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    Dr. Laurie S. Starkey, Organic Chemistry Lab CHM 318L

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    Sankar Adhikari
    13 C-NMR introduction

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    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd

    Dr. Laurie S. Starkey, Organic Chemistry Lab CHM 318L

    Uploaded by

    Sankar Adhikari
    13 views1 page
    13 C-NMR introduction

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    C-13NMRintro

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    13 C-NMR introduction

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    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    13 views1 page

    Dr. Laurie S. Starkey, Organic Chemistry Lab CHM 318L

    Uploaded by

    Sankar Adhikari
    13 C-NMR introduction

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    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
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    California State Polytechnic University, Pomona

    Dr. Laurie S. Starkey, Organic Chemistry Lab CHM 318L


    Introduction to 13C NMR

    - 13C ("carbon-13") NMR spectra show one signal for each unique carbon
    - chemical shifts ~0-220 ppm
    - signals are all singlets (called proton-decoupled spectra)
    - peak size is not quantitative, but C's without attached hydrogens are often small peaks
    - # of hydrogens attached to each carbon can be determined by a DEPT experiment
    (DEPT differentiates between signals arising from C, CH, CH2, and CH3 carbons)
    - C isotope is only ~1% of carbons so 13C NMR requires more sample and/or more scans
    13

    O
    O
    OH

    OH
    O

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