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    Material Test Methods: Chemical Resistance Scope

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    Nuno cipriano
    This document provides a test method for determining the chemical resistance of cured paint films, integrally colored plastics, and pressure sensitive decals used in agricultural and construction equipment. It outlines procedures to expose sample materials to chemicals like biodiesel, gasoline, antifreeze, grease and more. Effects are examined after set exposure periods and again after a recovery period. Any degradation of the material like discoloration or loss of adhesion would make it not acceptable for the intended use.

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    Download as PDF, TXT or read online from Scribd

    Material Test Methods: Chemical Resistance Scope

    Uploaded by

    Nuno cipriano
    100 views4 pages
    This document provides a test method for determining the chemical resistance of cured paint films, integrally colored plastics, and pressure sensitive decals used in agricultural and construction equipment. It outlines procedures to expose sample materials to chemicals like biodiesel, gasoline, antifreeze, grease and more. Effects are examined after set exposure periods and again after a recovery period. Any degradation of the material like discoloration or loss of adhesion would make it not acceptable for the intended use.

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    MTM0108

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    This document provides a test method for determining the chemical resistance of cured paint films, integrally colored plastics, and pressure sensitive decals used in agricultural and construction equipment. It outlines procedures to expose sample materials to chemicals like biodiesel, gasoline, antifreeze, grease and more. Effects are examined after set exposure periods and again after a recovery period. Any degradation of the material like discoloration or loss of adhesion would make it not acceptable for the intended use.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    100 views4 pages

    Material Test Methods: Chemical Resistance Scope

    Uploaded by

    Nuno cipriano
    This document provides a test method for determining the chemical resistance of cured paint films, integrally colored plastics, and pressure sensitive decals used in agricultural and construction equipment. It outlines procedures to expose sample materials to chemicals like biodiesel, gasoline, antifreeze, grease and more. Effects are examined after set exposure periods and again after a recovery period. Any degradation of the material like discoloration or loss of adhesion would make it not acceptable for the intended use.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 4

    Material Test Methods MTM0108

    CHEMICAL RESISTANCE

    1. SCOPE

    1.1 This procedure is used to determine the resistance of cured paint films, integrally colored plastic
    (ICP) materials, or a pressure sensitive decal (marking) to various chemicals used in the operating
    environments of CNH agricultural or construction equipment.

    1.2 This test method replaces Case Test Method MT-27 Fluid Immersion and New Holland FNHA-2-
    J-001.15 (86507650) Chemical Exposure.

    2. REFERENCE STANDARDS

    ASTM D4752 - Test Method by Solvent Rub.


    ASTM D6751 Biodiesel Fuel (B100) Blend Stock for Distillate Fuels
    EN 14214 Automotive Fuels, Fatty Acid Methyl Esters (FAME) for Diesel Engines
    ISO 22241-1 Diesel Engines – NO(X) Reduction Agent AUS 32 Quality Requirements
    CNH MTM0102 (86628045) Test Panel Preparation

    3. MATERIALS AND EQUIPMENT

    3.1 Paint materials: two standard Bonderite 1000 with chrome seal test panels prepared per CNH
    MTM0102 for each coating to be evaluated. Panels must be aged at room temperature (25° ± 5°C) for 14
    days minimum in a holding device which allows for air circulation around each panel.

    3.2 Integrally colored and painted plastic: panels shall be representative of the materials and forming
    process intended for use in part production or shall be from actual or comparable finish molded parts.
    Panels shall be 75 x 150 mm (3 x 6 inch).

    3.3 Decals: unpainted Bonderite 1000 paint test panels for application of decals to be evaluated. All
    decals applied to test panels shall age at room temperature (25° ± 5°C) for a minimum of 72 hours
    before testing.

    3.4 Supply of 2" watch glasses.

    3.5 Dropping pipettes.

    3.6 Chemical resistant containers constructed of plastic, stainless steel, etc. suitable for containing
    the chemicals and large enough to hold 4" wide test panels.

    3.7 Cheesecloth.

    3.8 Kimwipes, Kleenex or equivalent.

    ISSUED BY ECN NO. NAME

    GER 29MAR13 35166596 CHEMICAL RESISTANCE


    APPROVED BY REV. PAGE CNH NUMBER

    ENR 29MAR13 E 1 OF 4 86628048


    THE INFORMATION HEREON IS THE CONFIDENTIAL AND PROPRIETARY PROPERTY OF CNH GLOBAL N.V. AND/OR
    ITS SUBSIDIARIES OR DIVISIONS. ANY USE, EXCEPT THAT FOR WHICH IT MAY BE LOANED, IS PROHIBITED.

    UNCONTROLLED COPY When Printed


    Material Test Methods MTM0108

    3.9 CHEMICALS

    3.9.1 Aqueous Urea Solution (AUS32); solution of demineralized or distilled water and 32.5% by weight
    reagent grade urea. Urea content shall be 31.8 to 33.2% by weight. Commercial products developed as
    selective catalytic reduction (SCR) solutions, in accordance with ISO 22241-1, such as AdBlueTM
    (trademark of Verband der Automobilindustrie e.V) may be used as the AUS32 solution.

    3.9.2 B100 Biodiesel; biodiesel fuel per ASTM D6751 or EN 14214

    3.9.3 Unleaded gasoline, regular grade.

    3.9.4 Diesel fuel

    3.9.5 Isopropyl alcohol

    3.9.6 Ethylene glycol base antifreeze mixed 1:1 by volume with tap water

    3.9.7 Multipurpose grease

    3.9.8 Motor oil H.D., Multi-viscosity, 10W-30 or 15W-40

    3.9.9 Diesel engine oil; standard multi-viscosity grade

    3.9.10 Xylene

    3.9.11 CNH Companies aftermarket touch-up aerosol spray paint

    4. PROCEDURE; PAINT AND INTEGRALLY COLORED PLASTIC (ICP)

    4.1 Paint film and ICP exposure duration for each chemical shall be as indicated Table 1.

    Table 1 Paint - Chemicals/Exposure


    Chemical Exposure
    AUS32 solution (AdBlueTM) 1.0 hour
    B100 Biodiesel 1.0 hour
    Gasoline 1.0 hour
    Diesel Fuel 1.0 hour
    Isopropyl Alcohol 1.0 hour
    Antifreeze (50:50) 6.0 hours
    Grease 24.0 hours
    Motor oil (10W30) 24.0 hours
    Diesel Engine Oil 24.0 hours

    4.2 Keeping the test panel(s) in a horizontal position, using a separate pipette, dispense each
    chemical listed in Table 1 except the grease, in an area equivalent to the size of the watch glass cover
    on the test panel(s). Cover each area immediately with a watch glass.

    4.3 Place the multipurpose grease on area of about 6.5 - 13.0 square cm (1 - 2 square inches) and
    leave uncovered.

    NAME REV. PAGE CNH NUMBER

    CHEMICAL RESISTANCE E 2 OF 4 86628048


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    Material Test Methods MTM0108

    4.4 At the end of each designated exposure period remove the watch glass and wipe clean.

    4.5 Examine and record any paint film or surface finish degradation such as loss of gloss,
    discoloration, softening, blistering or loss of adhesion.

    4.6 Where any chemical has an adverse effect on the paint film or surface finish, examine again
    following a four hour recovery period and record.

    5.0 PROCEDURE; DECALS

    5.1 Decal exposure duration for each chemical shall be as indicated Table 2.

    Table 2 Decals - Chemicals/Exposure


    Chemical Exposure
    AUS32 solution (AdBlueTM) 1.0 hour
    B100 Biodiesel 1.0 hour
    Isopropyl Alcohol 1.0 hour
    Gasoline 15 minutes
    Diesel Fuel 2 hours
    Antifreeze (50:50) 2 hours
    Grease 24.0 hours
    Motor oil (10W30) 24.0 hours
    Water 24.0 hours

    5.2 Immerse each applied decal at least halfway in each chemical from Table 2.

    5.3 At the end of each immersion period, remove the decals and wipe clean.

    5.4 Examine and record any decal degradation such as loss of gloss, discoloration, softening,
    blistering, or loss of adhesion.

    5.5 Where any chemical has an adverse effect on the decal examine again following a four-hour
    recovery period and record.

    5.6 XYLENE EXPOSURE - DECALS

    5.6.1 Fold a piece of cheesecloth into a pad consisting of at least four thicknesses of the cloth. Dip the
    cloth in Xylene and rub the decal, exerting moderate pressure with the thumb using about a 50 mm
    (2 inch) stroke. Continue to rub across the test area 20 times (ten complete back and forth strokes).

    5.6.2 Repeat procedures 5.4 and 5.5.

    5.7 PAINT EXPOSURE - DECALS

    5.7.1 Shake the aerosol touch-up spray paint according to manufacturer's instructions and spray a
    heavy, wet film of paint approximately 25 – 50 mm (1 to 2 inches) in diameter on the test decal. Allow
    the paint to stand for three minutes. Wipe off the excess paint with a clean cloth to remove the paint.

    5.7.2 Repeat procedures 5.4 and 5.5.

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    6. REPORT

    6.1 Report the paint film, ICP or decal film condition at the end of each exposure period and after the
    recovery period.

    6.2 The paint coating, ICP or decal is acceptable if there is no visible deterioration following the four
    hour recovery period. There shall be no evidence of degraded adhesion, flaking, blistering, discoloration,
    or degradation of gloss.

    6.3 Decal adhesion is acceptable if there is no evidence of blistering or edge lifting after the recovery
    period.

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