5 M113 Screw for CPVC Corian top support

6 S104 Harness, umbilical cord (Jr, HP, MS, HT)

4
BOTTOM OF DigiPREP MS
2
1 M180 Screws to secure feet (all DigiPREP 6
systems)

2 M173 Rubber feet (all DigiPREP systems)

5
3 C584 Label: DigiPROBE
1 4
4 E346 RTD panel connector

5 S104 Harness, umbilical cord (Jr, HP, MS, HT)

6 M109 Teflon hole plugs

3
Other miscellaneous parts (MS)

A191 Aluminium plate Secures bottom insulation

C161 Hot label for Corian top Informs users of

possible hot surfaces

P149 White Corian top Fits MS, HP, classic

DigiPREP systems

J112 Insulation set Insulates the heating block

C176 RTD Returns temperature signals

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S125 HEATER HARNESS (MS, HP) 1
1 E391 Heater 115V/230V (MS, Classic, HP)
2

2 E106 Thermal protection relay

3 E239 Voltage selector 3

4 P147 Teflon tape 0.003 x 13.25 x 17.25

5 G102 Graphite block grade HLM (MS), coated 4

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 DigiPREP HP BLOCK DESCRIPTION

1. DigiPROBE Connector – Connection port shut off the digestion block when a
for DigiPROBE. DigiPROBE will allow pre-set sample volume is reached.
direct monitoring and control based on DigiSET dongle must be installed to run
actual sample temperature. DigiPROBE DigiPREP MS without the DigiSET
Dongle must be installed to run the option.
DigiPREP MS without the DigiPROBE
option. 5. DigiPREP Controller – DigiPREP MS is
designed to be used with DigiPREP
2. Cable Connector – Connection port for KeyPad* or Touch Screen* controller
the DigiPREP MS umbilical cable to (*Sold separately).
controller.
6. DigiPROBE well – Use with replaceable
3. Power Switch/ Power Cord Receptacle – glass liner.
On/Off switch – contains circuit breaker
and receives the female end of the power 7. Voltage Selector Switch-Select appropriate
cord. voltage. If 115 V is showing, system is
running at 115 volts.
4. DigiSET Connector – Connection port
for DigiSET. DigiSET will automatically

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DigiPREP HT BLOCK DESCRIPTION

1. Exhaust Manifold Module. Old format DigiBLOCK umbilical

cords are only 7 pins. The footprint
2. Dual Zone Tube Rack NOTE size is approximately the same as
that of a DigiPREP Dongle. If the
3. DigiPREP Controller – DigiPREP HT is instrument has 9 pins on the umbilical
designed to be used with DigiPREP cord, please refer to figure
Touch Screen* or KeyPad* controller
(*Sold separately)

4. Umbilical Cable – to connect to controller.

5. Glass Digestion Tubes – 40 / 100 ml

glass tubes or 20 / 250 ml glass tubes
are included with the DigiPREP HT.

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 1
DigiPREP HT (010-500-205)

1 C582 Thermostat – Panel Mounted

Other Miscellaneous Parts

C560 RTD Sensor HT RTD Sensor 90

degree bend

E667 Heater for HT Used in both 100 and

250 models

G502 Graphite Block 250ml HT only

G501 Graphite Block 100ml HT only

P616 White Corian Top Fits both 250 and

100 HT models

S127 House for HT Used in both 250 and

100 HT models

C398 DigiPREP HT Label for front of

instrument

S128 Heater pan Assembly Used in both

250 and 100 HT models

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DigiPREP LS SPARE PARTS LIST

C176 RTD Returns temperature signals G108 Graphite LS block coated Teflon coated
LS block
C630 Label, DigiPREP LS Attached to front
of instrument M180 Screws to Secure Feet All blocks
except COD
P200 Corian Ring Support All DigiPREPs
M173 Rubber feet for all blocks
M113 Screw-Corian Ring Support All Corian All blocks exceptCOD
Ring supports
E357 Heater 220V Heater for DigiPREP LS
P249 Corian Ring For LS unit only
J123 Insulation Set LS Only
E550 Power Cord Switch 15A Switch and
line filter combo A106 Aluminum Plate, LS Only

S183 Umbilical Harness All DigiBLOCK E346 RTD Panel Connector Dongle port, all
Models DigiPREP blocks

E106 Thermo Protection Relay Protects from P192 Teflon Tape Fits only on LS blocks
over temperature

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 SPARE PART LIST

SCP SCP
PART DESCRIPTION MANUFACTURER # PART DESCRIPTION MANUFACTURER #
PART # PART #
E600 Buzzer CCG-1206 E174 Resistor, 47 , 1/4 W CFR-25JB-47R
E190 Capacitor, 470 pF A471K15X7RH5TAA Exxx Trimpot, 5 K , 1/2 W PV36W501C01B00
E191 Capacitor, 2770 uF, 35V ELXY350ELL272ML40S E608 Resistor, 360 , 1/2 W CFR-50JB-360R
Exxx Capacitor, 470 uF, 10V UVR1A471MED E609 Resistor, 75 , 1/2 W CFR-50JB-75R
E186 Capacitor, 10nF, 1KV 5GAS10 TRIAC 600V 25A to
E611 BTA24-600BW
220AB
E189 Capacitor, 470 pF ECK-DNA471MB
Transformer, 28V A @1-
E601 Capacitor, 100 pF ECK-ANA101MB E199 CSM 2010-083
-kHz, 4KV
E145 Capacitor, 47 nF 2222 338 14473
Optocoupler, DIP,
E204 H11A817A
E184 Capacitor, 10 uF, 450V UVZ2W100MHD 70V/50mA, 5Kv
E185 Capacitor, 22 uF, 450V UVZW220MHD IC Switcher Off-line,
E198 TNY268P
E188 Capacitor, 10uf, 50V UVZ1H100MDD 8DIP, 700V

E603 Schottky diode MBR360RL Reference regulator, TO-

E197 LM431LP
92. adjustable, 2.5V-36V
E604 Diode, 200V, 600W P6KE200ARL
Regulator LDO 3.3V to
E194 Diode, 1000V, 1A 1N4007G-T E631 LM3940IT-3.3
220
Fuse, 0.75A, 250V, fast IC Reg Pos 100MA 3.3V
E337 313.750HXP Exxx L78L33ACZ
blow, 1/4 x 1 1/4 to 92
E209 Fuse, 15A/250 fast blow BK/ABC-15-R Optocoupler High Volt-
E612 MOC3163M
E902 Housing 3-pin W/R 22-01-2037 age
Exxx Housing 8-pin, 1.25mm 51021-0800 E769 Fan, 5Vdc/0.19A CR0405HB-G70
Inductor, 1500 uH, High Switchdraft Panel Mt. 2
E201 4590R-155K E225 EN3P2M
current Pin Male
E203 Inductor, 3.3 uH, radial RL622-3R3K-RC Switchcraft Cord, 2 Pin
E226 EN3C2F
Female
Inductor, 25 mH min.,
E607 BU16-2530R7BL
120 K  @ 200KHz Exxx 5.7" Display Module 51-0001-03
E175 Resistor, 33  CFR-25JB-33R 010-505-052
DigiSET Dongle
(4 Pin male)
E311 Resistor, 4.7K  CFR-12JB-4K7
DigiPROBE
E176 Resistor, 100 , 1/2W CFR-50JB-100R 010-500-051
(2 Pin Male)

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HEATER VERIFICATION

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 DigiPREP DISMANTLING PROCEDURES 2. Insert the key into one of the slots located
beside the rubber feet.
This section deals with dismantling the unit to
gain access to the components inside. There have
been several electrical revisions to the DigiPREP
systems. If you do not find instructions for your model,
continue reading.

REMOVING THE CORIAN RING

1. Turn the DigiPREP Block on its side to obtain

the key

3. Push the aluminium T into the slot until the

Corian ring begins to lift.

• If you find an aluminium T: Continue to step

2.

• If you don’t find an Aluminium T: The Corian

ring is designed to lift off the top of the
instrument manually. Pull up gently on each
corner until the top lifts off, and continue to
'Removing the graphite block'.
4. Repeat process for the three remaining clips,
and return the aluminium key to the base of the
unit.

If you are missing your aluminium

NOTE key, a substitution such as a flat
head screwdriver will also work.

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REMOVING THE GRAPHITE BLOCK 3. Gently lift the Kydex skin from the graphite block.
Unscrew the voltage selector switch so that you
Please ensure you have removed the have more freedom of movement when performing
Corian ring before removing the maintenance on the block.
block.

1. Flip the unit upside-down on a soft surface and

remove the 4 black caps.

DigiPREP TESTS AND REPLACEMENT

PROCEDURES
2. Using a 3/16-inch (4.5mm) Hex key, remove
the 4 screws and washers that secure the VOLTAGE SELECTOR SWITCH, E239
graphite block to the instrument housing.

The voltage selector switch has 6 connections:

1, 1a, 1b, 2, 2a, and 2b.

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 The following table shows what each terminal OVER-TEMPERATURE PROTECTION DEVICES
connects to:

Red Wire: Connects to pin 9 on the umbilical

1
cord
White wire: Connects to neutral of the heater
1a
pad
Parallel Connection: Between jumper from 2a
1b and black heater wire (live)

Parallel Connection: Black heater wire (live)

2 and over-temperature protection switch
Jumper from 2a to 1b and Black heater wire
2a
(live)
2b No connection E106 – New format
Instruments with the E106 installed are serial
numbers JR46040231 forward, MS46040120
forward, and HP03050060 forward, and all LS
blocks.

How to replace an E106

The E106 is mounted onto the side of the block
with two Phillips-head screws. There is no polarity to
this device—simply connect one end to the wire that
runs to pin 2 of the voltage selector switch, and the
other end to the wire that runs to pin 7 of the umbilical
cord.
W137 – Old format

Instruments with the W137 installed are serial

numbers JR46040231 and earlier, MS46040120
and earlier, and HP03050060 and earlier. No LS
blocks have this device installed.

How to replace a W137

The W137 is a cylindrical device that inserts into
the block itself. This model does not have quick
disconnects and must be soldered and isolated with
shrink wrap tubing to ensure a secure connection.
Like the E106, there is no polarity to this device—
simply connect one end to the wire that runs to pin 2
of the voltage selector switch, and the other side to
pin 7 of the umbilical cord

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To verify the over temperature protection switch 6. Measure between pin 7 (L) and pin 9 (N). This
is closed, measure between pin 7 and pin 9: this should return a resistance based on the following
should return a resistance based on the resistance table:
of the heater mat (see table on page 88).
VOLTAGE SELECTOR
MODEL RESISTANCE
SWITCH POSITION
UMBILICAL CORDS, S104 115V 18 ± 2
DigiPREP Jr
230V 71 ± 2
The S104 umbilical harness is the power, and
communication medium between the block and 115V 15 ± 2
DigiPREP MS
the controller. There are two formats of umbilical 230V 57 ± 2
cords: the new version includes Jr blocks with 115V 15 ± 2
DigiPREP HP
s/n JR640404137 forward, HP Blocks with 230V 57 ± 2
s/n 9241030022 forward, MS blocks with s/n 20 ± 2
MS45030019 forward, and any LS block. Any DigiPREP LS 230V
previous serial numbers have the old format umbilical
DigiPREP HT 230V 16 ± 2
harness.
7. Measure between pin 6 on the umbilical cord
New-style umbilical harness tests
(M+/EX+) and pin 1 of the dongle port. This
should return continuity.

8. Measure between pin 3 on the umbilical cord

(M-/EX-) and pin 3 of the dongle port.
This should return continuity.

Old-style umbilical harness tests

Instruments with the old-style umbilical harness

are for Junior blocks with s/n JR640404136 and
earlier, HP blocks with s/n 9241030021 and earlier,
and MS blocks with s/n MS45030019 and earlier.
Please note this style is discontinued and can no
longer be purchased. All LS blocks have the new
1. Place the multi-meter on the continuity setting.
form of umbilical cord.
2. Measure between pin 2 and the graphite block.
This should return continuity. Ensure you pick a
spot that is not covered with Teflon.

3. Measure between pin 2 (ground) and each pin

individually. No pins should return continuity.

4. Measure between pin 4 (EX+) and pin 6 (M+).

This should return continuity.

5. Measure between pin 1 (EX-) and pin 3 (M-).

This should return continuity.
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 1. Set your multi-meter to continuity. between pin 6 and pin 5 of the umbilical cord.
If you cannot read a resistance, visually inspect the
2. Measure between pin 4 (ground) and the wires running from the DigiPREP dongle port to the
graphite block. This should return continuity. RTD, as well as the wires from the port to the umbili-
Ensure you measure in a location that is not cal cord.
covered with Teflon coating.
To determine which style of umbilical
3. Measure between pin 4 (Ground) and each pin NOTE
cord you have, please review the
individually. No continuity should be detected schematics and serial numbers listed
between them. on pages 80 and 81.

4. Measure between pin 1 (EX+) on the umbilical HEATING PAD TESTING PROCEDURES
cord and pin 1 of the dongle port. This should
return continuity. The main methods for testing heater pads for
malfunctions are through resistance checks and
5. Measure between pin 7 (EX-) on the umbilical visual inspections.
cord and pin 3 of the dongle port. This should
return continuity. To measure the resistance of the heater: for new
umbilical cord models, measure between pin 7
6. Measure between pin 6 (M+) on the umbilical and pin 9. For old umbilical cord models, measure
cord and pin 2 of the dongle port. This should between pin 2 and pin 3.
return continuity.
To determine which style of umbilical
7. Measure between pin 5 (M-) on the umbilical cord you have, please review the
NOTE
cord and pin 4 of the dongle port. This should schematics and serial numbers
return continuity. depicted on pages 80 and 81.

8. Measure between pin 2 (N) and 3 (L) on the The following table displays the resistance values
umbilical cord. This should return a resistance of functioning heaters:
based on the table on page 85. VOLTAGE SELECTOR
MODEL RESISTANCE
SWITCH POSITION
INTERNAL RTD, C176
115V 18 ± 2
DigiPREP Jr
230V 71 ± 2
The internal RTD is a variable resistor whose
value changes as a function of temperature. By 115V 15 ± 2
DigiPREP MS
determining the change in resistance, the 230V 57 ± 2
controller’s programming is able to determine the 115V 15 ± 2
temperature of the block to a very accurate degree DigiPREP HP
230V 57 ± 2
(within 0.1 degrees).
DigiPREP LS 230V 20 ± 2
At room temperature, 21 degrees Celsius, the DigiPREP HT 230V 16 ± 2
internal RTD (C178) returns a value of approximately
108 ohms. Resistance of the mat will change
NOTE
depending on the voltage setting.
To measure the value of the internal RTD, insert
the 4-pin DigiPREP dongle into the block’s port.
For new models, measure between pin 1 and pin
4 of the umbilical cord. For older models, measure

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HEATING PAD INSPECTION PROCEDURES

If you notice that the heater mat’s resistance is

higher than normal, it is likely that there is physical
damage done to the heater. The following are
pictures of a defective heater:

The above picture is of damage caused by an

acid spill that has leaked under the graphite block
and eaten away at the heater. Notice the white acid
residue. Damage such as this is not covered under
warranty as it is caused by an acid spill or sample
boil-over.
The above picture is of damage to a heater caused
by a manufacturing defect. When acid causes a
heater malfunction, it typically leaves white residue HEATER REPLACEMENT PROCEDURES
around the burn mark. This burn mark has no acid
residue around it; it is therefore a manufacturing 1. Cut the three heater wires that join the heater
defect. to the voltage selector switch and umbilical
cord.

The above picture is of damage caused by an

acid spill that has leaked under the graphite block
and eaten away at the heater. Notice the white acid
residue. Damage such as this is not covered under
warranty as it is caused by an acid spill or sample
boil-over or not cleaning a major spill promptly.

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 2. Peel the heater off of the graphite block and 5. Place the new heater on the surface of the
ensure there is a Teflon sheet between the Teflon sheet and remove any air bubbles
heater and the graphite block. Check the between the Teflon sheet and the heater
integrity of the Teflon sheet. Clean any by planing a smooth but rigid piece of material
particles off the surface with alcohol. across the surface.

3. Apply silicon sealant to the Teflon sheet. 6. Reconnect the wiring of the new heater to the
wires originally cut in section 1; there is
no polarity to the black wires as they are AC.
Use the following table to connect the correct
colors to the correct locations:

White wire
1a
Connects to neutral of the heater pad
Parallel connection
1b Between jumper from 2a
and black heater wire (live)
Parallel connection
Between black heater wire (live) and
2
over-temperature protection switch
4. Using a smooth but rigid piece of material, spread
the silicon sealant evenly so that a thin layer covers
the surface where the heater will rest. 7. Check the resistance of the heater between
pin 7 and pin 9 to ensure that the heater has
been properly reconnected. Consult the
following table of resistances to ensure the
correct values:

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 SYSTEM FUNCTIONAL WITH DONGLE BUT NOT
VOLTAGE SELECTOR
MODEL RESISTANCE WITH DigiPROBE
SWITCH POSITION
115V 18 ± 2 1. Perform the umbilical cord test on page 85 and
DigiPREP Jr
230V 71 ± 2 ensure pins 2 and 4 are not connected to
115V 15 ± 2 the umbilical cord. This problem is typically
DigiPREP MS
230V 57 ± 2 caused by having the dongle port wired up
115V 15 ± 2 in reverse.
DigiPREP HP
230V 57 ± 2
2. Perform the DigiPROBE test on page 89.
DigiPREP LS 230V 20 ± 2
DigiPREP HT 230V 16 ± 2
HEATER DOES NOT HEAT UP, TEMPERATURE
DISPLAYS BUT DOES NOT CHANGE
DigiPREP DONGLE TESTING PROCEDURES
Ensure the dongle is functioning correctly, by 1. Ensure the umbilical cord is fully inserted into
measuring continuity across pins 3 and 4, and pins 1 the controller.
and 2 of the dongle. If no continuity is detected, the
dongle is defective and must be replaced. 2. Ensure 'COM 2' dongle is installed correctly

3. Ensure the voltage selector switch is properly

DigiPROBE TESTING PROCEDURES positioned.
Measure between pins 1 and 3 of the probe: it
should measure a value of 108 ohms. All other 4. Perform the heater tests on page 86 and if
connections should not return values. problems are found perform the replacement
procedures on page 87.

DigiPREP TROUBLESHOOTING 5. If no problems are found, test the solid-state

relay in the controller.
DigiPROBE ERROR DISPLAYING ON CONTROLLER

1. Perform the dongle test on page 88. HEATER CANNOT ACHIEVE DESIRED TEMPERATURE,
BUT CONTINUOUSLY TRIES TO RAMP
2. Perform the internal RTD test on page 86.
1. Ensure the umbilical cord is fully inserted into
3. Perform the umbilical cord test on page 85. the controller.

4. Verify resistance of the DigiPROBE. 2. Ensure the voltage selector switch is properly
positioned.
5. If problem persists, service on the controller is
needed. 3. Perform the heater tests on page 86. If
problems are found, perform the replacement
procedures on page 87.

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 HEATER CANNOT ACHIEVE DESIRED TEMPERATURE, CONTROLLER TEMPERATURE FLUCTUATES AROUND
STOPS HEATING TOO EARLY AND BEGINS TO COOL SET POINT

1. Ensure the umbilical cord is fully inserted into 1. Ensure the dongle is completely fastened to the
the controller. DigiPREP digestion block.

2. Ensure the dongle port is tight. 2. Visually inspect the dongle receptacle on the
block for damage.
3. Perform the over-temperature protection device
replacement instructions on page 84. 3. Perform the internal RTD test on page 86.

HEATER IS OVERSHOOTING TEMPERATURE BREAKER SWITCH ON CONTROLLER TRIPS ON THE

START OF DIGESTION
1. Ensure the 4-pin dongle is completely fastened
to the DigiPREP digestion block. 1. Perform the over-temperature protection device
replacement instructions on page 84. It is
2. Perform the internal RTD test on page 86. possible for the W137 to short to the block,
which may cause the solid-state relay to
3. Verify the solid-state relay on the controller. become defective.

4. Perform replacement procedures for the

voltage selector switch on page 84.

CONTROLLER TEMPERATURE FLUCTUATES

BETWEEN IMPOSSIBLE VALUES

1. Ensure the dongle is completely fastened to the

DigiPREP digestion block.

2. Visually inspect the dongle receptacle on the

block for damage.

3. Perform the internal RTD test on page 86.

4. Perform umbilical cord tests on page 85.

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 NOTES

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 SERVICE DEPARTMENT

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Tel: 1-800-361-6820 (Toll free)

Fax: 1-800-253-5549 (Toll free)

Outside North America

Tel: +1 (514) 457-0701

Fax: +1 (514) 457-4499

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Tel: +33 (0) 1 69 18 71 17

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Fax: +86 (10) 51905672

Technical Support
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