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Experiment No. 01 Objective: To Determine The Curie Temperature (T

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EXPERIMENT NO.

01

OBJECTIVE: TO DETERMINE THE CURIE TEMPERATURE (TC) OF THE GIVEN


FERRITE SAMPLE AND STUDY THE PERMEABILITY VARIATION IN THE VICINITY
OF CURIE TEMPERATURE.

INTRODUCTION:

Curie temperature is the temperature at which the ferromagnetic materials become


paramagnetic.

E.M.F. induced in secondary coils of a transformer is given, as per Faraday‟s Law, as


dB
VS  K (1)
dt
Where,
K: Constant dependent upon the geometrical factors and the turn ratio of the transformer.
B: The flux density depends on magnetizing field (H), which in turn is proportional to the
primary voltage (Vp) and permeability of the core (µ).

In the ferromagnetic state, the temperature dependence of Vs thus directly gives us the
temperature dependence of permeability. At Curie temperature (Tc) there would be a sudden
drop in the permeability of the material and hence a corresponding drop in Vs. So, the point at
which Vs starts decreasing defines the Curie temperature.

Figure 1: Schematic of the Curie Temperature setup.

At temperature exceeding Tc the materials is in the paramagnetic state where magnetic


susceptibility m (= µ-1) follows the Curie-Weiss Law:
C
 m (T )  (2)
T  Tc

Where,
T is a temperature close to Curie temperature.

Equation (1) in the paramagnetic state can be rewritten as:


dH
VS  K 0  m
dt
dH
 K 0 (  m  1)
dt

For a sinusoidal magnetising current

VS  K 0H (1   m ) (3)

Where  is the angular frequency of magnetizing current.


Incorporating equation (2) in equation (3)
C
VS  K 0H (1  ) (4)
T  Tc

Thus a plot of Vs vs 1/T-Tc should be a straight line with µ0K H as intercept and µ0KHC as
slope.
Thus ratio of slope to intercept gives C. This fully characterizes the equation (2) which gives the
temperature dependence of permeability in the paramagnetic state.

EXPERIMENTAL PROCEDURE:

1. Connect the primary turns of the coil over a ferrite core (figure 1) to an oscillator output.
2. Read the induced e.m.f in the secondary turns with the help of an ac millivoltmeter.
3. Heat up the sample in an oil bath and note secondary output as temperature increases.
4. At curie temperature the output will show a sudden drop. Once the secondary coil output
starts to drop note the output for every 10C rise in temperature.
5. Repeat the observation of Tc during the cooling (after completing the observations of Vs
vs T and shutting off the heater power).
6. To note temperature accurately locate the bulb of the thermometer in the vicinity of the
sample. While reading V at varying temperature monitor current in primary turns and see
that it remains constant. If needed, keep adjusting it to a constant (preset) value.
CALCULATIONS AND RESULTS:

1. Plot Vs vs. temperature and deduce Tc.


2. Plot Vs vs. 1/T-Tc plot (for T > Tc) and determine its slope, intercept and their ratio C.

TABLE:

S. NO Temperature (◦c) Vs (mV)


Conclude your report by answering the following questions:

1. If the same experiment was to be performed employing a ferromagnetic core would any
modifications be required in terms of experimental procedure theory and results deduced.

2. Equation (3) suggests that secondary output would be higher for higher frequency of
magnetizing current. In this should we perform the experiment at very high frequencies
(say RF)? Are there any difficulties in doing so?

3. What does parameter C in equation (2) signify?

4. Did you observe Tc to be different between the heating and cooling process? If so, how
do you explain this difference?

5. Ask your instructor about the ferrite materials used in the experiment and write a
paragraph on it after studying reference materials.

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