Industrial Metrology - Surfaces and Roundness
Industrial Metrology - Surfaces and Roundness
Industrial Metrology - Surfaces and Roundness
Industrial
Metrology
Surfaces and Roundness
, Springer
Graham T. Smith, MPhil (Brunel), PhD (Birmingham), CEng, FIMechE, flEE
Faculty of Technology
Southampton Institute
East Park Terrace
Southampton S014 ORD
U.K.
Apart from any fair dealing for the purposes of research or private study, or criticism or review, as
permitted under the Copyright. Designs and Patents Act 1988, this publication may only be
reproduced, stored or transmitted, in any form or by any means, with the prior permission in writing
of the publishers, or in the case of reprographic reproduction in accordance with the terms of licences
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should be sent to the publishers.
The use of registered names, trademarks etc. in this publication does not imply,even in the absence of
a specific statement, that such names are exempt from the relevant laws and regulations and therefore
free for general use.
The publisher makes no representation, express or implied, with regard to the accuracy of the
information contained in this book and cannot accept any legal responsibility or liability for any errors
or omissions that may be made.
The subject of this book is surface metrology, in particular two major aspects:
surface texture and roundness. It has taken a long time for manufacturing engineers
and designers to realise the usefulness of these features in quality of conformance
and quality of design. Unfortunately this awareness has come at a time when
engineers versed in the use and specification of surfaces are at a premium.
Traditionally surface metrology usage has been dictated by engineers who have
served long and demanding apprenticeships, usually in parallel with studies leading
to technician-level qualifications. Such people understood the processes and the
achievable accuracies of machine tools, thereby enabling them to match production
capability with design requirements. This synergy, has been made possible by the
understanding of adherence to careful metrological procedures and a detailed
knowledge of surface measuring instruments and their operation, in addition to
wider inspection room techniques.
With the demise in the UK of polytechnics and technical colleges, this source of
skilled technicians has all but dried up. The shortfall has been made up of semi-
skilled craftsmen, or inexperienced graduates who cannot be expected to satisfy
tradition al or new technology needs. Miniaturisation, for example, has had a pro-
found effect. Engineering parts are now routinely being made with nanometre
surface texture and fiatness. At these molecular and atomic scales, the engineer has
to be a physicist.
This book is intended to bridge the gap between technology and training. Dr Smith
has approached the subject from the point of view of aprecision engineer, but in
addition has made the reader aware, whenever appropriate, of new techniques and
instruments. He is admirably suited to the task, having served an apprenticeship in
industry which has led to hirn becoming a master toolmaker. He has balanced these
practical skills by in-depth studies leading to the degree of Ph.D in manufacturing
engineering. Taking these complementary paths has given hirn a unique pedigree
that has enabled hirn to write with authority.
Dr Smith is recognised as an expert in his subject of manufacturing and has lec-
tured extensively throughout Great Britain and North America. This book is a must
for those involved in inspection and quality control and could well be used as a co re
for training courses in metrology.
As the UK's national measurement institute the National Physical Laboratory (NPL)
has been at the forefront of research in the field of metrology - measurement
science - since its inception in 1900. NPL has always been involved in measurements
at the highest levels of accuracy in order to suppport its role as custodian of the
national measurement standards and to address the UK industry's most demanding
measurement problems. NPL also plays a key role in the dissemination of mea-
surement good practice to industry through its wide range of knowledge transfer
activities. It was therefore a pleasure for myself and members of the Dimensional
and Optical Metrology Team at NPL to contribute to this important book, which I
believe provides a rich source of information for anyone working in the field of
surface texture and roundness - areas which have been and will continue to be
among the most important but sometimes least appreciated areas of dimensional
metrology in industry.
In the 1970s much of the surface texture work carried out at NPL related to the
manufacture of X-ray optical components that required control of roundness to
within a few tens of nanometers, profile to a few nanometres and surface text ure
often to sub-nanometres tolerances. In order to control the manufacture of these
optical components, measurement techniques with sufficient accuracy had to be
developed. This led to an NPL-designed instument, subsequently marketed by
Rank Taylor Hobson, called "Nanostep", which was the first instrument of its time
to have sub-nanometre vertical accuracy with a large horizontal movement range.
In recent years one of NPL's key objectives has been to undertake research work
to support UK industry by providing calibrated references artefacts for surface
texture measurements. This work culminated in 2000 in a new NPL-designed
instrument, "NanoSurf IV", capable of calibrating surface texture reference arte-
facts with fully traceable measurements in all the axes, leading to a combined
expanded uncertainty of ± 1.3 nm.
Appendices. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 297
Appendix A - Previous and some current surface texture parameters 299
Appendix B - Amplitude-wavelength analysis: "Stedman dia grams" 317
Appendix C - Surface texture and roundness: calibration diagrams
and photographs .................................. 320
Appendix D - Hardness conversion chart .......................... 325
Jeol (UK) Limited were of considerable help and support in supplying informa-
tion and producing photomicrographs for the chapter on surface microscopy. Most
notably, I would like to express my thanks to Dr Larry Stoter (Sales Executive) for
supplying instrumentation photographs and relevant information, Mr John
Critchall (Applications Manager) and Mr Andy Yarwood (Application Specialist)
111
for undertaking SEM/AFM photomicrographs and to Mr Chris Walker (General
Manager) for further technical assistance.
Other notable support came from companies that have contributed information
and photographic support to the book, including Zygo/Lamda Photometrics
Limited - Mr Joe Armstrong (Technical Sales Engineer); VG scientific - Dr John
Wolstenholme (Marketing Manager): Nikon UK Limited - Mr Robert Forster
(General Manager) and Keith Poulton (Product Manager); also Rubert & Co.
Limited - Mr Paul Rubert (Managing Director).
This book would not have been possible without the help and guidance of some
of Great Britain's leading academics and I would like to single out several people
for special mention. In the first instance, an old friend Professor David J.
Whitehouse (formerly Chief Scientist at the University of Warwick). For conver-
sations on David's immense knowledge on the topics discussed here and for
previous instruction on all manner of aspects concerning both surface texture and
roundness, furthermore, I would like to express my sincere thanks for hirn kindly
agreeing to write the Foreword for this book. Likewise to Dr Brian J. Griffiths
(Reader at Brunel University), my previous mentor and dear friend, for his instruc-
tion and support on all topics appertaining to surface integrity; and to Professor
Tom R. Thomas (Chalmers University, Sweden) for conversations concerning
surface texture and amplitude-wavelength analysis.
Lastly, a considerable number of graphs, line and assembly diagrams were drawn
by me, and if there are any misinterpretations in their execution then they are a
reflection on the author. Further, in the body of the text some manuscript errors
may have inadvertently crept in, and if this is the case they are not to be associ-
ated with any of the companies or individuals that have supported the book.
Dr Graham T. Smith
West End,
Southampton
Surface texture:
two-dimensional
Waviness spacing
Waviness
Roughness spacing
Figure 2. The major eomponents that constitute a typieal surfoce texture, also exhibiting some degree of direetionality (lay).
r
Any manufacturing process
r
Material shall be removed
r
Material shall not be removed
6
3
KEY
NB: Surfaces exhibiting a defined directionality, or
a =2D parameter 1
"Lay" must be measured at right angles to this lay
b =2D parameter 2
pattern.
c =2D parameter 3
d =process
e =lay pattern
f =allowance
x = not allowed
Figure 3. The composition ofthe complete graphical symbol for surface texture. [50urce: 150 1302: 2001]
• profile - the overall shape of the surface - ignor- directional properties such as feed marks, or
ing roughness and waviness variations - is caused isotropie - devoid of apredominant lay direction.
by errors in machine too1 slideways. The lay of any surface is important when attempting
to characterise its potential functional performance.
Such surface distinctions tend to be qualitative - If the direction of the trace being produced by a
not expressib1e as a number - yet have considerable stylus instrument - re cord of the stylus motion over
practical importance, being an established pro ce- the assessed surface topography - is not taken into
dure that is functionally sound (Figure 3). The account, then a totally misrepresentative reading will
combination of these surface texture conditions, result from an anisotropie surface. This is not the
together with the surface's associated "lay", are ideal- case when measuring an isotropie surface, for
istically shown in Figure 4, where the lay of the example a "multi-directionallay" - as indicated in
surface can be defined as the direction of the domi- Figure 4. Under this isotropie condition, perhaps
nant pattern. Figure 4 also depicts the classification three different measurement paths could be scanned
of lay, which tends to be either anisotropie - having and the worst roughness trace would be utilised to
111 Industrial metrology
Parallel
d= --/----
Perpendicular
d..L I
lAB C D E
Crossed ~ I I I I,
I I I I I
I ' / I 1/ ,
-j I I / ! ..--- - - - -
Multi - directional
I ~.I
~ M-V V
Particulate A B c D E
I
SUPERFINISHING ~///~
LAPPING V7mij"/////ff/~
GRINDING V//////////.ffff////////.l
,
BORING V////////.ß7////j /'///~
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TURNING V////////h /'/////////h
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DRILLING V//P//////-
EXTRUDING v/////7//h':
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DRAWING V//////////-
MILLING V//////////.// / h
SHAPING V////////7-:/"//h:/"////////fi::
50
'"
~
N12
25 ~ N11
"\.
12.5 ~ N10
"-
6.3 \ N9
3.2
'"
~
N8
~
1.6 N7 INCREASING
ROUGHNESS
0.8 \ N6
0.4 '\" N5
0.2 ~
"-
N4
0.1 ~ N3
~
~
0.05 N2
0.025
~ NI
Figure 6. Anticipated process roughness and respective grades. [Source: ISO 1302: 2001.1
either too large or this is impracticable - due to face texture is closely allied to functional perform-
either stylus access to the surface or surface indina- ance, particularly when one or more surfaces are in
tion - then placing a small portable instrument on motion with respect to an adjacent surface. This sug-
the surface can allow a measurement. Occasions arise gests that the smoother the surface the better, but this
when even this is not an option and under these cir- is not necessarily true if the surfaces in question are
cumstances it may be possible to take a "cast replica" required to maintain an efficient lubrication film. The
of the surface, then present this to the instrument. apparent roughness of one of these surfaces with
Some surface texture measuring instrument manu- respect to the other enables it to retain a "holding
facturers offer "replica kits" for just this purpose. It film" in its associated roughness valleys. Yet another
should be remembered that this replica of the surface factor which may limit the designer from selecting a
is an inverted image. smooth surface is related to its production cost (see
Figure 7). If a smooth surface is the requirement then
this takes a significandy longer time to produce than
an apparendy rougher surface, which is exacerbated
1.2 Establishing the Ra if this is allied to very dose dimensional tolerancing.
20
19 \
18 \
17 \ .-/
Cylindrical grinding
.....
<Il 16
y- ./
U
0
:... 15 \
0
ar 14 \\
.5E-< 13
I--Surface grinding
c0
:cu 12 VI\ -----
= 11 \
"I:l
\
0
:...
Q., 10
\ \
~
.::..... 9
\ \ t - - Reamlng
.s~
8 \ \ I\- -\- End milling
Q:i
7
\ 1\ \ \/ Turning
6
1\ \ \ /\ / ' Peripheral milling
5 \ \ /- >(/ Shaping and planin
4
\ 1\ v ~ /"-. r--....
1\ 0 0-. / ' Drilling
3
2
"" ""'" ~ "'" ",'-
r--=:: -'" ~
.........
~
~K
~ ~
0.025 0.05 0.1 0.2 0.4 0.8 1.6 3.2 6.3 12.5 25.0 5.00
Ra Value (11m)
Figure 7. Relative cost, in production time, necessary to produce surface finishes by different production processes. (Courtesy ofTaylor Hobson.)
when used to calibrate stylus-based surface texture reference specimens from frequent use a hard boron
measuring instruments. A range of standard refer- nitride layer can be specified.
ence specimens can be purchased for this purpose
and will act as a "health check" on both the current
stylus condition - whether its point is worn or
partially broken - and indicate if the allied instru- 1.4 The basic operating
mentation/electronics has "drifted" since the last
calibration check. This enables the inspector to principle of the pick-up, its
speedily and efficiently remedy the situation and
bring the instrument back into calibration. Most of
stylus and skid
these calibration reference specimens are manufac-
tured from replicas of an original master production Prior to describing some of the more sophisticated
surface by nickel electroforming; this enables the instruments by which the surface is measured, it is
block to be a reproduction of the whole surface, with worth describing the basic function of a typical
the finest details being approximately 1 fLm in size. stylus instrument. In Figure 9, a schematic illu-
Each reference specimen offers exacting uniformity stration is depicted of the basic components for a
of profile shape. In order to minimise wear on these typical surface texture measuring instrument. The
..
(a)
Industrial metrology
(b)
.
Figure 8. (a) Utilising a comparator gauge to determine the surface finish for a specific manufacturing process. (b) Atypical comparator gauge,
for both visual and tactile assessment. (Courtesy of Rubert & Co Ltd.)
------r----l....--,
Trace Pen
unit
------'---_---l
Recorder
Figure 9. 5chematic diagram illustrating the major constituents of a stylus-type of surface texture measuring instrument. (Courtesy of
Taylor Hobson.)
u ace texture: two- Imenslona l1li
x5000 and horizontal magnification (Vh ) of xl00,
then in this situation the respective size of the stylus
is almost indistinguishable from that of a (vertical)
straight line or point contact (see Figure llb). This
significant size differential enables the stylus to
penetrate into quite narrow valleys, although its
finite size affects the accuracywith which the surface
profile can be traced. These stylus profile and size
limitations influence the following:
= 0. 1 ~ m
(e) The eurve tends to round the peaks (I) and reduee the depth of
the valleys (11), aIthough the peak height is not affeeted (111)
Figure 11. Stylus geometry and its mechanical filtering effect on surface texture. ((ourtesy of Taylor Hobson.)
right) must utilise an exceedingly low force, typically long as the skid's radius is greater than the peak
""'3 x 10- 5 N or less. The transducer assembly can spacing, the apparent line of movement of this skid
incorporate both a stylus and skid, with the skid will be virtually a straight line. Under such surface
offering a local datum for this transducer and with transducer conditions as the vertical skid moves
that of the surface. Moreover, the skid provides a from crest to crest, its relative horizontal skid
local datum for the stylus with respect to its vertical motion with respect to the test surface can be
and horizontal motion. Therefore, with the skid's ignored, as the skid's vertical motion is virtually
large curved radius to that of the relatively small insignificant. However, once the crests in the surface
surface under test, it rides along the surface being under test become more widely spaced, this hori-
measured (Figure 13), providing a "local datum". As zontal crest spacing tends to introduce a significant
u ace texture: two- Imenslona
Re-entrallt feature
on a surfacc Figure 14. A high-quality component's surface texture being
assessed without a skid which tends to be the "approved method", of
late. ((ourtesy of Taylor Hobson.)
Figure 12. IIlustrating how the use of a larger-radius stylus reduces
the apparent amplitude of closely spaced irregularities. ((ourtesy of
Taylor Hobson.)
1.5 Filters and cut-off
It was previously suggested that surface geometry is
comprised of roughness, waviness and profile (see
Figure 2). These interrelated factors also tend to have
different relationships to the performance of the
component. It is normally the case that they are
separated out during analysis. To obtain this sepa-
ration on surface texture measuring instruments,
selectable filters for roughness and waviness are
applied. In this section, only a superficial treatment
of filtering and its effects will be mentioned, as this
will be dealt with in greater depth later in the
chapter.
In general, selection of the desired filtering can
be established by the following "rules of thumb":
Figure 13. Surface texture of component being inspected using a
skid. ((ourtesy ofTaylor Hobson.)
• roughness filtering would be applied if control is
required of workpiece performance (for example:
resistance to stress failure; wear resistance; fric-
amount of vertical skid motion. If the skid's vertical tion; reflectivity and lubrication properties);
motion affects the subsequent surface texture • waviness filtering might be selected if control is
results, it is then preferable to use the instrument in necessary for workpiece or machine tool per-
the "skidless mode", as instruments employing a formance (for example, vibration or noise gener-
skid should be used for the measurement of rough- ation).
ness parameters (ISO 3274: 1996). To achieve skid-
less operation and minimise the unwanted affects of Once the type of filter has been chosen then the
vertical skid motion which might otherwise inter- filter cut-offs should be selected (see ISO 11562: 1996
fe re with the results, the skid must be removed, then for more detailed information) with a range, notably:
by utilising the instrument's in-built straight edge as ce••• mm; 0.08 mm; 0.25 mm; 0.8 mm; 2.5 mm;
a "sliding datum" the surface assessment can be 8.0 mm; .. :' (ISO 3274: 1996). However, this can only
undertaken, as illustrated in Figure 14. More will be be undertaken when the specific features needing to
mentioned on the influence of the skid and its asso- be measured are known. Generally, the following
ciated "phase effect" later. criteria can be applied:
.. InClustrial metrology
-1 ~ M
I\/\/\/V\IVVV\,
- I.
100 peaks
~
fV\IV\/V\IVVV\
100Hz
r-
0.02mm
B
~
-1 M ~
~
50 peaks
50Hz
O.01mm
C
-1 ~
I\JVVVVV\/\/'V'
0.5mm
--1 r- ~
~
50 peaks
50Hz
O.Olmm
D
-1 t-
/\/\A/\IVVV\IV ~
I-
2mm
~I
fI/\/INVIJ\/WJV
r 200 peaks
~I 200Hz
Traverse speed: A = 1 rnrn s-l; B = 1 rnrn s-l; C = 0.5 rnrn s-l; D = 2 rnrn s-l;
Figure 15. Signal frequeney depends on irregularity spaeing (compare A and B) and traverse speed (compare A, (and D). ((ourtesy ofTaylor
Hobson.)
and horizontally shiJted. Such an action by the ana- off. Figure 16(bi) shows how the unfiltered profile
logue filter may lead to serious errors Jor either equates to an electrically filtered one - Figure 16(bii)
plateau honed types oJ surJace or PM (porous) types - for the same value of cut-off, but related to 50% of
oJ topographies. its depth. The main difference between the (PC)
If a digital filter is employed, such as that shown digital filter and the analogue filter is that the former
on the graph in Figure 16(a), then the vertical distor- type evaluates the profile mean around a point -
tions of the profile caused by abrupt changes in the enabling it to anticipate changes in the profile height
height of the topography are minimised. The prin- - whereas the latter (analogue) filter cannot. It is
ciple operation of the digital filter can be explained possible to emulate the analogue filter's characteris-
as below. tics by employing a "weighting function" for each
Digital profiles are no longer represented by a ordinate height when adetermination of the arith-
smooth curve, but instead, are described by aseries metic average or mean point is required. However,
oJ ordinates (numbers) relating to profile heights at unless there is a large variation in the surface topog-
regular intervals. In order to estimate the profile's raphy, or special processing conditions apply - such
mean line the filter's action is to calculate the average as the "Gibb's phenomenon" - then the analogue-to-
height at a given point, as the arithmetic average oJ digital differences remain slight.
the ordinate points in its vicinity. Hence, if the profile
is divided up into "windows" the mean profile height
Jor each window can be estimated. A line joins these
window averages together, which represents the 1.6 Measuring lengths
profile mean line.
Such a digital filter allows up to 100% transmis-
sion of the profile, representing wavelengths shorter In order to determine a workpiece's surface texture,
than the actual cut -off length, together with zero three characteristic lengths are associated with the
transmission of wavelengths greater than this cut- profile (ISO 4287: 1997). These are:
(a) High-pass filter characterisation (Source: ISO 3274: 1996 - abridged graph)
~
6
50% " I'
" '\.
\
, \
"-
\
~
.:=
4
2 \ \ i\. \ 1\
.~'"
'"
= \ \ \ \ \
b
01
'"
"CI
10 1
8
6 \
, 1\ \ \
1\
B \ \ \ \ \
:s.Ei 4
\ \ \ \
-< 2 \ \
1 \ \ \ \ \
10-2 2 4 6 8 10-1 2 4 6 8 10° 2 4 6 8 101 2 4 6 8 102
Sine wavelength (A) mm
(bi) No filtration
1I
'-I---------'-V
1 1
I (bii) With filtration
&.
k
1
_
Sine wavelength
~
~
Wavinessdepth:50%
Ac=0.8mm
Figure 16. Effeet of an eleetrieal filter on the surfaee texture. (Courtesy of Taylor Hobson.)
---<[Li jL i
~
I I
~
I I
C I A I I I D
I I I
I B I
T I
~ I
~
I I T
~ ko----- u ~~
(b) Waviness only
selection of appropriate lengths can be demon- case, the waviness would playa greater role and for
strated in Figure 17(a). Figure17(a) indicates that this reason it is undesirable to increase the sampling
while the sampling length L is sufficient to reveal the length much beyond that required to obtain a repre-
whole of the roughness pattern, the waviness has sentative assessment of roughness.
very little influence over this length. Even if the The sampling length can be defined as the length
sampling length was increased, it would simply in the direction of the x-axis used for identifying the
include more roughness detail but would have litde, irregularities that characterise the profile under eval-
if any, effect on a roughness parameter value. In this uation. By specifying a sampling length, this implies
InClustrial metrology . .
, , ,
I Vß0W&~~ff
~ "'lWßdWZI
Allowance' I 2 3 4 5
L
'I
Figure 18. Determining surface texture analysis roughness parameter Ra, together with its arithmetic derivation.
that structure in the profile occurring over longer and waviness profiles. The evaluation length meas-
lengths will not be applicable in this particular eval- urement is the sum of the individual sampling
uation. The sampling length for Ir - roughness - is lengths. If a different number is used for the rough-
equal (numerically) to the wavelength of the profile ness parameter assessment, ISO 4287: 1997 advo-
AC, whereas the sampling length for lw - waviness - cates that this number be included in the symbol, for
equates to that of the profile filter Af Virtually all the example Ra6. In the case of waviness, no default
parameters necessitate evaluation over the sampling value is recommended. From a practical viewpoint,
length; however, reliability is improved by taking an the selection for the correct filter can normally be
average of them from several sampling lengths as ensured when at least 2.5 times the peak spacing
depicted by the evaluation length in Figure 18(a). occurs, with two peaks and valleys within each one.
Typically, this would me an that an evaluation length
of 0.8 mm would be selected, but there are occasions
Evaluation length (In) when either a larger or smaller evaluation length
might be preferable for the surface under test. The
A simplistic diagram of the relationship of the stylus metrologist's experience and judgement will come
to the material profile/topography for a pre-selected into play here.
traverse length is indicated in Figure 18(a). The eval-
uation length can be defined as the total length in
the x-axis used for the assessment of the profile under Traverse length
evaluation (see Figure 18a). As shown, this length
may include several sampling lengths - typically five The traverse length can be defined as the totallength
- being the normal practice in evaluating roughness of the surface traversed by the stylus in making a
measurement. It will normally be greater than the the total profile, which can be adjudged to be of most
evaluation length, due to the necessity of allowing significance in a particular situation. Conversely,
run-up and over-travel at each end of the evaluation the effects of filtering can be considered as a means
length to ensure that any mechanical and electrical of removing irrelevant information, such as instru-
transients, together with filter edge effects, are ment noise and imperfections. Therefore, filters can
excluded from the measurement (see Figure 18a).On select or reject surface topographical structure
shorter surfaces, it may be necessary to confine the depending upon its scale in the x-axis, in terms
measurements to one sampling length, under these of spatial frequencies, or wavelengths. The terms
circumstances the sampling and evaluation lengths low-pass and high-pass filters refer to whether they
are identical, but the over-travel necessary to either reject or preserve surface data. For example,
contribute to the traverse length must be retained. a low-pass filter will reject short wavelengths while
retaining longer ones, whereas a high-pass filter pre-
serves shorter-wavelength features while rejecting
longer ones. The term bandpass filter refers to the
1.7 Filtering effects (As, Ac combination of a low-/high-pass filter selected to
restrict the range of wavelengths, with both high-
and At) and low-pass regions being rejected. Filter attenua-
tion (rejection) should be somewhat gradual, other-
wise significantly differing results occur from almost
In Figure 19 a flow chart is illustrated showing the identical part surfaces, the exception being when a
manner in which surface assessment occurs, with significant surface feature causes a slight wavelength
the primary profile broken down into filtered shift.
elements to obtain the waviness and roughness The term cut-off refers to the 50% transmission
profiles of the workpiece surface. Algorithms enable (and rejection) wavelength filter, this being specific
suitable characteristic functions and parameters to to the topic of surface texture. In the case of the large
be obtained, scaled to an appropriate size. As has majority of surface texture assessments, it is
been mentioned previously in Section 1.5, filters are suggested that when the width of a specific surface
vital to any form of surface texture analysis. Today, feature is significant, but its size may only be 1% of
most forms of filtering are normally electrical or the overall width, this will make it less important.
computational, although they can occasionally be Under these circumstances that affect feature trans-
mechanical for analysis of the range of structure in mission/rejection, it is suggested that bandpass
Output
scaling
Roughness Profile
algorithm recording
Characteristic
functions
Parameters of
roughness,
waviness
Waviness
and
algorithm
primary
profiles
Primary
profile
algorithm
(a) Zv
Xs
dZ(x)/dX
(b)
dZ(x)/dX
(e)
Figure 21. (<t) Profile length, (b) local slope and (c) materiallength of a surface trace. [Source: 1504287: 1997]
1.9.1 Amplitude parameters (peak- not without some merit, as they can establish un-
usual surface features such as either a burr on the
to-valley) surface or sharp spike, and will indicate the presence
of scratches or cracks - possibly indicative of low-
grade material or poor production processing.
Maximum profile peak height Hp, Wp
andPp Maximum profile valley depth Hv, Wv
This parameter is represented by the largest peak andPv
height (Zp) within the sampling length, with its
height being measured from the me an line to This parameter is represented by the largest valley
the highest point (see Figure 22a). The Rp parameter depth (Zv) within the sampling length, with its
(equating to roughness) is generally less favoured, absolute value Rp (equating to roughness) being
with preference given to parameters based on the obtained from the lowest point on the profile from
total peak-to-valley height. Often Rp and its associ- the mean line (see Figure 22b). As in the case above
ated parameters Wp and Pp are referred to as for peaks, the maximum profile valley depths are
extreme-value parameters, being somewhat un- extreme-value parameters. In a similar manner to
representative of the overall surface, because their Rp, Rv can establish whether there is a tendency to
numerical value can vary between respective sam- workpiece cracking, spikes and burrs, detecting such
pIes. In order to minimise variation in Rp, it is features on the surface.
feasible to average readings over consecutive samp-
ling lengths, although in most cases the value
obtained is numerically too large to offer practical Maximum height ofprofile Hz, Wzand pz
assistance. The Rp and its Wp and Pp derivatives are
The maximum height parameter (for example, Rz -
for roughness) is the sum of the height of the largest
profile peak height (Zp), together with the largest
profile valley (Zv) within the sampling length (see
Figure 23a). In isolation, the Rz does not provide too
much useful surface information, and therefore it is
often divided into Rp and Rv, previously described.
(a) In fact, in ISO 4287: 1984, the Rz symbol indicated
the ten point height irregularities, with many of the
previous surface texture measuring instruments
measuring this Rz parameter - see the Appendix for
more information regarding this previously utilised
parameter.
Sampling length
Rz
(b)
Figure 23. (a) Maximum height of profile and (b) height of profile elements (examples of roughness profiles). [Source: ISO 4287: 1997]
(a)
c
Graphieal derivation or Ra
Ccntrc linc
(b)
I
I
I Sampli ng Icngth (L)
i- -I
Figure 24. Determination of Ra and Rq. ((ourtesy of Taylor Hobson.)
1 1 N
Rsk=-- ~ Z3
R q3 N I tft
The skewness parameter of an amplitude distribu-
Root mean square deviation from the tion eurve as depieted in Figure 25(a) indieates a
assessed profile Rq, Wqand Pq eertain amount of bias that might be either in an
upward or downward direetion. The amplitude
The root mean square of the ordinate values Z(x) distribution eurve shape is very informative as to the
within the sampling length is established by the overall construction of the surfaee topography. If
departures from me an line of the profile and ean be this eurve is symmetrieal in nature, then it indieates
mathematieally expressed in the following way: symmetry of the surfaee profile; eonversely, an
unsymmetrieal surfaee profile will be indieative of a
Amplitude
distribution
curve
Figure 25. How surface texture topography influences the amplitude distribution curve.
terised by Figure 25(c) might occur in the cases of bution curve can also relay useful information about
porous, sintered or cast-iron surface topography - the dispersion, or "randomness" of the surface pro-
having comparatively large numerical values of file, which can be quantified by means of a para-
negative skewness. The surface is sensitive to meter known as kurtosis (Rku).
extreme ordinate values within the profile under
test; this is due to Rsk being a function of the cube
of the ordinate height. As a result of this peak sensi-
tivity, it is a hin dran ce when attempting to inspect Kurtosis of the assessed profile Rku, Wku
plateau-type surfaces, although the Rsk parameter andPku
indicates a reasonable correlation with a compo-
nent's potential load carrying ability, or its porosity. The kurtosis parameter, typified by Rku, is the me an
The shape, or "spikeness" of the amplitude distri- quadratic value of the ordinate values Z(x) and the
(a) Kurtosis is influeneed by the distribution shape
(b) Material distributed evenly aeross the whole of the surfaee topography
Amplitude
distribution
Figure 26. Variation in surface topography influences the shape and height of the amplitude distribution curve.
fourth power of Pq, Rq or Wq, respectively, within surface topography, Rku is a useful parameter in the
the sampling length. However, unlike the skewness prediction of in-service component performance
parameters previously described, namely Rsk and its with respect to lubricant retention and subsequent
derivatives, Rku can detect if the profile peaks are wear behaviour.
distributed in an even manner across the sampling It should be mentioned that kurtosis cannot
length trace, as well as providing information on the convey differences between either peaks or valleys
profile's sharpness (see Figure 26). in the assessed profile.
Kurtosis provides a means of measuring the The kurtosis parameter indicative of Rku, can be
sharpness of the profile, with a "spiky" surface ex- mathematically expressed in the following manner:
hibiting a high numerical value of Rku (Figure 26c);
alternatively, a "bumpy" surface topography will
have a low Rku value (Figure 26b). As a consequence
of this ability to distinguish variations in the actual
1.9.4 Hybrid parameters
C
(a)
J
I I
o 20 40 60 80 100
Ib r - - -
Evaluation length
-----..,
Rmr(c) %
(b)
.\
.....
I"-
R&[-- CO
1---- -- - --'
NI ........ ~
~
Cl
I--- -- - - ~ f-- - - \...
I ~r\
I : \
I
I : \
I ,
I
I
o 10 20 30 40 50 60 70 80 90 100
I I
RmrO Rmr
Figure 28. (a) Material ratio curve. (b) Profile section level separation. [Source: ISO 4287: 1997]
Profile section height difference RBc, with the bearing ratio at the corresponding position
here being the Rmr (Figure 28b). The reason for the
WBc undPBc reference percentage is to eliminate any spurious
peaks from the assessment, as they would tend to be
This parameter can be represented as the vertical worn away during the initial burn-in/running-in
distance between two section levels of a given period. The slice depth will then correspond to a
material ratio curve (see Figure 28b). satisfactory surface roughness, or to an acceptable
level of surface wear.
(a)
I Amplitude density
I
I Evaluation length
foe:::::Jl--------
+y Amplitude
Profile graph distribution
(b)
-y
Figure 29. Profile height and amplitude distribution curve. [Source: ISO 4287: 1997]
Industrial metrology , .
over which the profile graph will attain any selected manufactured surfaces clearly indicate visible repet-
range of heights that are above or below the mean itive marks on either the material itself or indirectly
line (see Figure 29b). The profile's horizontallengths via the profile graph, while on other surfaces it
are included within a narrow zone width öy at a becomes difficult to distinguish any repetitive irreg-
height z and are represented in Figure 29(b) by "a, ularities from random occurrences. This visual diffi-
b, c, d and e". Therefore, by expressing the sum of culty is particularly true when the amplitudes of the
these lengths as a percentage of the evaluation repetitive irregularities are less than the random
length, this will give a measure of the relative occurrences. Moreover, the presence of repetitive
amount of the profile at height z. surface features - however small - can indicate
This graph is known as the amplitude distribu- factors such as tool wear, machine vibration or defi-
tion at height z, so by plotting density against height ciencies in the machine, with identification of them
the amplitude over the whole profile can be deter- being an important factor. Any random pattern
mined - producing the amplitude density distribu- occurring on the surface can reveal, for example,
tion curve. whether a built-up edge condition has transpired on
the cutting tool resulting in a degree of tearing of
the machined surface - this tends to be of a random
1.9.6 Overview of parameters nature and is not predictable.
The extent of this randomness of the surface can
In Table 2 are shown the more recent and previously be monitored and assessed by isolating random
utilised parameters, together with information from repetitive textural patterns, this being achieved
concerning whether the parameter has to be calcu- by auto-correlation. When a profile is perfectly
lated over the sampling or evaluation length. periodic in nature - typified by a sine wave - the
relationship of a particular group of points repeats
itself at a distance equal to the wavelength. Con-
versely, if the profile under inspection is comprised
1.10 Auto-correlation function entirely from random irregularities, the precise rela-
tionship between any specific points will not occur
at any position along the trace length, hence any
Every day of one's life, the technique of correlation repetitive feature or group of features can be identi-
is applied to compare sights, sounds, tastes, objects fied. Computers equipped with fast digital proces-
- the list is almost limitless - this being a process of sors have significantly reduced the tedious task of
comparison. The auto-correlation function (ACF) is determining a surface profile's auto-correlation.
essentially a process of determining the relationship The technique exploited by auto-correlation is to
of any point on the profile to all other points. Some compare different parts of the surface profile; in this
Table 2. Past and present parameters for surface texture
(b) A(ß)
Slope
Curvature
Profile
Length A(ß)
(e) Decrement
I
1----, Sampling length _I
Peakspermm
Co'
Figure 30. Comparison of surface parameters for typical surfaces showing those currently in use. [After Whitehouse, 1978.]
manner profile repetItlOns or similarities ean be Figure 30 shows an example of the ACF relating
discovered. When the profile of the surfaee displays to speeifie surfaee profile eonditions. As mentioned
either an isotropie or random shape then no above, the ACF eontains information relating to the
portions will be similar, exhibiting low auto-eorre- spacings of peaks and valleys in the profile. An alter-
lation funetion. On the other hand, if an anisotropie native to the ACF is the equivalent term known as
or periodic surfaee topography oeeurs - for example the power speetrum, or power speetral density, in
as in single-point turning operations - then repeti- whieh spacings are replaeed by frequencies - one
tion of the surfaee profile oeeurs and auto-eorrela- being a Fourier trans form of the other. For the ACF
tion will be high. examples shown in Figure 3D, the seale of the hori-
zontal axis can be the mean distance between peaks tion may mask significant hidden harmonie detail
or the average distance between mean line crossings. which could play an important role in its later in-
The ACF is derived from the normalised auto- service application. Results from the FFT analysis of
covariance function (ACVF) - this being as follows: the profile (Figure31 b) reveal the differing sine wave
amplitudes necessary to generate the original
A ) _ ACVF(Lix) profile. In this case, the largest sine wave amplitude
ACF.ux
( - ( 2 equals a value of 0.7 mm, this being termed the
Rq)
"dominant wave".
where It should be emphasised that the information
obtained from the FFT analysis will be exactly the
irn same as that acquired by the auto-correlation
ACVF(Lix) = lim y(x) y(x + Lix) dx method, but obviously it is displayed in aaltered
Im-----7 OO f
0 form. Due to the isolation of the harmonics into
specific bands for a particular surface profile, FFT
where 1m = assessment length,y(x) = profile height can impart valuable understanding as to how the
at position x and Rq = rms parameter. production process might have been inftuenced
The ACF does not contain information about the by variables in processing for that product. For
amplitude of the profile, with its values ranging from example, the dominant harmonie in the FFT display
plus one - giving perfeet correlation - to negative for a profile might give a valuable insight into the
one - this having a correlation of the inverted but vibrational frequency for a specific machine tool.
shifted profile. Due to the fact that the ACF is inde- Knowledge of this vibrational effect on the resulting
pendent of the amplitude of the profile it is more surface profile may enable the attenuation of this
popular than the ACVF. In the case of an ACF having vibrational signature by judicious adjustment of
an isotropie (random) profile, it quickly decays to either cutting data, or specific maintenance to the
zero (Figure 30a), with the profile trace being of an machine tool to improve the subsequent surface
unrepetitive nature. Conversely, the tendency for a profile's condition.
trulyanisotropic (periodie) generated surface is that
it does not decay to zero, with Figure 30(c) illus-
trating some periodicity in its profile trace - indi-
cating that decay here is significantly less than that
for Figure 30(a). Despite the fact that both Figure
1.11 Appearance of peaks and
30(a) and (c) have similar Rz values, their respective valleys
ACF are distinctly different and can be used as a
means to discriminate between surfaces and indicate
whether they will fulfil the desired in-service appli- For many engineering and statistical graphs no
cations, which might not otherwise be apparent. intrinsic relationship exists between the plotted
measurement units; for example, when plotting the
rise in temperature of a heat treatment oven against
Fourier analysis (FFT) elapsed time the ordinates would be represented by
both degrees Celsius and ho urs - two quite dissim-
Any surface profile will normally be of some ilar units. As a consequence of these disparate units,
complexity, this being comprised of an array of acceptance of the shape of the graph is acknow-
differing waveforms that are superimposed onto one ledged, whatever scales are applied for the ordinates.
another. An actual profile's specific composition will It is quite different when dealing with a surface
be dependent on the shape and size of the wave- profile graph, where both the horizontal and vertical
forms existing within the profile; both their ampli- ordinates are represented by the same units (i.e.,
tude and frequency, termed "harmonics", can be length). At first introduction, it may be difficult to
established by the application of Fourier analysis. appreciate that due to the difference of scale the
The technique known as a "fast Fourier trans- graph will not instantaneously give an indication as
form" - FFT for short - enables one to establish a to the shape of the irregularities. Figure 32 illustrates
series of sine waves being generated from the surface the effect, with this disparity being one of the most
profile, and when combined together contribute to difficult factors in surface texture analysis to
the original profile. Individual harmonics represent comprehend.
a specific frequency-wavelength, in combination It is very important to note that although the
with their associated amplitude. visual profile's shape is distorted due to the applica-
The surface profile depicted in Figure 31(a) was tion of different horizontal and vertical magnifica-
selected to illustrate a periodic form, which in isola- tions, measurements scaled fram the graph are
(a) Profile
(11m )
10
-s
-10
(b) Wavelength
correct. Such effects can be visually demonstrated peaks and valleys on the profile graph, this can lead
with reference to the peak angles of the profile illus- to considerable confusion when visually assessing
trated in Figure 32, indicating how the profile shape the actual graph. However, the geometrie relation-
varies as horizontallvertieal magnification is altered. ship between angles on the graph and those that
Figure 32(III) verifies this fact, as the horizontal occur on the physical profile of the component
magnification of the surface profile is increased under test are more easily determined. As an
(Figure 32II), the length x-x expands to Xl_XI and example of this interpretation, Figure 33(a), on the
the peaks; A, B, C and D appear flaUer. Increasing profile graph, depicts a symmetrieal peak with an
the horizontal magnification still further - until included angle 2a. Figure 33(b) exhibits the corre-
it equals the vertical magnification (Figure 321) - sponding peak, on the actual surface, having an
expands the sampling length y-y to yl_yl. Once angle 2ß. The ratio of the angles is determined by
again, with this still higher magnification, the peaks
E and G and valleys Fand H now have a much flaUer tan ß Vv
appearance. A point worth making is that the actual tan a Vh
difference in respective heights of corresponding
peaks and valleys in I, II and III are identical. This ratio is strictly true for symmetrical peaks,
As a result of the spiky appearance of both the although it is only slightly different for asperities of
(I) x5000
f=J--------C=-I
(11)
f
x5000
~
j /
I
I j /
(III)
xl00
i-=----P-I je /D
~ / /
x5000
Figure 32. Diagram illustrating how profile shape varies as the horizontal magnifieation is redueed: (I) surfaee profile magnified x5000 equally
in all direetions; (11) profile with A Vv: Vh ratio of 5:1; (111) profile graph recorded with a Vv:Vh ratio of 50:1. ((ourtesy ofTaylor Hobson.)
(a) Peak on profile graph true for the major ridges for a surface exhibiting
marked directionallay (see Figure SA) being traced
at 90° to the direction of the dominant surface
pattern lay. Conversely, for a surface displaying ran-
dom textural influences, such as the "multi-direc-
tional" example in Figure 4, it is extremely unlikely
that a stylus's path will trace across the summit of
every peak. In these circumstances, some peaks and
valleys will be displaced from the path of the stylus
by varying distances, with the result that the stylus
will also traverse across many flanks. Stylus vertical
displacement, although somewhat less than the full
(b) Corresponding peak on the surface peak height or valley encountered, will moreover be
correct for the traced feature. Assumptions made by
many are that every peak on the graph is the summit
of a peak on the actual surface, but where random
surfaces occur there will be sufficient actual sum-
mits encountered to prevent any significant inaccu-
racy as a result.
Table 3. Peak angles (2ß, Figure 33a) on the surface corresponding to peak angles of 2a on the graph
100
80
60
50 ~
i-'
..- -
40
V
30 V
20
'j
~
~....
10
8
1
/
..Q 6 /
I
5 5
4 I
'"'
"0
<U 3 /
~
~
2
V
....
~ /
e
<U 1 /
~ 0.8 11
0.6 I
0.5
0.4 /
0.3
0.2 /
1 2 3 4 5 6 8 10 20 30 405060 80100 200
Ratio - Stylus tip radius: Actual Ra of surface
Figure 34. Error due to finite stylus tip radius, for a specific surface. (Courtesy of Taylor Hobson.)
Illustrative example: When measuring a surface of 0.5 I-lm Ra with a stylus tip of 5 I-lm (10:1 ratio) the display will be approximately 2% low.
If the stylus has double this radius (i.e., 10 I-lm) this error increases to 8%.
Surface texture: two-dimensional
Stylus data:
f';1easuring range (tJ-m) x
Tip Radius (fLm) x
Tip angle (0) x
Measuring force (mN) x
Skid data:
Skid radius,
longitudinal/traverse x
Distance skid-to-stylus,
longitudinal/traverse x
stylus
Tip angle (0) 60° ± 5° or 90° ± 5°
Figure 35. 90° conical stylus tip mechanically tracing across a
portion of a honed surface. SEM photomicrograph, X200 magnifica- Tip radius (fLm) 2± 1 5± 2 10 ± 3
tion. [Courtesy of PTß ßraunschweig/Feinpruf Perthen GmbH.] Static measuring force
(ie at electric zero, mN)
Stylus force on the surface must not be great Variation in static measuring
enough to deform or scratch the surface as this may force (mN/m) ~ 0.035 ~ 0.2 ~ 0.8
promote erroneous results. Conversely, the force
imparted by the stylus must be of a sufficient level Skid
to ensure that it maintains continuous contact with Distance from stylus dependent
upon pick-up design;
the surface at the desired traverse speed. This factor
is important in the design of the pick-up, with most Radius
(longitudinal, mm) 0.3 1.3 3 10 30 infinity
surface texture instruments having a stylus tip
(lateral, mm) depends upon design of pick-up
radius ofbetween 1 and 10 !-Lm. However, the greater
the radius of the tip, the larger the allowable force Surface roughness (tJ-m) ~ 0.1
that can bear on the surface. If a tip radius is small, Skid force (N) for:
say 0.1 !-Lm (Figure lla), then a very low force must Hard surface ~ 0.5
The conieal stylus geometry was previously men- Linearity of system (%) ±1
tioned in Section 1.4 and illustrated in Figure 10,
invariably having a 90° tip angle. In action (Figure
35), the conical tip angle of 90° can easily cope with
surface features such as that shown, having the materials such as sintered parts. One problem asso-
anisotropie profile of a honed surface. When surface ciated with the chisel-type stylus is the difficulty in
features become greater than 45 ° to the horizontal, or maintaining its attitude at right angles to the lay,
the valley is smaller than, say, 5 !-Lm, then the being more sensitive to error from peaks rather than
mechanieal motion of the tip becomes to some ex- valleys. Stylus misalignment can be minimised by
tent distorted, as illustrated in Figure 11 (c). Specific- the application of "smart parameters" that mathe-
ally, under these conditions, the tip acts in a similar matically ignore certain features. NormaUy, it is
fashion to a low-pass filter with high-frequency fea- recommended to utilise a conventional stylus geom-
tures not being recorded. With a tip angle of 90°, this etry, unless particular problems are encountered
means that the stylus will foul any peak or valley that may cause the standard stylus to impair the
having an included angle of less than 45° - which validity of the resulting data.
may at first seem a considerable limitation, but in Manufacturers of stylus/skid geometries norm-
reality does not cause too much of a problem. aUy apply identifying marks on the piek-up, or at the
Chisel-edge styli (see Figure lla) are a practical very least on its accompanying transportation case.
variation on the cone-shaped stylus (Figure 35), Table 4(a) illustrates the piek-up markings, whereas
being particularly successful at entering porous Table 4(b) highlights the standard configurations.
InClustrial metrology , .
Carrier
IV\,
(i) ariablc induclancc (ii) Schcmatic diagram 01" a modul ~ltc carricr systcm
Magn.'
Slyfus
(i) Picl.O·clcctric pick-up (ii) Moving·coil pick-u!,
Figure 36. Basic design elements of pick-ups of the analogue transducer configuration. ((ourtesy of Taylor Hobson.)
that when the armature is centrally positioned acteristics. The silicone fluid exhibits low stiffness
between the bridge it is balanced, giving no output. and at lower frequencies; therefore large but slow
Movement of the armature unbalances the bridge, stylus displacements allow free movement of the far
providing an output proportional to its displace- end of the crystal, hence no bending occurs and zero
ment; the relative phase of the signal depends on the output is generated. At higher frequencies the fluid
direction of movement. This signal is amplified and stiffness increases, effectively preventing the local
compared with that of the oscillator, to determine in end of the piezoelectric crystal from moving; there-
which direction it has moved from the central (zero) fore the bridge deforms generating an output.
position. It is necessary to utilise an oscillator to A piezoelectric device is a position-sensitive
produce a constant AC output, because the pick-up device. A voltage on the electrodes persists while the
- unlike a motion-sensitive pick-up (Figure 36b) - element is deformed (providing no current is drawn
does not generate any output; it merely serves to from it), due to practical considerations such as
modify the carrier. Simultaneously, the knife edges finite input impedance of the amplifier and cable
exert light pressure from a very weak spring acting losses. These considerations ensure that it can only
on the beam, enabling subsequent stylus contact be utilised in the motion-sensitive mode.
with the surface under test. The ligaments prevent The moving-coil transducer pick-up (Figure 36bii)
unwanted motion of the beam in the horizontal operates on the same principle as a DC generator or
plane, with the result that stylus movement is only an electric dynamo. In operation, as the stylus
possible normal to the surface being assessed. motion occurs the coil moves inside a permanent
This type of pick-up is also fitted to newer ver- magnet, inducing a voltage in the coil. This voltage
sions of measuring instruments, particularly where is proportional to the velo city of the coil. This design
the range-to-resolution ratio has increased from allows the transducer element (the coil) to be
around 1000 to 64,000. Improvements in electronics coupled directly to the stylus without the need for
for the latest pick-up designs of this type have obvi- an extended arm or hinged beam. Because of its
ated the need for reliance on a skid, meaning that overall size it is somewhat restrictive in use and is
precise pivot bearings have replaced the knife-edge not generally popular today.
pivots. In a similar fashion to the piezoelectric trans-
The piezoelectric pick-up (Figure 36b) has been ducer, the moving-coil pick-up does not measure
widely used in the past, but now it tends to be used displacement, but velo city. Stylus velo city has to be
for the less sophisticated hand-held measuring integrated in order that the absolute position of the
instruments. When the stylus deforms the piezo- stylus can be determined. As a result of the coil
electric crystal, it has the property of developing velo city rather than measurement of stylus displace-
a voltage across electrodes, the advantage being that ment, integration errors will increase as the signal
it is virtually instantaneous. As the stylus follows frequencies decrease. Hence, this type of pick-up is
the contours of the surface, the piezoelectric crystal unsuitable for the measurement of either profile or
distorts by bending a flexure that causes crystal waviness (low characteristic frequencies). Therefore
compression and it becomes charged. The resulting the piezoelectric transducer is only suitable for the
charge is then amplified and electronically inte- assessment of roughness. Yet another disadvantage
grated, producing signals proportional to the surface of the moving coil transducer is its poor linearity. It
profile. A piezoelectric transducer exerts a propor- should only be used in the form of a comparator by
tionally larger stylus force to that of an equivalent comparing similar component surface roughnesses
inductive transducer, with the former pick-up poss- against a known roughness calibration standard.
ibly damaging softer and more delicate surfaces.
The operating mechanism of this piezoelectric 2. Digital transducers (Figure 37)
transducer can be described in the following With stylus motion along the surface under test,
mann er: the flexible ligament interposed between pulses occur that correspond to multiples of the
the stylus arm and the piezoelectric element has transducer resolution which are fed to an up-down
enough stiffness to transmit normal vertical motion electronic counter that displays the gauge displace-
of the stylus to the crystal, but will flex as the stylus ment, with its range being determined by physical
is suddenly subjected to instantaneous shock and in constraints of the gauge. Typical range-to-resolution
this way protection of the somewhat fragile piezo- ratios are of the order of 700,000, hence the advan-
electric element is achieved. A light spring force tage is that there is no need for range switching,
provides downward force on the stylus, keeping it in enabling the maximum resolution to be available
contact with the surface. A small drop of silicone oil over the complete operational pick-up range. The
is held by capillary force between the seeuring block displayed displacement is relative to the stylus posi-
and a thin metal blade fastened to the re ar of the tion, where the counter is zeroed. This means that
housing, giving the pick-up suitable dynamic char- every time the electronics are switched off and on
Industrial metrology , .
beam splitter
slI rfacc 1I.n d er t t
r
\
LASER DIODE
STYLUS ARM & COLLIMATOR
CONVEX DETECTORS
DIFFRACTION
SPRING GRATING
Figure 37. Basic design elements of pick-ups of the digital transducer configuration.
again, the counter must be zeroed at a particular the measurement reference. Interference patterns
datum position. In a similar mann er, if a certain are detected by multiple photodiodes, enabling
maximum stylus speed has been exceeded the an output signal to be interpolated, typically
counter may lose count, requiring zeroing again at giving a basic resolution of 10 nm with an oper-
the datum position. ating range of around 6 mm. A focal point of 2
The following pick-ups are typical of those f.Lm is typical, allowing soft or delicate surfaces to
currently in general use for surface texture instru- be assessed.
mentation: • Phase grating interferometric (Figure 37b). This
pick-up has been developed to complement the
• Non-contact laser (Figure 37a): These optical laser interferometric type of pick-up as it offers
configurations vary depending upon the meas- a greater range, with a corresponding reduction
uring instrument company, but most systems in physical size, by employing a laser diode
utilise a miniature Michelson laser interferometer instead of agas (HeNe) laser source.
with a laser wavelength of 632.8 nm to provide
The non-contact laser pick-up (Figure 37a) oper- The geometry of a skid can vary, from either a
ates on the following principle: infra-red light is large radius (Figure 38b) to a flat (Figure 38c). The
emitted by a laser diode; its path through the optical skid supports the pick-up, which in turn rests on the
system to the micro-objective is shown in Figure surface. The relative motion of the pick-up as it
37(a), with the beam being focused onto the surface traverses along the workpiece causes the skid to act
to a focal point of 2 fLm diameter. Light is reflected as a datum, giving rise to a "floating action" of rising
back by the workpiece surface, returning along an and falling of the pick-up (Figure 38b). The macro-
identical path, later being deflected onto a detector, irregularities of the surface, namely of waviness and
whereupon an electrical output is generated that profile, means that the stylus with its significantly
corresponds to the distance between the focal point smaller radius to that of the skid will follow this
and the surface feature. A powerful linear motor surface topography, sinking into valleys that the skid
continuously readjusts the hinged measuring lever bridges. However, if the crests and valleys in the
during the measuring cyde, enabling the focal point workpiece surface are too widely spaced, then this
to coincide with the surface feature(s) being distance with respect to the skid motion (Figure 38a)
measured. The focus follows the surface as its will also cause the skid to rise and fall and thereby
motion translates across that portion of workpiece lose the datum registration plane (Figure 38a). If the
under test, in a similar fashion to a stylus-based distance between the stylus tip and the skid (Figure
pick-up. The vertical movements of the measuring 38a) is half the waviness spacing, then these wavi-
lever are converted into electrical signals by an ness amplitudes are doubled. Conversely, when the
inductive transducer. Due to the relatively small size distance of the stylus tip (Figure 38a) corresponds
of the point of focus (approximately 2 fLm), quite exactly to that of the waviness spacing, then the
minute profile irregularities can be assessed. waviness is mechanically eliminated. The skid type
Some caution should be expressed in general of pick-up is only marginally affected by instrument
about non-contact pick-ups, as the surface features vibration, because the measurement reference is
being assessed can have a tendency to act as situated dose to the point of measurement. There-
secondary sources of light. When the radius of fore, the mechanical relationship of the pick-up-to-
curvature of a part feature is smaller than 10 fLm, skid system may be an important factor in its design.
diffraction effects appear which can affect the If different pick-ups are utilised for the same
beam's edge. This is not a serious problem for large measuring task, then in extreme situations these
surface features but becomes crucial for finer surface measured differences could approach that of 100%.
finish es, illustrating why optical instruments te nd to Ideally, the skid and stylus should be coincident,
produce higher values for surface texture than their thereby eliminating the "Abbe error"; the Abbe prin-
stylus-based equivalents. Other limitations for non- ciple states that the line of measurement and the
contact pick-ups are that they cannot easily measure measuring plane should be coincident. For practical
small bores, they traverse widely changing surface reasons, the stylus is slightly displaced from the skid
features, and they cannot "sweep aside" dirt on the and is situated either in front or behind the stylus.
surface, unlike stylus instruments. Phasing errors can be induced by the skid (Figure
The phase grating interferometric pick-up 38b), causing distortion of the graphical trace, while
(Figure 37b) has positioned on the end of the arm its magnitude depends on the waviness crest
of the pivoted stylus a curved phase grating, which spacing. In practice, if the waviness crest spacing is
is the moving element in the interferometer. The identical to that of the skid/stylus spacing, the skid
pitch (grating wavelength) provides the measure- will rise on one crest, with the stylus rising on an
ment reference. An interference pattern is detected adjacent peak. This relative motion completely
by four photodiodes, enabling the output signal to suppresses the peak. When the spacings differ, the
be measured, giving a basic resolution of 12.8 nm effect illustrated in Figure 38(b) occurs, where a
with a range of 10 mm - ensuring that it is a useful spurious valley is introduced into the graph at a
pick-up for form measurement. distance from the peak, this being equal to the
skid/stylus spacing. If two skids are used on either
side of the stylus, then the "phase effect" of the single
skid/stylus spacing is diminished. In some pick-ups
1.12.2 Skid or pick-up operation the line of contact of the skid is laterally offset, which
prevents the skid from burnishing the track
Two types of pick-up operation are normally (mechanically deforming asperities and giving a
employed for surface texture assessment: false reading) during repeated traverses; this is
particularly relevant when the instrument is auto-
• with a skid; matically setting the vertical magnification (auto-
• skidless with a reference plane. ranging).
InClustrial metrology , .
Skidmotion
=::::> Motion
=::::> 1I'lotion
Trace
Skid Illotion
0l>tical nat
Figure 38. Configuration of surfaee texture instrument and relative motion of the stylus with respeet to an independent datum. (Courtesy of
Taylor Hobson.)
Surface texture: two-dimensional
Form analysis
The introduction of wide-gauge ranges on high-
resolution pick-ups and the development of various
form options (reference line fitting) has meant that
guidance of the pick-up along a curved path has
been virtually eliminated. Typical of these surface
form-fitting features that are currendy available are
the following software-based options:
Pick-up traverse
---c:::o-
Stylus
(c) Side skid gauge - the stylus projects through the cylindrical form of the skid
Figure 42. Screen displays of ''Windows™-based'' software options available forform assessment. ((ourtesy ofTaylor Hobson,)
• complex symmetrical profile assessment - VIa eomprehensive list ean be enhaneed still further. In
an enhaneed "Dual Profile" faeility, allows the addition to a full range of surfaee texture parame-
measurement profile of a master shape or proto- ters, form analysis software ean provide:
type eomponent to be saved as a template, en-
abling future eomponents to be measured and • form error - ealculation with referenee to best-fit
simultaneously displayed along with template eoneave or eonvex cireular are, straight line
data for immediate eomparison (see Figure 42e); measurement, including surfaee roughness detail.
• analysis of gothic areh profiles - frequently em- Alternatively, referencing to the minimum zone,
ployed on the ball traeks for recireulating ball- this being the minimum separation between two
serews; parallellines eontaining the data set;
• three-dimensional eontour analysis - a represen- • radius - using the least-squares best-fit, coneave
tative 3D visualisation of the part surfaee: axono- or eonvex cireular ares ean be automatieally
metrie projeetion, eolour height distribution, ealculated from seleeted data, with the option of
wear simulation and form rem oval, with many being able to exclude any unwanted surfaee
additional features available (this topie is a features from the seleeted data. Conversely, the
subjeet on its own and diseussed in Chapter 2). absolute radius ean be set to analyse aetual devi-
ations from a design master, with other ealculated
The number of surfaee texture parameters avail- parameters including its eentre eoordinate and
able to define a surfaee's eondition is immense for the piteh;
form-measuring instruments. Typieally, these para- • angle - using a straight edge or minimum zone
meters include 22 profile; 22 waviness; 25 rough- algorithm, surfaee tilt ean be established and then
ness; 12 R+W; 9 aspherie parameters; and this removed, prior to parameter analysis, with other
u ace texture: two- Imenslona
calculated values including its intercept and • comparison of DFX files to the contour - if
pitch; measuring a known contour "best-fit" individual
• dimension - the linear relationship of surface geometrie elements are calculated with reference
features can be assessed and then compared, to a template and the comparison of each point
owing to the ability to calculate both the true in the contour is assessed against the nearest
X- and Z-coordinate positions. element in this template;
• geometrie element fit to an unknown eontour -
when measuring components of an unknown
Contours: profile curving, or an irregular- contour, the software finds geometrie elements
shaped figure that optimise the geometry of the profile
determining the size, position and relationship
A typical commercial system is currently available between profile features, plus other functional
for the analysis of contour measurement; assessment factors.
of features such as radii, angles, length and height
(see Figure 43 for a typical application) can be The most re cent form and surface texture
achieved with: analysis equipment has absolute positional control,
offering sophisticated high-technology instruments
• measurement maeros - these can be learnt and providing complex analytical abilities in a single
edited forming user programs for repeated traverse of the workpiece. Lately, with the high
inspection routines, which minimise repetitive thermal stability of the pick-up gauge (phase grating
operator input (achieved via aseries of definable interferometer - PGI), it typically has a large range
"fastkeys"); with around nanometric resolution, equating to a
• individual feature tolerancing - allowing indi- range-to-resolution of 780,000:1. One of the current
vidual seetions of the measurement template to developments in stylus proteetion employs a "snap-
be toleranced with a variety of values (a wide off" connector, allowing the stylus to be ejected from
tolerance on a Hat area of a surface can be the gauge if the loading stylus force exceeds safe
defined, with tighter tolerancing to the radii); limits - reducing possible damage to the gauge
because of operator error. Interchangeable styli can
be fitted to such pick-ups, for better access to the
component feature being inspected. If the part is of
a delicate nature and liable to deform, or could be
easily scratched, then non-contact gauge heads can
be utilised. These non-contacting types of gauges
comprise a focus follower with a programmable
controller for fast, simple use, replacing inductive
pick-ups. Non-contact gauges are used where the
component surface applications consist of:
beam
Specimen
over
sampIe
port
Output
port
/ ~ B,m,
Detector Photodetector
port
E~~~ ~~_
D
__
Inclined reflector
(optical) plate
As has already been mentioned, light interference cause phase changes in the light being reflected back
can be successfully used as a non-contact optical to the observer. The result of this reflection will be
technique to assess surface features. Essentially, the to promote alternate dark and light interference
principle of interference of light relates to how light fringes. The shape and spacing of these fringes will
rays are reflected between two surfaces; the differing depend on the regularity of both the surface and the
light path lengths along various points of the surface reference reflector. The surface texture irregularities
are reproduced as modifications in the interference may be slightly inclined to the work surface I, allow-
pattern and, when viewed under specific conditions, ing a wedge-shaped air gap to occur (detailed in
displacement of the fringes is a measure of the Figure 46b). Multiple reflections between the surface
roughness height. and the reflecting plate produce good-contrast,
For some interferometer instruments such as the sharp fringes (see Figure 47 for typical interfero-
Fizeau type, interferometric surface assessment metric images) wh ich are viewed in the eyepiece.
relies on the fact that a "wedge of air" occurs on the Utilising a spherical semi -reflecting surface, it is pos-
test surface, with the resulting interference lines sible to examine three-dimensional curved surfaces,
being of equal height and their respective height such as precision ball surface finishes (Figure 47c).
differences given by Multiple re fleet ion (Figure 46a) on the semi-silvered
surface E and the workpiece I means that all on-
Fringe spacing = Al2 coming beams are split into several partial beams,
which cause interference. Interference fringes that
where A = wavelength. occur are both higher in co nt rast and narrower as
Under examination, the surface roughness the reflection coefficient becomes greater. If too
produces air wedge thickness variations causing great a reflection coefficient occurs, the co nt rast will
deflection of the interference fringe, from which the degrade. Such conditions allow multiple beam reflec-
total height parameter Rt results. Hence the total tion to occur only when the distance to the reflection
height becomes surface and that of its test surface is quite small.
Large apertures can be utilised by this Fizeau
Rt= aIA(Al2) surface interferometer, enabling full exploitation of
the light microseope. When employing high aper-
where A = interference fringe, a = fringe deflection tures, the line standard (graduated scale) is depen-
and Al2 = fringe spacing. dent on the selected aperture and, considering the
The height of irregularities that can be resolved associated aperture angle, the fringe spacing is
range from 0.005 to 1 f.1m using conventional inter-
ferometric methods. The range can be extended by Fringe spacing = A/2 (2/1 + cos fL)
using the technique of oblique incidence, which
increases fringe spacings from Al2 to 2A, enabling where A is the wavelength, fL is a eosine error.
one to measure a surface roughness height four times Normally, the largest aperture (A) utilised is 0.65,
larger than that measured using a standard interfer- hence the fringe spacing equation above can be
ometric method. Furthermore, if cast replicas of the simplified to
test surface are made, then immersing them in fluids
of a suitable refractive index enables transmission Fringe spacing = 1.14A12
interferometry to assess roughnesses up to 25 f.1m.
Maximum contrast is important for optical inter- Generally, it can be said that applications of this
ferometry, and the wavelength of emitted light must particular Fizeau surface texture interferometer
remain constant to eliminate variations in the phase have limited use, although the technique does have
difference between interfering beams. Any defects in some merit:
optical surface quality within the interferometer can
promote areduction in fringe contrast, as can vibra- • it can examine a relatively large specimen surface
tions of optical components, together with parasitic area;
light caused by unwanted reflections. Due to the • it indicates any form error present;
strongly convergent light utilised in these interfero- • being a non-contact method, it may be possible
metric optical configurations (Linnick and Mirau to estimate the scratch depths.
interferometers), this can lead to obliquity effects,
which can introduce errors in estimation of, say, a An optical and practical limitation of this type of
scratch depth by as much as 12%. The magnitude of interferometry when applied to precision surfaces
error is dependent on the numerical aperture of the occurs due to visual viewing, which tends to be time-
objective and the surface's scratch depths. However, in consuming and somewhat fatiguing. By using auto-
the case of more commonly available full field tech- mated image analysis techniques for detection, this
niques this obliquity and hence error is not a problem. limitation could be overcome, but at a considerable
In essen ce, the Fizeau surface texture interfero- cost dis advantage to the user.
meter is basically a microseope, with a built-in Although three-dimensional surface texture
illumination and special-purpose optical system analysis will be discussed in Chapter 2, one instru-
(see Figure 46a). Between the objective and the mental technique has been included in this chapter.
surface a semi-reflector G can be positioned, which An automated surface profiling interferometer is
u ace texture: two- Imenslona
Use ofspeckle
(c)
(i) (ii) • (iii)
(h)
(a)
(e)
Figure 48. Automated non-contact three-dimensional surface profiling interferometer. (Courtesy of Zygo Corporation.) (a) Optical configura-
tion. (b) View of interferometer. (c) Typical screen displays.
u ace texture: two- Imenslona
(a) Optieal path of SehmaItz microseope (b) Optieal sectioning images, projeeted onto a sereen:
-
Eyc
• I. _............. t'r.~..... ,••
._ ~
I
I
the image plane, and secondly, dose to the diffraction Cusp height = h x -)2
or defocus plane. Yet another technique utilises the
polychromatic speckle patterns, while others employ where h is the actual profile height (Rt).
the correlation properties of two speckle patterns. Measurements are normally undertaken using
From both of these methods, surface texture values either an eyepiece gratide or an eyepiece incorpo-
ranging from 0.01 to 25 /-Lm have been estimated. rating a micrometer for topographical feature
assessment.
An alternative technique for optical sectioning
Optical sectioning can be achieved by utilising an optical projector, as
this has the added advantage of an enlarged image
The method of optical sectioning termed the being projected onto a screen. The surface's profile
Schmaltz technique after its inventor (sometimes height can then be quickly measured with a specially
termed the light section microscope) pro duces virtu- prepared and calibrated template, which compen-
ally identical results to that of physical sectioning, sates for any distortion introduced by the viewing
but in a simpler, non-destructive manner. However, angle.
the magnification and data obtainable from the The optical sectioning technique is suitable for
projected image are quite limited, when compared surface topographies having a roughness range of Rt
with stylus-based surface texture measuring instru- between > 1 and 200 /-Lm. Moreover, it is eminently
ments. The ratio of vertical to horizontal magnifica- suitable for the inspection of soft and slightly pliable
tion is around unity, meaning that the field of view surfaces (Figure 49biii, which could be deformed by
is small when a large magnification (x400) is used, a stylus), or for estimation of depths of surface
hence for fine surfaces it is rather limited. scratches/engraved lines (Figure 49bii).
The optical sectioning principle is illustrated in The reftectance of a surface is a "sensitive func-
Figure 49(a). The surface to be examined is illumi- tion" of its relative roughness, and consequently the
nated by a thin band of light delineating a profile wavelength of light is considerably greater than
section, which is then viewed at an angle with a the root mean square value of the surface tex-
microscope. Typically, illumination and viewing ture. Hence, the reftectance will depend only on the
angles are 45° to the work surface producing the surface roughness rather than the peak slope of any
dearest profiles (see Figure 49b). For example, the irregularities. Measuring reftectance at two distinct
projected surface indicated in Figure 49(bi) illus- wavelengths enables one to determine the surface
trates an apparent machined profile cusp height of roughness and slope of asperities (peaks).
%10O't/P
X14
XI0
4
3
L_
2
.' ...-/
1
-1
-2
Figure SO. Performance curves for the Schmaltz - optical sectioning - microscope, illustrating the relative error of indication for various micro-
scopes. [After Thomas, 1974.]
Performance tests undertaken for the Schmaltz x30 objective - with the added advantages of a larger
(optical sectioning) microscope (illustrated in field of view and depth of focus. In the case of the
Figure 50) show that for an objective of x60 magni- x30 objective, the relative error of indication does
fication the relative error of indication does not not exceed 8.6%. Now, if one enlarges its measuring
exceed 7.7% over the whole application range (Rt range (1.5-10 /-lm), up to values of Rtof 1.5-14.5 /-lm,
values between 0.8 and 3.0 /-lm). Accepting that prac- a practical accuracy of ±9% may be obtained. The
tical accuracy limits are in the region of 9%, then objective having a magnification of x14 has a rela-
there is little point in using a x60 objective, since tive error of indication within the recommended
the necessary accuracy can be achieved with the manufacturer's guidelines, namely, from 3 to 12 /-lm,
u ace texture: two- Imenslona
Optical Fibre
I~,--C-C-D-LA-rr-a-y--',~
Je::::::: / ;;;1
I Ä-' \
1\ Foc~sing ~+
~----8
;' " Ophcs ~ , Figure 53. Assessment of surface texture on a diamond-turned
~
I
I
I
I
0:--
~ -=-::::.:P
I
=> I
component, within the range 5-10 nm Rq, utilising a non-contact
optical instrument. ((ourtesy ofTaylor Hobson.)
I I I I
, , Beam I I
: : Splitter \ i
I ' I eomponents that might be inspected with this
~~~~: :~:~~:::::---~+- :!
instrument include diamond-machined brass (Naval
non-Ieaded type), aluminium (grade: 6061 T6) and
copper (OFHC) flats, germanium flats or similar
I I
Mirror I1 I 1 precision surfaces.
1
Cylindrical Lens 'i I :1 One of the principal reasons for utilising laser-
[
Filter
----...""'r:z:;:I IN based diffraetion techniques is their ability to ehar-
I I1
11
'I
, acterise low Rq surfaces, in particular the advantages
I- - - - - - - - - - -- - - -- - - II- - - r - - -
~ I
obtained from directly filtering the diffraction
samPle ~ pattern. Moreover, this instrument has the capability
of measuring a substantially periodic surfaee to an
Rq of approximately 140 nm. In addition, measure-
Figure 52. Schematic representation of the Talyfine instrument. ments of Rq on a rotating surfaee can be achieved
((ourtesy of Taylor Hobson.) with no distinetion between whether the surface is in
motion or statie (unlike a stylus-based instrument).
• to act as a spatial filter, by selectively transmitting The surface diffraction physics is rather complex
the Gaussian TEM 00 mode; and is therefore beyond the scope of the current
• providing a eonvenient method for the produe- discussion on the general operational and perform-
tion of spatially coincident wavefronts. ance characteristics of this laser-based instrument.
Op"ca' pa.h
d'.gtlm 0' CF
..
In'lnlfy Correclecl
Ophel l Sy'lem
Tube lens
Adjus'able
!
~
GI
R
._.
E Analyzer. OIe
mmOf bkx::k
~
:5 OtCpnsm
Objee1rve
P,nhOle
apenu'e
doaphrag
,mage
(ex,' pu ptI)
L--.._ .........-J
INSPECTION MODES
Figure 54. Microscope applications for surface assessment. ((ourtesy of Nikon UK Ltd.)
Industrial metrology , .
Confocal microscope
Confocal microscopes gene rally utilise the principle
Harne of depth discrimination. Essentially, the imaging
and receiving optics are identical, offering excellent
properties. In a similar manner to the so-called
"flying spot technique", the optics project a point
onto the surface, with the reflected light being picked
up by a point detector (see Figure 56). The resulting
Source ~ signal is utilised to modulate the spot brightness on
Dichroie the CRT screen, which is scanned in synchronisa-
tion with the object under test. Essentially, the lens
focuses a diffraction-limited spot onto the object,
with the lens collecting light only from the same
vicinity of the surface that was previously illumi-
nated. As a consequence of employing the single-
point detector, both the image forminglreceiving
systems contribute to the signal at the detector.
Thus, by rotating the variable aperture over the spec-
imen, which itself in some systems rotates, it will
Collimaling
build up an optical image (via software data capture)
lens
A
of the sample's surface. By this means, the "flying
spot" covers the complete specimen's surface to the
same optical magnification and resolution of a
conventional microscope, but with the advantage of
"
a significant improvement of the field of view. These
',. images can be optical slices or sections through the
" ' I>ecimen
sm'face surface, which can be processed providing non-
contact three-dimensional information about the
Figure 56. Schematic diagram of an optical profiler. ((ourtesy of Dr surface.
R. Leach/NPL.)
Trace
Silver deposit
Glass substrate
Figure 57. A typical "Talystep" graph of silver deposit on a glass substrate. Thickness of the deposit is approximately 0.03 f.lm. (Courtesy of
Taylor Hobson.)
Figure 58. Constructional detail of the "Nanostep" and its associated Figure 59. Detail of the interchangeable "Nanostep" stylus.
precision slideway in low coefficient of expansion (Le., glass ceramic: (Courtesy ofTaylor Hobson.)
"Zerodur"). (Courtesy of Taylor Hobson.)
table, which in turn is mounted on a carriage. This ment, producing ultra -low instrument noise down to
carriage is equipped with kinematically positioned 0.03 nm under optimum conditions. The motor can
dry polymerie pads, forming an interface with a drive the micrometer at measurement speeds vary-
highly polished precision slideway, giving a linear ing from 0.005 to 0.5 mm/s. The stylus/transducer
translational motion of 50 mm. The horizontal assembly illustrated in Figure 60 can be vertically
micrometer (shown in Figure 58) displaces (via a positioned on the workpiece and in contact with it
"slave carriage") the slideway along its desired via the vertical micrometer (depicted in Figure 58),
length of travel, providing minimal disruption to the giving a vertical step height range up to 20 ILm.
measurement process.Anti-vibration mounts isolate Finally, measurement control and signal output are
the DC motor/gearbox that drives the micrometer provided by a suitably configured Pe.
from the main structural elements of the instru- The software offers various levels of surface
Surface texture: two-dimensional
",:."
'" ' ~~------~----~--r---~~
Thbe
" ',',
:.'. . ...... .
" ..
.. : "
..
'.'
,' , .. ' "',' , ,, "
',.
....
.':'. : "':"
.' '. . . . .. ' '
,','
Dialllond stylus
\---/
Rollers I
" /
Material:
Transduccr stern G lass cerulllic
Leaf s pring
\ luminium alloy
X) Invar
~.~
Stylus holder
/ tylus as cmbly "howing kincmatic IOClltion.
Vicw in dircction X - X
Figure 60. Internal construction of the "Nanostep" instrurnent. ((ourtesy ofTaylor Hobson,)
texture analysis, assessed relative to the best-fit or least-squares are) and then removed, enabling
referenee line, eovering a diverse range of inter- the texture of the surfaee to be analysed;
national parameters. Additionally, the form software • angle - providing a faeility to remove any eom-
provides for pound surfaee tilt prior to parameter analysis;
• dimension - provides for the linear relationship
• form removal - best-fit form is ealculated (least- of surfaee features, whieh ean be assessed and
squares straight line, minimum-zone straight line eompared.
Software has also been developed for this instru-
ment enabling it to assess an enhanced dual profile.
References
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a "master component", which can then be saved as Journal and conference papers
a template; any subsequent components can then
be both measured and simultaneously displayed Bell, T. Surface engineering: past, present and future. Surface
with this template for immediate comparison. A Engineering 6(1),1990,31-40.
statistical process control software package can be Bjuggren, M., Krummenacher, 1. and Mattsson, 1. Noncontact
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packages. 1997,33-45.
A number of interchangeable styli (see Figure 59) Bousefield, B. and Bousefield, T. Progress towards a metallography
can be fitted to the instrument to suit a range of standard. Metals and Materials March 1990,146-148.
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filometry. Sensor Review January 1990,35-37.
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Proceedings 0fSPIE-1009, 1989, 14-17.
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Garratt, J. and Bottomly, S.c. Technology transfer in the develop-
stylus when repositioning or changing sampies. For ment of a nanotopographic instrument. Nanotechnology 1,
the measurement of ultra-fine surfaces, the instru- 1990,38-43.
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Gee, M.G. and McCormick, N.J. The application of confocal scan-
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Hongai, Z., Zhixiang, C. and Riyao, C. The control of roughness
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• ultra-precision bearing and surface defect meas- Leach, R.K. Measurement of a correction for the phase change on
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• integrated circuit production - process monitor- Leach, R.K. Traceable measurement of surface texture at the
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Prostrednik, D. and Osanna, P.H. The Abbott curve: weil known in
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measurement of surface topography. Precision Engineering 3, 1997.
1981,63-83. Dyson, J. Interferometry as a Measuring Tool. Machinery Pub. Co.,
Westburg, J. Opportunities and problems when standardising and 1970.
implementing surface structure parameters in industry. Inter- Gayler, J.F. W. and Shotbolt, C.R. Metrology for Engineers. Cassell,
national Journal of Machine Tools and Manufacture 38(5-6), 1990.
1998,413-416. Haycocks, J.A. Nove/ Probes for Surface Texture Metrology. NPL
Whitehouse, D.J. Some ultimate limits on the measurement of Report MOM105, July 1991.
surfaces using stylus techniques. Measurement and Control 8, Hume, K.J. Engineering Metrology. Macdonald, 1970.
1975, 147-15l. Hume, K.J. A History of Engineering Metrology. Mechanical
Whitehouse, D.J. Beta functions for surface topology? Annals of the Engineering Pub., 1980.
CIRP27,1978,491-497. Leach, R.K. NPL Good Practice Guide No. 37, Measurement of
Whitehouse, D.J. Surfaces: a link between manufacture and func- Surface Texture using Stylus Instruments. NPL, 2001
tion. Proceedings of IMechE 192, 1978, 179-187. Leach, R.K. and Hart, A. Investigation into the Shape of Diamond
Whitehouse, D.J. Conditioning of the manufacturing process using Styli used for Surface Texture Assessment. NPL Report CBTLM
surface finish. Proceedings of the Third Lamdamap Conference, 10, April 200 l.
Mainsah, E., Greenwood, J.A. and Chetwynd, D.G. Metrology and
Computational Mechanics July 1997, 3-20.
Properties ofEngineering Surfaces. Kluwer Academic Pub., 200 l.
Whitehouse, D.J. Some theoretical aspects of surface peak para-
Mummery, L. Surface Texture Analysis: The Handbook. Hommel-
meters. Precision Engineering 23, 1999,94-102.
werke GmbH, 1990.
Whitehouse, D.J. Surface measurement fidelity. Proceedings of the Nicolls, M.O. The Measurement of Surface Finish. DeBeers
Fourth Lamdamap Conference, University ofNorthumbria, WIT Technical Service Centre, DeBeers Industrial Diamond Divi-
Press, July 1999,267-276. sion, Charters, UK, 1980.
Whitehouse, D.J. Characterizing the machined surface condition Reason, R.E. The Measurement of Surface Texture. Cleaver-Hume
by appropriate parameters. Proceedings of the Third Industrial Press, 1960.
Tooling Conference, Southampton Institute, Molyneux Press, Sander, M. A Practical Guide to the Assessment of Surface Texture.
September 1999,8-31. Feinpruf GmbH, 1991.
Wyant, J.C. Computerized interferometric measurement of sur- Stover, J.c. Optical Scattering. McGraw-Hill, 1990.
face microstructure. Proceedings of SPIE-2576, 1995, 122-130. Thomas, G.G. Engineering Metrology. Butterworths, 1974.
Zahwi, S. and Mekawi,A.M. Some effects of stylus force on scratch- Thomas, T.R. Rough Surfaces. Imperial College Press, 1999.
ing surfaces. Eighth International Conference on Metrology and Whitehouse, D.J. and Reason, R.E. The Equation of the Mean Line
Properties of Engineering Surfaces, University of Huddersfield, ofSurface Texture Found by an Electric Wave Filter. Rank Taylor
26-28 April 2000. Hobson Pub., 1965.
Whitehouse, D.J. Handbook of Surface Metrology. Institute of
Physics, Bristol and Philadelphia, 1994.
Whitehouse, D.J. Surfaces and their Measurement. Hermes Penton
Science, 1991.
Williams, D.C. Optical Methods in Engineering Metrology.
Chapman & Hall, 1993.
Surface texture:
three-dimensional
69
Stylus
Stylus pivot tip
z
Surface
Bearings
Photodiode Hairspring
Optical shutter fin
(c) One of the compound flexure spring mechanisms, showing position of sensor and actuator
used in feedback control system
Flexu re spring c1amp
A
Electromagnetic
- ---, .-- J
actuator \ Flexure spring
-----, r==-=l ~f
LED -
/--
-n tr]::~
I-- - Flag
Ph otodiode
Optical position
- I-- --r --
Figure 61. Conventional stylus, with a comparison to the high-speed variety general arrangement fitted to a "Talystep" instrument. (Courtesy
ofTaylor Hobson.)
As a consequence, this now allows a shorter, light- separation of the average peaks. Ihe formation of
weight stylus to be fitted, which ensures that any the artificial two-dimensional envelope curve is
mechanical resonances in the stylus arm are at a obtained by shifting down the loci of circle centres by
high frequency and as a result do not unduly a linear distance equal to its radius (illustrated
compromise its performance. in Figure 62a). With the latest development of this E-
Ihe arrangement of the scanner, which is based system technique, both the computational time and
on aprecision compound flexure spring (Figure 61c) ensuing processing speed have been considerably
allows the stylus gauge to be rapidly and precisely enhanced by previously identifying prominent
moved across a surface in two orthogonal directions. peaks.
Being of compact design, this has the benefit of Ihe three-dimensional envelope system is simply
ensuring that the measuring head is both robust an extension of that for two-dimensions (see Figure
and portable, being ideally suited for industrial 62b), with the envelope surface resulting from
applications. Furthermore, the instrument's higher shifting down the radial distance of the locus of the
sampling rates ensure that three-dimensional spatial sphere's centre as it rolls over the three-dimensional
resolution can be maintained. Hence the require- data points. A "mean surface" can be obtained, as in
ment was to ensure that the stylus gauge had suffi- the "M-system", by shifting the envelope surface
cient bandwidth to cope with the increased data down below the highest contact point (peak) in
rate, together with minimal mechanical resonance in order that an equal volume of material to air occurs.
the stylus system at the desired bandwidth, which Ihis new "M -system" envelope approximates the
might otherwise lead to distortion of the measured previous envelope surface of the original rolling
profile. Recently, such instruments (typified by the sphere radius. In this mann er a form of three-
"Ialystep") have allowed stylus traverse speeds to dimensional filtering can be attained, with the filter
be increased lO-fold by this careful redesign of the being controlled by the radius of the rolling sphere.
stylus gauge. Ihis enables stylus speeds of approxi- In practice, the envelope surface consists of just
mately 5 mm/sec to be used without losses in either portions of these rolling spheres, with each having a
tracking or signal fidelity as it measures areas up to radius equal to that of the rolling radius. Complex
500 x 500 /-Lm, with a sampling rate of 1 /-Lm, illus- mathematical definitions for the envelope system
trating that the operation can be completed in less would be extremely difficult to derive; therefore data
than aminute. is stored numerically and processed by suitable algo-
rithms to speed up processing time.
Loci centre
Profile
Envelope profile
A - Roughness
B - Waviness Surface profile
Figure 62. The two- and three-dimensional evaluation of a surface, according to the "E-system". (After Haesing, 1964, Tholath and
Radhakrishnan, 1999.)
InClustrial metrology , .
rolling/texturing industries, particularly for fluid characterisation will also be developed in due
retention applications, but more will be said on this course. A range of amplitude or height distribution
topic later in the chapter. However, some confusion parameters can be selected for the examination of a
exists in either parameter classification into appro- three-dimensional surface and include the
priate subgroupings as well as their associated desig- following:
natory letters and prefixes, because the continuity of
groupings has as yet not been fully established. • Dispersion (5q) - this is the root mean square
Generally, three-dimensional parameters can be deviation of the surface which relates to surface
classified by the following groups, which are departures within the sampling area, being statis-
assigned by their mathematical derivation: tically termed the standard deviation of the
height distribution:
f-± t
• amplitude characterisation;
• spatial characterisation;
• functional characterisation; 5q = Z2 (x, y) dx dy
• hybrid characterisation;
• fractal characterisation. where domain of integration is the measurement
area A = dx dy.
• Extremes (5z) - this is the ten point height of the
Amplitude characterisation surface, being an extreme parameter which can
be defined as the average value of the absolute
Ihe characterisation of surfaces by statistical heights of the five highest peaks and deepest
methods has been widely exploited by industry and valleys - by the "eight neighbours method" -
academia. Because surfaces tend to be represented within the sampling area.
by random data, it seems natural that statistical tech- • Asymmetry (5sk) - this is the skewness of topog-
niques can be applied to them for appropriate raphy - height distribution, which measures the
analysis. In two-dimensional parameter characteri- asymmetry of surface deviations above the mean
sation, ISO 4287: 1996 describes surface texture and plane. Ihis parameter describes the shape of the
the techniques for defining terms and parameters, topography height distribution. For example, for
while ISO 4288: 1996 deals with the rules and proce- a "Gaussian surface" - having symmetrical shape
dures for surface texture assessment. It is anticipated to its surface height distribution - this would
that the equivalent three-dimensional parameter equate to zero skewness, whereas an asymmetric
distribution of surface heights may produce a length and is used to determine aspects relating
negative skewness, when it has a longer tail on the to a surface texture's uniformity via the auto-
lower portion of its mean plane. This skewness correlation function. Principally, the texture
parameter provides an estimation of the exist- aspect ratios vary between 0 and I, with values
ence of "spiky topographical features": <0.5 indicating that no defined lay occurs and
ones of >0.5 exhibiting a pronounced lay. In some
1 m n
Ssk = -
mn
Sq L L Z~,j
i=! j=!
instances with a finite size of the sampling area,
the possibility exists that for certain anisotropic
surfaces the AACF's slowest decay will not reach
• Sharpness (Sku) - this is the kurtosis of topog- 0.2. Under such conditions, the surface's slowest
raphy - height distribution, which measures the decay direction should be employed;
sharpness of the distribution, characterising its • Sal - this is the fastest decay auto-correlation
spread. For example, a "Gaussian surface" equates length, defined as the horizontal distance of the
to a kurtosis value of 3; conversely, a surface AACF having the fastest decay to 0.2. This value
topography that appears centrally distributed of 0.2 is the shortest auto-correlation length that
would produce a kurtosis value in excess of 3, the AACF decays to in any direction. For example,
while a more evenly spread topography would with an anisotropie surface, Sal occurs perpen-
have a value less than 3. By combining both the dicular to the lay surface and a large value of Sal
Ssk and Sku parameters, this may allow identifi- denotes that the surface is dominated by long-
cation of surface topographies having reasonably wavelength components. Conversely, a small
flat tops with deep valleys. value indicates short wavelengths;
• Std - this is the texture direction of the surface,
whieh determines the most conspicuous direc-
Spatial characterisation tion of surface texture (lay) with respect to the
Y-axis within the frequency domain (Fourier).
Parameters relating to the a surface's spatial proper-
ties offer some difficulty in their characterisation,
due to their general wavelength randomness Functional characterisation
combined with multi-wavelength variations, which
in turn are coupled to their high sensitivity to the The classification of three-dimensional surfaces by
sampling interval. Techniques utilised for spatial its "bearing area" implies that a set of techniques are
characterisation include the following: engaged relating to specific functional properties of
a surface. Unfortunately, due to the diverse range
• Auto-correlation - aversion of this technique in of functional aspects demanded by industrial appli-
surface texture characterisation is that of areal cations, no single functional characteristic can
auto-correlation function (AACF), where the adequately cover all of these techniques. However, it
dependence of one position of data values is is possible to utilise the following parameters to
dependent upon another. Typieal parameters that establish the potential in-service performance of a
originate from the AACF, might be: surface:
• Sds - this is the density of peaks, being the
number of peaks of a unit sampling area, by the • Sbi - this is the surface bearing index, which
"eight neighbours method": relates to the Sq parameter over the surface's
height at the value of 5% bearing area, with a
Sds = (~) (::)
greater surface bearing index indicating superior
bearing properties;
• The RMS deviation Sq is defined by analogy with
where its two-dimensional form;
• Sei - this is the core fluid retention index, being
2[R(O) - R(Llx)] the ratio of void volume of the unit sampling area
m2 = (LlX)4 at the co re zone (i.e., 5-80% bearing area) over
parameter Sq. Good fluid retention occurs with
2[3R(O) - 4R(Llx) + R(2Llx)] greater values of Sei and for a "Gaussian surface"
m4 = (LlX)4 the index is approximately 1.56:
Svi = -1
A
l
Sq 1 - JZ*0008 p(z*) dz*
z*1
l was prineipally concerned with discovering the
existence of fractal behaviour over a large variety of
distinct eircumstances. Later, fractal research was
influenced by attempting to understand and uncover
where z* = zlSq and any suffices refer to bearing the causes and relevance of this behaviour and,
area fractions. in particular, trying to find functional dependen-
eies and relationships that correlate fractal dimen-
sions of engineered surfaces to speeific in-service
Hybrid characterisation performance.
A considerable body of research-based publica-
tions has been written on the measurement of fractal
The result of combining two or more of the prev-
dimensions, with some techniques being inappro-
iously discussed three-dimensional classification
priate for surface assessment, namely of a general
techniques is termed a "hybrid". By combining such
self-affine nature, as opposed to those being self-
parameters, it is possible to acquire many hybrid
similar, while other work has proved unsuitable for
parameters, with the most significant being:
anisotropic surface characterisation. For most of this
fractal research work the techniques employed have
• SLlq - this is the root mean square slope of the been used to estimate the bounds of the fractal
three-dimensional surface texture, within the dimension with varying degrees of numerical preei-
sampling area: sion. Generally, the lack of speeific physical mean-
SLlq = !1 Jt z'(x,y) dx dy
ings in fractal characterisation has meant that work
in this field has been restricted in the main to acad-
emia.
where
Opcn
an:3
J
10 cd
aren
7
Equi alcllt
arcas
Figure 63. Abbott-Firestone curve with closed areas. (After Sacerdotti et al., 2000.)
Function Characterisation
****
****
Joint stiffness
Slideways
Electro-contracts
Bonding and adhesion
****
****
**it"
**
****
-**
****
****
****
**-
-
**
****
**
Fatigue *** ****
...
Stress and fracture
Reflectivity
Hygiene
Bearings
**
**
*-
****
**
**
.***
**-
**-
****
--
**
*.*-
Seals n_
***" ** ****
Related 3-DParameters Sa, Sq, Sz, Ssk, Sku Sds, Str, Std, Sal Spk, Svk, Sk, Srl, SD.a, 55(, Sdr
Sr2, Svi
Table 7. Two- and three-dimensional stylus profilometer usage • colour representation - for example, an axono-
metric surface characterisation - either of the
Industry applications: Surface texture usa ge wired or meshed type (Figure 64);
• colour altitude co ding - indicating relative heights
Two- Three- of peaks and valleys (Figure 64 again);
dimensional dimensional • autocorrelation imaging - analyses directions
(isotrophy) and periodicity of the 3-D relief (not
Aerospace 10% <2% shown);
Automotive 75% 2%
Electrical 10% <1 %
• photo-simulation with lighting effects - which
Paper 10% 0% enables the captured image to be rotated or
Cosmetic 10% <1 % inverted to gain a complete visual impression of
Academic 5% 94% the measured surface's terrain (Figure 65);
• volume studies - defining, say, a hole's volume,
After Griffiths (1999).
perimeter, area, mean depth and maximum depth
Many of the three-dimensional software systems of an irregular cavity in the surface (Figure 66);
employ a Windows( -based software interface, giving • surface filtering - employed to separate out any
the user a highly intuitive visual capability with waviness, roughness and form data into discrete
logical, menu-driven functions having comprehen- entities; this occurs by FFT filtering to separate
sive help facilities for on-line user support. Typical out components of the 3-D relief, frequency by
of such fast operational industrial-based software is frequency and direction by direction (Figures 67
that illustrated in the following self-explanatory and 68);
examples, giving not only clear visual and easily • contour diagram studies - enabling points having
interpretative imagery but also considerable direct identical heights to be joined (Figure 69);
surface-related 3-D information. • pattern recognition - highlighting the points
A representative example of such comprehensive with specific topological properties (Figure 70);
3-D surface software is described below. This soft- • threshold operator utilisation - enables excessive
ware enables the user, once the 3-D profilometry raw peaks to be removed or extreme holes to be filled
data has been captured, to manipulate a measured in (Figure 71);
surface in numerous ways by selecting appropriate • a re-sampling operator - this technique clarifies
colour palettes or individual colours - for clarity - the image after successive zooming operations
together with zoom function ability, giving: have occurred and insufficient data points exist
Surface texture: three-dimensional
I ...
In
Figure 64. 3-D representation of an axonometrie surfaee produeed from a stylus-based instrument. ((ourtesy ofTaylor Hobson.)
Figure 65. A continuous 3-D axonometrie representation of a surfaee repradueed fram a stylus-based instrument. ((ourtesy ofTaylor Hobson.)
InClustrial metrology . .
143 IJm
88.6 IJm
(d)
Figure 66. 3-D software manipulation used to indicate important features on the surface topography. ((ourtesy of Taylor Hobson.l
(3) (b) (c)
Figure 67. The filter operator can be used to separate out waviness and roughness. (al The unfiltered surface. (bl The waviness ofthe surface. (cl The roughness ofthe
surface. ((ourtesy ofTaylor Hobson.l
I
The original surface .. . can be separated into the form . .. and the surface - allowing form to be removed I
~.
""'
6
+
o
Once the form has been removed, the waviness . . . and the roughness . . .
~. ..... V·
6 2.5
0 .5
9.4
1. 5
0 .3
1+ 9 .2
0 .5 0.1
I) 0 o
Wa v in es~ Parameiers (Cut Off : 0.25mm) Ro u ghll cs~ Parnmetcrs (
~ Wa = 0.332 IJ Ill ~Ra = 0.0536 IJI1l
sW v = 1. 24 IJ m ,R v =0.31 1 IJm
~ Wp = 1.32 IJI11 .. Rp = 0.272 IlI1l
~ Wt = 2.57 IJ Ol ~ Rt = 0.584 IJI1l
sWq = 0.41 3 IJI11 ~ Rq = 0.0698 IlI11
sWsl.. = 0.0173 , R ~ 1.. = -0.0376
sWl..u = 2.9 sR ku = 3. 16
... can be separated (i.e., using the filter operator) and parameters computed
Figure 68. It is possible to remove form from the surface utilising the filter operator. ((ourtesy of Taylor Hobson.)
Surface texture: three-dimensional
IJm IJm
198
178 173
149
133
124
99.1
88.9
74.3
44 . 4 49.5
24.8
Figure 69. A 3-D contour diagram study joins points which have the same height. (Gourtesy of Taylor Hobson.)
Figure 70. Pattern recognition study highlights the points with In many industrial applications speed of data manip-
specific topological properties. ((ourtesy of Taylor Hobson.) ulation is paramount and if identical analytical pro-
cessing is necessary then "macros" allow operations,
calculations, studies and comments added to the
to enhance the image; this can be achieved by image produced - to be efficiently executed in a few
increasing the number of pixels, which includes seconds. In many industries there is a fundamental
optimising the "z resolution" (Figure 72); requirement for the measurement of surface holes
• profile extraction - this enables the 3-D topog- and depressions, this being necessary, when:
raphy to be examined and at particular positions
of interest on the surface the user can pre-select • "surface engineering" is the requirement where
a line - straight, or manipulated around and cavities or holes in the surface topography are
across specific surface features - to be drawn and designed for fluid retention;
a two-dimensional trace at this "cut surface" can • texturised surface features - depressions - need
be illustrated (Figure 73). to be confirmed by 3-D measurement;
• cavities present in the surface need to be
measured that might affect in-service perform-
ance.
InClustrial metrology . .
,..
",
~m
150
140
130
120
110
100
90
80
70
60
50
~0
30
20
10
Figure 71. By utilising the threshold operator excessive peaks can be removed. This also applies to the filling in of excessive holes. [(ourtesy
ofTaylor Hobson.
Re-sampling enhances the representations when there are no longer enough data points (e.g., after successive zoom operations).
Figure 72. The re-sampling operator allows one to change the data sampling space. ((ourtesy of Taylor Hobson.)
Surface texture: three-dimensional
100 +----r""""'cc------l
so
0 +----+----.----+----~--~----~--~--~----~~~
o 0.5 1. 5 z
Length
2.53 "'"
rs.t z
x :
155 "'"
0.93 "'"
01Aft
2.42 rm'I
~ .
4 0+---~
20
0 +----4-------lr--~~--~----~--~----+_~~----+__+
o 0.7
length : l'C~ z : 57.9 L.Jf"I 0..-
0 . 97 """ ~ x. : 0 .54 rrm 0 . 76 lmI
"m
40
Z0
o 0.5
L "9l1\ : z : 62.3 ""' r7TZ 'O~
2.58 11m ~ : 1.67 ftWI'I V':* )t : 0 . 04 nnI
NB: the path followed along the surface can be a straight line, the bottom of a valley, a circular line, or any other user-defined contour.
Figure 73. The profile extraction operator allows one to extract one trace out of the surface. ((ourtesy of Taylor Hobson.)
(a) Contour map illustrating critical points and lines, with peaks "P", pits "V" and saddle points "S".
(b) "Change tree" chart derived from the surface contour lines.
Heighl P4
10
0+ __
va
·2
V3 V2
Figure 75. Topologieal surfaee texture eharaeterisation by fraetal analysis. ((ourtesy of Taylor Hobson.)
which is surrounded by a ring of course lines that • dale change tree - which represents the relation-
connected the pits and saddle points together ships between pits and saddle points;
(Figure 7Sa). Moreover, within the dale or peak in • hill change tree - representing relationships
question, there may be other pits/peaks, but they are between peaks and saddle points;
irrelevant compared to dominant pit/peak features. • Jull change tree - representing relationships
In this example a dale is considered to be the between critical points in hills and dales (Figure
"areal equivalent" of the profile motif, while the hill 7Sb), from which dale and hill change trees can
can be thought of as a useful complementary be calculated.
concept. Similady as for the profile motif method,
several types of surface-specific lines and points can In all of the previous discussion on these change
characterise dales and hills, respectively. These trees it was assumed that the lands cape did not have
features include the critical points (peaks, pits and edges, which unfortunately in practice is not the
saddle points) and critical lines (ridge and course case. Four types of edge critical points can occur:
lines; see Figure 7Sa). these are edge peaks, edge pits, saddle peaks and
saddle pits.
Change tree charts
The topographical "change tree" chart (Figure 7Sb) Areal combination
is ideal for organising the connectability relation-
ships between critical points in hills and dales, while Due to noise and other factors, in practice change
still retaining relevant information. The change trees tend to be dominated by quite short contour
tree represents the relationships between contour lines that impede interpretation. Therefore in order
lines from the surface, with the vertical direction to reduce factors such as noise, a mechanism is
representing height. At a predetermined set height needed to "prune" the change tree while still
all individual contour lines can be represented by retaining relevant information. By utilising the tech-
a point which is part of a line representing that nique of areal combination, this simplifies the
contour line continuously varying with height. change tree and any relevant information is still
Saddle points occur by the merging of two or more kept. For profile motifs, they can combine with adja-
of these lines into one. Peaks and pits are indicated cent features, while in the areal case the problem is
by the termination of a line. somewhat more complicated. Eleven different types
For example, consider a dale that gradually fills of possible combination on a change tree exist for
with water. The point where the water eventually areal combinations (see Table 8); Scott (1998) gives
flows over the edge of the dale is a saddle point. The a full descriptive account of such combinations.
pit in the dale is connected to this saddle point, as The logical steps developed below highlight how
indicated in the change tree. By continuing to fill the the areal combination algorithm has been developed
new lake, the next important occurrence where for a fuH change tree. This algorithm can be modi-
water flows out of the lake is again another saddle fied for hill and dale combinations, although for dale
point. As before, the line on the change tree repre- combinations (see Table 8) six occur, but in practical
sents the contour of the lake on the shore line, being terms types 3 and 11 are not usually applied, leaving
connected to this saddle point in the change tree. only four basic types of dale combinations.
This process can be continued, establishing connec- The following rules apply when attempting to
tions between the pits and saddle points in the develop an outline for the areal combination algo-
change tree. If the landscape is inverted, so that now rithm for a full change tree, but they are not a
the peaks become pits and so on, then a similar comprehensive account of all the potential hill and
process establishes connections between peaks and dale combinations, as they can be modified, as expe-
saddle points and the change tree. In general, at least rience dictates:
three types of change tree can be utilised:
Type 2 3 4 5 6 7 8 9 10 11
Dale combination )( t/ t/ t/ )( )( t/ )( )( t/ t/
Hili combination t/ )( t/ )( t/ t/ )( )( t/ )( t/
Full change tree t/ t/ t/ t/ t/ t/ t/ t/ t/ t/ t/
F F
I I
'L - - - - - - - - - - /J
/:
Tool
/
/
/
F /
~~::-
I
I
I
I
Figure 76. Definition of three-dimensional surface parameters - textured metal sheets. (After Pfestorf et al., 1998.)
Output
Output
layer of
nodes
layer of
Input nodes
layer of "Feed-forward ANN"
nodes
NB: these "multi-layered perceptrons" (i.e. ANNs) can also utilise "error-back-propagation".
Figure 77. Sehematic diagram of a feed-forward "artifieial neural network" (ANN) arehiteeture.
error is applied to adjust the node strengths of con- analysis by the ANN approach. The learning algo-
nectivity amongst the network's neurons, via a feed- rithm constrains the arrangement of pattern con-
forward propagation in the case of Figure 77. Hidden nectivities, although the concept of these learning
layer nodal capabilities are developed during net- algorithms can be adapted to any architecture.
work training, so that the extracted features are From the training data, the fundamental ANN
optimised for the classification task. Within the learning problem can be resolved in the follow-
ANN's algorithm, it can be configured around ing manner, by determining a set of network weights
the number of input-to-hidden-to-output nodes re- that can operate in the required manner. This assign-
quired for a given application, which may necessitate ment of weights can be achieved by initially assign-
some initial trials in order to optimise the correct ing minute values of randomness to these weights,
architecture. The greater the layers and nodal struc- then progressively adjusting them according to the
ture the better the discrimination, but at the expense following formula:
of longer "training" of the ANN. Hence a "trade-off"
occurs between a highly accurate and robust system, Adjustment of new = Wold
W jk jk
+ .uW jk
A
Surface topography utilising ANNs tion (ACO), which has been the goal for many years
in unmanned manufacturing environments.
In any application of 3-D surface topography assess-
ment utilising ANNs, reduction of dimensionality is
vital, as training becomes lengthy and tedious, being
exacerbated by considerable noise. Dimensionality 2.7 Non-contact measurement
reduction can considerably restrict the number of
degrees of freedom of the ANN, typically from
16,384 (128 2 data points), down to 1024 (32 2 data Non-contact measurement provides a means of
points); the latter might be employed to suitably assessing not only rigid components but, more
train the network from a moderate amount of data importantly, fragile and delicate parts which would
samples. either distort under the measuring pressure -
For example, to perform an intra-surface char- causing induced measurement errors - or, more
acterisation - to discriminate between worn and significantly, degradation to a delicate and unsub-
unworn surfaces for a particular manufacturing stantial surface under test. In fact, for the latter case,
process - it is desirable to identify surface topo- it is the only real means available to inspect soft and
graphy features, whose presence/absence might sometimes pliable part surfaces with any degree of
uniquely characterise the surface. When attempting confidence in a speedy and efficient manner.
to discriminate between, say, the worn and unworn Many of the optical systems previously mentioned
surface conditions that might be apparent from an in Chapter 1, can operate in 3D, especially the inter-
isotropically manufactured surface, such as honed ferometers, confocal microscopes and triagulation
bores in automobile engines, then a demarcation systems.
between them by some geometric or statistical para-
meter provides a degree of objectivity in the system.
An obvious choice for this plateau-honed surface in
the selection of three-dimensional parameters would
be one to measure amplitude, such as that of disper-
sion Sq ("root mean square deviation" - relating to
surface departures within the sampling area). Shot-
blasting is another production process that can
benefit from utilising the Sq parameter. Conversely,
for the more anisotropic a surface topography, such
as that resulting from face turning, the greater would
probably be the discrimination by using another 3-D
parameter, such as the spacing parameter Sds
("density of peaks" in the unit sampling area). The
major strength of the ANN approach to 3-D surface
topography assessment lies in the fact that, once
trained, little human intervention is required - elim-
inating the tedium associated with the conventional
approach - and consistency occurs, provided the
basic data integrity rules have not been corrupted.
Systems can be built that are independent of the
methodology of data capture and a practical system
might link the ANN to an automated data capture
station - such as a vision system - to investigate, for
example, on-line the effects of process variables for
a turned surface finish. Such a system would be able
to highlight any changes within the production
process, e.g. the too1's flank wear, which might
unduly affect the surface finish. The complete system
could then be incorporated into a feedback loop to
modify some or all of the cutting data, such as the
feedrate, cutting speed, depth of cut or coolant, as
necessary to maintain consistent turned products.
This artificial intelligence (AI) technique can be Figure 78. Multi-sensing scanning instrument for contact/non-
considered as a form of adaptive control optimisa- contact 3-D measurement. ((ourtesy ofTaylor Hobson.)
Surface texture: three-dimensional
Slides
Straightness:
Profile (measured in Xdirection) 10 mm traverse 50 mm traverse 95 mm traverse
Peak-to-valley 0.25 fl-m O.6fl-m 0.9fl-m
PHT p (O.l t099.9%)
Maximum angle of
measurement surface 90 0
illumination is applied aeross the eomplete field of delieate/pliable parts, as previously mentioned, is
view, prior to extensive data being obtained during relevant with this teehnique.
inspeetion. This measuring eyde is aehieved in The software features are enhaneed for both
approximately 2 minutes, with a Z-resolution of visual and surfaee measurement output, providing a
0.1 fLm; the system ean also eater for batehes of eomprehensive 3-D reporting proeedure, and this
parts to further inerease throughput. The instru- allows the following advantages:
ment is equipped with three field-of-view options -
50 mm 2, 175 mm 2 and 300 mm 2 - with eaeh eapable • measurement of eomplex and diseontinuous
of aehieving >1,000,000 data points. The measure- surfaees for flatness;
ment is aehieved by a 3-D holographie inter- • automatie levelling of the workpieee measure-
ferometer, utilising a diode laser, with precision ment planes;
opties and a diamond-turned parabolie mirror, • ineorporation of advaneed funetionality, the
eoupled to a high-resolution CCD eamera having system being simple to operate.
proprietary data-proeessing software algorithms.
The depth of foeus is 100 mm (fixed window), with Holographie interferometry is at the pinnade of
a Z-axis display resolution of 100 nm. All the advan- development for three-dimensional eapabilities of
tages relating to precision measurement of hardl today's instrumentation, offering new means of
solid parts are still valid for non-eontaet inspee- visually representing 3-D surfaees, giving unique
tion; in addition, the enhaneed ability to inspeet insights into surfaee inspeetion assessment.
Morrison, E. The development of a prototype high-speed stylus
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421-425. Physics, Bristol, 1994.
Surface microscopy
101
a complete book in their own right. However, it was apparent field of view, with minimal feature distor-
thought reasonable to include abrief res urne of tion. Etched surfaces are normally necessary on
some of the current equipment available and to metallic surfaces to preferentially etch the surface
attempt to show where, when and how such instru- and to reveal otherwise hidden surface detail.
ments complement our understanding of surfaces, In Figure 80(a) can be seen the application areas
which would otherwise be lacking if only two- and for a range of complementary electron microscopic
three-dimensional surface characterisation had instrumentation, indicating their vertical and lateral
been undertaken. resolutions. Such equipment can be exploited at a
range from the picometre (i.e., 10- 12 m) area for an
AFM, to an area weIl over 1 mm 2 using an SEM. In
(a) Range of lateral and vertical resolutions of instruments
Vertical resolution
SEM
Imm
Inm
0.01Ä.
Ipm l Lateral resolution
1 1nm l~m Imm
lÄ.
STM/AFM
\ \ AES
Figure 80. Range and resolution of a selection of surface microscopy instruments. ((ourtesy of Jeol (UK) Ltd.)
u ace mlcroscopy
Figure 80(b) a tabulated chart of the resolutions, to become proficient. Instrument size has been
excitations and observations available from this significantly reduced by utilising PC-based tech-
group of analytical instruments is shown. nology and the complete equipment is not much
larger than an office desk in terms of its working
area (see Figure 81).
Many of the latest instruments available can
3.2 Scanning electron examine objects up to 200 mm in diameter, weighing
microscope up to 3 kg, while still retaining micrometre precision
movement of the sampie (10- 6 m positional resolu-
tion). The SEM process of examination is non-
SEMs can overcome the limitations of optical destructive in nature, thereby retaining the value of
microscopy by offering depths of field of several an expensive sampie being investigated. As a quality
millimetres at low magnifications (x20-200) and control tool the SEM can quickly examine either
their resolution is similar up to x2000, whereupon random or sequentially produced sampies, which if
the SEM significantly extends its range, at x100,000, necessary can then be reintroduced into the produc-
or greater, over conventional optical techniques. tion line, if they prove to be acceptable. After many
Instruments of the SEM variety are not a new devel- years of development, the SEM has become a "work-
opment: were first designed in Britain about 50 years place-hardened instrument" that can be utilised in
ago, but then they were big, complicated and some- reasonably controlled production environments,
what temperamental instruments requiring great necessitating minimal component preparation with-
skill, patience (and some luck!) to produce generally out damaging the parts in any way.
mediocre results. The modern SEM is a totally
different instrument, controlled by PC technology
with Windows™-based software, having a minimum Basic SEM operation
of knobs and buttons to manipulate the specimen
and necessitating minimal training for an operator The principle of operation of the SEM is quite
simple. At the top of the column (see Figure 82) an
electron gun is situated, consisting of a tungsten fila-
ment in a strong electrical field. As a result of the
electrical field the electron gun emits electrons
(negatively charged atomic particles), which are
then accelerated to high speeds. These high-speed
electrons travel down the column, being influenced
by lenses lower in the column which squeeze them
together, forming an electron beam of very small
diameter. This electron beam is then focussed so that
it collides with the specimen in the microscope spec-
imen chamber as a diminutive spot. This minute
spot is scanned from left to right and up and down
over the surface, in an identical manner to that of a
normal TV as it scans the screen. By way of an
analogy for its visual operation, the SEM can thought
of as a TV manipulated so that its screen faces the
floor. Under these conditions, an SEM "tube" is rede-
fined and can be thought of as a column, whereas
the screen becomes the specimen being examined.
Although in the case of an SEM a considerably
smaller "screen" is scanned with an appropriately
smaller spot. In the same manner that anormal TV
tube is operated under a vacuum, the SEM column
and sampie chamber are also evacuated.
Once the electron beam strikes the specimen
surface many different processes occur, but for a
Figure 81. A typical "basic" scanning electron microscope, based on basic understanding of the mechanism it is only
proven PC technology and Windows TM-based software, which can be necessary to state that secondary electrons are gen-
equipped with a range of analytical tools for diagnostic investigation. erated. These secondary electrons can be thought of
[Courtesy of Jeol (UK) Ltd.) as electrons on the specimen's surface which will
Sccondary
clcctrons Elcctron beam
X-rays /
..... /
/'
Baclm:attered
/'
..- eleclrons
Cathodo-
lumincscence __ Auger
electrons
b orbed
eleclrons
Backscattercd eleelrons
(in Ihe sevcral 10's of nm
range to 100 nm)
Electromotive ,/ ~LL.<..L.o<~,\
force
Characteristic
Transmitted _ X-rays (in the lJ.ßl
range)
electrons
Continuous
X-rays
Condenscr Icns
Where:
I =sizl! of clcctron bcam
scanning on the specimen
Objcctive lens aperture
L =size of image on the CRT
Magnilication M =/lL
Signal detector
Figure 82. Underlying principles of the scanning electron microseope. [(ourtesy of Jeol (UK) Ltd.]
have been displaced by the high-speed electrons that the X-ray analysis indicates what causes them; given
originated from the electron gun. Any secondary this information it is possible to deduce why the
electrons that are emitted from the specimen surface problem arose. Once this level of understanding of
as the beam strikes are collected and counted. The the problem has been gained, preventive measures
total number of electrons counted for a particular can be defined and implemented.
point on the specimen is converted to a spot of light Apart from telling the investigator what a spec-
on the SEM display screen. The intensity of the spot imen's chemical constituent elements are, micro-
depends on the total secondary electron count. An probe analysis can determine respective quantities
identical operation is performed for each point on of each element. Such instruments can provide
the specimen being scanned and, an image is built- analytical accuracy to better than several parts per
up which represents the secondary electron yield million on a routine basis. X-ray detectors can also
over the surface. Fortunately, one of the main factors be "tuned" to detect only specific substances and
influencing secondary electron yield is the shape of then monitor their concentration while the electron
the specimen's surface, hence if the SEM display beam scans, thereby"mapping"the distribution over
(viewing screen - eRT) is scanned at the same rate the sampie surface. Using the SEM in conjunction
as the electron beam over the surface, an identical with X-ray analysis and mapping, provides all the
image occurs of the specimen's surface. To ensure information needed to characterise the problem,
ease of use, the SEM display and electron beam are thus:
synchronised at the TV frame speed, enabling a TV
image of the specimen surface to be viewed on the • imaging locates potential problem areas;
SEM screen. • normal X-rays determine what causes them;
The spot on the eRT is shown in real time, with • X-ray mapping deduces where else problems
the information emitted from the specimen surface occur in the specimen.
being displayed as an image. The magnification of
the displayed image is defined as the ratio of the size Yet another vital facility available to the SEM user
of the image on the eRT to that of the electron beam is backscatter electron (BE) detection. Here, some of
scanning on the specimen surface. The type of infor- the electrons that strike the specimen do not
mation obtained can be changed by switching the "interact" with it (i.e., producing secondary elec-
signal. In this way, the specific desired characteris- trons or X-rays), but simply collide with atoms in the
tics of the specimen surface can be viewed on the specimen and bounce immediately back - termed
eRT in a magnified scale. backscatter. The closer together the atoms are within
An SEM can be regarded as a miniature labora- the specimen, the more potential collisions, and
tory, with the specimen chamber being used for hence the greater the certainty ofbackscattered elec-
dynamic experiments such as heating, cooling, trons. This backscattering of electrons can be
tensile, compression and hardness testing, which detected, giving an atomic number contrast. Denser
can be examined in real time and at an appropriate materials exhibit tightly packed atoms, resulting in
magnification. Not only are secondary electrons increased collisions and causing more backscatter
collected for imaging, but also many other emissions than their lighter material counterparts, wh ich have
occur and can be employed to yield additional spec- looser packing densities. The resultant image in the
imen information. üf these additional emissions, eRT will indicate the well-known saying: "Dense is
perhaps the most useful one is the generation of bright and light is dark!" The technique is often
characteristic X-rays. When an electron beam strikes utilised to determine irregularities, since they
a specimen X-rays are emitted (see Figure 82), the usually appear as bright or dark areas on an other-
energies of which are directly related to the chem- wise uniform (normal) background. In many
ical constituents of the specimen at the focal point circumstances, the backscatter electron detector is
of the beam. This is the principle of microprobe utilised in conjunction with X-ray analysis, because
analysis, where a finely focused beam in the SEM is the backscattered electron image is normally less
aimed at a particular surface feature that has been complicated than the secondary electron image, and
identified by normal imaging, the object here therefore it is simpler to select areas for analysis.
being to determine its local chemical composition. X-ray analysis and backscattered electron detec-
Unlike analytical techniques based on "wet chem- tion are essentially the most widely used supplemen-
ical" methods, X-ray analysis is very fast, typically tary techniques, although many other characteristics
100 s being the standard acquisition time. As may be determined from the results of the inter ac-
opposed to normal optical microscopy where only tion of an electron beam with the specimen. Other
the image can be seen, using an SEM the chemical supplementary techniques include crystallographic
composition can be determined. Hence, an SEM and magnetic information, surface topography and
enables one to establish where problems occur and composition, semi-conductive or electrical charac-
InClustrial metrology , .
teristics; however, it should be stressed that some of now that image-processing procedures have been
these methods require quite complex analytical developed, to further expand the visual impact to
stages to obtain valid information. the observer - more will be mentioned about this
shortly. The number of secondary electrons emitted
from a specimen surface greatly depends on the
Principle of magnification incident angle of the electron beam to that surface.
In other words, the secondary electron signal
If a specimen surface is scanned with a finely focused depends upon undulations of the specimen's surface.
electron beam of only a few nanometres (see Figure Furthermore, since the energy of secondary elec-
82), then information will be emitted from each point trons is very low, they are only emitted from a
of the scanning operation. This emitted information thin layer on the specimen surface. Thus, secondary
is converted into an electrical signal, amplified, then electron signals are considered to be the most
fed into the eRT for subsequent observation. On the appropriate signal for observing a specimen's topo-
eRT, the information is used to control the bright- graphy.
ness of the corresponding spot. The spot on the eRT The following describes just some of the fields of
is shown in real time with the electron beam scan- science and engineering that might exploit SEM
ning on the specimen surface. Hence, information observation techniques:
emitted from the specimen surface is displayed on
the eRT as an image. In Figure 82, the magnification • materials science - utilised in most advanced
of the displayed image is defined as the ratio of the materials science fields, typically for supercon-
size of the image on the eRT (L) to that of the size ducting materials, or for advanced composites,
of the electron beam scanning the surface (I). The etc.;
type of information that could be obtained can be • biology - particularly biotechnology applications
changed by switching the signal; in this manner a or for the examination of entomological taxon-
specific desired characteristic of the specimen can be omy (insects, bacteria, viruses and animal
visually displayed on the eRT in a magnified scale. tissues);
• electronics - utilises the power of such instru-
mentation in the R&D and quality control fields,
SEM applications typified by the semiconductor/electronics appli-
cations for failure analysis techniques, etc.;
As previously described in this section, various • mechanicallindustrial engineering - for investi-
kinds of signals can be obtained by an SEM. These gation of process technologies, machinability
signals carry distinct types of information and, as research, component failure modes and metal-
such, are employed for different purposes, as listed lurgicallmetallographical investigation.
in Table 10.
SEM: images
Topographical observation: secondary
electron imaging In Figures 83-86 are depicted aseries of photo-
micrographs produced across a diverse range of
This secondary electron image (SEI) technique is metallic - ferrous and non-ferrous - non-metallic
probably the most utilised method of general and biomechanical structures. It is only not only at
applications for an SEM by industry, particularly so the high-resolution range of magnification that
(a) Cleavage planes on natural dia mond surface: 15 kV x200. tially worked to achieve the inclined geometrie
facets so admired in cosmetic jewellery. Conversely,
Figure 83(b) shows a more mundane, but neverthe-
less important surface - that of paper - which must
absorb the ink or colour pigments from printed
media. With such surfaces good adherence on the
surface is essential; therefore the quality and texture
of this paper surface are vital if it is to respond to,
say, the ink and not blot/spread, thereby losing
line delineation and definition. Figure 83c illustrates
a typical semiconductor memory surface, where
surface structure and separation of discrete memory
elements are vital for efficient operational perfor-
mance of these IC chips.
The two SEM photomicrographs displayed in
Figure 84(a and b) are notable not from the images
(b) Paper surface: 15 kV xl 00. themselves, which are markedly different in texture
and composition, but because of the information
provided overlaying the actual images. Of particular
relevance is the "error bar" or linear scaled bar which
automatically changes its dimensional magnitude as
magnifications are either increased or decreased.
Such an auto-scaling facility can be employed as a
form of "indirect measurement" of notable dimen-
sional/surface features, weIl beyond the range of
most conventional dimensional techniques, certain-
ly up to the nanotechnology level (10- 9 m) and even
approaching that of picotechnological values (10- 12
m) in size. Each SEM image can be labelIed with an
identifying number for subsequent later reference
and the mode of operation can also be displayed
(for example, Figure 84a: SEI = secondaryelectron
image).
(c) Semiconductor memory surface: 15 kV x1500.
In Figure 85 is shown an SEM "soft scanned" image
of an "ultra-high-speed" face milled austenitic-grade
stainless steel surface machined at 3500 m/min. The
SEM processed data in this instance was magnifica-
tion xlOO, accelerated voltage 20 kV, working dis-
tance 20 mm, pressure Pa 200 /-Lm, with secondary
electron imaging. üf particular note was that the
original photomicrograph was in fact a left-hand
stereo image of the surface. Both a left- and right-
hand stereo image can be superimposed/merged into
one image. If the original of such a "merged pair of
images"had been viewed through 3-D glasses (green
and red - as worn in the early days of 3-D cinematog-
raphy), then this combined image would take on a
three-dimensional aspect. This visual enhancement
Figure 83. Low-vacuum scanning electron micrographs. (Courtesy is often useful when attempting to interpret whether
of Jeol (UK) Ltd.) peaks or valleys are being viewed, this being a partic-
ular optical distortion that is visually difficult to
interpret in plan view, as shown in Figure 85. More-
useful analysis can be undertaken, but also at lower over, this face-milled image has a topographie al
magnifications, where these instruments' large height profile superimposed onto the surface, show-
depths of field are exploited. In Figure 83(a) can be ing peak and valley features, giving greater dimen-
seen a fractured natural diamond surface, illus- sional and visual interpretation of the machined
trating the cleavage planes which can be preferen- surface topography.
.. InClustrial metrology
MAG:xSOO
Acc.V:1SkV
Signal:SEI
WD:22mm
SS:20
Pressure:Pa
40.0pm
(b) High-speed face-milled surface: 316 grade stainless steel, peripheral speed 2500 m/min.
MAG:x2S
Acc.V:30kV
Signal:BES
WD:36mm
SS:40
Pressure:Pa
800pm
Figure 84. Scanning electron microscope images. [(ourtesy of Jeol (UK) Ltd.]
u ace mlcroscopy Im
Height Profile
Heighl (pm)
Figure 85. 5canning electron microscope photomicrograph with "soft imaging" and topographical height profiles. [(ourtesy of Jeol (UK)
Ltd.]
SEM: image processing ports. Angled detectors are preferred for practical
reasons, because they are less likely to be damaged
Digital images can be subjected to a variety of post- by movement of the specimen within the working
processing functions, with processed images being chamber of the instrument. The X-rays are discov-
separately stored from the original images. ered by employing either a thick- or thin-frame
Therefore, when writing reports the image data can window (typically an Si (Li) detector), for heavier or
be converted into a suitable form for the content of lighter elements, respectively. This semiconductor
the report. Windows™-based software enables a host detector is positioned at the tip of the detector (see
of image processing techniques and enhancements Figure 87). The height of current pulses that are
to be carried out; some these are as follows: generated by the X-ray illumination is proportional
to the energy of incident X-rays. By calibrating
• On-screen measurement - this is a cursor the. multi:channel analyser prior to performing
measurement function allowing measurements test mg usmg a standard specimen, characteristic
between two cursors at 90° to each other (Figure X-rays from a previously unknown specimen can be
86i), or a multi-point measurement function measured for element identification. The sophist i-
which measures many points in any direction cation of these EDS systems enables the investigator
(Figure 86ii); to determine by an analysis of the specimen, its
• Look-up table (LUT) and pseudo-colour display - percentage weight of elements in the vicinity of the
when a stored image is to be downloaded, the sampling area, spectra for specific elements that
LUT allows the image to be optimised for visual might be located in the test zone, or a general spec-
impact, through adjustment of the contrast and trographical search for a totally unknown specimen,
brightness of the original image (Figure 86iii). when attempting to identify its overall elemental
Furthermore, the image can be visually enhanced composition.
by the application a pseudo-colour display (Fig- When an electron beam irradiates a specimen,
ure 86iv); characteristic X-rays are emitted (Figure 87). By
• Dual and quad displays - either two or four detecting and analysing these X-rays, identification
images can be combined into an overall new of elements contained within them can be under-
image (see Figure 86v and vi, respectively); taken (qualitative analysis). More specifically, it is
• Dual magnification and digital zoom displays - possible to determine weight concentrations of the
the digital zoom function provides an enlarged contained elements (quantitative analysis). Electron
portion of the stored image, which allows the beams are finely focused, so by utilising the "spot
images to be positioned adjacent to each other mode" on the instrument an elemental analysis of a
(Figure 86vii). The dual image shown in the very small area on the specimen can be investi-
previous Figure 86(vii) can be increased in size gated, or the more general averaged element concen-
to any desired magnification to observe notable tration, mentioned above. Furthermore, both a "line
features, for further investigation, or analysis analysis" and "areal analysis" can be performed as
(Figure 86viii). well as X-ray image observation, the procedure
being:
The following two sections relating to SEM
enhancement attempts to describe and illustrate observing the specimen surface with a secondary
several types of the large array of instrumental electron image and/or a backscattered electron
equipment that can be fitted to an SEM. Such inves- image;
tigative items considerably increase the versatility 2 designating the point to be analysed with the
and the scope of the SEM as an analytical too1. cross-point of the cursor lines displayed on the
image;
3 positioning the electron beam at the designated
point on the specimen, then performing a quali-
3.2.1 Energy-dispersive X-ray tative analysis;
spectrometer 4 observing the distribution of an element, by
electing a specified characteristic X-ray.
The characteristic X-rays emitted from the specimen
under test have energies that represent individual Such procedures as those just described for EDS
elements. These energies can be detected with an analysis enable considerable elemental data to be
energy-dispersive spectrometer (EDS) fitted at a derived, then interpreted for appropriate future
specific location port on the SEM. Its detector orien- actions, based on sound and factual judgements.
tation and angular relationship to the axis of the X-
ray beam is conveniently located in one of the SEM's
u ace mlcroscopy Im
(i) Cursor measurement (ii) Multi-point measurement
X-ray dctcctor
l\lulti-channcl
analyser
Si ( Li) detcctor
Figure 87. The energy-dispersive X-ray spectrometer (EDS) - block diagram. [(ourtesy of Jeol (UK) Ltd.]
canninl: coil
/ J_
Dclcclor
/~\I
/: "
\ ,.,
" --_/
\ / SIJ.:nal IIltcnslty
/
Figure 88. The principle underlying the SEM transmitted eleetron image observation, [(ourtesy of Jeol (UK) Ltd.]
than that found on many earlier instruments, basic diagrammatic representation of aTEM is
without sacrificing long-term emitter stability. One shown in Figure 90. Recent progress in analytical
of the advantages of high-grade versions of this microscopy has enabled improved theoretical reso-
instrument is its ability to instantaneously select the lution, this being calculated from the spherical aber-
analysis point, while observing a high-resolution ration coefficient, with yet further enhancements in
image, with certainty that both the observed and analytical capability through improvements in the
analysis points coincide. Other applications for illumination system. Such improvements include
TEMs might include electron holography and micro-area diffraction, convergent-beam electron
coherent convergent beam electron diffraction. diffraction and high-sensitivity analysis employing
finely focused probes.
The illumination lens system might consist of a
Operational characteristics of the TEM series of lenses (four), in conjunction with an
imaging lens system (i.e., six lenses) - see Figure 90
A typical field emission gun might use either a (many of the lenses are not shown, for simplicity).
ZrO/W (100) emitter, or a W (100) emitter. A very This imaging system provides various illumination
InClustrial metrology . .
Condenscr lens
! \
'\
'-::
~ 0.5 d3" " d /d 1
"--- /
°0~~~5~=d~1=0===215~~
a?~- ~ ==_ ___ Minimum disc due to chromatic aberration,
a(mrad) A
d3 = 1.22-
a
(ii) Specimen high-tilt configuration.
Blur due to diffraction (Airy disc).
(c) An image of carbon graphite, observed with a scanning image observation device. A lattice image
of 0.34 nm is c1early observed, proving that the probe was this order of diameter.
Figure 92. Measured probe diameter and image of carbon graphite taken on aTEM. [(ourtesy of Jeol (UK) Ltd.]
atomic lattice images - with probes configured to where X-rays of known wavelength (A) and
approximately 1 nm diameter. Such diagrams are measuring angle «(}) can determine the atomic
visual representations of the physical associated spacing (d) for various planes/orientations in a
and geometrical positioning of atomic lattice crystal;
structures within materials; 3 convergent-beam diffraction - simplistically
2 diffraction patterns - diffraction can occur speaking, the atomic structure here closely resem-
whenever the Bragg law is satisfied, varying for bles that observed in elementary "bubble-raft
each material and its orientation, this being patterns", which are used to simulate simple
related in the following manner: grain boundaries and dislocations in crystalline
materials.
A = 2d . sin () (Bragg law)
3.3.1 Transmission electron surface reflection conditions are governed by the
"Bragg law", so they also must vary. The inter fe ren ce
microscopy: general application between both the transmitted and diffracted beams
will produce intensity variations of the brightfield
In X-ray diffraction, X-rays incident on a crystal are
image - termed extinction contours. Such an effect
diffracted by parallel sets of atom planes, in a similar
appears as dark bands across the image, which indi-
manner to that of light reflection from a mirror. The
cates that a set of planes near these bands has a
position of the diffracted beam will be in accordance
significant diffracting orientation. Therefore, when a
with the "Bragg reflection conditions", described in
foil bend occurs in the TEM during its observation,
the previous seetion, and they are similar to the way
"extinction contours" seem to appear to move across
an electron beam is scattered by a crystal. Any dislo-
the test specimen. From a simplified analysis tech-
cations and stacking faults in the surface region can
nique, this approach can be employed to account for
be revealed by a technique which examines the inter-
the contrasting effect resulting from surface regional
ference between transmitted and diffracted beams,
dislocations. Moreover, "stacking faults" in the spec-
resulting from a beam of electrons incident on a
imen will also produce a characteristic diffraction
crystal foil of between 100 and 500 nm in thickness.
image. Hence, the study of specimen defects by these
The technique for forming images of these diffracted
various diffraction techniques is applicable to all
elements has previously been mentioned. In oper-
materials that can be produced as adequately thin
ation, a parallel beam of electrons - typically accel-
sections.
erated by a potential of 100 kV - is transmitted
In order to show the potential of the TEM's abil-
through a thin foil and is diffracted in a variety of
ities as an analytical tool, Figure 93 illustrates a
directions by the crystal under test. The diffracted
TiAl/Ti3Al two-phase alloy in lamellar form. This
beams are subsequently focused forming a diffrac-
particular material has shown promise as a new
tion pattern that can be magnified for investigation,
dass of lightweight high-temperature structural
as necessary. A diffraction pattern (see Figure 93)
material. Three different types of TiAl/Ti3Al inter-
normally consists of a two-dimensional array of
variant lamellar boundaries, in such a TiAI-based
spots, with each spot representing a specific series of
alloy containing Sn are observed by high-resolution
reflecting planes. From this diffraction pattern, the
electron microscopy. Of the three types of bound-
foil orientation can be determined.
aries shown in Figure 93, the ternary element Sn,
Individual diffraction pattern spots are the
which is added to improve the mechanical proper-
product of the incident beam's diffraction from a
ties, is observed to preferentially segregate onto two
reasonably large vicinity on the test specimen (typi-
types of high-energy boundaries. In Figure 93 the
cally 104 atom spacings in diameter). A single elec-
visual image and diffraction patterns, together with
tron beam can produce a corresponding image by
graphical displays, show just some of the investiga-
inserting an objective aperture into its path.
tive/analytical abilities of the TEM.
Two main optical conditions can arise:
• brightfield image - resulting from the aperture
being centred on the main transmitted beam;
• darkfield image - produced by situating the aper- 3.4 Atomic force microscope
ture over a diffracted beam.
Generally, the predominant amount of analysis The atomic force microscope is just one variant of a
occurs in the brightfield mode of illumination, wide variety of scanning probe microscopes and
although some critical applications required the accompanying techniques that were developed in
darkfield illumination technique. the early 1980s and indude the following:
Hypothetically, if a test specimen was completely
flat and without defects, under these conditions a • atomic force microscope (AFM) - contact; AC; also
completely homogeneous image would result when visco-elasticity operational modes;
the objective lens was centred over the main trans- • scanning tunnelling microscope (STM);
mitted beam. Subsequent changes in image bright- • scanning tunnelling spectroscopy (STS);
ness are the result of any effect that changes the • friction force microscope (FFM) - static and
diffracted beam's path, so that it enters the objective lateral operational modes;
aperture and interferes with the transmitted beam. • magnetic force microscope (MFM);
If very thin test specimen foils are buckled, the • scanning near-field optics microscope (SNOM).
orientation of the specimen's surface with respect to
the electron beam will be slightly varied for different This section on scanning probe microscopes, will
zones on the specimen. These variations for local almost exdusively discuss an overview of the AFM
InClustrial metrology , .
10
e......c 5
0
c'"
'S -5
Q"
-10
-15
-20
0,8 1.2 IA 1.6 1.8 2
Sn (al. %)
--1
(b) Pseudo-twin boundary
AI, Ti (at. %)
J5 40 45 50 5S 60 6S
20+---~~~--~--~--~--r
15
10
ec 5
~
AI
!Jc 0 -o- Ti
-0- D
'E -5
Q"
-10
-15
-20
0.5 1.5 2 2.5 3 3.5
Sn (at. %)
I
(c) 120°, rotational boundary
6~
AI, Ti (at. %)
35 40 45 50 55 60
20
15
10
e......
c
5
0
!l
c
'ö -5
~
-10
-15
-20
0.8 1.2 1.4 1.6 1.8 2 2.2 2.4
n (at. %)
Figure 93. TEM sub-nanometric elemental analysis (Le., point analysis), ((ourtesy of Jeol (UK) Ltd/Dr H. Inui and Prof. M. Yamaguchi, Kyoto
University, Japan.)
u ace mlcroscopy
STM/AFM
AES *
EPMA * * *
nlR * * *
SEM * *
SIMS *
TEM *
XPS * *
* *
AES: Auger electron spectroscopy; EPMA: electron probe micro-analysis; FTIR: Fourier transform infra-red absorption spectroscopy; SEM:
scanning electron microscope; SIMS: secondary ion mass spectroscopy; TEM: transmission electron microscope; XPS: X-ray photoelectron
spectroscopy.
Courtesy of Jeol (UK) Ltd.
instrument and just some of its potential applica- • specimens having no conductivity require an AFM
tions. Today, with the diverse range of scanning used in either contact or AC mode, depending on
probe microscopes and observation methods that the sample's surface roughness and its softness;
exist, they can offer a wide range of analysis tech- • specimens with conductivity - both the AFM and
niques, as indicated in Table 1l. STM may be utilised.
Recently, scanning probe microscopes have been Any scanning probe microscope allows specimen
utilised across a diverse variety of disciplines, in- observation in various environments, from normal
cluding fundamental surface science and routine atmospheric conditions, to liquids, also with an
surface roughness analysis, together with three- ultra-high vacuum. Conversely, some electron
dimensional imaging. The scanning probe micro- microscopic applications necessitate situating the
scope is an imaging tool with a large dynamic range, specimen in a vacuum and in certain instances the
encompassing the realms of optical and electron sampies need to be either stained or coated with a
microscope applications. These instruments can be conductive film. Certain types of specimens in their
employed as a three-dimensional profiling instru- original form may be destroyed by such sampie
ment - with superb image resolution abilities - that
in certain cases can quantify physical properties
such as surface conductivity, static charge distribu-
tion, localised friction, magnetic fields and elastic
moduli. The instrumental applications for scanning
probe microscopes can be shown on achart relating
to their lateral and vertical resolutions, as previously
indicated in Figure 80.
Coarse
positioning
system
bringing
tip into
sampIe
vicinity
Feedback system
controlling vertical
tip s position
SampIe
-==:::l==
Piezoelectric scanner moving
sampIe under tip, or tip over sampIe,
in a raster pattern
~c=J
Computer system to
drive scanner, for
L----=.J
measured data converting
it into an image
Figure 95. Schematic representation ofthe generalised operation of a scanning probe microscopes (Le., STM/AFM). [(ourtesy of Nikon/Park
Scientific Instruments.]
treatments. If observation occurs in an atmosphere, important surface-related factors, but care is needed
gas or liquid, the scanning probe microscope can be when quantitative measurements are required.
effectively used, but careful interpretation of images The scanning tunnelling microscope (STM) can
is necessary, due to the potential of adsorbed impu- be considered to be the forerunner of all derivative
rities. These AFM/STM microscopes can be used as types of scanning probe microscopes. It was
an effective means for measuring specific physical invented by Gerd Binning and Heinrich Rohrer at
properties, such as surface magnetism, friction IBM (Zurich) in 1981, who later received a Nobel
force, viscosity, elasticity, surface potential and other prize (Physics, 1986) for this invention. This STM
instrument was the first of its type to generate real- 3.4.2 Atomic force microscope:
space surface images at atomic resolution. STMs use
a sharp conducting tip (see Figure 95, detail), with a operating principle
bias voltage being applied between the tip and
sampie. When the tip approaches the sampie to The AFM's tip will probe the sampie surface with a
within 10 A ("d") electrons from the sampie will sharp tip having dimensions of several micrometres
"tunnel" through this gap into the tip or vice versa, ~ong and approximately 100 A in diameter. The tip
depending on the bias voltage sign. The resulting IS located at the free end of a cantilever which is
tunnelling current is variable, this being related to between 100 and 200 j-Lm long (see Figure 96).
the tip-to-sample spacing which, in turn, is used in Applied forces between the tip and the sample's
the creation of the STM image. In the case of the surface cause the cantilever to either bend or deftect.
STM, both the tip and the sampie must ideally be Cantilever deftections are measured as tip scanning
conductors, or at least semiconductors, which is not occurs over the sampie or, conversely, with the
the case for an AFM that can image insulating mate- sampie being scanned under the tip. These deftec-
rials. tions of the cantilever allow the production of a
From Figure 95 it can be seen that the tunnelling computer-generated surface topography map.
current is an exponential function of the tip-to- The AFM cantilever can be deftected by the con-
sampie distance relationship. If this separation tribution from several microscopic surface-related
distance changes by 10% (i.e., equating to 1 A), then forces. The principal one of these minute forces is the
the tunnelling current will change by an order of inter-atomic force termed van der Waals force. The
magnitude. Such an exponential dependence van der Waals theory states that atomic attraction
enables an STM to have a notable sensitivity, increases as atoms are progressively brought together,
allowing surface imaging to sub-Angström vertical until their electron clouds begin to electrostatically
precision, with lateral atomic resolution. STMs are repel each other. However, the electrostatic repulsion
designed to surface scan in either of two mo des: progressively weakens this attractive force, as the
inter-atomic separation continuously decreases.
constant height mode - where the tip's travel is in Eventually the van der Waals force reaches zero,
a plane horizontal to and above that of sampie when the separation distance between the atoms
and variation of the tunnelling current is related reaches several Angströms - which is approximately
to the local surface topography and the electronic the length of a chemical bond. When the atoms are in
properties of the sampie. This tunnelling current contact, then the total van der Waals force becomes
is measured at each sampie surface feature, which positive (i.e., repulsive). As a result of this repulsive
constitutes a data set for the topographic image; van der Waals force, any attempt to force the atoms
2 constant current mode - the instrument uses into a doser atomic bond are negated.
feedback to maintain the tunnelling current, by In practice for the AFM, this results in the
constantly adjusting the height of the tip at each cantilever pushing the probe's tip against the
measured topographical feature. If the system sampie, and under this condition the cantilever
detects an increase in tunnelling current, the bends rather than forcing the tip and sampie atoms
voltage is adjusted to the piezoelectric scanner to doser.
increase the tip-to-sample distance. The potential energy that acts between two
neutral atoms can be expressed from the formula
In constant current mode the scanner's motion derived by J.E. Lennard-Jones, as follows:
constitutes the topographic data set, such that the
system maintains a constant tunnelling current to
within several per cent. This control equates to a tip-
to-sample distance constancy of less than several
hundredths of an Angström. where, by calculating the potential energy of say, Xe
The main consideration in the following text is atoms, using e = 0.02 eV, a = 0.4 nm; it is possible
principally reserved for a discussion related to the to derive a "distance-potential energy graph" (not
AFM type of scanning probe microscope, its design, shown). Moreover, using the relationship for the
operating principle and potential surface-related total potential energy of two adjacent atoms this can
applications. be obtained and the force acting on these two atoms
may be found, after differentiation, to be in the
region of 0.2 nN.
Additionally to the repulsive van der Waals force,
two other forces often occur during the AFM -contact
operation:
InClustrial metrology , .
N .--'- ur
- Figure 96. Atomic force microscope probe geometry. [(ourtesy of Jeol (UK) Ltd.]
cantilever force - exertion applied by this cantilever bends as contact with the surface occurs,
mechanical device; resulting in the laser beam's position shifting in the
2 capillary force - exerted by a thin layer more often detector. The PSPD is capable of discriminating light
inspected in an ambient environment. measurement displacement down to lOA, with the
ratio of optical path length between the cantilever
The cantilever force tends to act in a compressive and its detector to that of the actual cantilever giving
spring-type manner, with the magnitude and its a mechanical amplification. This further mechanical
associated sign being either attractive or repulsive amplification enables the overall system to detect
in nature, depending upon the cantilever deflection sub-Angström vertical motion of the cantilever tip.
and its spring constant. The spring constant k can be There are other methods of detecting cantilever
found by the following relationship: deflection, such as optical interference, or simply by
manufacturing the complete cantilever arm from a
Bad 3 piezoresistive material and detecting its deflection
k=4[3 electrically - due to the fact that any mechanical
deformation causes changes in the arm's material
where B = Young's modulus for cantilever material, resistivity. Once the AFM instrument's electronics
a = cantilever width, d = cantilever thickness, I = have detected the deflection of the cantilever, it can
cantilever length. compute and then generate a topographical data set,
To obtain the atomic resolution with an AFM, the by operating in two distinct modes - as previously
spring constant needs to be 0.01 nm and, to detect mentioned, these are the constant height and
10- 9 to 10- 12 N between the atoms the constant constant force mo des.
needs to be
1XlO- 12 N
k = 1X 10- 9 - ---:-c--
11
1 X 10- m
3.4.3 Atomic force/scanning probe
microscope: applications
Therefore
The diagrams schematically illustrated in Figure 97
k = 0.1 - 10 [n/m] are just some of the typical applications for either
an AFM or some form of STM, most notably:
The capillary force arises when water "wicks" its
way around the tip, enveloping it and applying a • Static AFM (contact AFM, Figure 97i) - this mode
strong force attraction (10- 8 N) holding the tip in obtains sampie surface structure by scanning the
contact with the sample's surface, with the magni- surface, while keeping a constant repulsive force
tude of the capillary force being dependent upon the acting between the tip and sampie. The tip is
separation distance of the tip-to-sample. So long as normally in contact with the sampie during this
the probe's tip maintains contact with the sampie mode of imaging. Historically, the contact mode
surface (in contact mode of operation), then the was the first probe microscope mode of operation
capillary force would normally be constant due to that enabled the imaging of non-conductive
the distance between tip and surface being virtually sampies.
incompressible. An assumption is made that the • STM (scanning tunnelling microscope, Figure 97ii)
retained water layer is relatively homogeneous, with - this mode of operation applies a bias voltage
the variable force in the contact mode being the between a sharp conductive probe and sampie
force exerted by the cantilever. Hence, the total force exhibiting conductivity. When the probe and
exerted by the probe's tip on the surface of the sampie are in elose proximity, some of the elec-
sampie, being the sum of the capillary and cantilever trons can "tunnel" between the tip and sampie
forces, must be balanced by the repulsive van der without ohmic contact. Scanning the surface
Waals force for the contact AFM. The total force while using a feedback loop to maintain a con-
magnitude exerted on the sampie will vary around stant tunnelling current reveals the structure of
10- 8 N - with the cantilever being repulsed as hard the sampie surface.
as the water provides attraction to the tip - to the • LFM (lateral force microscope, Figure 97iii) - this
general operating range of typically 10- 6 to 10- 7 N. technique is sometimes termed friction force
The cantilever arm's measurement positioning microscopy. It measures the friction between the
must be accurately known and optical techniques tip and sampie by measuring the torsion al
are the most common form of sensing media. bending of the cantilever. LFM is both a static and
Typically, the cantilever bounces back a laser beam contact mode technique which simultaneously
onto a position-sensitive photodiode (PSPD). The acquires an AFM topography image.
• Force modulation/phase detection (Figure 97iv) - signal. In the case of "discrete contact" mode of
the technique adds a modulation signal in the operation, qualitative visco-elasticity images of a
Z-direction, while observing the sampie with sampie can be obtained by measuring the phase
static AFM. Qualitative elasticity of the sampie is lead or lag of the cantilever relative to the modu-
obtained by measuring the displacement of the lation signal.
cantilever with respect to the modulation signal. • Dynamic AFM (non-contact and discrete contact
The "phase detection" technique measures the AFM, Figure 97v) - dynamic AFM is accom-
phase lag of the cantilever relative to the driving plished by oscillating the cantilever near its reso-
(i) Static AFM (i.e., contact AFM). (v) Dynamic AFM (i.e., non-contact, or
discrete-contact AFM).
Photo Laser beam
128
(Hi) LTF (i.e., lateral force microscope). (vii) LTF (i.e., lateral modulation).
Friction min.
(iv) Force modulation/phase detection. (viii) MFM (i.e. magnetic force microscope).
Figure 97. Atomic force/scanning probe microscope applications. [(ourtesy of Jeol (UK) Ltd.]
u ace mlcroscopy
nant frequency and using forces at or near the method, this technique removes most of the
sample surface to damp the motion of the "artefacts" associated with the scanning direction
cantilever. Non-contact mode utilises attractive and sample morphology.
van der Waals forces to damp the cantilever's • MFM (magnetic force microscope, Figure 97viii) -
motion, allowing imaging to be undertaken this is a variation on the NC-AFM that uses a can-
without the tip contacting the sample surface. tilever coated with a magnetic material. The mag-
Discrete mode uses tip-surface contact to damp netic coating makes the tip sensitive to magnetic
the motion of the cantilever. Discrete contact domains on the sample surface. Further, the mag-
mode of operation is sometimes referred to as netic domain distribution can be simultaneously
"tapping". Additionally, it is possible to use an obtained with a topographical image.
"FM detection" method .
• STS (scanning tunnelling spectroscopy) and CITS Figure 98 illustrates an AFM image resulting from
(current imaging tunnelling spectroscopy, Figure the face milling of an austenitic (316-grade) stain-
97vi) - STS is a measurement of current versus less steel specimen being machined in the ultra-
voltage (1- V curves). These 1-V curves can pro- high speed region - 3000 rn/rn in. The image area is
vide an insight into the characteristics of a sample; 80 /-Lm 2 , which shows the passage of the milling
typically these 1- V curves are taken at a point. inserts and the periodicity of the feed motion at a
However, the CITS technique acquires an 1- V rate of approximately 30 /-Lm/cutter revolution. Such
curve at each point in the topographical image. three-dimensional images can impart valuable
• Lateral modulation LFM (Figure, 97vii) - in this information on the surface topography, the shearing
technique a lateral modulation signal is applied mechanism and the influence of cutting geometry
in the scanning direction while taking an LFM across the surface, which might otherwise remain
image. Compared to the non-modulated LFM unseen.
Figure 98. An atomic force microscope (AFM) 3-D image of an ultra-high-speed face-milled austenitic stainless steel surface. [(ourtesy of
Jeol (UK) Ltd.l
3.4.4 Ultrasonic force microscope: tion of the UFM to local elastieity (i.e., finer than 4
nm), with sensitivity differences in the elastic
developments moduli to better than 0.5%.
UFMs have the ability to detect cracks and delam-
The relatively re cent development of an ultrasonic inations, based on the prineiple that cracks interrupt
force microscope (UFM) amalgamates acoustic the propagation of acoustic waves - a widely used
microscopy, with its sensitivity to elastic properties, technique in ultrasonic non-destructive testing
with atomic force microscopy, having nanoscale (NDT) and acoustic microscopy. The UFM has the
resolution imaging for materials. In the UFM instru- capability of inspecting either surface or subsurface
mental technique, a high-frequency ultrasonic cracks to nanoscale resolution. Although the UFM
vibration with a frequency of several megahertz is instrument offers considerable scope in assessment
applied to a sampie that forces it to elastically of surface and subsurface conditions, its physics
"indent" itself against a static AFM tip. This tip is have yet to be fully understood. By way of example,
positioned at the end of a force-sensitive cantilever, the thin layers of water that cover virtually every
which has very high stiffness at megahertz frequen- surface in an ambient environment act at ultrasonic
eies (see Figure 99a). The contact between the AFM frequeneies as a tough sticky film, modifying the
tip and the sampie, being only a few nanometres in UFM signal. Fortunately for the aspect of UFM
size, serves as a mechanical diode, detecting the imaging, the images can be acquired at different
amplitude-modulated ultrasonic vibrations in the "normal" forces and this enables differentiation of
kilohertz frequency range. The mann er in which the the elastic and adhesive contributions, resulting
system operates is analogous to that of a crystal from the influence of minute levels of water. This
radio (see Figure 99b). The UFM instrumental tech- approach to discrimination of contributing effects
nique takes advantage of the intrinsic properties of suggests a way towards quantitative measurements
the AFM cantilever, being of high stiffness at the of nanoscale elastic and surface adhesive properties,
indentation frequency (i.e., 10 2 to 104 times greater while another manner of controlling the surface
stiffness than at the lower modulation frequency) adhesion problem is to use the UFM in a liquid envi-
and has significantly better force sensitivity at this ronment. This development of an "underwater
modulation frequency. UFM" not only reduces potential damage to delicate
Owing to the advantages found when using the material, but also enables a direct study of nanoscale
UFM, the elastic properties of many materials can elastic properties of materials such as biopolymers
be readily determined and this indicates the remark- and medical materials in their natural environment.
able co nt rast between them, from soft polymers to One of the latest discoveries is that ultrasonic
very hard ceramics. For example, the AFM topo- waves can be direcdy propagated from the base of
graphic image shown in Figure 100(a) indicates an the minute AFM cantilever, travelling down to its
interface on a surface as a jagged trench that divides end, in a similar manner to light propagating along
a silicon carbide fibre (i.e., positions land 2) and a an optical fibre. These ultrasonic waves can vibrate
mullite matrix (Al z0 3 -SiO x ) at position 4. By util- the AFM tip at megahertz and even sub-gigahertz
ising the "elastieity image" in Figure 100(b), much frequeneies. The cantilever simultaneously acts as a
greater definition - and hence detail - of the inter- stiff and high-quality conductor of high-frequency
face structure can be seen. In Figure lOO(b) a rela- ultrasonic vibrations, while also acting as a gentle,
tively soft intermediate concentric carbon-rich layer sensitive detector of non-linear ultrasonic force at
(position 2) and a softer reaction layer (position 4) the sampie frequency of several kilohertz. This dual
separate the higher-stiffness regions of both the Sie ability is of significant benefit, enabling bulk mate-
and mullite. Other images (Figure 100c and d) are rial sampies of materials to be studied by the UFM,
also depicted, comparing topographical images that as access is only necessary from one side of the
were simultaneously acquired to the FMM image sampie.
(different region; Figure 100c) with an FMM image An intriguing further development in the UFM is
of the area shown in "c" (Figure 100d). When applied the combination of ultrasonic vibrations from both
to semiconductor low-dimensional structures such the sampie and cantilever. When such vibrations
as that found in quantum wells and dots, this mate- occur at adjacent frequeneies, the AFM tip detects
rial-dependent elastic contrast enables one to differ- the oscillating force at the difference frequency, in a
entiate between areas of disparate material similar manner to that of a heterodyne radio
compositions - for example, image the percentage of receiver, prompting the name for this new instru-
Ge in the SiXGe 1_Xcompound - together with high- ment: heterodyne force microscope (HFM). Just as
lighting the growth defects, or to detect residual modern heterodyne radios are far superior to crystal
polishing damage. Defect-free areas such as nanos- detectors, the HFM has superior sensitivity to small
tructures can be employed to test the lateral resolu- vibrations than that of a UFM. Even more significant
u ace mlcroscopy
(a)
Microfabricalcd canlilever
~
La er
(b)
\ j_
Insta nt force acting on thc tip, " recUfied" by the tip-surface
F , force acting belween non-linear contact
AFM tip and surface
r.= ""«Iod 'y'fM
Ö, tip-surface distance
Figure 99. (a) Design of the ultrasonic force microscope. (b) Principle of non-linear detection of ultrasonic vibration in UFM. [(ourtesy of Dr
O. Kolosov, Isis Innovation and University of Oxford.]
InClustrial metrology , .
o 4 8 12 16 jJ.m 0 4 8 12
Figure 100. Topography (al and UFM (b), topography and FMM (dl images of a sam pie made of coated SiC fibre embedded in a mullite matrix
(A 120l -Si0 2), image width 10 f.lm. [Courtesy of Dr 0, Kolosov, Isis Innovation and University of Oxford.]
(a) Photoelectron spectrum of lead superimposed (b) Sigma Probe is an XPS instrument and is optimised for
on a schematic diagram of the electronic analysis of small areas.
structure of the element
4f
4p 4p4s '
Binding
cncrgy cncrgy
Analyscr
Figure 101. The important elements of an X-ray photoelectron spectroscopic (XPS) instrument. [(ourtesy of VG Scientific.]
example, even factors such as the sub-monolayers of (for chemical analysis) and has the following char-
material can affect bonding properties. Hence, acteristics:
gaining an understanding of these surfaces requires
sophisticated and powerful analysis techniques, • surface sensitivity - typically, the information
typified by that of X-ray photoelectron spectroscopy depth is less than 10 nm; by comparison, an EDX
(XPS). information depth might be several micrometres;
The XPS instrumental technique and associated • elemental detection - all elements with the excep-
equipment are shown in Figure 101; the technique is tion of Hand He can be detected;
sometimes referred to as "electron spectroscopy" • chemical state identification - chemical shifts in
InClustrial metrology , .
(a) Spectrum of barium acquired in 10 seconds using a (b) An overlay of two silicon images.
monochromated X-ray source
Bn 3d
2.0
-( I)
CI.
u
S OKLL
C 1.0
.... Ba N
.-
~
s Ba ~p
BIl4d
Ba ~ s I
Cl
0~10
~0~
0---8~0~
0---6~0~
0---4
~O=
O--~~~~0
Binding Enel'gy (e V)
--
=
----. -
(c) ARXPS measurements from a GaAs
surface, showing the presence of an
oxidised region at the surface. Right: a
montage of
As 3-D spectra taken at aseries of angles,
showing the change in relative intensity of
the As in the oxide and GaAs states
20 40 60 80
Angle (Degrees)
Figure 102. Just some of the X-ray photoelectron spectroscopic (XPS) graphs and images available from quantitative surface assessment.
[(ourtesy of VG Scientific.]
the spectrum indicate the chemical state of the surface region. For many technological disciplines,
element; it is essential to be able to analyse very small surface
• quantitative analysis - the sensitivity of XPS to features. These surface features may be such prob-
an element is independent of the matrix in which lems as conductive tracks on semiconductor mate-
it is found. Sensitivity factors can be used to rials, areas of impurity on ceramics, or likewise for
quantify the spectra produced. polymers impurities. Apart from taking spectra
from small areas, some XPS instruments produce
The XPS method relies upon the photoelectric chemical images or maps from the surface of the
effect, where the material to be analysed absorbs the specimen. The illustration shown in Figure 102(b)
X-rays and electrons are rejected; these are then depicts an overlay of two XPS images from a semi-
detected and their kinetic energy analysed. The conductor device. Both images use the Si 2p peak,
kinetic energy of a photoelectron depends upon but one (red) is of elemental silicon, while the other
(green) is from silicon in the form of its oxide. These
1 the element from which it was ejected; are representations of chemical state images and
2 the orbital in the atom from which the electron have a spatial resolution of approximately 1 fLm.
originated; X-rays generate photoelectrons from deep within
3 the chemical state of that element. the matrix, with those in the top several nano-
metres being able to escape from the solid without
As an example of this XPS spectrum, that of lead undergoing inelastic collisions. If the electrons are
is shown in Figure 101(a), superimposed onto a collected along the surface normal, then consider-
diagram showing its electronic structure. This able information can come from this region, near the
diagram indicates where the electrons that form surface. However, if electrons are collected at a
each of the peaks originate. grazing emission, then the surface sensitivity is
All XPS instruments have three major compo- further increased. The escape depth varies with the
nents: the X-ray source, the energy analyser and the sine of the take-off angle, relative to the surface.
detector (see Figure 1OIc). The X-ray source can be In angle-resolved XPS (ARXPS), this phenomenon is
either monochromated, or non-monochromated. It exploited to study the variation of composition of
is accepted that monochromators provide an the specimen with depth. An ARXPS assessment
improved energy resolution over their non-mono- is usually performed by setting the angular accept-
chromated counterparts, providing a focused spot ance of the spectrometer to a small value (typically
size of the X-ray beam to smaller than 15 fLm - 1-10°) and measuring the XPS spectra at a range
which can be the case. The energy analyser is usually of sampie angles. Figure 102(c) shows ARXPS data
of the spherical sector type. A lens is normally fitted from GaAs, which has a thin oxide layer at its
to the energy analyser to maximise the number of surface. Measurements were made of the Ga, As and
photoelectrons entering the analyser and to define o peaks as a function of angle and for the Ga and
the area from which the electrons are collected. The As both the elemental and oxide peaks were meas-
detector is usually an array of channel electron ured. The data observed at small angles is dominated
multipliers or a channel plate. The complete instru- by the surface composition, while the data at larger
ment must be housed in an uhra-high-vacuum angles has a greater inftuence from the bulk mate-
(UHV) system, so that surfaces remain uncontami- rial. The decrease in the oxygen and oxide peaks will
nated and the photoelectrons have a sufficiently therefore indicate the presence of a thin surface
large mean free path to reach the detector. A typical oxide.
variant of this type of instrument is shown in Figure Many more analytical activities can be under-
101(b), where it has a spatial resolution that is less taken with an XPS instrument, such as surface
than 15 fLm. topography (Figure 102d), depth profiles or sputter
An XPS experimental procedure would usually profiling, to identify impurities at interfaces and so
commence with the acquisition of a survey spec- on, as it is a quantitative chemically specific analysis
trum, to identify the elements present in the spec- instrument for both conducting and non-conduct-
imen. This acquisition tends to be rapidly taken ing surfaces. A wide range of XPS-based instruments
over a wide range of bin ding energies at low resolu- are available to suit specific and general analysis
tion (see Figure 102a). After acquiring the survey needs, often being the principal surface analytical
spectrum, aseries of high-resolution spectra are instrumentation purchased for surface science labo-
normally acquired for each element of interest, ratory and industrial studies.
providing quantitative information about the
Uchida, H. et al. Single-atom manipulation on the Si (111) 7 x 7
References surface by scanning tunneling microscopy (STM). Surface
Science 287/288,1993,1056-1061.
Warren, P.D. et al. Characterisation of surface damage via contact
Journal and conference papers probes. Nanotechnology 7, 1996,288-294.
Wolstenholme, J. XPS reveals all about the state of the surface.
Dinelli, F. et al. Elastic mapping of heterogeneous nano-structures Materials World 7(7), 1999,412-414.
with ultrasonic force microscope. Proceedings of Surface and Yoshimura, M. et al. Low-coverage, low-temperature phase of Al
Interface Analysis, Basel, Switzerland, 1999. overlays on the Si (111) (-7 ( 7 structure by scanning tunneling
Griffith, J.E. et al. Characterization of scanning probe microscope microscopy. Physical Review B47, 1993, 13930-13932.
tips for linewidth measurement.Journal ofVacuum Science and Yuan, C.W. et al. Low temperature magnetic force microscope uti-
Technology B9 (6), 1991,3586-3589. lizing a piezoresistive cantilever. Applied Physics Letters 65,
Hill-King, M. Measurement in the detail. Quality Today March 1994,1308-1310.
1999,22-26.
Hibino, H. et al. High-temperature scanning-tunneling-micro-
scopy observation of phase transitions and reconstruction of a
vicinal Si (111) surface. Physical Review B47, 1993, 13027-13030. Books, booklets and guides
Hutter, J.1. and Bechhoefer, J. Calibration of atomic force micro-
scope tips. Reviews of Scientific Instruments 64, 1993, 1868- Barrett, C. and Massaiski, T.B. Structure of Metals (3rd edn).
1873. Pergamon Press, Oxford, 1980.
Ichimiya, T. et al. Formation of (21 ( (2l structure by gold deposi- Briggs, D. and Seah, M.P. Practical Surface Analysis, Vol. 1. Wiley,
tion on Si (111) (3 ( (3 Ag surface and the wavering behavior. NewYork.
Surface Review and Letters 1, 1994. Cullity, B.D. Elements of X-ray Diffraction. Addison-Wesley,
Kolosov, O. and Yamanaka, K. Nonlinear detection of ultrasonic Reading, MA.
vibrations in an atomic force microscope. Japanese Journal of Gonzales, R.C. and Woods, R.E. Digital Image Processing. Addison-
Applied Physics 32(Part 2, No. 8a), 1993, Ll095-Ll098. Wesley, Reading, MA, 1992.
Kolosov, O. Imaging the elastic nanostructure of Ge islands by Hull, D. Introduction to Dislocations (2nd edn). Pergamon Press,
ultrasonic force microscopy. Physical Review Letters 81 (5), 1998, Oxford,1979.
1046-1049. Jeol (UK) Ltd. Invitation to the SEM World.
Kolosov, O. UFM shakes out the details at the nanoscopic scale. Howland, R. and Benatar, 1. A Practical Guide to Scanning Probe
Materials World December 1998,753-754. Microscopy. Nikon Corp.!Park Scientific Instruments, 1996.
Kuk, Y. and Silverman, P.J. Scanning tunneling microscope instru- Kuzmany, H. Solid-State Spectroscopy. Springer, Berlin, 1998.
mentation. Review of Scientific Instrumentation 60(2), 1989, Vickerman, J.c. Surface Analysis: The Principal Techniques. Wiley,
165-181. New York, 2000.
Markoff, J. A novel microscope probes the ultra small. New York Walls, J.M. Methods of Surface Analysis. Cambridge University
Times 23 February 1993, Ci, C8. Press.
Nechay, B.A. et al. Applications of an atomic force microscope Watts, J.F. An Introduction to Surface Analysis by Electron
voltage probe with ultrafast time resolution.]ournal of Vacuum Spectroscopy. Oxford Science.
Science and Technology May/June 1995,1369-1374. Wiesendanger, R. Scanning Probe Microscopy. Springer, Berlin,
Sato, T. et al. Dynamic observation of Ag deposition process on Si 1998.
(111) surface by high-temperature scanning tunneling micro- Yates Jr, J.T.ExperimentalInnovations in Surface Science. Springer,
scopy.Japanese Journal of Applied Physics 32,1993,2923-2928. Berlin, 1997.
Schöfer, J. and Santer, E. Quantitative wear analysis using atomic Desjonqueres, M.-C. and Spanjaard, D. Concepts in Surface Physics.
force microscopy. Wear 222(2),1998,74-83. Springer, Berlin, 1996.
Stahl, U. et al. Atomic force microscope using piezoresistive can-
tilevers with a scanning electron microscope. Applied Physics
Letters 65, 1994,2878-2880.
Roundness and
cylindricity
135
Dialgauge
Maximum
measured
difference
_____ J
Vertical
movement
of
workpiece
Bearing
Lubricating film
Eccentric undercut
~_
I
_ Axis of ehe (WO end bearings • an elliptical shape - having a major and minor
axis of different lengths (Figure 107 "B");
• a trochoidal or three-Iobed shape - exhibiting a
difference in distance points on the periphery to
its centre (Figure 107 "C").
c
B
r
25 111m inserted.
this hole is 1125.1 Olm.
LCJhcd s harc
Figure 109. Differenees between measured and effeetive sizes. (Courtesy ofTaylor Hobson.)
4.1.1 Roundness measurement: basic in a vee-block (BS3731 : 1987) and carefully rotate it
with a dial gauge or dial test indicator in contact with
approach the surface (Figure 103a, b). A truly round part will
show no movement on the dial gauge pointer;
In the previous section it was mentioned that however, if the component is not round then irregu-
departure from roundness cannot always be fuHy larities as they contact the vee-block's sides will
detected, or indeed measured by dial guage static cause the part to move up or down. These component
techniques (BS3730: Part 3). If access to sophisticated irregularities (Figure 103a and b) will dis pi ace the
roundness instrumentation is not available, then dial gauge's plunger as the part is slowly rotated; "cor-
some degree of elemental roundness measurement rection factors" should be applied. The amount by
by the rotation technique can be made. The simplest which the gauge pointer is displaced depends on
method that can be adopted is to place the part several factors:
InClustrial metrology , .
• in-phase - with a wide vee-block face angle Figure 110. Multidimensional modular receiver gauge and concen-
(Figure 103c); tricity inspection with data capture and manipulation. [(ourtesy of
• out-of-phase - with a narrow vee-block face angle Marposs Ltd.)
(Figure 103d).
NB: See BS3730 Part 3 (Figure 103 "Summit and rider
tion of the measurement status, even from a distance,
method").
where for example:
Vee-block roundness measurement is essentially
• green illumination indicates the part is within the
a three-point technique, with several variations in
tolerance limit;
the mann er in which it can be applied, such as when
• yellow illumination indicates the part feature is at
inspecting a large external diameter or a similar
the tolerance limit;
internal bore.
• red illumination indicates measurement is out-
A simple artefact can be manufactured that in-
side the pre-set limits.
corporates the dial gauge and datum feet, its body
shape designed to suit the particular metrological
Multiple diameter assessment with such
application. Bench centres for longer parts, with
modular-constructed receiver gauge elements allows
centre-drilled ends, are a useful inspection apparatus
the part's functional performance to be assessed.
for assessing either roundness or concentricity of a
By arranging the transducer indicators in suitable
stepped-diameter shaft, in conjunction with a dial
banks (see Figure 110) a host of the component's
gauge. This technique is further refined when bench
centres are employed, as they allow all of the above geometric features can be simultaneously assessed.
roundness parameters to be assessed, together with
tapered diametrical features, although care must be
taken to prevent component gravitational sag for
long slender parts. The dial gauge previously men- 4.2 Roundness: measuring
tioned can be replaced by an electronic gauging head
and its associated meter unit, the main advantage
instruments
being that both range switching and data-Iogging
can be undertaken. These latter refinements to radial
The design of a roundness instrument (see Figure
measurement are necessary when many parts are
111 for a schematic diagram of a rotating worktable
required to be inspected and for statistical process
type) incorporates a number of extremely accurate
contro1!quality control applications. This aspect of
parts that are configured to assess specific elements
multi-gauging can be quite sophisticated, as shown
of a part's roundness. The roundness-related
in Figure 110 for a typical modular component
features are:
feature set-up of the myriad of industrial applica-
tions, where a multiple receiver gauge station can • rotation - rotary motion providing the reference
simultaneously inspect critical elements of stepped axis;
diameters and geometric features. Such electronic • rotational axis - this must be independent of the
indicators equipped with a digital display provide part being measured;
both numeric and analogue visualisation of mea- • measuring device - some form of stylus, and a
surement. A three-colour analogue display (e.g. transducer (pick-up), which converts mechani-
green, yellow and red), provides clear visual defini- cal stylus motion into a proportional electrical
Roundness and eylindridty
Horizontllll1djustmcnt
Levclling adjustmcnl
Stylus
Componcnt
under
te t
Ce ntring adjuslmcnt
Table
rotation
Precision
lable
Base
Figure 111. Schematic diagram of the main features of just one configuration for a roundness-testing machine.
piece rotates while the pick-up remains in a set instrument's design; also long shafts, crankshafts
position. For large and notably heavier parts, the and many more large parts can be simply accom-
rotating pick-up type, which rotates the piek-up modated on the table;
(Figure 112b), is preferred. Each type of instrument 3 in order to speed up the measurement task and
has advantages and is more suitable to certain types minimise uncertainty of measurement, com-
of measurement, the choiee of instrument being puter-aided centring and levelling is available as
largely dependent on the antieipated measurements an option on the more basic versions, or a stan-
to be undertaken and the shape and size of the dard feature with the sophisticated versions. This
parts. latter feature is true for both instrumenntal types.
The first equipment available commercially,
"Talyrond I" was of the rotating pick-up type. • Turntable type (Figure 114).
The rotating piek-up design became the model
from which all other manufacturers' roundness- Operational characteristies of this instrument's
measuring instruments were developed. The success roundness configuration include the following:
of the roundness instrument's design was such that
over the years only minor modifications were neces- due to the pick-up not being directly associated
sary to enhance the equipment's capabilities. Most with the spindie, this type of the roundness
of these modifications were necessary to change the
machine is more easily adapted to other measure-
electronics from valve amplification to transistor
ments in addition to roundness, notably concen-
amplification, resulting in the "Talyrond 2" design.
tricity and alignment. Repositioning the pick-up
Later, integrated circuit electronies replaced the
transistors in the design of the "Talyrond 4". The on a component - transferring it from external
current instrument is illustrated in Figure 113; this diametral measurement to an internal surface -
instrument has the ability to accommodate an has no effect on the reference axis. Further, pick-
extremely large workpiece size and weight, featuring up positioning is simple; enabling it to reach into
automatie component cent ring and levelling - an slots or to the undersides of shoulders becomes a
important feature with parts that are very large and straight forward operation, without having to
less moveable. resort to using long, or cranked stylus arms;
2 by incorporating a straight vertical movement of
the pick-up, any straightness measurements can
Comparison of instrument types be made without modification to the spin dIe, or
its mounting;
This seetion will discuss the reasons why two types 3 the turntable weight, together with the part
of roundness instruments (Figure 112) were devel- being measured, has to be supported by its
oped, explaining design differences and, more spindie bearings, which places a restrietion on
importantly, the situations why one type is more the weight of the part requiring measurement;
suitable than the other for certain kinds of round- moreover, it also limits the amount of offset that
ness measurement: can be permitted;
4 computer-aided centring and levelling are stan-
• Rotating pick-up type (Figure 113). dard on the more sophisticated instruments. If the
centre of gravity of the workpiece falls into the tri-
Operational characteristies of this roundness instru- angular demarcation marks engraved into the top
ment's configuration include the following: of the table's surface (see Figure 114), the manual
and somewhat time-constraining centring and
the precision spindie need only carry the com- levelling activity becomes an automatie adjust-
paratively light and constant load of the piek-up ment function.
- its high accuracy is attainable without excessive
cost;
2 as the worktable is not part of the measuring
system it can be of substantial construction, 4.2.2 Spindie and bearings
so the weight of the part is not a limitation of
measuring capacity. Moreover, large parts - like In any roundness-measuring instrument, the instru-
the four-cylinder engine block shown being ment's spindie is the most vitally important com-
inspected in Figure 113 - can be of asymmetri- ponent in its assembly. Here, the instantaeneous
cal shape, with the bore or surface being error of rotation is the key feature of the spindie;
measured offset from the centre of gravity of the since it is from the axis of rotation that all measure-
part. This offset load is not a limitation with this ments are taken, it must allow only minute deviation
(a) Thrntable type of instrument
Radial adjustment
Component
Stylus
Table
Radial adjustment
Component
from its fixed centre as the spindie rotates. To without loss of accuracy. Moreover, it allows the
achieve this minimal spindie error, not only must the spindle's kinematics to be quite sophisticated,
spindle's bearings be of the highest quality, but also as it can be traversed axially for straightness
they should approach almost perfect roundness. measurement and, as the same bearings are
Several types of bearing design can be employed employed for either rotary and linear motions,
in the construction of precision roundness spin dies; the axis of rotation is also the axis of linear
these include: movement;
• hydrodynamic bearing - oil (Figure 116) - from
the original roundness instrument concept, this
• dry bearings (Figure 115) - these are normally type of bearing has predominantly been used
dry, but can be of the type that are lightly lubri- for the rotating pick-up instruments. Metal-to-
cated, using a steel ball rotating in a plastic cup metal contact occurs between the two spherical
for the thrust bearing and pads of the same mate- bearing members when the spindie is stationary,
rial for controlling radial movement. This type of but as the spindie rotation reaches or exceeds 6
bearing requires minimal maintenance, having rev/min a thin and even film of oil is maintained
constant accuracy under varying conditions of between the surfaces - due to the hydrodynamic
speed and load, accepting li mi ted radialloading. "wedging effect" - resulting from the action of
Its main limitation is that the load-carrying the rotating surfaces. This film of oil is of constant
capacity is restricted; thickness at a steady speed. At either slow speed
• ball bearings (not illustrated) - these are of a type conditions or heavy loads the oil film may cease
in which the balls support the spindie both cir- to exist. These latter operational conditions
cumferentially and longitudinally. This axial and means that such hydrodynamic bearings are
radial support enables the spindie to be utilised mainly used where the load is relatively small and
in either a vertical or longitudinal orientation, rotational speed is constant. One factor that needs
Roundness and eylindridty
Figure 116. Hydrodynamic bearing for rotating pick-up roundness-testing machine. ((ourtesy ofTaylor Hobson.)
InClustrial metrology . .
• the bearing stiffness is increased (meaning are the preferred selection for highly sophisticated
that sideways force applied to the bearing precision instruments having heavy load-carrying
has comparatively litde effect on the axis of capacities.
rotation).
____ 1- _ _ _
Oilout on out
Oilin Oil in
Figure 117. 5chematic illustration of the principle of hydrostatic bearings used for turntable-type roundness machines. ((ourtesy of Taylor
Hobson.)
(a) Dry (b) Hydrodynamie
Bearing housing
Instrument's
spindle
Oil
Spindle
Air pressurised
Best C D D C D D
i D B B D C C
J, B C C B B B
Least good A A A A A A
Air 0.025 12
Hydrodynamic 0.100 n/a
Dry 0.030 20
Air 0.040 50
Hydrostatic 0.050 225
Horizontal surfaces
In most instruments the pick-up can be positioned
to detect vertical displacements of a horizontal
Figure 120. "Self-centring iris" accessory for speedy set-up and effi- surface, such as an end face (Figure 121, trace 9), or a
cient processing of batch production requirements. ((ourtesy of shoulder from a plane that is square to the axis. The
Taylor Hobson.)
whole geometry can include measurements similar
to those shown in Activities D and E illustrated in
Figure 121. By now it should be appreciated that the
• Activity B (traces 1,2,3 and 4) - can be utilised trace is taken only around a circular track and, there-
to establish a new datum running through the fore, does not indicate true flatness of the surface.
whole component. A component feature that has previously been
• Activity C (traces 7,8 and 9) - having completed centred which has a spherical geometrical form
Activity B, a flatness profile of trace 9 will not only would give a trace that superficially appears to be
show the peak-to-valley of the circular trace on flat. However, it is normally only when aseries of
the plane, but can also be displayed with its traces taken at different radii are assessed in rela-
squareness relationship to the defined axis. Flat- tionship to each other that the true value of flatness
ness traces 7 and 8, can once again be compared can be appreciated. This assessment can only be
for squareness to the established cylinder axis, or undertaken if the instrument has a known relation-
for parallelism of their flatness planes. ship between the horizontal and vertical datum.
• Activity D (traces 5 and 6) - the vertical traces When assessing the ftatness of horizontal surfaces,
(5 and 6) can be displayed in relation to a "least the probe must not be moved to the surface between
squares" line or "minimum zone straightness". By traces.
assessing one of the traces as the datum and
comparing it with the trace obtained at 180°, it is Straightness
possible to display and print out the parallelism
ofthe bore. Straightness can be measured using a pick-up
• Activity E (trace 10) - using the datum previously traversing vertically with the worktable stationary
derived from traces 1,2,3 and 4 anyadditional (Figure 121, trace 5). Measurements can be made
roundness profiles can be assessed for eccen- relative to the line of traverse, which is normally
tricity, concentricity and runout (trace 10). parallel to the roundness axis of rotation; this allows
for both the roundness and straightness measure-
One of the main features of the modern analysis ments to have the same datum and can therefore be
packages is the flexibility to store data in raw form, related to each other without difficulty. Such combi-
which can then be manipulated for additional nations of component roundness and straightness
roundness analysis to give a more precise picture of employing the same initial set-up are another
component accuracy. feature of the whole geometry measurement.
InClustrial metrology , .
180· f-Ir----f---I+-- O·
2 4
270· , ...... . .. 1
3
4
Roundness Cylindricity Coaxiality
Datum
9
Measurement Points on Part:
C: Flatness/Squarenessl
Parallelism
1"7""--,.'" ••••••••••••• ;. •••••••••••••• "17"-+"--'"'1
O·
t+1±1
90· 180· 270·
i
360·
...............
4~ ~-~
~10
D: Vertieal Surfaces
E: ConcentricitylRunout 5 6 5
90·
1
I
11
I
I
..
10 270·
Straightness Parallelism
Figure 121. Typical roundness, straightness and functional part measurements that can be undertaken. ((ourtesy ofTaylor Hobson.)
Roundness and eylindridty
Figure 124. Comparison of various sizes of ball-tipped and hatchet-shaped styli. (Courtesy of Taylor Hobson.)
factory output on a week-by-week basis. Conversely, In many cases, if the roundness instrument has a
in the case of roundness assessment, it is often diffi- built-in recorder this allows the traced profile to
cult at first to comprehend that the visual image of have a direct angular relationship to the component,
the displayed profile does not give a clue to the shape because the recorder rotates at the same speed as the
of the undulations on the part. The reason for any spindie. The PC-based roundness instruments have
confusion in displayed profile interpretation was just analytical capabilities, with the display showing the
mentioned, this being the result of the radial peak data at the 0° angular position of the spin dIe on the
and valley heights being retained at their correct screen at the (conventional) 3 o'clock position. This
magnification. While the radial enlargement is great, rotational and angular datuming facility enables the
the accompanying circumferential magnification is user to relate any roundness angular feature abnor-
often less than xl, this being a reduction resulting malities to a known spin dIe position.
from the trace diameter, which must of necessity be
smaller than that of the vast majority of parts that are The displayed profile is shown relative to a reference
measured. The effect on the polar plot of this dis- circle.
parate magnification can be visually shown by the
group of displayed profiles of a four-Iobed part, Current roundness instruments can display the
which in these examples has a 3 f.1m variation in measured profile with one of the four reference
radius and is illustrated in Figure 126. Using a low circles superimposed on it - more will be said on
magnification (Figure 126a) the displayed profile will this topic in Section 4.5. This facility allows the oper-
visually differ only slightly from a perfect circle. At ator to obtain, say, a peak-to-valley value based on a
higher magnifications, the radial distance between pre-selected reference circle centre, by the simple
the outermost and innermost portions of the trace expedient of assessing the largest peak and the
will be proportionally increased (Figure 126b), until deepest valley from the reference. Most software can
at an optimum magnification the displayed profile output the peak-to-valleyvalue, together with eccen-
appears exaggerated, as shown in Figure 126(c). tricity and the runout of the profile - the latter being
These visual effects emphasise the fact that the dis- related to a selectable datum such as the spindle
played profile's shape is not simply a visually aXlS.
enlarged view of the cross-section: the displayed
profile does not contain concave portions. This visu-
ally based fact can be demonstrated by adjusting the
magnification still further to produce a square dis-
4.5 Roundness measurement
played profile (Figure 126d). In all four displayed from the display
profiles the measured maximum departure from
roundness (negating the inftuence of different scales) Previously it was explained that the roundness of a
is identical, namely 3 f.1m. component was expressed as the difference between
'" '.'" ~
....
'A A' 'A
A'
A. ..... A. .....
~.
. ...
..'.
(a) • ~-++----:----+----;--++---: ... • :..-..+---;.----t----:--t-+---:.... (b)
"'.
",. .
..
",
~.
"' .
.... . ...
....
.... ....
'" '"
'. ~
'"
... ' . ~
....
.... A .... •
'A
A' 'A A' ,
, . .... , .....
A. I
, A.
~.
I \
.... ....
(c) • :....-_-'--+---f---t----:'---+-- ... • :..--+-----t----+----+-+--- ... (d)
"'.
",. ....
.. "'.
....
.
. ...
.
... ...
.... ....
Figure 126. Effects of magnification on the visual shape of the displayed profile. (Courtesy ofTaylor Hobson.)
The scale indicates that each division represents (a) 5 fLm, (b) 2 fLm, (c) 1 fLm and (d) 0.5 fLm on the trace.
the greatest and least distance of the profile from manual technique allows the highest peak and the
an origin. To enable a measurement of this distance, deepest valley to be found and, using the pre-set
or more correctly to assist in identifying the distance magnification utilised in this roundness assessment,
between two features, it is normally necessary to the departures from roundness can be determined.
utilise a reference circle, or a pair of circles, which The difference between the two features on the
can be drawn, recorded or otherwise superimposed displayed profile can be numerically assessed. This
onto the graph. Positioning the reference circle(s) operator-dependent procedure was somewhat sub-
with respect to the displayed profile is not an jective in interpretation and therefore accuracy and
arbitrary activity, as its chosen to fulfil specific repeatability were open to conjecture. The actual
conditions. Only in this manner can an unambig- positioning of the reference circle cannot readily be
uous and repeatable value for the departure from determined by manual methods, but this problem
roundness of any particular roundness profile be can be overcome by software that can display and
obtained. print out the reference circle(s) on the profile. These
The roundness value has historically been calcu- software facilities will not only display the peak-to-
lated by situating a transparent template of radial valley information, but can also indicate its com-
rings over a graphed profile and with the aid of the puted centre and any other relevant data to a
radial rings, centralising the profile visually. This selected datum.
4.5.1 Roundness reference circles for more exacting preClslOn, instrumentally.
Hence, the departures from roundness is the
distance of the lowest valley (V) from the circle,
Standardisation once again being equal to P + V, as now the value
of P in this case is zero (ZJ;
The measurement of roundness, like the majority of 3 Minimum zone circles (MZC) - these are two
other types of measurement, is subject to national concentric circles enclosing the traced or
and to international standards. These standards measured profile such that their radial departure
specify the manner in which measurements should is a minimum (Figure 129). The roundness value
be made and how the results are to be expressed - is then given as the radial separation Zz;
for example, which reference circles are preferred. 4 Maximum inscribed circle (MIC) - this is the circle
Conformity to these standards will ensure that any of maximum radius which will be enclosed by the
measurements undertaken on different instruments profile data (Figure 130). The departures from
are compatible. This conformity requirement is roundness is then given as the departure (peak) of
essential when components are manufactured in one the profile from the circle and is occasionally
country, or by a subcontractor, that have to be
matched to parts made elsewhere.
Manufacturers of roundness-measuring instru-
ments try to ensure that their products closely
conform to the requirements of a standard. Thus,
when a designer comprehends that a certain round-
ness tolerance is specified this component can be
inspected, measured and either accepted or rejected,
according to whether it conforms to tolerances spec-
ified unambiguously not only within the company
but in fact anywhere in the world.
The standards in Britain, Germany, Japan,
America and elsewhere have accepted four reference
circles, fulfilling different roundness requirements:
(a) Examples showing how the relative positions of peaks and valleys can influence the
"minimum zone width"
MZC and component MZC not coincident
axis are coincident with component axis
(b) An example of how a single large peak can increase the apparent departures from roundness
Exceptional peak
Figure 131. Ca ses where a single dominant peak, or its relative position, (an increase the "minimum zone" width, hence the apparent
departures fram raundness. (Courtesy ofTaylor Hobson.)
)
1
Minimum zone circles
Circumferentiallay
Trochoidal, or three-Iobed
geometrie shape
the same manner as a polar plot roundness calcula- its surface roughness, which would otherwise give
tion. The linear plot of a roundness trace can visually misleading information concerning the relative
highlight any harmonie departures from roundness roundness of the part's profile. Mathematical
by the trace's sinusoidal deviation from a straight filtering can be applied to the roundness profile, or
line, as indieated in Figure 132, where a three-Iobed modified profile, to separate out the roughness from
(trochoidal) component geometry is depicted on a the general form. As an alternative action, the depar-
traced profile and its associated linear plot. tures from roundness can be suppressed, enabling
examination of the periphery for surface irregulari-
ties at higher roundness magnifications (see Figure
4.5.3 Filtering and harmonics 133). Internationally accepted filters are:
..
.. ..... performance. The component's harmonics are a
product of various factors, such as component
geometry, part material and its method of manufac-
ture. In general terms, the harmonics of a profile can
be grouped together in the manner indicated in
• ~~--~------+-------~--~~ Table 14.
.. ."
"
On a circular profile the harmonie can be thought
of as a uniform waveform (sine wave) that is super-
imposed onto the part's surface (see Figure 134) .
". . Unless a "true cireIe" occurs during roundness
measurement, it can be stated that any roundness
profile will consist of aseries of sine waves that are
combined to form the overall roundness shape and
A its resulting trace. This harmonie feature can be seen
in the series of minimum zone circle (MZC) polar
Displayed profile B: The same traces on an identieal part illustrated in Figure 135,
profile with the lobes filtered where different filters have been utilised to filter out
out to allow the display to be
the relative harmonics (a-d) at aseries of undula-
shown at 1 !lm, enabling the tion cut -off values.
smaller irregularities to be
The calculation of harmonies in a representative
more c1early seen.
polar trace for the harmonie behaviour exhibited in
Figure 134 is comparatively simple to achieve, in
essence by counting the number of harmonics, with
their respective amplitudes being relatively straight-
..•
forward to measure. When a more complex har-
....
monie profile occurs, consisting of either one or two
. harmonics (though typically a component often has
between 10 and 12), then it is essential to use soft-
• ware to perform the harmonie analysis. These dis-
·..
~
Harmonk Cause
1st (1 upr) Function of measurement - only caused by the setting-up error on the instrument being utilised to measure the
departures from roundness. The amplitude of this harmonie is equal to the eccentricity of the part, relative to the
spindie axis of the roundness instrument
2nd (2 upr) Function of measurement or manufacture - this aspect of harmonics is generally termed ovalityand can be caused
either by a setting-up error of the roundness instrument, or the part being machined out-of-square to its axis of rotation
3rd- 7th Function ofmanufacture - these harmonics are normally introduced by the work-holding technique during
manufacture. By way of illustration, if a three-jaw chuck were used to hold the part and excessive clamping force was
employed, then upon machining and removal of the clamping forces a three-Iobed part would have been produced
lSth-upwards Function of material and manufacture - this aspect of harmonie behaviour is usually introduced to the part by either
machine instability (self-exciting vibration - chatter) or by the reaction of the materials used in the component, cutting
tool and lubricant - if used
5th harmonie
Figure 134. Typical harmonics occurring on the roundness displayed profiles. ((ourtesy ofTaylor Hobson.)
error (eeeentricity of the part to that of the spindie to the influenee of the eomponent's geometry on the
axis), whereas the seeond harmonie mayaiso be due stiffness of the grinding maehine. The harmonie
to setting-up error, in this ease probably due to the histogram given in this example illustrates the diag-
part not being level, that is, the axis not parallel with nostie eapabilities of the software, for interrogation
spin die axis. Conversely, the small group ofharmon- of the departures from roundness eondition of the
ies in the region of the 64th upr level is probably due surfaee profile.
(i)
Damping faetor
12 dB/oet
(c) 150 upr (15 Hz) (d) 500 upr (50 Hz)
(upr: undulations per revolution)
Figure 135. Effect of filtering on an identical profile assessed using the "minimum zone centre" (MZC) at a range of cut-off values.
InClustrial metrology . .
(a) Typical harmonie histogram (FFT) for a part's Mean Square (MS)
roundness profile
Magnitude Compared to the previously discussed RMS tech-
nique, the MS value tends to be more sensitive
to slight variations in the component geometry
and, under these established conditions, it is used
in preference to RMS, where a greater degree of
control is required. It should be obvious to the reader
that
MS = (RMS)2
Gaussian filters
Gaussian filters and, indeed, double Gaussian filters
are now available for many roundness and surface
textureIform instruments; however, they differ from
some current and previous filter types such as the
2CR, RC ISO second order and RC phase-corrected
filters in two distinct ways:
Figure 137. Filtering a eomponent's profile for differing harmonie
• Gaussian filtering does not simulate a specific effects. ((ourtesy ofTaylor Hobson.)
electronic filter, but is purely a mathematieal
function whieh is applied to the profile data;
• the results obtained from a Gaussian filter have
no phase shift and therefore offer more realistie
results.
(a) Establishing a "weighting factor"
Weighting factor
Points of inflection
Cut-off value
Conventional jiltering - "driver" unable to detect the contour of the road ahead until
the car senses the upward or down ward turn of the road and possibly overshoots at
the top of a steep rise.
Gaussian type - "driver" has the ability to look, as in daylight and get a better
reaction to the profile of the road ahead. In this case, the "driver" can see the general
contour of his route.
Figure 138. Weighting and filtering of roundness and surface texture instruments. ((ourtesy ofTaylor Hobson.)
A Gaussian filter has a weighting factor which has such curve inflection points mark the linear distance
a Gaussian shape (Figure 138a); this gives the ability from the arithmetic me an to each of these points,
to take account of data before and after the effective denoting its standard deviation. In Figure 138(b) a
stylus position when calculating the me an line. In simple but effective pictorial representation is given
weighting, one set of numbers are assigned as multi- illustrating the effect of employing a Gaussian filter
pliers to quantities to be averaged, indicating the compared with conventional types.
relative importance of each quantity's contribution
to the average. The cut-off can be established by the
width of the Gaussian curve and is defined as the stope and windows
width between the points of inflection (Figure 138a),
namely the two discrete points on the curve where The term slope refers to the rate of change of radius
the direction changes. In statistical terminology, with respect to angle (dr/dO). In some roundness
instrumental software, the average and maximum the slope can be calculated in terms of a rate of
slopes are given with respect to a window. The main change per degree, in J-Lm/degree. Once the slope at
reason for the measurement of slope would norm- each data point in the window has been calculated,
ally be to control component performance. For then an average value is derived for the window's
roundness assessment, the slope values have similar slope, which is known as window slope. In this
functions to those used in surface texture. The in- instance, the sign (positive ar negative) of the slope
fluence of slope in roundness analysis can be appre- is taken into account, as follows:
ciated if one considers a large slope value; this
will indicate a greater frictional force when utilised Window slope = slope at each data point in window/
in, say, a bearing application. Normally, but not number of data points in window
true for every case, if the visual finish is degraded
this denotes poor wear and hence reduced in-service Since the sign of the slope at each data point is
characteristics for the part. Displaying the average considered in this calculation, it is possible for the
and the maximum values of slope can also allow slopes at each data point to cancel each other out. By
the determination of whether the manufacturing way of illustration, if far example (Figure 139b) a
process was or is consistent. If an increase in the profile window of 5° was selected this would repre-
relative difference between the maximum and aver- sent a window slope of zero J-Lm/degree, whereas a
age slopes occur, then it may indicate that the window of 2.5° would give a much larger value,
production process has changed for one reason or hence introducing a filtering effect. As the 5° window
another. is indexed around the component's profile, the
window slope will change and it will not remain at
zero J-Lm/degree; similarly the 2.5° window would
Windowassessment eventually yield a zero J-Lm/degree. However, the 5°
window would give a lower average slope value when
The window variable operator is usually set to 5° compared to the 2.5° window.
making it, in effect, a filter. The window is the aper- Once the preliminary window slope has been
ture from which the slope values are calculated, the calculated, then this window is moved around the
calculation method being by the number of data profile by 1 data point, allowing a new window slope
points in this window, which are based on the to be automatically calculated (Figure 139c). This
following relationship: procedure is repeated - 1 data point each time - until
a window slope has been calculated for all 3600 data
Number of data points = n/360 x 3600 points. The average slope represents the mean value
far all of the individual window slopes, that is, 3600
where n = window selected (degrees) and 3600 = window slopes are averaged. The maximum slope
number of data points in the profile (one revolution can be considered to be the largest of the window
of the part). slopes.
For example, if a window of 5° were selected, then The two diagrams given in Figure 139(d) illus-
the number of data points used for each assessment trate the "filtering effect" of the window. For a round-
will be ness profile which consists of 6 upr a window of 60°
would not be sensitive enough; it would therefore
5/360 x 3600 = 50 data points yield a result of zero J-Lm/degree. However, if a
window of 30° were selected, this would be most
Pressing this point further, if a window of 15° were sensitive since it would always be in at least one posi-
chosen, then the number of data points used far each tion where it was at the true maximum slope on
calculation would represent the component. This is a "general rule" that should
be used in slope analysis, or more specifically: "The
15/360 x 3600 = 150 points most sensitive window is half the wavelength of the
undulations under consideration, and the most
As has been mentioned, each profile typically insensitive window is equal to the wavelength of the
consists of 3600 data points and, the slope or rate of undulations under consideration". If, for example,
change at each point is calculated. The slope at any just a small difference occurs between the maximum
given data point is derived by taking three adjacent slope and the average slope, it may suggest that the
data points on either side of the respective data point size of the window needs to be reviewed to deter-
- a total of seven data points (which overcomes mine whether it is sufficiently sensitive.
aliasing) - and then fitting a line through all seven Therefore, by selecting an appropriate window as
points. From this newly created line (Figure 139a), a filter and monitoring both the maximum and
InClustrial metrology , .
10 3~ 50 70
---~-------
2° 4 6°
\ / I
-
I /
\ / ~
I/
~ ~5°window
\ / I !'-- 2.5" window
V V
Window slope is
calculated for the
-r------,-..:~::.-.. first window +-===:::!:~z Window slope is
position. calculated for the
second window
position.
Figure 139. Effect of "window slope" and the "window filtering effect" on slope and harmonie analysis. ((ourtesy ofTaylor Hobson,)
average slope values, a high degree of control of meter is so that it acts as an indicator as to whether
component performance can be achieved. For the window is set at a suitable angle. If the average
example, if a bearing has high slope values this will and maximum values are similar, then it is likely that
tend to be "noisy" and, as such, will be more likely the window is at an angle that is not sufficiently
to suffer from premature failure in service. The main sensitive to the component features.
purpose in monitoring the maximum slope para-
4.6 Geometrie roundness
parameters (ISO 1101: 1983/
o =Conc
Ext 1: 1983)
Eccentricity
180° 0°
The parameter eccentricity (Figure 140) is a round-
ness term used to describe the position of the centre
of a profile relative to so me datum point. Eccentricity
is a vector quantity, in that it has both magnitude Datum point
and direction. Moreover, the magnitude of the eccen-
tricity can be simply expressed as the distance
between the profile centre and the datum point,
whereas the direction is expressed as an angle from
this datum point.
Figure 141. Roundness parameter: concentricity.
Concentricity
The concentricity parameter (Figure 141) is similar Runout
to that described for the term eccentricity (above),
but only has magnitude and no direction. Con- The term runout (Figure 142) is occasionally refer-
centricity can be described as the diameter of the red to as total indicated reading (TIR). This para-
circle described by the profile centre when rotated meter attempts to predict the behaviour of a profile.
about the datum point. It may be appreciated that the The definition of runout is: the radial difference
value of concentricity is twice the magnitude of between two concentric circles centred on the datum
eccentricity. point and drawn such that one coincides with the
nearest and the other coincides with the farthest
point on the profile. As a practical parameter runout
is useful, as it combines the effect of both form error
and concentricity to indicate the predicted perfor-
E =Ecc
Datum point
mance when rotated about a datum.
I = Runout
Profile centre ~ ------ - ---- ~ Nearest point
Runout ~ to datum
/ ~
E \
180° ----------~~--------
0°
\
!
/
/
~ //
270° Furthest POi~ '------- ~
from datum ~ ----
NB E =eccentricity value
e =eccentricity angle Datum point
Figure 140. Roundness parameter: eccentricity. Figure 142. Roundness parameter: runout.
the reference plane. The term squareness is a useful
indicator of the fitment behaviour of two adjacent
=FLTt parts in aprecision assembly.
LS reference line I
Coaxiality
k--AxiS
The coaxiality parameter (Figure 145) refers to the
relationship of two cylinder axes, one of which is used
as a datum. This term is useful when attempting to
control the relative motional behaviour ofaxial and
roundness alignments between two adjacent diame-
ters.
F =flatness
Cylindricity
The cylindricity parameter (Figure 146) refers to
two, or more roundness planes used to produce
Figure 143. Associated parameter: flatness. a cylinder where the radial differences are at a
minimum. This cylindricity term will be discussed in
more detail in the following seetion.
Flatness
In the case of flatness (Figure 143) a reference plane CD ISO/DIN
is fitted such that its ftatness is calculated as the = Coax ISO,
peak-to-valley departure from that plane. In round- or Coax DIN
ness reference terminology, either "least squares
-+---~- Coaxiality
circle" (LSC) or "minimum zone circles" (MZC) can value
be utilised for ftatness determination.
Component "B"
Squareness
Once an axis has been confirmed, its squareness
parameter (Figure 144) can be described as: the
minimum axial separation of two parallel planes
normal to the reference axis and which totally enclose Axis"B"
~=sqr I
Component
~Datumaxis master
Axis"A"
(datum)
I,r
?~/--
I~--~"'"
II~~=_-~ I
I ---- ~
stringent tolerances as greater fuel economy
becomes the norm.
Cylindricity measurement
Figure 146. Associated parameter: eylindricity.
In order to measure cylindricity, reference must be
made to the basie definitions previously described;
namely we require an instrument that will measure
4.6.1 Cylindricity radial form or roundness, axial form or vertical
straightness, dimensional uniformity or parallelism.
For many mechanical design and assembly applica- Two possible metrological sources are available to
tions cylindrieal features are crucial as they signifi- perform these measurements:
cantly contribute to the performance of a range of
products, typically revolving equipment, transmis- (a):
sion and part assemblies, precision metrology equip-
Straightness Circularity Taper Combined effects
ment, precision gauges and injection moulding dies,
enabling them to achieve their intended functions.
During the production process several factors can
cause a cylindrical feature to depart from its
intended geometrie shape or profile. Adefinition of
the measure of cylindrieity was given in Seetion 4.6,
but a simpler working description may be in order
here to appreciate its importance in precision engi-
neering applications. If a perfectly Hat plate is
inclined at a shallow angle and a parallel cylindrical
component is rolled down this plate, if it is truly
round then as it rolls there should be no discernible (b): Curved Waisted BarrelIed
radial/longitudinal motion apparent. However, if the
same plate is inclined and now a less-than-cylindri-
cal component is tested that exhibits one of the
departures from a cylindrical shape shown in Figure
147, then as the component rolls down this incline it
will either wobble or deviate in some radial or longi-
tudinal manner - this condition can be said to be
qualitative proof of a lack of cylindricity.
The schematic diagrams in Figure 147 show just
some of the combinations of geometrie departures
from cylindricity, which are invariably caused by NB Cylindrical features having similar deviation levels,
their inherent production processing - more will be aIthough with distinctly differing characteristics
said on this topic in Chapter 5. As can be seen
(Figure 147a), the combined geometrie shape is the Figure 147. Assessment ofthe geometry in eylindrieity.
InClustrial metrology . .
1 coordinate-measuring machine (CMM); tainty for both radial and axial form has been weH
2 form/roundness-measuring instrument. documented, but what is sometimes forgotten is that
the parallelism of the instrument's spindie with
In the former case (CMM), actual volumetrie respect to the column axis needs to be addressed.
assessment of parameters such as cylindricity re- Specifically, such potential spindle-to-column align-
quires a considerable number of measurement points ment error can inftuence measurement - more will
to be made, whieh of necessity takes more time and be said on alignment checking in Chapter 6. These
provide limited accuracy. The exception to these radial slices and their axial displacement factors link
CMMs is when a very expensive CMM is utilised hav- the two-dimensional roundness and straightness
ing sophistieated continuous scanning software with measurements to the three-dimensional or total
rotational datums coupled to analogue probes. Under form analysis that is required for cylindricity
these operational circumstances, the latter case of measurement. It is therefore essential that any
using form/roundness-measuring instruments for measuring instrument used to determine cylin-
cylindricity assessment offers an ideal alternative dricity has the ability to accurately measure radial
measuring technique. form and axial form, together with dimensional
It is convenient when measuring cylindrieity to uniformity.
represent the cylinder by aseries of horizontal slices As mentioned previously, geometrie form toler-
of the radial profiles, where the axial separation is ances and measurements are described in aseries
known (Figure 148). Conventional form and round- of standards, notably ISO 1101: 1983. The inspection
ness-measuring instruments are capable of per- procedure and associated algorithm to determine
forming this type of representation, provided certain the precise measurement requirement are not pro-
criteria are observed. The contribution to uncer- vided in these standards. However, based on the
(~) ..
2883
33.011
3738
41.87 "
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: :
: .
45.9&
50.25
·, · •
:
: : .
54083 : I :
!51104 , :
I
,
83.45
157.811 · :
:
I
n30 : I
78.71 " :
81 .011
85.44
·, · : : :
81178
M.OS
9834
·,:
: :
:
: :
,
10280 '. : : I
10688 I ,
111.18
115.53
11988
124 211
, :
:
·· , I
: ,
:
128.76
13317
. _-
Figure 148. Wire eage eylindricity display, utilising Windows™-based software. ((ourtesy of Taylor Hobson.)
(a) Minimum zone cylinder (MZC) (b) Minimum circumscribed cylinder (MZC)
Cylinder axis
~-r-=-:,- __ Cylinder axis
Peak-to-valley ~---
---
Peak-to-valley ~~
-T
11
1
1 1
I 1 I
I~
I~I
I I'
I I I
I~',
l( --
",-I
--- - , ~
(c) Maximum inscribed cylinder (MIC) (d) Least squares cylinder (LSC)
___ "
~
_'
"--- - - -_/.
- I
I I
I I
I I
I I
I I
I
I
I
I
I I
I
I I
1
Peak-to-valley v""
_--_
' -",
I
~- -
~ - - /
-...!....--- '--
Figure 149. The four referenee eylinders.
standards definitions, the cylindricity of a feature is • maximum inscribed cylinder (MIC; Figure 149c);
normally assessed in two stages: firstly, a reference • least squares cylinder (LSC; Figure 149d).
cylinder is obtained utilising data obtained from
measurement of the profile; and, secondly, these A brief review will now be given for each cylin-
measured points are then compared with the refer- dricity method of assessment.
ence cylinder, allowing the derivation of cylindricity.
There are four types of reference cylinders to which Minimum zone cylinder (MZC).
data can be fitted:
The MZC technique requires information on the
total radial separation of two concentric cylinders
• minimum zone cylinder (MZC; Figure 149a); (having the same axis) which totally enclose the data
• minimum circumscribed cylinder (MCC; Figure generated during measurement and are positioned
149b); such that their minimum radial separation is known.
Due to this MZC assessment method it places equal tric. Furthermore, unlike the three previously
emphasis on the internal and external profile imper- described "cylinder fits", the axis of the LSC is very
fections to determine the reference axis. The main stable and much less infiuenced by the effects of
industrial application for MZC would be where asperities.
running (clearance) fits are required.
point on the surface of a cylinder and, even if this 152 shows a three-dimensional "bed-type" plot of an
were technically feasible, the calculation itself would LSC component.
be prohibitive.
The effect of the selection of a number of planes
to be used on a cylinder has already been discussed
and, when widely spaced, results in their inability 4.7 Non-contact spherical and
to detect geometric cylindrically based shapes
such as the curved, waisted or barrelled figures roundness assessment
(Figure 147b). A potential measurement problem
can occur in the number of data points used in
each plane, because if insufficient numbers are Non-contact measurement of roundness is valid and
used then this can me an that certain profile detail has been possible for some time. Abrief discussion
will be lost, such as occasional dominant peaks of the range of instrumentation that has been devel-
and valleys. This loss of surface detail resulting oped is worthwhile, albeit if discussed in depth,
from inadequate numbers of data points means this would significantly increase the scope of the
that both inaccuracies and instability may result. current work and be somewhat counter-productive.
There are numerous ways in which the data can Despite these self-imposed objections, it is worth
be displayed by sophisticated software, notably the reviewing two techniques: one interferometry-based
multiplane screen image depicted in Figure 151. instrumental method for determining sphericity of
This figure illustrates roundness on a component at journal balls and another employing an optical
differing diametral points, indicating run out (f.Lm) sensor in conjunction with a displacement probe for
at these pre-selected locations. Conversely, Figure applications in both roundness and sphericity
assessment.
...
1,,-,.MtQ.l~)
, ;3.75
7.200
....
0,000
3.000
....
7<518
75.30
.. .34
2._ 8714
'.200
.,000 ....
03.30
Figure 151. Multiplane roundness/f1atness display, Windows™-based software. ((ourtesy ofTaylor Hobson.)
Figure 152. A three-dimensional "bed-type" plot of least squares eylinder results. ((ourtesy ofTaylor Hobson.)
InClustrial metrology , .
Refereocc hemisphere
• •
Figure 153. Sphericity interferometer and interference patterns on spherical surfaces. ((ourtesy ofTaylor Hobson.)
This type of optical interferometer can be consid- 4.7.2 Spherical and roundness
ered very much a single-purpose instrument of
limited application, but it does illustrate one method assessment by error separation
of non-contact roundness measurement. It is par-
ticularly relevant for use on precision highly Components produced to nanometric accuracy are
polished soft surfaces, which could be unintention- becoming increasingly important of late, with the
ally scratched by the action of a stylus-based round- demand for on-machine measurement to improve
ness instrument. Moreover, it is limited in the manufactured parts. The separation of potential
diameter range of spheres the technique can workpiece roundness errors from those imparted by
measure. the spin dIe error from the machine tool are important
111
for on-maehine inspeetion. For some years, non-con- Relatively reeently, however, it has been proposed
taet measurement utilising error separation tech- that several multi-probe methods will eliminate
niques employing multiple probes to perform on- mueh of the harmonie suppression, more specifie-
maehine measurement has been undergoing devel- ally, by adopting an orthogonal mixed method
opment. As has been previously mentioned, any form (Figure 154a)j this virtually overeomes any high-fre-
of single-plane roundness measurement involves the queney suppression. In the latter arrangement, only
produet of several essential parametersj these are: single displacement and angle probes are usedj they
are arranged at an angular orientation of 90°, whieh
• workpiece roundness error - intrinsie errors has been found to yield good operation al eharaeter-
generated during the produetion proeessing isties. This orthogonal mixed method system eonfig-
technique whieh are superimposed onto the partj uration is shown in a working arrangement for
• kinematic motions - of the X- and Y-directional sphericitylroundness assessment in Figure 154(b).
eomponents. The measurement system consists of assessment of
workpieee for roundness by use of angle and dis-
In 1972, Donaldson introdueed a "Ball reversal placement probes, an air-bearing spindie motor-
technique" for error separation, whieh is analogous drive, optical rotary encoder, together with an
to that of"Straightedge reversal". This "Ball reversal analogue-to-digital eonverter and PC. In the present
teehnique" (see Figure 242, Appendix C) oecurs, eonfiguration the displacement and angle probes are
where the radial motion - given by R(8) and the ball angular-oriented at 90° with respect to eaeh other.
roundness - given by B(8) are in the prescribed rela- The roundness specimen (workpiece), is mounted on
tionship as shown. Therefore, the angular informa- the air spindie and the round/spherieal profile ean be
tion is assured to be derived from the spin dIe sampled by the prob es as it rotates. In this eurrent
position, the indicator output and the two positions configuration, the probe's output signals are input to
In(8) would produce the following relationships: a PC by a 12-bit A/D converter, as a trigger signal. To
For the two positions: avoid errors that might otherwise be introdueed as a
result of delay due to the sampling time, output
11 (8) = R(8) + B(8) signals are simultaneously sampled. The workpiece
12 (8) = -R(8) + B(8) can be adjusted in both the X- and Y-directions (via
adjustment serews), enabling any eecentrie error to
and be removed, allowing the workpiece to be inspected
within the measurement proximity range of the
R(8) = 11(8) -1 2(8) sensors. Eaeh probe is mounted on individual XYZ
2 mierostages allowing the relative positions of eaeh
sensor to be set at the desired orientation to the
B(8) = 11 (8) + 12 (8) workpiece. Results from this orthogonal mixed
2 method instrumentation are given in Figure 154(e,
d), indieating for part (c) the measured roundness
It is worth noting that this technique gives the errors of two distinet measurements and the repeata-
errors of the test ball exactlly, together with the radial bility error between them. From the test trials (c-ii)
motion of the spin dIe along the indieatorr (sensor) the roundness error was around 60 nm, with a
test direction. If the orthogonal component of the repeatability error of 5 nm. The largest individual
spin dIe radial motion is needed. It ean be found from repeatability error (e-iii) oeeurred at the third-order
a single (added) test with the indieator and ball harmonie, namely 0.6 nm, this may have been the
rotated 90°, using the known ball roundness error. result of initial set-up positioning error. Conversely,
Furthermore, with a known roundness error, the ball the relatively large measured spin dIe errors in this
ean then be employed in any of the axis of rotation eonfiguration (d) for the repetition trials gave a
test eonfigurations. spindIe error of 800 nm, with a differenee of 140 nm.
Most of the sensors used for non-eontaet round- It should be mentioned that a major contributing
ness assessment have employed a three-point factor to this spindie error was vibration compo-
method, normally using three displaeement probes nents. If a comparison is made between the plotted
that are strategically positioned to measure the results in Figure 154 for this instrumental configura-
workpieee profile. The problem with this triple- tion (small differences: c-ii and c-iiij against large
sensor technique is that high-frequency eomponents differences: d-ii and d-iii), then the roundness error
of roundness error cannot be aecurately measured (e) is separated from the large spindie error (d) with
due to harmonie suppression. Even when more high repeatability, thus eonfirming the effeetiveness
than three displacement prob es are used, this sup- of the orthogonal mixed method of non-eontaet
pression problem cannot be entirely eliminated. roundness assessment.
InClustrial metrology , .
AdjuSlmcnl
O scrc\\'
Encoder
(c-i) polar plot of roundness error r( e) and (d-i) Polar plot of spindie error cx(e) and
repeatability error &(e) difference ßC x (e)
(c-ii) Rectilinear plot of roundness error r( e) (d-ii) Polar plot of spindie error cx(e) and
and repeatability error &(e) difference ßCx (e)
,.
=5 0-
Spindie crror ex(e j
E:: =5
;
E::
... 0
.,..
; =>
..'".,
E
... e
......
=>
'"
:: Repe'llahilit~' crror t!.r (e ) ~
Dill'crcncc e... (O )
'1:0 '1:0
:: ::
::0
0 '5.
rJ)
~
0 60 120 180 240 300 360 0 60 120 180 240 300 360
Angle e deg. Angle Odcg.
Figure 154. Measured roundness and spindIe error in error separation by the orthogonal mixed method. [After Gao et al., (1997).]
(c-iii) Spectrum of the repeatability error (d-iii) Spectrum of the difference
/' n=3
2 125
Frequency n Frequency n
This chapter has briefty reviewed some of the Evans, c.J., Hocken, R. and Estler, W.T Self-calibration: Reversal,
redundaney, error, separation, and 'Absolute Testing'. Annals of
wide range of concepts, methods and techniques for the CIRP, 45, 1996, 617 -634.
roundness assessment, although for reasons of space Fan, Y., Zhang, S. and Xu, W. Kinematic and mathematical research
it has not been possible to discuss much of the other on three-point method for in-process measurement and its
valid instrumentation equipment that is currently applications in engineering. Proeeedings of the 7th Inter-
national Precision Engineering Seminar, Kobe, 1993,318-328.
available, but simply to indicate the potentialities Gao, W., Kiyono and S. Nomura, T. A new multiprobe method of
of roundness measurement to the reader. In the roundness measurements. Precision Engineering 19(1), 1996,
following chapter the surface integrity aspect of 37-45.
modifications to both surfaces and roundness will Gao, W., Kiyono, S. and Sugawara, T. High-accuracy roundness
measurement by a new error separation method. Preeision
be pursued. Attempts will be made to try and explain Engineering 21(2/3), 1997, 123-133.
how, why, where and when the surface condition can Giardini, W. and Ha, J. Measurement, characterization and volume
be inftuenced by either its production processing determination of approximately spherical objects. Measure-
ment Seienee and Teehnology 5, 1994, 1048-1052.
conditions, or through some form of material phase Gleason, E. and Schwenke, H. Spindless instrument for the round-
changes, together with any plastic deformation via ness measurement of precision balls. Proeeedings of the ASPE
mechanical working that is present. 11th Annual Meeting, 1996, 167-171.
Henke, R.P. et al. Methods for evaluating of systematic geometrie
deviations in machined parts and their relationships to process
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NBSIR79-1758, June 1979. sion Engineering 23,1999,264-272.
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Suen, D.-S. and Chang, C.N. Interval polynomial regression by use 1990.
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Seien ce and Technology 9,1998,913-921. national Organization for Standardization, Geneva, 1983.
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Tsukada, T. et al. An evaluation of form errors of cylindrical Taylor Hobson, 1966.
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18th MTDR Conference 1977,529-535. Roundness. BS 3730: 1964.
Tsukada, T. and Kanada, T. Minimum zone evaluation of cylin- Thomas, G.G. Roundness. Ch. 9 in Engineering Metrolagy.
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18-23. Physics, Bristol, 1994.
Tsukada, T., Kanada, T. and Liu, S. Method for the evaluation of
form errors of conie tapered parts. Precision Engineering 10(1),
1988,8-12.
Machined surface
integrity
185
Table 15(a). Summary ofthe potential surface alterations occurring as a result of metal removal production processes
Conventional Non-conventional
5teels
Non-hardenable Roughness Roughness Roughness Roughness
Plastic deform. Plastic deform. Microcracks Selective etch
Laps and tears Recast metal Intergranular attack
5tainless steels
Martensitic (416 grade) Roughness Roughness Roughness Roughness
Plastic deform. Plastic deform. Microcracks Selective etch
Laps and tears Microcracks Recast metal Intergran. attack
Microcracks Untemp. mart. Untemp. mart.
Untemp. mart. Overtemp. mart. Overtemp. mart.
Overtemp. mart.
Maraging
(250 grade) Roughness Roughness Roughness Roughness
Plastic deform. Plastic deform. Recast meta I Selective etch
Laps and tears Resolutioning Resolutioning Intergran. attack
regime, these being directly related to the cutting is depicted schematically in Figure 156. Here, for one
process and associated feeds and speeds. However, of the less complex machining operations, namely
this is not the complete picture for surface integrity, as turning, the surface integrity - from onlya simplistic
many other interactions influence the surface during viewpoint - is shown grouped as follows:
either its forming or generating process. Machining,
being a complex relationship of interrelated factors, • surface condition - surface texture & roundness;
affects the outcome of the production process, which • micro-structural changes - microcracks, etc;
Table 15(b). Summary ofthe potentialsurface alterations occurring as a result of metal removal production processes
Conventional Non-conventional
Titanium al/ar
(Grade 5: Ti-6A 1-4V) Roughness Roughness Roughness Roughness
Plastic deform. Plastic deform. Microcracks Selective etch
Laps and tears Microcracks Recast metal Intergran. attack
Refractary al/ar
(MolyTZM) Roughness Roughness Roughness Roughness
Laps and tears Microcracks Microcracks Selective etch
Microcracks Intergran. attack
Tungsten
(Pressed and sintered) Roughness Roughness Roughness Roughness
Laps and tears Microcracks Microcracks Selective etch
Microcracks Microcracks
Intergran. attack
Abbreviations: (Machining) EDM: electrical discharge machining; ECM: electrochemical milling; ChM: chemical milling; (Metallurgy) Plastic deform.: plastic defor-
mation: Untemp. mart.: untempered martensite; Overtemp. mart.: overtempered martensite.
After Bellows et al. (1975).
• surface displacement - bulk material transporta- turning which will have harmonie departures from
tion and residual stresses; roundness characteristics present.
• surfacelsubsurface micro-hardness - plastic de- The exposed sterile surface (Figure 157) occurs as
formation and residual stresses. a result of highly localised temperatures and
transient, but cleanly cut metal resulting from this
Machined surfaces are even more complex than machining, which will instantaneously oxidise
seems at first glance; their performance can be influ- and adsorb contaminants. The outermost adsorbate
enced by external layers (chemical transformations layer is often termed the Beilby layer; it is approxi-
and plastic deformations), and/or internal zones mately 1 fLm thick and consists of many complex
(metallurgical transformations and residual stresses). factors, notably the presence of hydrocarbons and
For example, the anisotropie (periodie) turned sur- water vapour, that originated in the coolant or
face depicted in Figure 157 is influenced bythe tool tip atmospheric environment, respectively. Underneath
geometry and the regularity of the cusps (peaks and this metallic surface there is normally a plastically
valleys) is dominated by the pre-selected feedrate. A strained region that may have been metallographi-
range of other micro-topography features mayaiso be cally and metallurgically altered. The depth of this
present, superimposed onto the machined surface, layer will vary significantly, but is typically in the
such as tool wear, vibrational influences and, to a region of 10 fLm, according to the plastic deforma-
lesser extent, machine tool-induced errors. In the tion induced by the passage of the sharp tool over the
circumferential direction the lay is both periodic and surface and, is exacerbated by the metallurgical
regular, albeit this round surface is generated by composition of the metallic substrate. This plastic
Cutting tool monitoring
I----~
Surface texture I
I
Tool wear r--------, I
Roundness I
Microstructural "------------' I
changes
r---------. I
Microcracks, etc. I
Surface
displacement I
I
Surface/sub. I
I surface Il-hardness stress I
I- - ____________
Surface integrity -.JI
Figure 156. Major factors that influence the output from a turning operation.
deformation depth, as a result of residual stresses, The physical condition of critical components
can in certain circumstances penetrate to fractions of requires to be known, including an understanding of
a millimetre.As an approximation, the depth ofhard- surface layer residual stresses l prior to in-service
ness penetration is about 50% of that for the residual applications. As has been previously alluded to, the
stress penetration depth, whereas the depth of obser- process of machining parts will generate function-
vational plastic deformation is around 50% greater ally relevant surfaces that have some significance for
than this penetration. This theme of residual stresses the development of the physical state of the surface,
resulting from machining production processes will influencing the somewhat unpredictable distribu-
be the subject of the following section. tion of its residual stresses. In many industrial appli-
cations the properties of the component's surface
dominate the functional behaviour of the part in
5.2.1 Residual stresses in machined service. The effects of residual stresses on mechan-
surfaces ical and electrical components are summarised in
Figure 158(a). This family tree of factors that affect
The residual stresses in a component are a function usage is not complete, as there are notable omissions
of the previous material process route, in combina- such as optical, acoustical and thermal results of
tion with its machining history. The fact that residual residual stresses, which are outside the current
stress levels are present may either enhance or, more narrative. Each of the residual stress effects indi-
likely, impair the functional behaviour of a machined cated in Figure 158(a) will now be briefly reviewed.
workpiece. Internal stresses in a component are gen-
erally unstable and over aperiod of reasonable time
can produce alterations in either dimensional size or Residual stress deformations
geometry. For example, in the case of certain alloy
gauge block materials, over aperiod of greater than Any residual stresses acting within a body (compo-
25 years their length has been reported to have nent) occur without external forces or moments.
changed by approximately 0.8 ,....,m with little in the Internal forces form a system that is presently in a
way of wear through usage, which is a serious dimen- state of equilibrium and if sections of this body are
sional error that cannot be ignored. removed - by machining - the equilibrium status is
Zoncd h,)cr " in genen,l machined surfaces
~
ir
Oxides and
adsorption
Re iduul stress
Substrate
/ \
/
\
Oxides
stress
(i.e. substl"ate)
Figure 157. Cross-seetion of an anisotropie (Le., periodic) surfaee illustrating the surfaee eontaminants (oxides and adsorbates) together with
subsurfaee plastic deformation (the residual stress zone) and unaffeeted substrate.
usually disturbed, resulting in potential deforma- effects of residual stresses resulting from the previ-
tion. This distortion resulting from the machining ous production processing route.
condition is well known to industrial engineers The release of internal residual stresses must
when, for example, machining one side of a thin com- not be confused with the input of such stresses by
ponent. If either a forging or casting has not been machining, as indicated in Figure 158(b). The mach-
heat treated for stress relief and requires asymmetri- ining process gene rates residual stresses by plastic
cal machining, it will deform somewhat after deformation (Figure 159) or metallurgical trans-
unclamping from its work-holding device in the formations. As mentioned, residual stress depths
machine tool. In order to alleviate this problem an can reach several hundredths of millimetres, which
experienced machinist will release the clamping on large parts will cause little in the way of compo-
forces after roughing cuts so that stressed surfaces nent distortion when compared to the same effect
are equalised, prior to taking a finishing pass. Com- on thinner parts. For example, if a single-point
ponent deformation is approximately proportional asymetrical "light" machining operation such as
to the removed cross-section of material. Any further planing is undertaken on a 1000 mm long bar of 20
finishing is usually concerned with removing only a mm thickness, the deflection will be around 1 mm.
thin layer of material, minimising any detrimental While machining, or immediately afterwards,
InClustrial metrology .
Residual stress
effeets
1/
11
J\.
L v v
Statie Dynamic
Deformation
strength strength
Chemieal Magnetisation
resistanee
V
Hcat effi'cels
B -- HHHH
Heat
induction
Figure 158. Effeets of residual stress and deformation of a workpieee by maehining. [After Brinksmeier et al., 1982.1
in practiee across a variable and wide range. For with a highly positive and honed insert geometry is
example, shot peening intro duces an isotropie com- that the component's surface exhibits little in the way
pressive stress tensor into the surface, as does rolling, of subsurface plastic deformation, on materials that
but with distinct principal directions (anisotropie are not prone to work-hardening. When machining
surface behaviour) these are typieal of mechanical with a sharp cutting tool, where the corner intersec-
influencing processes, whereas EDM affects the part tion between the rake and clearance faces meet, the
in a thermal manner, introducing equal tensile ele- tool's edge will become progressively more rounded
ments to the surface integrity. because of the tribologieal action. This "rounding
effect" will me an that at a certain height above the
rounded portion of the tool's chip/tool interface it
5.2.2 Tribological cutting effect on will cut material and, below this contact point, it will
surface plough the surface. Ploughing is highly inefficient
and will plastieally compress the surface, acting in a
When machining a component's surface the resulting "burnishing-like" manner, as depicted in Figure 159.
machined topography will be significantly influ- Burnishing is an abusive regime of machining,
enced by the wide range of fixed and variable cutting although it is often intentionally used to produce
parameters. The ability to modify and improve this subsurface work-hardening to improve the wearing
cutting process is based on the judgement and expe- ability of the surface, yet at the same time a burnish-
rience of the operator, or on the inherent capabilities ing tool will improve the finish, by flatten-
of the computer-aided manufacturing (CAM) ing local asperities and cusps, from a previous
package. The scope to modify the cutting process is machining pass. Sometimes a material that can
considerable, with the outcome improving the work-harden will have a machined surface that gives
surface integrity, often at the expense of production the appearance of a high-quality surface texture,
output, part quality or tool life. Tool companies whieh in reality disguises the fact that considerable
expend considerable time and effort in developing work-hardening has taken place due to the burn-
tooling geometries to efficiently cut material and ishing effect of tool flank wear. A surface of this
evacuate chips from the cutting zone. Many cutting unstable type can create reliability problems at a later
inserts today have highly complex surface profiles, stage in the component's life, due to the instability of
often having a particular edge preparation - T-hone, the subsurface promoting potential for fatigue.
parabolic, etc. - either to improve tool wear charac-
teristics or to facilitate the retention of a multi-
coating for cutting inserts. Honing of the tool's rake Machinability testing
face allows a sharp cutting edge to result, which has
the ability to cleave through the workpiece material In Figure 160 are shown the results from an acceler-
in an efficient mann er. The outcome of machining ated machining test performed on Fe-Cu-C powder
Machining time
Shllrp 1001 ~=============='~\.J=============C====-1 Worn 1001
Figure 159. Distortion to the machined surface topography and integrity due to the tibological action of cutting.
(a) Sehematic illustration of "aeeeierated (b) Tabulated results from turning
machining test": 10 facing passes then test proeedure
surfaee texture and insert wear eheeked
Specimen
Saneh ik hlo('k UNII huldC'r"
2 4
"-,-,,. c•••
itN.'r1 (j.!rotd{': 1'25)
F 0 I
"-:{ii}! 11
0
0.9 0.9
0.8 0.8
r-\ e
~
0.7
/ \ 0.7
~
e 0.6 / 0.6 ~
....
5....
/!"'- \ e
....os
os
'"~
'"
0.5
l ~ --- -----
~I~
'" '''--s os
0.5 Q,
~
I::
"
e;::
0.4 ~ 0.4 .s~
II ----- ~
'"
0.3
l'l /--~- 0.3
oS"....
=
rJJ
0.2 1; /: 0.2
0.1 d 0.1
0L-~1~0~20~7.30~4~0~5=0--6~0~7~0~8~0~90~1~OO~1~10~17.20~13~0~14~0-1~5~0~1~60~1~70~17.80~19~0~20~0-2~1~0~2~2~0~2~30~O
No. of facing-off passes
1:0: 2:""': 3:0: 4: No symbol
Solid curves: refer to flank wear
Broken curves: refer to surface texture (Ra)
Figure 160. An "accelerated machining test" for assessment of tool wear and surface texture.
metallurgy (PM) compacts that were subjected to a PM surface is highly undesirable and should be the
face-turning operation at constant surface speed on cause of workpiece rejection, despite the fact that all
a CNC turning centre (Figure 160a). The results of the metrological indications state otherwise. The
four different powder mixtures are illustrated in reason for part rejection in this case would be
Figure 160(b), with graphical plots in Figure 160(c). because of surface pore closure, unique to PM
This particular accelerated machining test has the compacts, which could make these parts useless for
objective of assessing the relative machinability of porous bearing applications.
components based on a relatively short time. scale
(termed "ranking"), this being an amalgamatiOn of
the previous degraded tool and rapid facing tests, 5.2.3 Micro-hardness testing
devised by the author. The test quickly establishes
the relative machinability of differing specimens, Utilising micro-hardness testing techniques for
with a slightly degraded tool and marginally faster surface integrity assessments pro duces an indirect
rotational speed for the facing operation, this being comparison of the potential residual stress in ~he
undertaken with a constant surface speed feed func- mechanically affected layer (MAL). Such destructlVe
tion engaged on the turning centre. techniques require sampies to be sectioned - the
The tool life and wear curves are shown for the sectioning technique and the reasons for under-
four specimens in Figure 160(c), with the toollife in taking it will be discussed shortly - although the
particular showing the anticipated three stages of method should be used with caution, as any hard-
wear (Taylor curves) associated with steady-state ness plots obtained cannot show whether forces are
cutting operations. These reported wear stages are compressive or tensile in nature. A major benefit
the initial edge breakdown (tool point rounding), from utilising micro-hardness testing is that it
steady-state wear as the flank progressively ?egen- allows metallographically prepared specimen fea-
erates while in-cut, and finally catastrophlc tool tures to be optically investigated and assessed with
edge breakdown as the edge completely fails. The the test sampie in situ on the instrument. A range of
elemental additives to these powder compacts repre- micro-hardness tests are currently available, the
sent the major variable in the cutting process, this indentation being of two distinct types:
interplay of elements and their relative proportions
within the sampie significantly alte ring the shape of the geometric shape of the impression left after a
the wear curves (some specimens are more abrasive hard indentor has been pressed into the surface
than others). feature to be measured - typified by Vickers and
Superimposed onto Figure 160(b) are the circum- Knoop indentors (Figure 161b);
ferential surface finish results for each testpiece. It is 2 where a inden tor penetrates into a specimen and
curious to note from these graphical plots that orig- relative depths to which the indentor penetrates
inally a high Ra value was established during the are the measure of the specimen's hardness -
early stages of the operation during the initial tool typified by the Rockwell indentor.
edge breakdown; however, this surface .Ra va~ue
dramatically improves during the succeSSlve facmg
passes, regardless of metallurgical composition. This Vickers hardness
improvement is thought to occur because the flank
wear that is present on the cutting insert pro duces a The faces of the square-based diamond pyramid for
burnishing effect on the machined surface topog- a Vickers indentor are inclined at an angle of 136°;
raphy. Burnishing produces plastic deformation and this angle approximates the most desirable ratio of
in essence compresses the surface asperities and indentation size to that of a ball diameter in Brinell
localised surface layers, giving rise to an improve- hardness testing. Because of the shape of the
ment in the recorded surface texture. However, a indentor it is often known as the diamond-pyramid
surface condition of this type is misleading, as both hardness test. It is defined as the load divided by the
the surface topography and subsurface integrity are surface area of the indentation. The Vickers hard-
locally extremely work hardened. This work hard- ness number (VPN) may be determined from the
ening continues to progressively degenerate until the following equation:
insert edge completely fails; furthermore at the latter
stages of the flank's life the surface texture is exac- 2P sin (812)
erbated. A secondary effect of this burnishing action VPN =
by the insert's flank is the transport of workpiece
material and its sub se quent deposition in a highly
work-hardened state at new sites on the previously
machined surface. This smearing of the machined
(a) Tapered section of component, for metallographical and micro-hardness assessment
I
I NB: An inverted capital "A" is the
I symbol for Surface Integrity in the
I
I USA, dealing with sub-surface features
I (American Standard B211.1).
I
I
I
\
\
\ I ' -........I<.AI
\
,' - /
/
Micro-Vickers indentations
Machined cusps
Figure 161. Tapered seetioning of a component, for metallographieal inspeetion and miero-hardness "footprinting".
r:=E
(b) Split-point drill (feedrate: 0.127 mmJrev)
115mm • 115mm
l~,rn ~ 150llm
:1 l
,
I 100
1lm
,50 llm<l---- I
I
,
:~100Ilm 1
,50 llm-Q- I l
225 198 157 (Hv ) 251 222 198 (Hv )
~ ~ ~ ~ ~ ~
8 8
8 8
....
0
~
8 115mm
I
'''',rn
100 11m J
115 mm
~100flm1
150 11m
1
I I
50llm<l--
I
! 1~50Ilm~ I
e
8
f- ~ ~ ~
8
8
f- ~ ~ ~
....
0
....
0
Figure 162. Influence on localised residual hardness, near the drilled hole edge, with variations in drill geometries and component hardnesses.
increased from 234 H y @ top, by l3% and 8% at such as phase transformation, plastic ftow zones,
a depth of 10 mm and 20 mm respectively; localised cracking, and bulk transportation of
• split-point drill with a penetration at high feed material (redeposited material, re-entrant angles
(Figure 162d) - the mean micro-hardness in- and under-cutting) can be undertaken that would
creased from 264 Hy top, by 11% and 16% at a otherwise have been missed if only profilometry
depth of 10 mm and 20 mm respectively. assessment had been used. As its name implies,
"tapered sectioning" overcomes the limitation of
These hardness data plots illustrate that for a perpendicular sectioning by modifying the mag ni-
given feedrate and, in nearly all cases, the jobber drill fication of the subsurface features without undue
did not promote significant plastic deformation in distortion to the transversely cut surface topog-
the hole's surface region when compared with to a raphy. The procedure is illustrated in Figure 161 (a),
split-point drill. This hardness increase globally where previous production processes, in this case
ranged from 6-7% at higher feeds to 21 % at the turning and boring, have been produced and the
lower feedrate. The mean difference in micro-hard- subsurface detail would otherwise have been lost (as
ness, at its extremes, ranged from 47% from the top these modifications may occur in a relatively small
surface of the low-compaction specimen to the and localised surface zone), if a conventional per-
bottom of the high-compaction variety, with this pendicular section had been taken. Taper sectioning
difference increasing to 56% in the case of the high- can overcome the potential distortion problem, by
feedrate/compaction specimens at the deepest hole. selecting a section angle that increases the vertical
The overall increases in plastic deformation values magnification without unduly inftuencing the metal-
from the jobber to the split-point drills are thought lographical and topological features of interest.
to be due to three factors: Figure 161(a) illustrates the transverse component
cutting procedure, showing that an 11 ° section has
the greater bulk hardness of the high-compaction been made. This 11 ° sectional cut improves assess-
PM varieties increasing the overall hardnesses of me nt discrimination by increasing the vertical
the compacts after drilling; section magnification by around five times. Thus, the
2 as the point angle increased from 118 (jobber
0
taper section angle (TSA) will be 79°, the vertical
drill), to 135° (split-point drill), this induced magnification being obtained from the following
greater plastic deformation - hardness - in the expression:
hole's surface region;
3 as penetration of the respective drill types TSM = secant (TSA)
occurred, the abusive regime of drilling also
increased because of higher drilling tempera- where TSM = taper section magnification and TSA
tures, toward the hole bottom, and this was exac- = taper section angle.
erbated by poor ejection of the work-hardened Such vertical magnification by taper sectioning,
chips and compounded by the drill's margin increases the ability to obtain valid hardness infor-
inftuence on the hole's wall- "burnishing effects". mation on, for example, a machined surface, by
taking staggered hardness readings across the cut,
In all of the above drilling operations, the PM polished and etched surface as illustrated in Figure
compacts were drilled without coolant, which if 161(b). This subsurface feature of interest that has
utilised would have reduced the abusive hole been plastically deformed/mechanically altered is
generation procedure considerably, towards a "gende often quite small in width, somewhat less than 0.1
regime". However, this discussion illustrates the mm wide, requiring a small micro-hardness inden-
information that can be gleaned from undertaking tor such as the Knoop, as this indentor geometry and
hardness data studies and the effect that abusive associated readings can be more closely packed than
machining plays in just one aspect of a machin- the equivalent micro-Vickers impressions. It is
ability/surface integrity study. normally advisable to obtain several micro-hardness
readings in the subsurface area of interest, as an
otherwise spurious result can heavily inftuence the
Taper sectioning overall hardness profile result; therefore it is advis-
able to take severallocalised hardness readings and
In order to improve the metallographical assessment then average them to obtain mean values to
of a sectioned surface and its subsurface features, minimise such inftuences.
while achieving greater discrimination in hardness Caution and some degree of care must be taken
profile analysis across the viewed area - after appro- when attempting to section a metallurgically altered
priate polishing and etching - tapered sectioning can subsurface workpiece feature prior to assessment, as
be employed. Interrogation of subsurface features when sectioning the component heat can be acci-
dentally induced into the transversely cut surface by • an increase in the susceptibility to stress-corro-
the previous process of cutting and polishing the sion;
surface for etching and then testing. This undesir- • increased probability of surface material break-
able heat induction due to sampie preparation could out and generation of debris;
"swamp" the potentiallocalised subsurface hardness • higher wear rates resulting from "three-body
values and give significantly misleading and unrep- generation";
resentative hardness profile results. • surface delamination and fatigue.
Rotation
Milling cutter
Surface tensile residual stresses
Plastic deformation
[ ~~<>:::7_1
~~~~~~-l
Depth
Surface cracks ofcut
tend to open up
"Abusive machining"
Crack
Rotation
rPlastic deformation
ne
Surface compressive residual stresses ,k!lr""(""1=ri=:-T--c-,-",- ~
~~~~tf1ttifj}-1
Unaffected substrate Depth
Surface cracks ofcut
(if present) tend
to dose up
Figure 163. Fatigue characteristics of the surface region being influenced by the mode of machining.
In Figure 164(b) a white layer exists beneath a be very hard and in this example (Figure 164b) the
re cast and redeposited layer, resulting from abusive recorded hardness was 62 HRe> with a significantly
drilling with a dull drill. Due to ihe fact that the softer layer beneath this zone. In this situation, the
re cast layer has a similar metallurgy to that of the white layer-generating unit was probably a combi-
white layer, the delineation of their respective zones nation of both thermal and mechanical events.
is not clearly defined. Underneath the white layer is The thickness of a white layer in the drilling exam-
a complex metallurgical zone consisting of some pIe is strongly infiuenced by both the potential plas-
white layering, untempered martensite (UTM), tic deformation that can be created in this vicinity
together with over-tempered martensite (OTM), and to a lesser degree by the thermal infiuence of the
while beneath these layers the bulk material of the passage of the dull drill as it penetrates through the
substrate remains unaffected. White layers tend to workpiece. The problem is compounded by lack of
(a) Surface produced by a new drill, indicating no surface thermo-mechanical generation. The point has
aIterations already been made that many machining processes
impart residual stresses into the machined surface
layer; this can significantly increase the tendency
toward component distortion. For example, when a
face-milling operation occurred on 4340 steel that
was quenched and tempered to a bulk hardness of 52
HRe> a tensile residual stress was the less-favoured
machined surface condition, as illustrated in Figure
165. Even with cutting inserts on a sharp tool, a cer-
tain degree of tensile residual stress was apparent in
the immediate surface region, directly under the sur-
face (zone width of around 50 fLm); this stress con-
centration changed to one of compression. After
successive milling passes, the flank wear increased in
proportion to the Taylor wear curves:
(b) Surface produced by a dull drill, indicating "white layering"
together with surface cracking. NB untempered Taylor's general cutting tool wear relationship:
martensitic phase of the workpiece 62 HRc
C= VTn
::0 ~ 345
.,'"'"
.l: 0
~ ",,- //
--...----
--
---
~~ ~
f--
\, / ./
-;'" .",/ --~
:::
"CI
.,
'(jl
c
0
'(jl 345 /
,,~ . J /
/' /
.,...'"
~/
i:.::
c- /'
E
0 690
//
U ,/
Figure 165. Residual stress in a milled surface of 4340 steel quenched and tempered to 52 HR c [After Field and Kahles 1971.1
machining of a potential work-hardening material, fied heat-affected zone (HAZ) normally occurs, this
then some plastic deformation will be present in the being a product of either (UTM) or (OTM). As the
grains immediately adjacent to the surface. A certain effect of either of these HAZ's conditions diminishes
amount of over-tempering may be associated with further into the workpiece, then the original sub-
this machining operation that extends a Httle way strate condition will predominate. The white layer
into the material's substrate. In this example, as the effect tends to be significantly harder than the
tool's flank wear increases from 0.2 to 0.4 mm during substrate, with typical values for the substrate being
successive in-cut operations, then significant over- 50 HR c, while the UTM can quite easily reach hard-
tempering occurs, with the effect extending consid- nesses of >62 HR c, with a local tensile residual stress
erably further into the substrate, until it diminishes. present. This purely thermal event that occurs
Such significant plastic deformation of the substrate during the EDM process results generally from a
combined with the unstable metallurgical condition non-contact process, occurring as a result of the
may possibly lead to premature failure of a highly extremely rapid heating and cooling of the EDM
stressed component member in service, which might continuous cyclical operation. The white layer is
have a catastrophic influence on an assembly, with strongly dependent upon the energy density, result-
disastrous consequences weIl beyond its original ing from the interplay of two process parameters,
and intended purpose. namely the current magnitude and associated pulse
Electrical dis charge machining (EDM) can ini- duration. As both of these parameters increase, so
tiate a "thermal event" such as white layering and its does the depth of these metaIlurgically altered states.
associated martensitic transformations, which exist The influence of the unwanted by-products of the
as re cast and redeposited layers. Due to the fact EDM process can, on some electrical dis charge
that the re cast layer has a similar metallurgical machines, be minimised by switching on a surface
formation to that of a white layer, the delineation integrity (SI) generator (Figure 166). The advantages
between them is not readily apparent. Beneath this of utilising this SI generator are significant and
white layer the existence of a metaIlurgically modi- include the following:
Without SI WithSI
- parts machined with a - parts machined with a
standard generator: surface integrity generator:
CARBIDE
-micrographic cross-sections
of workpieces in carbide
STEEL Presence of an affected layer (cracks) Absence ofan affected layer (cracks)
-micrographic cross-sections
of workpieces in steel
Figure 166. 5urface integrity of electrical discharge machining (EDM) with/without an 51 generator. [Courtesy of Charmilles Technology.l
• surface integrity of the material improves above, then the consequences are for a poor surface
through areduction of unwanted and undesirable integrity workpiece to result. These problems may
metallurgical effects; include shorter tooling life, through impaired
• using the SI generator, the electrical dis charge mechanical characteristics of the metal; reduced
machine tool allows fine surface finishes? Ra 0.2 resistance to wear, promoting surface fragility on, for
f.1m up to component heights of 100 mm; example, dies and punches; and bad adherence of
conversely an Ra of <0.1 f.1m can be achieved at surface covering, on materials such as titanium
around 5 mm component heights); nitrate (TiN) and titanium carbide (TiC). Other
• output from the whole production process can be metallurgically related surface integrity EDM prob-
increased, while obtaining the equivalent level of lems may include the following:
surface roughness and integrity;
• as a result of utilising the SI generator, the compo- • Thermal damage - during the process a large
nent's parallelism is improved for high work- proportion of energy contained in the spark is
pieces. transmitted to the material being machined,
causing localised heating. The temperature differ-
If the electrical dis charge machine does not have ence inside the material generates constraints,
enhanced features such as the SI generator discussed resulting in surface micro-cracks;
InClustrial metrology . .
• Corrosion effects - on ce micro-cracking has range of surface topographical effects and sub-
occurred, small quantities of water stagnate in surface integrity modifications, depending upon
these cracks and are not deionised. Hence, the whether the operation was of agende or abusive
properties of these minute reservoirs of water are nature. In Figure 167 the abrasion performance of a
modified and the liquid corrodes the material by conventional grinding wheel consists of a number of
dissolution; variable factors; these include its abrasive, grit size,
• Electrolysis - during the EDM process, an electric grade, structure and bond type. Today, grinding
current passes through the water, which in turn wheels can be manufactured from ultra-hard abra-
increases the quantity of OH- and H 30+ ions, sives, but for brevity and to simply illustrate the
exacerbating the surface integrity still further. problems that occur in grinding operations only the
conventional grinding wheels will be addressed
The use in EDM of enhanced control features, typi- here, to highlight their infiuence in the overall
fied by these SI generators, significandy reduces the grinding process. Prior to this discussion of the rela-
likelihood of white layering and other unwanted tive merits of wheel selection and their anticipated
process-induced surface defects. effect on the ground surface topography/integrity, it
The process of grinding, whether of the surface, is worth iterating that several factors infiuence
cylindrical or centreless variety, can introduce a grinding wheel selection; however, they are outside
Waviness -
out-of-balance
_l
Deptb ofeut
Grit size of
grinding wheel
NB Cross-feed travel will also iofluence the traosverse roughness of the surface
Figure 167. Influence on the ground surface promoted by both the wheel's grit size and out-of-balance effects, when surface grinding.
the scope of the current topic, but nevertheless are integrity effects in combination with a range of
worthy of amention. These grinding factors are the residual stresses, depending upon whether the
workpiece material, condition of the machine tool, grinding process was gentle or abusive, the latter
wheel speed, work speed and angle of contact regime significantly increasing residual stresses in
between work and wheel. the workpiece surface layers. Under an abusive
A conventional wheel's abrasive make-up tends to regime, the dominant feature will be of a thermal
be of two distinct types - either aluminium oxide or nature in combination with tensile stresses in the
silicon carbide - the former abrasive wheels, being localised surface layers. Equally, if a gentle grinding
softer than those of silicon carbide, are employed for regime occurs with copious amounts of coolant
harder workpiece materials, as new grains are present, then reduced frietion resuIts and the "unit
broken and sharp cutting edges are continuously event" tends toward the mechanieal, promoting a
exposed. The grinding wheel's grit size influences compressive residual stress in the subsurface. If the
the ground surface as illustrated in Figure 167, as grinding conditions utilise more conventional
does the wheel out-of-balance. The wheel out-of- cutting and grinding data, this introduces a thermal
balance in surface grinding causes it to "bounce" event that has residual stress magnitudes approach-
across the ground surface, introducing medium- ing those of the abusive regime, but tend to be of
frequency waviness, the relative surface roughness shallower depth below the surface. The peak residual
being a function of the grit size that is superimposed stress in conventional grinding virtually coincides
onto this waviness. If a fine or small grit is selected, with that from abusive grinding regime and the
then the anticipated ground surface will also be fatigue endurance limits are alm ost identieal. It has
smoother than if a coarser grit had been selected. been reported that there is an inverse relationship
Both an isotropie and anisotropie surface can be between the fatigue limit and peak residual stress.
produced by the action of grinding. Wheel grade In Figure 168 white layering is shown to be
selection is important as this can affect the overall present in the subsurface regions for both surface
strength of the wheel, enabling it to be used for and cylindrical grinding operations. Even if the
either low or high production output. The structure selection of wheel, work and associated cutting data
of the grinding wheel is an indication of the propor- are optimised, then if the wheel is not "self-sharp-
tion of bond to abrasive, an open-structure or ening" and the wheel wear pattern is toward the
porous wheel having around 30% bond, whereas a outer edges, rather than at the centre of the wheel's
closed wheel may only have 10% porosity. Bonds can width, it will "glaze". A glazed wheel will introduce
vary considerably, rubber-bonded wheels being the abusive machining and in its worst condition it can
strongest, whereas shellac bonds are used for fine become "loaded" with totally inefficient cutting,
surface-finishing operations. Generally, a good guide further exacerbating the workpiece surface integrity.
as to the type of wheel and grinding conditions to Therefore under either a glazed or loaded wheel
recommend in obtaining efficient workpiece output local hardness will increase, as will the white
and surface topographies would be as follows: layering tendency, which further degrades the work-
piece surface texture and integrity.
• "harder work, softer wheel" - relating to work-
piece production;
• "larger angle of contact, softer wheel" - relating in Altered materiallayers
the main to either internal or external cylindrical
and centreless grinding operations; In order to gain an overview of the aItered material
• "good rigid machine, softer wheel" - relates to layers (AMLs) that occur in diverse surface and
machine tool rigidity and its associated vibra- subsurface topographieal features ranging from
tional tendencies, which may be superimposed differing metallurgieal processes, mechanieal appli-
onto the workpiece surface; cations and uses, see Table 17, whieh highlights their
• "high wheel speed, softer wheel" - this refers to the particular influence on functional performance.
fact that when wheel speed is high the work In the majority of cases shown in Table 17 the
moves a relatively small distance while the abra- influence of these subsurface defects tends to be of
sive grains pass, hence its grinding forces are low; notable importance, specifically with respect to an
• "high work speed, harder wheel" - when the work abusive regime producing a machined white layer. In
speed is high an abrasive grain has to remove some instances the aItered material zone (AMZ) can
more workpiece material during each pass, which affect component in-service performance in a
increases the grinding forces. variety of ways. For example, where the in-service
tribological situations produce either redeposited or
The resuIt of all of these variables in the grinding recast layers in the surface region, it has been known
process will be to introduce inconsistent surface that such defects will influence wear and affect reli-
ni:tustrial metrology .
SURFACE GRlNDING ,
-+ -
<;, Whccl
--8 -i3-
wear:~
I Wheel :
Whccl:
out-of- balance '
t
I >~
r
Localised Minimal Localised
white layers distortion white layers
CYLINDRlCAL GRlNDING
I r- >~
Wheel : Feed
- ~-3--
Minimal Localised
distortion white layers
Wh·Itc ayer
K\,I HAZ
-
- - - Abusive
_ _ Gentle
_.\ - ,
0
/
U
o 0 ·25 0·50
Figure 168. Effeet on maehined surfaee integrity du ring surfaee/eylindrieal grinding of high-strength steels and alloys.
Im
Table 17. The influenee of subsurfaee features on funetion
UTM OTM Aust IGA WL Plast Burrs Cracks Tears Tool Redp Res
orWL rev defn and frags matl stress
laps
Wear
Strength
•• • • • •• •• •• •• •• • • ••
0 0
0 0
•• •• • •• •• •• ••
Chemical attack 0 0
Fatigue
Magnetism
• • 0
0 0
0
Bearings
Seals 0• • • •• •• •• •• 0
0 0 0
0
0
Friction
Bonding and adhesion
0
0
•• •• •• •• • •0
0
Forming
• • • • • • • •
Key:.: strong influence on function; 0: some influence on function; (>: possible influence on function.
0
Abbreviations: UTM: untempered martensite; OTM: over-tempered martensite; Aust rev: austenitic reversion; IGA: interangular attack; WL: white layer; Plast defn:
plastic deformation; Tool frags: tool fragments; Redp matl: redeposited material; Res stress: residual stress.
After Griffiths et al. (2001).
ability. This often undetected subsurface condition surfaces and particularly a turned surface, refers to
degrades the functional performance; because they any surface undulations that are regular/periodic
are the product of hard, brittle and unstable layers (anisotropic) that are deemed typical for that surface
with tensile residual stresses present, combined with condition. Such roughness can be considered to be
an acute change to the bulk substrate, they are likely the constant and predictable nature of the surface
to spall (delaminate and break away). Conversely, if and not the random variations and disturbances that
a subsurface feature pro duces severe plastic defor- may be present overlaying the fundamental surface
mation, evidence has shown that in the case of the geometry. Conversely, a machined surface's topo-
die and tool industry some dies benefit from graphy describes the real surface including the
increased life due to this enhanced abrasion resis- texture and any disturbances present; therefore if
tance. Table 17 indicates to the design engineer that there are no surface disturbances then the topog-
simply selecting a production process without an raphy equates to its texture or roughness. Further, if
intimate knowledge of how it is to be manufactured no disturbances occur within the macro/micro-
will affect the subsequent part's performance. textures of this machined surface, then its finish can
Moreover, due regard must be given to the compo- be considered as the quantified description of the
nent's potential subsurface state, as this condition topography defining the basic structure.
will inevitably lead to problems when the part is In Figure 169, if consideration is given to the
utilised in service with its potential reliability being "idealised" turned surface topography, then for
impaired. constant tool no se geometry and an undeformed
chip thickness (often wrongly termed the "depth of
cut" in turning), as the feed per revolution is in-
5.2.5 Machined surface topography creased the surface texture is degraded. The residual
cusps that periodically occur on the turned surface
after the tool's passage along the part are the product
Turning of two phenomena: the so-called "moving step
effect", in conjunction with the associated condition
When a component has been machined this can be of the "emerging diameter". This relationship
considered to be a permanent re cord of the "unit increases the notable height of the cusps with larger
event" and, as such, can be diagnostically investi- feed per revolution and diminishes in height with
gated to obtain invaluable information of the reduced feeds. If proportionally larger feeds per
production process and the data utilised in its revolution are selected, this increases the residual
manufacture. The term "roughness", relating to most influence of the tool nose contact region on the
15° Plan
approach 40° Point angle
angle with 1.5mm
surface and as a result heightens the turned cusps, raphy will markedly differ. This topography differ-
promoting a larger recorded value in Ra and greater ence is shown to good effect when turning ferrous
angles for 6.q values. The opposite effect takes place PM compacts as depicted in Figure 170, where two
in the case where feed per revolution is reduced. extremes of cutting insert no se radii are utilised. In
Namely, as smaller tool no se contact region occurs, Figure 170(a) the no se radius is 0.8 mm, whereas in
this results in a smaller cusp height and accom- Figure 170(b) it has been increased to the equivalent
panying Ra; this also gives a shallower 6.q due to the of a 6 mm no se radius, by employing a large button-
partial curvature of the tool nose tending to zero as type of insert geometry. In the case of Figure 170(a),
it approaches tangency with the workpiece axis. The it is visually apparent that the periodicity of the
height, profile shape and periodicity of the cusps surface is indicated by the regularity of these cusps
resulting from the feed and tool geometry signifi- and, despite the fact that a new tooling insert was
cantly influence the measurement and magnitude of employed in this turning operation, the surface
the surface topography, and hence resultant para- shows significant signs of tears, laps and burrs. By
meters. Therefore if the Ra value alone was utilised, way of comparison in Figure 170(b), the surface
it cannot adequately describe the nature of the topography appears significantly smoother in pro-
surface topography condition in any meaningful file, with no noticeable cusps present, although the
way. overall surface topography is marred by similar te ars
If the cutting data is standardised (rotational and so on which could be cause for the part's
speed, feedrate and undeformed chip thickness are potential rejection. This smoother surface due to the
constant) and only the tool nose geometry is significantly larger cutting insert tool no se radius is
changed, then the resulting turned surface topog- not unexpected, as the feedrate was considerably
smaller than the nose curvature of the insert; there- (a) Thrned surface iIIustrating partial tool nose
fore it could blend out and as a result obliterate any geometry, from a 0.8 mm tool nose radiused insert
potential cusps on the turned surface. This tech-
nique of improving the surface by using a large tool
no se geometry has been employed by precision
turners over the years and can be summarised in
terms of the resultant cusp height by the following
relationship:
Therefore
f2
Ra=-
32r
Milling
Milling operations represent the main produc- Instrument:JSM-5600
tion processes for the manufacture of aerospace Acc.Voltage: kV 15
Photo mag. x200
and many high-quality precision parts requiring S.E. image
prismatic features to be incorporated into their Vacuum: Pa
design. Basically, a prismatic feature on a component WO: 46
consists of a machined face or facet - not necessarily
at 90° to an adjacent surface - which normally acts Figure 170. SEM photomicrographs of typical turned ferrous P/M
surface topography with constant feeds and speeds, but varying tool
as a location face or datum in aprecision assembly. nose geometries. [(ourtesy of Jeol (UK) Ltd.)
Predominantly, the aerospace industry would tend
to manufacture these prismatic features from
wrought material by utilising one of two machining enabling HSM machining centres to cover similar
strategies: areas even quicker than their counterparts
described in the former case.
face milling - allowing sizeable surface areas to
be generated by large-diameter face mills, In fact, many more industrial processes and
running at conventional speeds and feedrates; applications tend to be utilising the latter approach
2 high-speed milling (HSM) - employing smaller- of HSM. Major production benefits accrue from
diameter end-milling cutters rotating at very high milling surfaces by this technique, not least of which
peripheral speed and moving at higher feedrates, is the minimal cutter deftection - enabling thin-
InClustrial metrology . .
walled machining to be undertaken - together with milled surface topography will also vary. Returning
negligible subsurface damage inflicted by the HSM to the previous scenario using a standardised
strategy and in many cases enhanced milled surface feedrate, the rotation in combination with the feed
texture. for a given cut-off will change the milled surface
The end- or face-milling process is an interrupted topography, introducing various cusp height effects
cutting operation that imparts an isotropic surface along the surface. Here, the periodic nature of the
topography, as schematically illustrated in Figure surface topography is regular (Sm), but its period-
171. If in Figure 171 (top) stock is removed by icity changes according to whether the surface is
milling, the resultant milled surface exhibits quite a measured at the centre or at some point across the
complex surface topography, due to the "recutting surface; this in turn modifies the relative height
effect" of the cutter's trailing edge as it moves over of the cusps. Conversely, across the milled surface
the surface at a periodic and set speed. This periodic at arbitrary positions denoted in these examples as
surface topography will not be the case if some form "X-X" and "Y-Y" (Figure 171), the topography fluc-
of milling incorporating adaptive control constraint tuates at a predetermined quantifiable interval
(ACC) is employed. The reason for this variation is depending upon where the surface trace was pos i-
that as the cutter progresses over the surface - in, tioned. Milled surfaces with a non-directional or
for example, torque-controlled machining (TCM) - undefined lay, as is the case for the recutting effects
its torque is monitored and the stock height may introduced by either end- or face-milling opera-
vary. The adaptive control system constrains the tions, should not simply have an Ra quoted on
machine tool's feed function, thereby protecting the the engineering drawing. Such design information
cutter from damage, but more importantly from a concerning the milled surface becomes somewhat
surface's viewpoint, the feed varies and hence the meaningless and at best only indicates the worst
Fccd
---
X, C ut-off I V
r
I
Cut-off
'I I
Cusp
hClghts
--~: =
-- ~::::::
~l-
I I I I
~~
I I
Figure 171. Milling operations impart an isotropie maehined surfaee topography to the workpieee. [After Whitehouse, 1999.]
Category (enlarged Examplesof Posslble reasons for variation
profile view) kindof
variation
1 Variations in Unevenness Errors in the guideways of the machine tool or of the
shape Out ofround component
Incorrect clamping of the component
~
Vibrations of the machine, tool or component
~
the tool
4 Minor imperfections Scores How chips are produced (tear chip, shearing
-
Flakes chip, built-up edge), deformation of the
Arches component at the sand-blasting, serration
(after galvanic treatment)
surface roughness that the designer will tolerate, ability to the functional performance of milled
saying nothing about the surface topography or its surfaces in critical and highly stressed component
functional performance. environments. Therefore, "wiper inserts" are some-
In Figure 172 several milled surface topography times incorporated into the face-milling cutter body
categories are indicated, with examples of the kind (Figure 173b), where they are accurately preset to
of topographical variation that might occur and the few micrometres below those of the normal cutting
possible reasons for this disparity. Milling opera- inserts (50-100 fLm). Firstly, these wipers will
tions can be performed in a number of different minimise cusp effects, thereby enhancing the sur-
ways and the resultant milled surface topography is face topography, and secondly, they gently remove
heavily influenced by the numerous varieties in a small depth from the transient milled surface,
cutter insert geometry, plan approach angles and minimising the plastically altered subsurface
tool path cutting data selected, as simply shown in layer.
the few examples depicted in Figure 173. Not only The term spindie camber describes a slight incli-
will the relationship of these interdependent milling nation of the milling spindIe axis normal to that of
factors influence the surface topography but also, as the machine's table, or zero inclination (Figure 174).
was shown previously in Figure 163, the subsurface This camber technique is used to avoid the recutting
integrity is heavily influenced by residual stresses effect on the surface previously mentioned and,
induced by the cutter's passage over the surface additionally, it minimises cutter insert wear, partic-
being milled at conventional cutting data. This ularly at the cutter insert's periphery. In reality, the
problem of subsurface modification is one reason spindIe camber tends to be very slight, generally
for the upsurge in the popularity of HSM strategies, only amounting to between 100 and 300 fLm over a
as the technique imparts minimal influence on the length of 1000 mm. If this camber is converted to
plastic deformation of this subsurface region after angular measurements, the value ranges between 20
milling. It is often recognised that the recutting and 60 seconds of arc, this effect being greatly exag-
effect introduces a certain amount of unpredict- gerated in Figure 174 (top).
(a) Surfaces obtained with radiused edges True centre line
Facemill
Cusp
height :;:::::~'7-~>-::.-?-?--r'~
Insert radius
1000mm
25 0=100
(d) Surfaces obtained from peripheral milling e~ 20
18
..c 16
~
14
-lli Variation in
12
."
10 0=160 shape,f, caused
.5 9 by spindIe
] 8
7 ./ camber
e 6 ,/ ./ /' 0=200
Ei 5 /' V rD=2&
Cusp height
Q
~
/ /1/ V V 0=315
/ / /1/ V ~
"...
...:;
/ / r//~ v
..
oS 2
~
.5 IIiL ~
rt
c
=
<=
Figure 173. Examples of variations in the surface topography
·2
~
resulting from milled surfaces. 0.01 0.02 0.03 0.04 0.05
I
/'
depth of b ody
* I
chisei edge III.Ist be web-thinned as regrinding occurs - due to web thickening.
Figure 175. Drilling geometry and chisei point shape: influence on hole generation.
Despite the relatively simple design of the most p
popular type of drill, this being the twist drill, its
material rem oval mechanism is quite complex and a
slight digression to give some understanding of how
the hole generation technique occurs will aid in the
interpretation of hole surfaces. Near the bottom of
the drill's flutes where the radii intersect with the
chis el edge (Figure 175), the drill's clearance surfaces
form a cutting rake surface that is highly negative in
geometry. As the centre of the drill is approached,
the tool's action resembles that of a "blunt wedge-
shaped indentor" (Figure 176). Under the chisei edge
the cutting process is inefficient and a region of
severe deformation occurs. These deformed prod-
ucts are extruded, then wiped away into the flutes,
whereupon they intermingle with the main cutting
edge chips (from the lips). The chis el edge in a
conventionally ground twist drill has no "true
point", this being a major source for a hole's dimen-
sional inaccuracy. The twist drill geometry of a
conventional point is shown in Figure 175, together
with associated nomenclature for critical features
and tolerance boundaries. From the relatively
complex geometry and dimensional characteristics x
shown in Figure 175, the obtainable accuracy of
holes generated while drilling is dependent upon
previously grinding the drill geometry to within
prescribed limits. Any variations in geometry and
dimensions, such as dissimilar lip lengths and
angles, or chisei point not centralised, will have a
profound effect on both the hole dimensional accu-
racy and roundness. "Helical wandering" of the drill
as it passes through the component will occur with
these geometrie drill inaccuracies present (Figures
177 and 178). Hole accuracy, particularly the "bell-
mouthing effect" (Figure 177), is minimised by
previously centre-drilling prior to drilling to size.
One of the main causes of a "bell-mouthed hole"
is inconsistency in either the lip lengths/angles
(Figure 175), or employing a straight (conventional)
chisei point, or a combination of both. This "bell-
mouthing" at workpiece surface entry by the drill is
attributed to the chis el point. This effect is produced
by a line contact as the point initially touches the Figure 176. Cutting force generation and the effect that thrust and
torque play in hole quality.
component surface, causing it to "walk" until the
drill feed/penetration stabilises at the outer corners
(margin) ente ring the part and guiding the drill
(Figures 177 and 178). Such degraded hole effects are metrical and the cutting load and torque on the lips
exacerbated by longer series drills because of the vary (Figure 176). Galloway defined the drilled
"rigidity rule", which states that cutter rigidity hole slope angle cf> and hence the hole's subsequent
decreases by the square of the distance. Namely, if a roundness and circularity in the following manner:
drill is twice as long, then it is four times less rigid.
It follows that the greater the drill penetration into Slope in drilled hole:
the workpiece, the progressively larger the deflec-
tion and the further from the true axis will be the
drill's subsequent path. This drill deflection is com- 3 R(
(cf»=2 1y 1- (ktank)1
I)
pounded when the drill point geometry is not sym-
(a) Relative lip height difference (i.e., 0.125 mm), (b) Relative lip height difference (i.e., <0.25 mm),
without centre-drilled hole with previously centre-drilled hole
0-5
0·5
revs 5-7
0-5
before contoct
contoct
0·5
Figure 177. The roundness of a hole is influenced by the initial drill's progression into the part, causing "bell-mouthing"
[After Galloway, 1957].
10o"um
1OOtum x
Cutting conditions: speed In): 173 rpm fee d IfI = 0·012 mm/rev depth Id) =0·5 mm
Figure 178. Influence played by an increasingly larger chisei point on the resulting Lissajous figures of drill deflection, as hole depth is
generated. [After Onikura et al., 1984.]
where I = length of deftected element, R = ratio of 5.2.6 Machined roundness
the transverse re action at the drill point, T = thrust
force, I = system's "moment of inertia" and k =
...J(T/E)I. Harmonie departures from roundness
As this slope suggests, the error is initiated when and surfaee texture eorreetion
the chisel edge begins to penetrate into the work-
piece, and unless the feed is discontinued or the In the previous seetion it was mentioned that oper-
error is corrected in some way, the magnitude of ations such as drilling can impart a range of hole-
deftection will increase as drill penetration con- gene rating mechanisms that could be the cause for
tinues. Typically, the magnitude of deftection can part rejection, such as roundness, cylindricity and
reach up to 60 f.lm under exaggerated conditions and surface topography errors. In this seetion roundness
this could be the source of component rejection. will be the main point of discussion, as it will be seen
Due to the drill cutting edges and lip lengths that machining operations and their accompanying
(Figure 175) not being ground correctly, the cutting tool geometries can seriously inftuence the resultant
forces - thrust and torque (Figure 176) - will be both shape of the roundness profile. If, for example, a drill
unbalanced and uneven. This imbalance can lead to has an asymmetrie cutting action (unbalanced),
the drill spiralling down as it penetrates the work- then this condition is likely to impart changes to the
piece, causing the surface profile to exhibit the generated hole as penetration continues through the
dassical effect of a "saw-toothed profile" on the part. In Figure 179(a) just such a situation is
resultant surface topography. This "saw-tooth effect" depicted, where at the top an almost three-Iobed
on the topography is the result of the partial geom- roundness profile is shown; this becomes more
etry of the lip corner and its adjacent margin, regular in the middle, but the lobes are partially
repeating itself at the periodicity of the feedrate, rotated through an angle, and at the bottom the
which could cause problems if the hole is subjected polar plot has become almost round. This improved
to cydical stresses in service. roundness at deeper depths of penetration is prob-
The chisei edge has been shown to playa crucial ably the result of increased support by the drill's
role in drilling hole quality, not least of which is the margin as it progresses through the workpiece.
result of the inefficient behaviour of the chis el In order to improve the drilled hole quality in a
point's extruding operation as the hole is generated. number of significant ways, such as in its apparent
If the chis el point on the twist drill with respect to roundness, surface texture and integrity, together
its diameter is relatively large, then the Lissajous with the correction for any geometric errors present,
figures, as depicted in Figure 178, will show large then reaming may well be employed. Drilling, being
ftuctuations in the drill's axis of rotation; conversely generally considered to an abusive regime, will
at a smaller chisei point size, this motional behav- inevitably introduce more undesirable errors during
iour is significantly smaller. One of the reasons why hole generation than the complementary and more
the chis el point length and its profile play such a gende reaming operation. The advantage of utilising
major role in producing "bell-mouthing" of the hole reamers after the drilling process is shown to good
at entry is the result of much greater thrust forces, effect in Figure 179(b), where several different
with a proportional increase in the smaller torque reamers are utilised on identical drilled holes,
values (Figure 176). When the forces on the drill with the roundness being assessed at the same
increase as a result of the higher cutting force and vertical "slice level". On the left-hand illustration,
torque levels, this tends to cause the twist drill to a six-edged carbide-tipped machine reamer of the
unwind slightly. This subsidiary drill behaviour conventional type was firmly supported in an appro-
introduces the potential for dynamic instability, priate adaptor that directly fitted into the spindie
resulting in an increased tendency toward vibra- nose taper. This positive location and reamer
tion and additional harmonie out-of-roundness restraint mean that the reamer will introduce into
effects, coupled to the likelihood of a degraded the hole any inaccuracies apparent in the machine's
drilled surface topography. If a through-drilled hole spindIe, although even here the accuracy is a signif-
is required rather than a "blind hole", then there is icant improvement - five times better in fact - than
the potential for the generation of "bell-mouthing" the previously drilled hole (Figure 179a). If the
at the exit point of the workpiece, resulting from the reamer is allowed to "ftoat" (having lateral/radial
so-called "trepanning effect" as the drill breaks play) in the machine's spindie, any spindie errors
through the part's underside. here will not be superimposed onto the reamed
surface and the reamer, with its longer cutting edges
than the previous drill, will correct for many of the
geometrie inaccuracies introduced during the
drilling operation. In Figure 179(b, middle) a "ftoat-
(a) Typieal roundness error (i.e., "displayed profiles") produced by asymmetrie cutting action.
Hole position/s:
Figure 179. The effect of harmonie departures from roundness change with different drilling hole depths or reamer types.
ing reamer" replaeed the eonventional type and In some maehining eases, the errors introdueed
was driven through the drilled hole at too high a by the drilling proeess are anticipated to be quite
penetration rate, introducing sixth upr harmonie large, as shown by the displayed profiles in Figure
equating to the equispaeed six-edged reamer. In 180 (bottom left) , illustrating the relative radial
Figure 179(b, right), an identieal re am er was used to movement in the displayed profiles and their
ream a similar hole, but at a slower penetration rate, associated harmonies. Henee, it is often prudent to
producing an aeeurately reamed hole with minimal introduee aboring operation prior to reaming
harmonie disturbanee. (Figure 180). After previously drilling a slightly
PRODUCTION OPERATION
DISPLAYED PROFILES I
Floating
reamer
Twist
drill
Bored hole-circularity and
geometrie alignment errors
corrected
l-
I
I
,I
Figure 180. Exaggerated errors caused by incorrect drill geometry and the technique for its subsequent correction.
smaller predetermined diameter hole, aboring oper- • thermal growth effects - changing the both the
ation will then correct any abnormalities (roundness spindle's growth (axially) and modifications of an
and helical wandering effects) as indicated in Figure elastie nature to the relative axis orthogonalities
180 (left, towards the top). Aboring operation does of the maehine tool;
not follow the hole's contour and, as such, will elimi- • working clearances and motor drive configura-
nate these drill-induced errors by machining away. tions - these are neeessary to allow for relative
Finally, the reaming operation will impart the fin- thermal growth and eomponent "running fits"
ished dimensional size to the hole and simultane- within the spindie assembly, which are com-
ously improve both the circularity and surface pounded by arrangement of the motor drive
texture (see polar plot in Figure 180 (top left). system.
In order to improve the boring process still
further, adjustable twin- or triple-boring heads with This latter feature of spin dIe inaeeuraey is present
indexable inserts can be utilised. These special- in headstocks on either lathes or turning centres, as
purpose multi-boring tools balance out the cutting illustrated in Figure 181. Direet-driven headstocks
forces associated with the boring operation and, in for turning centres offer eonsiderable advantages
so doing, improve surface text ure and hole accuracy, over their belt-driven counterparts. The working
together with repeatability and consistency of bored clearanees and drive eonsiderations found on
holes. In fact, triple-boring heads in partieular can conventional belt -drive maehines suffer from a
sometimes eliminate the need for the succeeding combination of the effeets of spin dIe motor drive
reaming operation, giving a significant saving in the plus associated drive belts on these clearanees. This
value-added machining costs. headstoek's motor drive arrangement eauses an
Reaming technology has radically improved in undulating and irregular harmonie rotational
recent years, reamer design and development con- motion on the work-holding equipment, whieh is
sisting of asymmetrie replaceable blades having a then translated onto the resultant roundness and
floating action with accompanying burnishing surface texture of the workpiece as turning opera-
pads for cutter edge support. Reamers of this level of tions occur. The influenee of this irregular harmonie
sophistieation are typieally employed in the high- rotational belt-driven rotation can be gained from
.volume end of production for automotive engine the schematic representation shown in Figure 181,
part Irtanufacture, such as when reaming out the high where a "tumbling three-Iobed harmonie" shape is
silicou:aluminium alloy camshaft bearing supports. reprodueed on the workpieee. The irregular but
In this production situation the high silicon content periodic nature of the rotational action of the head-
in the aluminium alloy produces ideal (small) grain- stock is reproduced on the workpiece by aseries of
refining effects. As a result of additions of silicon, it kinematie combinations of headstock rotation and
can introduce hard and abrasive inclusions, requir- linear motion supplied by the eutting too1. If a
ing either a cemented carbide or synthetic diamond direct-drive headstoek configuration is used instead
reamer bhlde to be fitted, with guidance through the of the conventional belt-drive variety, then there is
camshaft's location length provided by support from virtually no harmonie influence on the part and
the bearing pads. Today, "hard reaming" is emerging more consistent turned eomponents will result, in
as an important technique in some industries. terms of their geometrical and linear dimensions.
Hard reaming allows components made from mater- Direet-drive systems offer other benefits, not least
ials such as austempered ductile iron (ADI) to be of whieh are lower maintenanee problems, as there
machined directly after initial heat treatment, intro- is no need to periodically adjust belt tension and
ducing not only an appreciable cost saving but also the bearings operate under a more eonsistent and
enhancing the surface texture and roundness levels uniform loading, with better thermal growth char-
of the finished part. Moreover, it has been alluded to aeteristies, resulting in high er spindie aecuraey and
previously that the machine tool's spin dIe and to a improved damping capacity. These positive merits in
lesser extent its overall structural configuration can using a direct -drive spindie promote significant
impart significant errors to the manufactured com- improvements in the overall harmonie roundness
ponent, due to a variety of machine tool-induced throughout the eomplete length of larger turned
inaccuracies. These can be identified as: parts, with less variation in the medium-to-Iarge
frequency surface texture components, resulting
• spindie imbalance - introducing dynamie lower- from this turning operation.
frequency harmonics on the part; If one ignores the fact that either a conventional
• cutterforces - that dynamieally affect the machin- or direct-drive system might be incorporated into
ing process, causing aseries of high-frequency the headstock's design, then the problems associated
harmonics to be superimposed on the lower- with the former type can be ignored. Instead it is
frequency harmonic resulting from imbalance; possible to eoncentrate purelyon the rotational
In(justrial metrology
(a) SpindIe
v v v
(b) SpindIe plus motor and drive
(e) ResuItant
(e) The "harmonies" are virtually eIiminated if direet-drive spindIes are employed
Figure 181. Improvement in roundness quality, via "harmonie suppression" oeeurs if direet-drive spindies are utilised.
effect of the workpiece, allowing the problem to be E.I = flexural stiffness (I = cross-sectional moment
somewhat simplified. In Figure 182 the overall of inertia), Mt = boring bar mass and L = length of
machine-workpiece-tool system can be isolated to cantilever.
consider the simple effect of a tool that is either Therefore, for large length-to-diameter ratios,
inadequately supported or the unlikely occurrence the boring bar's rigidity will influence either the
of too small a cross-section making it under- harmonics of the hole profile or its surface texture.
strength. The main cutting force in turning opera- If the boring tool is too long and unsupported by
tions is the tangential force, resulting from several either bearing/burnishing pads, or via additional
factors, such as: end support - as is normally the case for "line-
boring" operations - then geometrie hole and form
• resistance to rotation - caused by the workpiece deviations will inevitably occur.
material's shear strength; If moderate bar overhangs are utilised in the hole
• undeJormed chip thickness - resulting from the generation process, then the operation can correct
radial depth of cut selected; hole deviations resulting from either the manu-
• orientation oJ cutter rake angle geometry - this facturing process (such as cored holes in castings)
being a combination of either a positive, neutral or drilled hole deviations (promoted by a drilling
or negative rake angle, plus the effect of tool edge operation). In Figure 183 a schematic representation
preparation (if any) and the shape and size of the of the helieal wandering of the drilled hole is
tool no se radius; depicted, along with the correction for geometrie
• Jeedrate - the feedrate, in combination with the error resulting from boring hole generation.
depth of cut, will heavily influence the size of the Notably, as the drill progresses through the work-
effective chip thickness and playa dominant role piece material, minute variations in its geometry
in affecting the resultant turned surface texture. cause the drill to helically wander, producing a
regular but undesirable eccentricity to the hole,
In the top diagram of Figure 182 the tangential whieh needs to be corrected by another operation
force is simplistieally shown contacting the cutting such as boring. This hole correction is necessary
insert at the point. This cutting force application because the drill's cent re line follows the path as
causes a large bending moment to occur at the pivot, indicated" "visiting" the four quadrant points as it
or fulcrum point, as shown. The resultant dynamic spirally progresses through the part. Hole eccen-
action is represented in an exaggerated form in the tricity along with harmonie departures from round-
lower diagram of Figure 182, where the tool is elas- ness can be excessive if lip lengths and drill point
tically deflected in a downward manner by this angles are off-centre. Moreover, the combination of
bending moment. As the resistance to deflection drilling faults pro duces drill out-of-balance forces;
increases with the tool's downward direction, this these can result in an oversized hole, this effect being
causes increased pressure from the inherent tool exacerbated by high-volume production demands
body mechanical strength, enabling a certain degree and necessitating significantly greater drill penetra-
of recovery and hence a partial upward motion of tion rates. The cross-hatched circular areas represent
the too1. This cydieal upward and downward tool the excess stock material removed in the passage of
point motion is repeated at a periodic medium the boring bar along the hole's length, as the boring
frequency, causing sinusoidal motional effects to be insert corrects for harmonic departures from round-
reproduced on the turned surface. High-frequency ness. In this case, if the boring bar is relatively rigid
harmonie behaviour can be superimposed onto the it will not be unduly affected by the variation in
medium-frequency harmonies and can be shown to material wall thickness as it bores out the eccen-
good effect in the power spectrum analysis of tricity caused by the drill's wandering action.
harmonie behaviour during machining. This subject
will be discussed later in a relevant seetion in this
chapter.
Boring operations tend to be somewhat less Cutting forces and tool geometry affects
rigid than turning operations because the rigidity on roundness
decreases by the cube of the distance, as the
following equation predicts: The cutting forces resulting from a combination of
the material's shear strength, undeformed chip thick-
'IT~ 3 EI ness, tool geometry and accompanying no se radius
Jo = U(Mt + O.23Mb ) in turning operations have a significant affect on the
harmonie departures from roundness of the compo-
where Jo = normal force acting on the "free end" of nent. In order to show the effect of these variables in
the cantilever, Mb = modulus of elasticity of the bar, the cutting generation process and to simplify the
Tangential
force
/
-----_--t---_
Cutting insert
// I
I
-t----- -
\
+-- I
I
~~-'------------1~r
\" I
/
Stock to be removed
Tool post
"True circ\e"
"True circ\e"
1- _ _ _ _ _ _ +_ _ -__ _
I
I
I
~
Radial
force
r-----l_Deflection
Harmonie behaviour-resulting
from force variation henee defleetion
and vibration
Figure 182. Harmonie departures from roundness resulting from rigidity/damping effeets while turning.
"True" diameter-after boring operation
Zone of eccentricity
Harmonie departures
from roundness
Boring insert
Figure 183. Harmonie and geometrie correetions by aboring operation previously eaused by the helieal drift of the drill's path through the
workpieee.
discussion, only external-diameter turning opera- piece speeds that can be employed, but this is at the
tions will be discussed. In Figure 184 a typical expense of less rigidity within the work-holding
precision turning operation is shown partially arrangement.
completed, with the "light-turning and finishing" As the orthogonally oriented insert (zero plan
tool progressing along the part. The turning situation approach angle) turns along the part, a "moving
here shows that a long slender part is held in some step" is seen to be present as the "emerging dia-
work-holding device such as a collet, or a chuck at meter" occurs to the desired dimensional size.
the headstock end, with additional support supplied However, if a very high quality part is required, then
by the "dead centre" held in the tailstock. The general it is necessary to look at the turning operation more
trend today is to fit a "rotating centre" in the tail- criticallyas some unexpected and unwanted features
stock, but this can introduce its own eccentric error are present in the final part. As the turning insert has
into the turning process. Rotating centres have an orthogonal orientation to the axis of rotation of
become popular because of the high rotational work- the part, it might be thought that no radial force
component occurs, but this is not the case as the tool component eccentricity/runout. On many sophisti-
nose radius can introduce a radial force that can cated turning centres "programmable-steadies" can
affect the turned surface. The radial force has little be employed to overcome the problem of turning
effect onthe part's harmonics elose to the support long length-to-diameter ratios, where there is a
provided by the tailstock, as shown by the cross- significant tendency to introduce negative out-of-
sectional harmonie and surface texture effect indi- roundness effects into the production process. If the
cated in section "C-C" (Figure 184). As the tool turning centre is equipped with twin turrets, then
progresses along the part the influence of the contri- the technique of "balanced turning", using a tool
bution of the tailstock's support lessens and hence situated in the top and bottom turret with one
the effect of the radial force component increases, as cutting edge slightly ahead of the other, virtually
shown in section "B-B" and to a greater extent in eliminates the radial force affects.
section ''A-X'. Here, the harmonic departures from If the tool is inadvertently set either too 10w or
roundness is significant and has been recognised for high then this will cause either "barrelling" along the
many years by precision turners. Such experienced part, or the "candlestick effect", as it progressively
machinists fit either a "fixed-steady" or the more narrows toward its centre, before increasing in size
preferable "moving-steady" elose to the tool cutting in the same manner as the tool travels along the
zone - on the opposite side of the workpiece - to workpiece's length. Similar effects can occur if the
counteract this radial force problem and to minimise tailstock is not directly aligned to coincide with the
"Moving step" A B c
-+---~-
Headstock
end
Feed
<:J~--
DISPLAYED PROFILES
- exhibiting harmonies - exhibiting large - some harmonie - indicating
andRa harmonie departures departures from little departures
from roundness roundness from roundness
Figure 184. Effect of a combination of several and factors influencing roundness, including lack of support and a non-integral headstock
spindie drive system.
headstocks centre. These setting-induced errors able in the process will be the shape of the cutting
compound the problem occurring as a result of insert. The forces significantly vary in magnitude
the inadequately supported cutting process. The due to the plan approach angle. In the case of the
machine tool alignment problem can be simply orthogonal insert (0°) plan approach angle the axial
rectified by using calibration artefact-based or laser- force dominates, this being associated directly with
based techniques, but this topic is outside the scope the feedrate. A very small radial force is present,
of the present discussion. resulting from the small nose radius on the insert,
Cutting forces can be directly linked to the geo- and its effect on the harmonie trace (A-A) is virtu-
metrie shape of the cutting insert, this effect being ally negligible. If a triangular cutting insert geom-
illustrated in Figure 185; in these cutting force repre- etry is utilised, in this case with a 15° plan approach
sentations the tangential or cutting force is not angle, then there is a slight reduction in the axial
considered in the diagrams. If the overall cutting force component and a corresponding increase in its
conditions remain the same - rotational speed, radial counterpart. This minor increase in radial
feedrate, undeformed chip thickness, workpiece force in combination with a slightly longer cutting
material and insert rake angle - then the only vari- edge in contact with the workpiece's transient
Displayed profiles at sections but in the same position on part:
A C
I
I
I
,
I
- - -,- - ----1-
,
I
I
I I
I I
Feed
<J----
Curved = Plan
Approach
Insert shape: Angle
Weak Strong
~~----------------------------~~
~--------------------------------~~
Less prone to vibration Vibrational tendencies
NB Tangential, or main cutting force not shown
Figure 185. The effect that insert shape and its approach angle has in influencing the cutting forces, hence harmonie departures from roundness.
surface (the workpiece surface to be removed during the result of two principle factors: firstly, the length
the next rotation) leads to a marginal increase in of the transient surface has increased; and secondly,
harmonics on the polar trace (B-B). As the obliquity as a result of this first condition, the part rigidity is
of the insert's plan approach angle increases, as compromised, leading to this exacerbated workpiece
shown by the square-shaped cutting insert inclined roundness.
at an angle of 45°, then the axial and radial force If a round insert geometry is selected, this leads
components equalise. The considerable radial force to a vast increase in the radial force component,
component in this case has a significant effect on the which in turn causes significant harmonic out-of-
polar plot as shown in C-C, where the harmonics roundness in the resulting polar plot (D-D). Here,
have increased along with a notable vibration the polar plot shows major sinusoidal tool motion
tendency that is superimposed onto the primary (see Figure 182, lower diagrammatic representation)
harmonic. An increase in vibration during cutting is with a significant increase in vibration present on
(a) Forces acting on a round geometry insert at a variety of depths of cut: constant feedrate
(i) (ii) (iii)
Resultant
force
(mean) Radial
force
(b) Harmonie departures from roundness on machined component resulting from differing cut depths
Sm all harmonie effect Large harmonie effect
I I
-+- -+- I
-+- I
Figure 186. Harmonie departures from roundness resulting from the radial cutting force pressure on the component.
Im
this trace. The reason for this notable increase in square rule", which states: milling cutter rigidity
harmonics using round inserts is the product of decreases by the square of the distance from its
several factors. The transient surface in contact with holder. In reality what this is attempting to infer is
the tool has markedly increased and the plan that if a cutter was originally 50 mm long and a
approach angle at the tangency point is at maxi- cutter of twice this length is fitted instead (100 mm
mum; the combination of these two factors leads to long), then the rigidity of the complete assembly
a momentous deterioration in workpiece rigidity will be four times less rigid. This lack of milling
and, as a result, vibration especially is increased. cutter rigidity will cause a number of unwanted
The problem associated with the harmonie effects to appear on the final part feature. Cutter
behaviour of cutting insert geometry is of less deflection will introduce distortion to a square-
importance for large stock removal operations; milled shoulder and harmonie variation, degrading
roughing cuts as a strong insert can be employed, the departure from roundness of the workpiece, as
hence the use of either square or round inserts. If illustrated in Figure 187. In order to introduce
vibration is a potential problem, then the light minimal changes to the milled profile cutter lengths
turning and facing insert of the "trapezoid geom- need to be kept to aminimum, conducive with
etry" shown in this case, with a 0° plan approach correct operational practices.
angle, may be the production solution. In order to fully appreciate the significance of
The round geometry insert is worthy of closer the schematic diagram shown in Figure 188,
investigation and a more detailed sketch of its featuring milling by circular interpolation and its
effect on the harmonie machining behaviour is indi- relationship to the circular feature produced, a slight
cated in Figure 186. Here, identical rotational speed, digression into basic machine tooI-induced errors is
workpiece material but differing undeformed chip necessary. Machine tools that are typified by the
thicknesses (depth of cuts) are utilised to isolate popular three-axis vertical machining centre config-
variability in the machining process. In Figure uration of conventional orthogonally orientated
186(ai) a small undeformed chip thickness is used, slideways (square to one another) can introduce
creating a significant radial force in combination considerable error into the quality of the final part.
with a minute axial force component, leading to the It has been established that three orthogonal slide-
polar plot shown in Figure 186(b, for a "finishing ways - X- and Y-axes in the horizontal plane,
cut"). The argument put forward above, concerning together with the Z-axis in the vertical plane - can
the influence of the large radial force component introduce up to 21 kinematic errors into the cutting
leading to poor harmonics in Figure 185, is not process. The kinematics are quite complex for any
contradicted here, because the cut depth is very machine tool having the ability to move all its
smalI, hence transient surface contact will also be of axes simultaneously, but these small though im-
litde influence. portant errors can be simplistically said to occur as
To give an impression of the influence that the cut a result of:
depth plays in the magnitude of cutting component
forces, the following discussion needs consideration. • six linear motions - produced by displacement of
As the undeformed chip thickness increases from the forward and backward motion of the X-, Y-
the left in Figure 186(ai, aii to aiii), then the are of and Z-axes slideway movements, introducing
contact along the transient surface also proportion- particular non-linearities into slideway posi-
ally increases. This larger effective cut length creates tioning;
a significant departure from roundness harmonie • three rotational motions - yaw, pitch and roll
behaviour on the polar plot, as depicted in Figure on each axis. Yaw is the side-to-side "crabbing
186(b, for a "roughing cut"). motion" along the slideway. Pitch occurs through
waviness in the slideway, introducing a backward
and forward rocking (pitching) action, normal to
Interpolation and its effect on harmonics the slideway, as the moving element traverses
along the axis. Roll may be introduced by two
In CNC milling operations circular features on pris- adjacent ways on the slideway not being coinci-
matic components such as bosses can be produced dent (laying in the same respective plane), causing
in a number of ways, most notably by milling using an upward and downward pivoting action with
the circular interpolation function. This CNC func- respect to the "line-of-sight" along the axis, as the
tion allows accurate circular control of two slideways moving element traverses along its length;
simultaneously, while the cutter mills around the • three squareness errors - these errors occur due
part, as illustrated in Figures 187 and 188. Cutter to the fact that each axis may not be normal
rigidity plays an important role in the quality of the (square) to one another.
final machined feature, being based on the "rigidity
Constant pull-stud force
Spindie
taper
Gauge line
Milling
Milling cutter
cutter -deflected
-no deflection
e
e
0::>
lI'l
e Milling
e
0::>
cutter
:: -undistorted
m~,
VI
I
I
Workpiece
distortion
+-
I
Figure 187. Exaggerated effect of cutter length on the resultant circular interpolated profile on the workpiece.
These kinematic machine errors can be appre- campensatian system have been shown to extensively
ciably reduced by the application of calibration reduce the effects of the variety of errors that can be
through laser-based techniques, or to a lesser extent present on the machine tool, but on ce again this
via baUbar artefact-based methods. These machine topic is outside the scope of the present discussion.
tool calibration techniques are outside the scope of Considering the circular interpolation of milled
the present discussionj the same can be said of the profiles as shown in Figure 188, the departures from
thermaUy induced errors and how they can also roundness of the workpiece is a function of the
influence the machined part surface and profiling previously discussed kinematic machine-induced
qualities. Moreover, errar-mapping techniques and and thermally induced errors, together with load-
in-process control by an associated dynamic errar induced errors. The diagrammatic representation
True circular
path Tolerance of linear
approximation to
programmed path
Yaxis ~
Circulation interpolation
(Down-cut milling)
"-
Rotatio. ~
\
_+-____ -~;.t-C: =-! X ni,
I
I
/' "\
\~ -
True circular
-Yaxis V Servo-lag
Actual profile
path
Backlash Y axis
Servo-spike
Figure 188. Generated circular interpolation exaggerating the calibration/machine tool errors associated with climb milling.
shown in Figure 188 indicates that several of these Servo-spikes result from areversal of one of the
errors on the circular profile of the workpiece are axes at this angular position and a motor power
present. As the simultaneous motions of the two axes surge (spike) occurs with a corresponding local-
occur (to produce the circular feature), then by ised slack here, as take-up begins (see Figure 188
increasing the interpolation speed for the cutter the at the quadrant points on the circular feature);
roundness will degrade; this is the result of several • backlash - this is present here in some form at
interrelated factors, some of the most notable being: the axis reversal position, because of the forward
and backward motion at the axis transition
• servo-spikes - these occur at the axis transition points, resulting in "play" (backlash) in the ball-
points at their respective 90° angular intervals. screw (attached to and controlling the slideway
motion). This backlash is present despite the fact (in-cut) until it becomes completely worn out. In
that a recirculating ballscrew on each axis has Figure 189(b, top) the surface profile appears as
been utilised that should have previously been aseries of periodie and regular machined cusps,
pre-loaded, which was meant to negate such indieating that an efficient turning operation has
backlash problems; occurred, whieh can be confirmed by the power
• servo-errors - when both axes are moving simul- spectrum in Figure 189(c). This turning operation's
taneously, their respective linear speeds should power spectrum, as expected, indieates distinct
have been matched, allowing either a perfect frequencies, the fundamental frequency relating to
circular feature or partial arc to be reproduced. the feed spacing of the cusps and the harmonies to
If any non-synchronised motion occurs (servo- the non-sinusoidal tool geometry - its shape. After
mismatch) between these two axes, then an ellip- successive passes along consecutive workpieces the
tical profile normally set at a 45° angle would tool begins to show signs of localised insert flank
occur. If the contouring interpolation is changed and face damage, with the ratio of the height of these
from a clockwise to an anti-clockwise circular harmonics to that of the fundamental frequency
feed motion, then the angular elliptical profile increasing. This harmonic increase is a direct result
shape will "mirror-image" (flip) that of the oppo- of the imposition of the insert's imprint in the
site profile; turned surface. The increased harmonie activity
• squareness - if orthogonality (squareness) is not here occurs due to the wear scars that correspond-
maintained between the two axes, then this will ingly occur on the insert's cutting edges; these are
result in yet another similar milled angular ellip- then faithfully reproduced on the surface topo-
tical profile (as discussed above, for servo-mis- graphy. Moreover, at this position the baseline of the
match), but the difference here is that the shape fundamental frequency can be expected to rise; this
orientation does not change (that is, reverse its increase will probably be because of random effects
shape) if either clockwise or anti-clockwise feed due to the formation of arbitrary chips and the
motion is applied. turned surface exhibiting micro-fracturing. If it is
adjudged that these surface random effects of
Considerably more factors can affect a milled machining are significant, it is probably a more
circular interpolated shape and many of these appropriate strategy to consider their examination
machine tool-induced errors can be diagnostically by utilising the auto-correlation function.
interrogated by using dynamie artefacts, such as the In Figure 190 (right) harmonie information
ballbar. Such instrumentation can find the sources within the power spectrum is depieted, in this case
of error, list their respective magnitudes and apply to the left-hand side of the fundamental frequency
corrections that can be fed into the CNC controller (feed). Here, periodicities occur which are of consid-
to nullify the errors, enabling circular contouring erably greater wavelengths than that of the feed.
milling performance to be significantly enhanced as These harmonics are the result of machine tool-
a result. induced problems, such as bearing chatter and
slideway errors, together with other unwanted
effects. The position of the harmonies related to the
bearing problems appear closest to that of the
5.2.7 Power spectrum analysis of fundamental frequency, whereas the very long wave-
machined surfaces lengths, for example, can be attributed to form errors
in the slideway, or perhaps are the result of struc-
In many situations of a stochastic (variable) tural distortion of the machine tool itself.
machining nature, the power spectrum is a useful A major advantage of using the power spectrum
aid in process control monitoring of the cutting as a diagnostic aid is that it can separate out the
capabilities and gives a good interpretation of the process-related problems, as depicted by the power
anticipated surface topography. Once again the spectrum diagram shown at the bottom left-hand
turning operation, because of its relative simplicity side of Figure 190. Hence, to the left of the funda-
of a single-point machining operation, will be used mental frequency (feed) in this diagram, in region
to show how the power spectrum can be employed "/\', the harmonics of the machine tool problems can
to identify tribologieal factors such as tool wear and be isolated out; and to the right of region "B" those
how this influences the surface topography of the of the feed frequency can be established, with the
workpiece. In Figure 189 the main feature here is workpiece material properties occurring displaced
that it is possible to identify and then quantify tool even further to the right in region "C". The separa-
wear by an examination of the power spectrum. To tion into discrete power spectrum frequencies can
the left-hand side of Figure 189(a) a tool is shown be established, although such diagnostic interpreta-
when new, then it progressively degrades with time tion cannot be readily detected in surface profiles at
(a) New tool (b) Surfaee profile (e) P(w)
~-----~__~'__'_~-L__~____~
Stightly worn
toot
~-----l~_ _F_~LI ____L -_ _ ~ ~_e~
___
~ A+ 1\ I\j
~-
o A+ 1\: 1\
I
+
+
I
I
+ I
I
I A~ ______~A~____~~
Badtyworn
toot
:I
( l I<~~~~~
~
+
I II<~~~ Wearscars
Surface micro-fracture
I
------c:::::- Process
! ~
~.
BuHt-up edge I I Feed, wear scars and
+ microfracture I I surface micro-fracture
~ Sampling length ~
(Long) .... Frequency.... (Short)
Figure 189. Power speetrum analysis harmonies for a maehined surfaee. [After Whitehouse, 1997.]
Bearing chatter
surface profile
~ Feed w
Freq
I Slideway error
I
~ Feed w
Long-wavelength summed
land scaled
~ Feed
Subharmonies w
Added roughness
..
I
P(w)
I Region A-Machine tool
I Region B-Process
I Region C-Material properties
I
I
Figure 190. Power speetrum analysis, sub-harmonie and total speetrum. [After Whitehouse, 1997.]
this initial stage in the life of the tool by the senses 5.2.8 Manufacturing process
- either visually or by its sound during machining.
This application of the power spectrum to process- envelopes
related manufacturing problems gives an early
warning of the performance of the complete produc- The principal feature of manufacturing process
tion process, enabling remedial action to be taken to envelopes and, indeed, for many amplitude distrib-
rectify a minor problem before it becomes critical. ution curves is that they can be approximated by the
A note of caution is required here, as there are occa- so-called "beta function" (Figure 191a). Here, the
sions when even the application and interpretation function has two parameters that are independent
of the power spectrum may prove inadequate to of one another, enabling them to be utilised as a
identify problems in production. This limitation to means of characterisation. The notation a is the allo-
the use of such powerful diagnostic aids can arise in cated weighting for the profile ordinates measured
situations where either time or space varies; further- from the lowest valley and above, with the notation
more, if workpiece variability through unanticipated b being given to weighting the profile from the
defects is present in the production batches this will highest peak down. Hence, peaks and valleys have
nullify the technique. accordingly different weights. One of the problems
(a) The beta function: (i) symmetrical and (ii) asymmetrical case. (After Whitehouse, 1994)
(i) (ii)
0=b=5 3.0 0=5
b =1.5
o =b=3 0=2
b =1
0=3
o =b=2 b =1.5
a =b =1 0=1.5
b=3
a =1.5
b=5
0 0.5 1.0 0.5 1.0
\ \ Plateau honing
12
\ ~ Milling
10
-2 -1 o +1 +2
Skewness
Kurtosis
12
-2 -1 o +1 +2
Skewness
b = Rp (RV Rp - Rq2)
Rt Rq2 Ternary manufacturing envelopes (TMEs)
The reality that any dominant peak or valley within In machining operations the dominant factor that
the assessment length is only raised to a unit power influences both the resultant cutting forces and the
infers additional stability over the skewness/kurtosis surface topography has been shown to be the tool's
approach. The trouble with this method is in accu- feedrate. In Figures 193 and 194 the feedrate, in
rately determining sound results from Rv and Rp, conjunction with the principal factors of surface
which confirms the problem that obtaining infor- texture (Ra) and roundness (by least squares cirde
mation from peak/valley measurement and then - LSC), are used to define the limits for these TMEs.
deriving valid information from them can be fraught Utilising these diverse surface texture, roundness
with difficulties. In Figure 191(a) both symmetrical and processing parameters (feedrate) for the major
(i) and asymmetrical (ii) graphs for the beta func- axes on the ternary diagram enable a machined
tion are illustrated, based on a dass of Pearson surface to be characterised in a new manner. As
distributions. In the symmetrical case the skewness might be anticipated, these TMEs differ markedly
equates to zero; conversely, for an asymmetrical from the more usual and restricted manufacturing
series of results, skewness can be either positively or envelopes previously alluded to above; the latter type
negatively skewed. Nevertheless, even allowing for of skewness and kurtosis axes might otherwise
these limitations, an example of a range of the manu- mask crucial information. The "TME approach"
facturing process envelopes that can be produced gives a pseudo three-dimensional graph that can be
using this technique is illustrated in Figure 191(b). exploited to illustrate how the influence of changing
Here the production processes can be simplistically a parameter such as feedrate modifies the relation-
dassified and grouped into either a "bearing" or ship of the surface texture and roundness values in
"locking" surface topography (Figure 191c). This the final machined result. Furthermore, such a three-
bearing/locking grouping shows that certain pro- dimensional graph can be exploited to illustrate how
duction processes can achieve specific functional the influence of changing the feedrate modifies the
surfaces for industrial applications. However, the interrelationship of surface texture and roundness
general picture is not as distinct as the grouping values.
shown in Figure 191(c), because certain processes As an example of the usefulness of this TME
cannot only run across each dassification but may approach to complex machining analysis, Figures
fall between both the bearing and locking envelopes. 193 and 194 for dissimilar production processes are
A typical "intermediate envelope" that normally presented. The TME graph for a particular range of
occurs in just this vicinity of the skewness/kurtosis turning and boring processes, indicated in Figure
graph would be machined surfaces manufactured by 193, shows how at low feedrate (0.10 mm/rev) the
the PM route, as shown in Figure 192. Here, in both surface texture is dosely confined to a relatively
a twist and split-point drilling operation, the porous small spread of values - nominally around 0.5-1.5
nature of the PM compacts creates pores that are f.Lm Ra, whereas its associated roundness lies
Kurtosis: Rku (!-tm)
Feedrates (mmJrev)
Jobber Split-point
0.127 GJ--IZ>'I--
(SAMPLES: 1 to 8)
0.254 o ~--
-4 -2 o 2 4
Skewness: Rsk (!-tm)
Figure 192. Manufacturing envelopes for jobber and split-point drilling operations: skewness v. kurtosis.
Surface texture: Ra (11m)
16
15
14
13
12
11
10
Feedrates (mmlrev)
Turning Boring
0.10 8-- ®--
0.25 0 - - (n/al Feedrate (mmlrev)
0.40 8. - - A - -
Figure 193. Ternary manufaeturing envelopes of the produetion processes: turning and boring - feedrate, roundness and surfaee texture.
between approximately 5 and 30 /-Lm LSC. As the is only the result of linear motion (being caused by
feedrate increased in an arithmetic progression to the fee ding motion along the part) and it is not sur-
0.25 mm/rev, the range of the surface texture band- prising to note that a direct relationship exists
width proportionally expanded to l.5 at approxi- between selected feedrates and tool nose geometries.
mately 5-6.5 /-Lm Ra, with a corresponding increase The boring proportional bandwidth can be ex-
in roundness from 8 to 48 /-Lm LSC, giving a propor- plained, allowing for its overhang, which must be
tional bandwidth of l.6. As the feedrate was raised present to avoid fouling on the workpiece. This over-
even high er, to 0040 mm/rev, it was not surprising to hang creates a reduction in stiffness based on the
note that this also produced increases in both the cube of the bar's overhanging length; when com-
surface roughness and its proportional bandwidth, pared to the process of turning this is its OD opera-
with similar values with respect to its roundness. tional counterpart. Aboring tool intro duces a
Similar trends occurred for the boring operation "phase-damping" effect on the out-of-roundness
on Figure 193, but here only two feedrates were and, as such, reduces the overall magnitude of the
employed. At low feedrate (0.10 mm/rev) the surface LSC value obtained. When utilising the 0040 mm/rev
texture range was approximately 0.5-2 /-Lm Ra, with feedrate, boring in this case will generate a propor-
roundness being between 8 and 36 /-Lm LSC. Once the tional bandwidth increase in LSC of l.7, while an
boring feedrate had been raised to 004 mm/rev, this equivalent OD turning operation produces a value of
produced an increase in the surface texture to l.92. The more compliant and less rigid boring bar
around 13-18 /-Lm Ra, with a corresponding propor- will have a greater tendency to deflect the cut, leading
tional bandwidth of 33.33. Furthermore, the round- to slight tool bending termed a "spring cut", intro-
ness also degraded to 15-63 /-Lm LSC, which resulted ducing a form of "phase-damping" behaviour that
in the bandwidth being proportionally increased to tends to smooth and blend out the harmonie factors.
l.7. Discussion of these proportional bandwidth dif- Conversely, the opposite is true for the behaviour of
ferences can be used to explain why either the the proportional bandwidth in machined surface
outside diameter (OD) turning or internal diameter texture parameters, where an increase was observed
(ID) boring operational performances vary. In the in boring with respect to turning at identical feed-
case of the OD turning operation (a schematic of the rates. This difference can be explained in terms of the
turning process is shown in Figure 169), as the fee- associated boring bar overhang and its reduction in
drate is progressively increased both the surface rigidity. Increased tool deflection would tend to be
texture and roundness will degrade. This expected superimposed onto the bored surface topography,
deterioration occurs because as the feedrate in- leading to greater dispersion in data points, whieh
creases it results in coarser machined surface topog- then increases the proportional bandwidth if com-
raphy, and as the cutting forces are proportionally pared to a similar turning operation, with both
high er this provides a destabilised cutting-edge cutting inserts having identical nose radii.
condition, which subsequendy leads to greater The drilling TME depicted in Figure 194 shows a
departures from roundness, resulting in secondary limited range of drilling operations using both an
harmonie roundness error. There was a larger uncoated jobber drill and a TiN-coated split-point
proportional bandwidth expansion for surface drill. In this case the TME shows how the generation
texture as a result of the influence of feedrate rather process of dynamieally drilling holes influences the
than for departures from roundness. This bandwidth simultaneous procedure of surface roughness and
increased in the same fashion to the increases in roundness production at different feedrates. The
respective feedrates, namely in an arithmetie pro- normal technique is to consider each metrologieal
gression - lengthening at the rate of l.5. Such condition in isolation and thereby potentionally
increases in dispersion of resultant machining data missing some vital information. In Figure 194a "com-
can be substantiated by earlier work, whieh suggests parison of extremes" can be made to establish how
that there is a geometrie relationship between the differing tool lengths combined with changes in
insert nose geometry and selected feedrate on the point geometry influence the resulting surface
respective machined surface texture. However, this texture and roundness parameters. Most surpris-
proportional behaviour did not extend itself to ingly, at a 0.127 mm/rev feedrate the split-point drill's
machined roundness values, which are a function of mean range of surface texture was worse
a more complex interactive cutting path action. Such than that obtained with a jobber drill, ranging over
action is promoted by combined rotational and 2.8 /-Lm Ra; this was possibly due to the "rounding
linear motion (as the workpiece rotates and the tool effect" on the drill's lips and point edges. Equally, the
is fed along the part), leading to differential primary, LSC roundness range showed that the jobber drill
secondary and tertiary (an so on) harmonie depar- was far worse than that for the split-point, its vari-
tures from roundness. The machined surface topog- ability increasing by 33%, being present over 30 /-Lm
raphy, indicated through the Ra surface texture trace, LSC. What this variation illustrates is that the jobber
Surface texture: Ra (~m)
4
I
I
I
3
Feedrate (mmJrev)
Feedrates (mmJrev)
Jobber Split-point
0.127 8 - - 181- -
(Sampies: 1 to 8)
0.254 0-- ~ - -
Figure 194. Ternary manufaeturing envelopes of produetion processes: jobber and split-point drilling - feedrate, roundness and surfaee
texture.
drill, at low feed, had a smaller and more consistent The in-depth discussion on the use of the TME
spread of results for surface roughness than that of technique with their related production processes
the split-point drill, although its level of recorded and associated metrological parameters, together
roughness was high er. This drilled hole variability with subsequent results above, was included to illus-
suggests that the slightly larger drill margin on the trate how machined components and specific
jobber drill burnished the resulting saw-toothed processes can be combined into pseudo-three-
profile topography and, in so doing, reduced the Ra dimensional diagrams. Such graphs may give a new
range. Hole roundness deteriorated using the jobber insight into what constitutes a machined surface,
drill. This deterioration came as no surprise, as its indicating that surface text ure parameters alone
longer and flatter chisel-edge profile, combined with should not be separated out from those of round-
a greater overall drilliength to that of the split -point, ness. The combination of these previously disasso-
inevitably meant that the drill produced a degraded ciated surface texture and roundness parameters
self-centring action. Coupled to the jobber's greater may offer a new approach in the manner that the
length, reduced drill integral rigidity occurred; this machined surface condition is assessed, allowing an
led to inferior drilled hole roundness. Once the fee- appreciation of the whole surface and not just some
drate was increased to 0.254 mm/rev, a similar trend associated parameters in isolation.
occurred for drilled hole roughness. The split-point
drill's range was 41 % larger and of similar magni-
tude to that of the jobber - ranging over an Ra of 3.9
/-Lm - illustrating that drill burnishing was present in
this case at higher feedrates. However, the trend for 5.3 Surface engineering
roundness at this high er feedrate was reversed. The
split-point drill showed a larger error in the range
of departures from roundness, being 25% worse, Historical context
coupled to a similar magnitude - ranging over an
LSC of 32 /-Lm - indicating that at higher feedrates the The currently accepted definition of the subject
self-centring action was a negligible factor. of "surface engineering" was adequately coined in
If a comparison is now made of the surface the late 1980s by Professor Bell of the University
texture and roundness parameters against feedrate, of Birmingham. It states that surface engineering
in the first instance for the jobber drill and then involves the application of traditional and innovative
considering the effects produced by the split-point, surface technologies to engineering components and
a significantly different pieture emerges for the materials in order to produce a composite material
drilling process. When utilising the jobber drill, and with properties unattainable in either the base or
as the feedrate increases from 0.127 to 0.254 mm/rev, surface material. Frequently, the various surface tech-
there is a slight improvement in the range of surface nologies are applied to existing designs of engi-
texture from 2.6 to 2.3 /-Lm Ra, for the low-to-high neering components but, ideally, surface engineering
feedrates, respectively. This 11.5% improvement in involves the design of the component with a know-
the spread of Ra at higher feedrate is somewhat ledge of the surface treatment to be employed.
misleading as the magnitude is greater, which Historically, some of the earliest references on the
conforms to the published literature. This partial yet subject of surface engineering are somewhat vague
slightly confusing improvement in surface texture allusions to the metallurgical treatment of armour,
using the jobber drill at high feedrate also occurred notably quench hardening of weapons by the
with respect to roundness, as the LSC ranged from process of blinding the Cyclops in the Odyssey, by
8 to 39 /-Lm at high feedrate. Once again, it would Homer. This Greek saga was written about 880 BC,
seem that the wider jobber drill's margin influenced but referred to an earlier Bronze Age period (1400-
the burnishing both linearly with respect to variance 1200 BC). However, in the Iron Age the carburising
in asperities and circumferentially, by minimising of weapons by some form of case hardening, or more
harmonie departures from roundness. The drilling specifically carbonitriding, was widely practised.
behaviour of the split-point was more predictable. This heat treatment process was in reality an austen-
In the case of surface roughness, this ranged from itic thermo-chemical procedure involving the diffu-
2.8 /-Lm at low feedrate to 3.9 /-Lm at high feed, with sional addition of both carbon and nitrogen to
similar magnitudes with respect to Ra levels. The austenite. This was a somewhat long-winded process
trend in roundness variations was much the same; and was followed by rapid and agitated vertical
at low feedrate the range was 20 /-Lm, while at high quenching to harden and improve the wear charac-
feed it degraded to 32 /-Lm, with similar magnitude teristics of the weapon, followed by tempering to
in LSC level. This degradation is wholly consistent enhance the toughness. Notably, in the eleventh
with increasing penetration rates. century AD a German monk, Theophilus, in his work
Schedule diversarum artium, mentioned the word nous and impracticable within the scope of the
temperamento, meaning to quench and self-temper current work; however, only an overview can be
in goat urine - after certain complex pre-treatment given here. The level of technological development
of the goat! This prior management of the goat was for surface engineering technologies across various
necessary to increase the acidity level of the sub se- manufacturing industries will be markedly different,
quent fluid media necessary for heat treatment and although their natural sequence of events for
hence enhance its severity, enabling the liquid to be component production may be summarised in the
utilised for severe quenching applications. Although following manner:
they did not know it at the time, such practical heat
treatment enhanced the critical cooling velocities Application => Properties (required) => Design =>
through the time-temperature transformation (TTT Materials (selection) => Engineer (substrate) =>
curve), obtaining the desired mechanical properties.
In Japan the swords of the samurai were uns ur- Engineer (surface) => Lubrication =>
passed in their keen edge and cutting ability. Their Performance
success relied on very complex manipulation of the
sword's grain structure (up-setting and folding by (After Bell, 1990)
hammer blows of the weapon on the anvil) and intri- Recent and traditional surface technologies con-
cate heat treatment processes, in order to obtain the tribute to a multifarious assortment of treatments
desired metallurgical and mechanical properties. enabling design and manufacture of a diverse range
Contemporaneous with the Japanese were the early of metallic-based composites. By modifying a com-
metallurgical developments by Chinese dynasties, ponent's structural characteristics/composition, it
whereby soya bean pro tein that had decomposed intrinsically changes its engineering properties. In
was employed to enrich the red-hot edges of steel simplistic terms, non-mechanical surface treatments
swords with carbon and nitrogen, and in so doing can be classified into various groupings, as follows:
enhance their mechanical properties.
In Britain a 1727 publication entitled Husbandry • thermal treatment;
and Trade Improvement by John Houghton FRS • thermo-chemical treatment;
made reference to surface hardening. In the West • plating and coating;
Midlands techniques for surface improvement "... • implantation.
as being done at Wolverhampton in a different
manner; with burnt hoofs and horns, bag felt, old For an engineering designer, the technological
burnt leather and tartar all mixed together with selection of a means to manipulate and change a
urine" again seemingly found the latter ingredient surface becomes an integral part of component
essential! Pre-dating this time was the first scientific design. The decisive step taken to enhance a compo-
investigation of surface treatments undertaken by nent's material surface signifies the fact that one of
Reaumur in France in his magnum opus published the existing base material properties needs manip-
in 1722. In fact, some rather dubious materials ulation in some way, in order that it satisfactorily
(burnt leather in particular) were being employed fulfils its functional performance, while at the same
for case hardening, by pack methods, prior to the time being economically acceptable. An engineered
First World War. These natural forerunners of later surface can have its coating thickness varying from
surface engineering processing and treatments for several millimetres, by weId overlays, to just a few
enhancement of metallurgy, typified by techniques micrometres - for either physical vapour deposition
such as grain refining and surface quench hard- (PVD) or chemical vapour deposition (CVD) coat-
ening, could be utilised without reliance upon elec- ings - and surface depth modifications to approxi-
trical heating/phenomena to induce modifications mately 0.1 /-Lm - by ion implantation (Figure 195).
to surface properties. Only with the advent of an In a similar manner the hardness of coatings spans
active research programme into electrical pheno- a wide range; typically these might be:
mena in the late nineteenth and early twentieth
centuries was it possible to envisage surface tech- • spray coatings - ranging from >250 to 350 Hy ;
nology applications, many of which are now becom- • nitrided steels - around 1000 Hy ;
ing mature commercial technologies. • detonation gun (D-gun) carbide-metal cermet
coatings - ranging over 1300-1600 H y ;
• titanium nitride (TiN) coatings by the PVD
(ontemporary surface engineering process - up to 3500 Hy •
If the subject of surface engineering was only Initially when selecting a surface modification
partially developed, then the text would be volumi- treatment, it is important to comprehend what the
10
==!~~f/Wß
cv~t0WA1
I W~ Electroless ~ickel
I 01)
=
~
Composi~e~ 8
"0
=~
~M Thermal SfraYingi
c:::
r-:-
~ Ion Implantation
-- I I
BorO~iSing ~
I
~~~ carboNitridi;n g
Carburisi~g ~~
I
Figure 195. Typical thicknesses of surface layers for engineering components. [After Bell, 1990.]
249
(a) Hairs vary remarkably in size - orten used as a stan- consistent parts more economically enables signifi-
dard of minute measurement (magnification x270) cantly higher levels of precision and the attendant
higher value-added tolerances, surface texture and
other exacting features to accrue.
In Table 18 the currently achievable tolerances by
contemporary precision CNC machine tools and
specialised associated equipment are listed.
When it is considered that Taniguchi made his
prediction of machined accuracy in 1974, he was
remarkably accurate in his extrapolated data for
normal, precision and ultra-precision machining
accuracies (Figure 198). The advent of the term nan-
otechnology, coined by Taniguchi in 1974, heralded
the concept of actually machining at nanometric
accuracies (10- 9 m), which is very dose to the atomic
lattice spacing. Today nanometric machining is a
reality, with components of quite large dimensional
size being held to diameters and surface textures of
(b) CIose-up of an individual strand of hair, iIIustrating nanometric accuracies and finishes respectively, or a
good diametrical consistency (magnification x1500) combination of both. Conversely, minute compo-
nents can be manufactured to within nanoscale
resolution and this technique is fast becoming
increasingly popular, as part miniaturisation be-
comes essential in many industrial applications.
Nanotechnology instrumentation
The general rule of thumb that inspection instru-
mentation should be at least ten times more accurate
than the equipment manufacturing the component
is exceedingly difficult to achieve at present for parts
made in the nanotechnology range. Nanotechnology
instruments have been developed to both explore
and measure surface properties in the vicinity of
the atomic range, typically investigating surface
topography, grain boundary coherence, atomic dis-
locations or similar - some of which were briefly
touched on in Chapter 3. These nanometric require-
Figure 197. Hair size has often been seleeted to illustrate the magni-
tude of size. [Courtesy of Jeol (UK) Ltd,]
ments exceed the concept of performance of dimen-
sional tolerances on a machine tool, or the attainable
surface text ure for apart. Notionally, the surface
production and its accompanying measurement can
precision machine tools, but particularly the engine be categorised as follows:
lathe. Notably others such as Sir Joseph Whitworth
(1803-1887) developed the 55° induded angle Vee- Functional performance for specific topographical
form screwthread, allowing precision feed motion to and surface features
be accomplished through suitable ge ar trains on
machine tools. These technological advances and • surfaces of magnetic heads and compact disks for
fundamental work by others, for example Joseph R. storage capacity;
Brown (1852), who designed a "dividing engine" for • coatings on cutting inserts and tools, for wear
the production of precision engraving, further properties;
enabled a wider range of machine tools, such as that • tribological investigation on bearings, or adhe-
by Eli Whitney (milling machine) to be designed and sion and adsorption problems;
developed, and then refined. With the considerable • surface effects produced by non-conventional
technological strides in precision engineering in the mechanisms (EDM, ECM, USM, laser and WJM,
last hundred years, today the ability to reproduce etc.);
Quality and calibration techniques
200 Normal machine and home-made General-purpose electrical Camera and telescope
parts parts (switches, motors and bodies
connectors)
50 General purpose mechanical parts Packages (electronic parts) micro- Camera shutters, lens
(gears and threads), typewriter motors, transistors, diodes and holders (for cameras and
and engine parts magnetic heads (video/type microscopes)
recorders)
5 Mechanical watch parts, accurate Electrk relays, condensers, disk lens, prisms, optical fibres and
gears, threads, machine tool memory, silicon wafers, TV colour connectors
bearings, ballscrews, rotary masks, video head and cylinder
compressor parts, shaver bl ades
0.5 Ball and roller bearings, precision Magnetic heads (video cassette Precision lens and prisms,
drawn wires, flapper servo-valves, recorders, CCDs, magnetic scales, optical scales, elastic deflection
gyro bearings, air bearings, quartz oscillator, magnetic bubble mirrors, IC exposure masks
precision dies, roll thread dies, memory, ICs, magnetrons, thin (photo/X-ray), laser polygon
ink jet noule film-pressure transducers, thermal mirrors, X-ray mirrors
printer heads, memory, electronic
video disks
0.05 Gauge blocks, diamond indentors, IC memory, electronic video disks, Optkal flats, precision Fresnel
high-precision X-Ytables, high- large-scale I('s, micro-vacuum lens, optical diffraction
precision stamping and dies, tubes, TFHCD gratings, optical video disk
microtome cutters (dia mond) (CD)
0.005 Ultra-precision parts (plane, ball, VlSI's, super-Iattices (synthesis) Ultra-precision diffraction
roller, thread) thin films gratings
(Special features) Shape (3-0) preciseness Pattern (2-D) fineness Mirror grating (1-0) accuracy
• damage monitoring of both pure and hybrid graphie al processes, a large number of instrumental
materials at the atomie scale; techniques have been developed to encompass these
• semieonductor and similar electrically based investigative procedures. Each instrument in this
surface properties, with respect to either charge large array of equipment needs to be calibrated at
injection or storage; periodic intervals to ensure that data obtained is
• surface catalysts and reagents concerning chem- traceable to known international and national stan-
ical processes and reactions; dards, so that some form of consistency in inves-
• surfaces of biological molecules in both liquids tigative procedure is assured. The following section
and membranes and their changes in real time. will explore both the underlying philosophy and the
route in achieving traceable measurements.
Specific measurement requirements
t"m. I
____ ~C'::,,>~ -x~~~- __ ~:1~. _---L __ ___ ~ ~~~~~~~_ :u~~ ~~s~n~ ~~~~~ ______O~~c~I~~~a~a~o~s____ _
OI,.~ (\.~~:9 I ' , Preclsl.o~ gnnd,~g machl~es.
': Optical or magnetic scales
">~ 1> " l I
precision lapplng machlnes, electrical comparators
"1", I 1 : ' , (opticallens grinding machines)
~? X I: I Electronics comparators
"...
______ -Allowab~ ~__ ':'~I'_"2. ~~1~~ ___ :______ ~r:.c~.i~n_d~~o~~~~~ __ j~<3~a5.t~_._____ _
0.lpm.l0- 1
achi 'ng accurac y "'..... I 'O.051'm
-N-J
I (D.U.V. mask ahgner). laser measunnglnslruments
~rror~) (r) : . . . : (opticallens finish grinding machines). Optical fibers, Talysurts,
,-..-f-L---.j I :', 'precision diamond grindlOg Talyronds
I ' I " ..
(systematic I" mac h'Ines, uItrapreclslon
0.0Ipm.10 4 --: ~ errors «(A» --- -~N--
~ -'-'-~~':'O_I~~_g.!:.i~d~[~~c~i~~ -- --- - - - - -- - - - ------
.... a. I '0. 005 m I" (diHraction grating ruling engine)
p High precislon laser
I101:)
, ... 41 random errors «(.)
I
I I
--- I ,
,(electron beam hthographer)
. . •
measunng Instruments
:.8.~ / ' I " " Super high precision grindingmach. (Doppler,
I § :il . : I ',: ' super high precision lapping multi·reflection)
:z E Vartance (2<1) I I ' .... I and polishing machines Talysteps
O.OOI"m. 10-3
1nm. --, - - -;- --:0,0011';;,1:::::- ÄiOm,-mC1~cule-örion oeam -SCanning electrö'n" mi~oscopes,
" , .......... machlOlng. atom or. . transmission electron microscopes.
O.3nm ..... -;tIl • 'I =". - - - - , - - - - - - .1......
I' - - - - ........ -molecule de~sltlon
- _________ el e ctr on d'ff .
I rac t'loneqUlprnen. t
Average Dimension : I : .... , . ion analyzers.
(Atomic I Specified
dimension I I I (Substance syntheslzlOg) X.ray miero analyzers
lattice dirrynsion, , n I I I I •
distance) 1900 1920 1940 1960 1980 2000 year Auger analyzers, ESCAR
Realisation as an iodine-stabilised
10- 11 laser wavelength
arises over the subject of accuracy and repeatability, by the manufacturer of the instrument is not wise,
as they do not have the same origin; hence: without.ascertaining this fact for oneself. Returning
to the current theme of traceable measurement, if
• repeatability is a function of the instrument's the traceability chart illustrated in Figure 199 is
design; considered, the route from metrological and inspec-
• accuracy is a function of calibration. tion equipment in daily use, through the traceablity
chain to the primary standard of dimensional
For example, an instrument may repeat with great measurement, can be shown. In each case, as cali-
precision, but it is only by calibrating the equip- bration progresses toward the primary standard,
ment that we know whether to believe the results. more exacting measurements are made, thus
This seems an obvious point to make, but it is often ensuring that each piece of instrumentation in the
a widely misunderstood distinction that is very "chain" is calibrated to a high er order of accuracy
important whenever a new instrument is purchased. and precision. This process of calibration against
To take for granted the positional accuracies claimed known artefacts is both costly and, more important,
a time-consuming process, taking valuable and often proliferation an alternative option might be to
delicate instrumentation out of the metrological describe the surface by way of its Fourier compo-
chain, but is essential to ensure traceability. nents. Anyone familiar with the complex waveforms
Today, many of the primary standards are now existing in acoustics will be able to comprehend
"derived" and do not exist as discrete entities; this is Fourier concepts. For instance, a musical instru-
particularly true for many electrical and physical ment's range can be described by its relative prop-
standards. As a result of such "pseudo-standards", a erties at different frequeneies in a harmonie series,
move in recent years in the United Kingdom has in the same manner that areal surface is described
been an attempt to mitigate the losses in cost and in terms of a succession of sinusoidal corrugations,
time as essential calibration occurs, by employing each having particular frequeneies, amplitudes and
virtual gauging concepts, which have yet to be intro- phases. When a surface has a periodic profile, this
duced into conventional dimensional measure- can be described by sine waves of infinite series,
ments. By way of illustration of the potential for this whose actual periods are integral fractions of the
technique for dimensional measurement, that of an fundamental; alternatively, if periodieity is not
electrical calibration will be briefty reviewed. Here, represented on the surface, then all spatial frequen-
users obtain calibration through on-line Internet eies are probably present. If for simplieity, consider-
access to the National Physical Laboratory (NPL), by ation is given to the cross-section of a random
way of its appropriate website - via encrypted se cu- surface, two facts can be established; these are:
rity stages.1t is important that in order to gain access
to the calibration facilities the sensitive nature of the the surface can be represented by a graph of
data to the site must be secure. Once access has been height -versus-position;
confirmed, users then enter information such as the 2 another graph can be made to represent ampli-
type of equipment they wish to calibrate, together tude versus spatial frequency.
with the calibration kit and frequency ranges. This
data is transferred to the NPL, where it is sub se- The relationship between both graphs is in effect
quently evaluated and the correction values are a Fourier transform. To obtain a complete descrip-
displayed on the PC's screen. Thereafter, a need to tion of this arbitrary surface, consideration must
evaluate any imperfections that can arise via elec- be given to the relative phases of the individual com-
tronic noise and other outside approval by the user ponents. In effect this is the power spectrum, but
needs to be substantiated, with the values sent back as the power is proportional to the square of the
to the instrument, which will automatically calibrate amplitude it will not have any phase information.
itself. A major benefit in utilising the Fourier transform
Although Figure 199 shows the traceability route for surface description is that surface data can be
to be relatively straightforward, in reality the devel- simply extracted and as a consequence metrology
opment of the route to effieient calibration can equipment can be more easily assessed as the instru-
involve some quite complex practical problems and mental response function, or more notably on Sted-
philosophical interrelationships, as depicted in man diagrams, yet to be described.
schematic form in Figure 200. The traceable route from the concept of an ideal
sinusoidal surface to its practical realisation, and
from there to more complex surfaces to provide
Surface description standards against which to compare real surfaces of
functional performance, is depicted in Figure 200.
Any given surface can be described in a variety of Achieving this goal represents considerable seien-
ways (Figure 200), the most obvious being where the tific research in both fundamental and applied fields.
height of each data point is plotted in relation to a Even when much practical metrological work is
reference plane. For example, in two-dimensional undertaken, it cannot be guaranteed that it will be
sectioning this is what the surface texture instru- possible to accomplish instrumental calibration to
mentation would in the main be measuring. How- the level of accuracy one might expect, nor even that
ever, such information tends to be quite speeific and this accuracy will co in eide with the sensitivities of
relates to both the surface stylus probe interaction typical instruments. However, it should be possible
and the measuring conditions. These inspection to establish uncertainty levels and, in the majority of
parameters make it problematical to extract from instances, the causes of this uncertainty. Further, it
the surface the required information to enable com- cannot be certain that this exereise in establishing
parison of surfaces to each other. This problem has uncertainty will lead to improvements in measure-
led to roughness parameters considerably multiply- ment determination, but it enables the metrologist
ing in number, many with quite limited practical to obtain a clearer understanding of the present
applications. In order to minimise this parameter instrumentallimitations. The following section
Quality and calibration techniques
T'-><etJcaI 2 HarmorllC'
In>,runenl
Respons<>
Furocbon
NV\
iU
VVVVV
f\N\
WlII't!tenglh
~
'\IV\
~ A.f\.A
'3.
~ .~ .. I
Sloo; ~E~S I
Wavelenqlh
.
ModoH",'l
Expenmenl
Figure 200. Route towards absolute standards for measurement of surface texture. [(ourtesy of R.K. Leach & M.C Hutley/NPL.]
briefly describes how, and in what manner, the influ- has a measurable output and operating under a
ence of process capability on the production of stable set of conditions causing the output to vary
components by industry is affected by calibration about a central value in a predictable manner. Such
and recalibration of inspection equipment. Measure- an output is depicted in Figure 201, where the process
ment uncertainty will then be described and how it capability (Cp ) index is initially estimated at the
can be determined, enabling instruments, arte facts beginning of a batch run to have a value of <1.0.
and their users to establish the probable causes of Process capability is an extremely important meas-
metrological uncertainties. ure of production performance and can be simply
expressed in the following manner:
Gaussian distribution
Lower Higher
specification specification
limit limit
\\ \
\\
\\ \ \
Time
\\
\\ \
\
\
I ,
I ~>U I
~-----~
Figure 201. The process capability (9 index may change with time.
(a) Manufacturing process mean may change with a systematic error present
TIME
-<:::JI-----
Drift in the process (i.e., systematic error present) .A-"""".."....,~
Scrap
Recalibration
required
Drawing tolerance
TIME
4
(b) Variable manufacturing output Variable output
resulting from changes in the
process capability index
Scrap Scrap
_=::s:s5~~~~~~~~~w.::;~~:o::.- Cp =0.75
Recalibration
required
...::::::J-*",=i~"'>u''>'''>'~''':'':~'":'-'~~-::::-H~ Cp = 1.33
Drawing tolerance
Figure 202. Illustration showing how (al the manufacturing process mean changes with time; (bl process capability index changes with time;
or how both can change with time.
fication limit (tolerance) and 0" is the standard has the output situated at the me an, but with time
deviation for the process. the variability has increased from an initial level of
In this case the Gaussian (normal) distribution Cp 1.33 to an intermediate value of Cp 1.0, where cali-
from the output at the beginning of the pro duc- bration is necessary. Finally, toward the end of the
tion run is centred on the me an value (x bar) and run, an undesirable situation occurs at a Cp value of
fills the complete statistical band (60").As the process 0.75, where scrap will be present.
continues to produce components the output is still If some form of in-process gauging and associ-
centred on the mean, but the spread (variability) has ated traceable calibration procedure had been
increased considerably with respect to time. Here is introduced to limit the "process drift" or variability
an undesirable situation as the process capability in output (or indeed both), then scrap parts are
has decreased to a value of Cp 0.8; this will inevitably unlikely to be present in a batch production run.
introduce scrap into the process. Some reworking What has been said here for the control of produc-
may be possible for certain parts outside one limit, tion processes is equally true for the calibration of
depending upon whether this is a non-critical im- general metrology equipment, through acceptance
posed limit in the process. However, the process of the fact that uncertainty will arise in any produc-
capability has highlighted the fact that in this case tion or metrological process requiring appropriate
there is an unacceptable variability occurring that action to minimise these effects.
needs drastic action if most of the production run
is not to be lost. What was unusual about the pro-
duction output in Figure 201 was the fact that the
mean value had not changed, but the variability had 6.4 Measurement uncertainty
increased. In the case of Figure 202(a) the mean
value has changed with respect to time - it has intro-
duced some "drift" as a systematic error in the Geometrical product specification (GPSj
production output has proportionally increased.
This drift has caused the process capability to The GPS procedure enables the designer to define
change from an initial value of Cp 1.33, being well in the geometrie shape, dimensions and surface char-
control, to an intermediate value of Cp 1.1, indicating acteristics of a component in a way that ensures
that calibration was required before this point had optimum functioning of that workpiece. The proce-
been reached in the production run, as some scrap dure normally adopted includes adefinition of the
is now inevitably being produced. The situation is optimum value and its dispersion for its intended
exacerbated with time until a Cp 0.90 production function, enabling it still to be satisfactory. The
output occurs, indicating the whole process is out production process will in many circumstances
of control, because of this tendency to drift. In the produce parts that are not perfeet, in that they may
case of Figure 202(b) once again the production run demonstrate some form of deviation from a defined
FUNCTION
COMPARISON
[Designer)
Specification Measured
(Drawing) Values
[Industrial
Engineer)
Extracted
Data/Signal
Figure 203. The basic geometrical product specification (GPS) framework: a new approach.
Quality and calibration techniques
optimum. If a eomparison is undertaken between and the associated geometrie toleranees are defined.
the eomponent and its specifieation (Figure 203), it In box 1 the eodifieation of the geometrie toleranee
requires the following to be eonsidered: that the symbol for straightness with its associated toleranee
workpieee (BS 8888: 2000): is depieted. Box 2 indieates the definition of this
straightness toleranee and box 3 is the specifieation
• is eoneeived by the designer; operator, indieating the manner in whieh this
• is as manufaetured; straightness deviation may appear within the toler-
• is as measured. anee. Box 4 illustrates the anticipated uneertainty
associated with the upper and lower toleranee limits;
The standards introdueed in the GPS field more will be said on this subject later when
provide the fundamental rules for geometrieal speei- diseussing Figure 206. Boxes 5, 6 and 7 illustrate the
fieation, such as the basic definition, symbolic repre- metrologieal assessment of the real surface and the
sentation and measurement principles (see ISO metrology instruments with their antieipated eali-
TR 14638 for an overview of these eoneepts). Several bration requirements. In this visual manner these
eategories of the standard are eoneerned with boxes depiet the eomplete geometrie produet speci-
eoneepts, dealing with fundamental rules of specifi- fieation ehain, this being presented in a logieal and
eation, others provide global principles and defini- praetieal approach to the topie.
tions, or various geometrie eharaeteristies, the In the GPS philosophy the specifieation and
latter including workpieee eharaeteristies relating verifieation operators are slightly more complex than
to differing production processes, together with first appearanees would seem to indieate, as illus-
specifie maehine elements, as shown in Table 19. GPS trated in the fiow diagram in Figure 205. The linking
prineiples are neeessary throughout a produet's of design intent and metrology is the objeetive here
development: design, manufaeturing, metrology and - the duality principle, with geometrie features
quality assurance. oeeurring aeross three disciplines. These are:
In Figure 204 one of the "ehains of standards" is
depicted, illustrating a typical eomposition of a specijication - this is where the designer eon-
funetional performance standard, such as the eeives several representations of the workpieee;
geometrie toleranee for straightness. In boxes 1, 2 2 workpiece - as it would appear in the physieal
and 3 are shown the manner in whieh straightness world;
3 4 5 6 7
1 2
Comparison Measurement
Codification Definition Specification Verification Calibration
with tolerance equipment
on a drawing of tolerance Operator Operator requirements
limits requirements
I-I I ~ t------>- m m
0.1 ~ I
UU
1
I I I
UU
I
I I
es:- )L ~
Figure 204. The (hain of standards, e.g. straightness.
3 inspection - where a given workpiece repre- width of the margin - its interval - the second is the
sentation is created by sampling of the part by confidence level; this latter value states how sure one
measuring instruments. is that the actual value oceurs within this margin.
Typically, a stylus length might be 100 mm plus, or
To comprehend the nature of the relationship minus 0.5 mm at the 95% confidence level. This
between these three disciplines is of great impor- uncertainty could be expressed as follows:
tance and Figure 205 depicts the parallel or
"mirror" activities that connect those between the Stylus length = 100 mm ± 0.5 mm,
design intent and metrology. The design intent will
result in specification characteristics - the concep- at a level of confidence of 95%.
tual perfect operator - with the metrology creating In reality what this statement is implying to a
the evaluation of characteristics - the actual oper- metrologist is that they are 95% sure that the stylus
ator. These "operators" can then be compared length williie between 99.5 mm and 100.5 mm in
with each other for comformity, as indicted in length. In this discussion it is essential not to confuse
Figure 205. the term uncertainty with error. They can be
Some of the key questions raised today by the distinetly dassified thus:
manufacture of parts to tighter tolerances are:
• errar - the difference between the measured value
• "What is the best manner to interpret metrology and the "true value" of the item being inspeeted;
data, whenever there is a measurement uncer- • uncertainty - the quantification of the doubt
tainty factor in a tolerance band?" existing with regard to the result of this measure-
• "How to standardise on tolerances across the ment.
design, production and inspection functions, so
that measurement uncertainty is accounted for In most situations one tries to correct for any
throughout the creative procedure in the prod- known errors; this is attempted by the application of
uct's design and build life eyde?" corrections from certificates of calibration, although
any error occurring that is not known will be a
The term uncertainty has been mentioned here source of uncertainty. The estimation of measure-
on numerous occasions and this will be the main me nt uncertainty is important because precise and
theme from now on in this section. accurate quality measurements enable the metrolo-
gist to comprehend the results without ambiguity.
However, the expression of the measurement uncer-
Uncertainty issues tainty is significant when taking any form of
measurements, because they may be part of:
The question often asked in calibration-related
tasks, is: "What is measurement uneertainty?" • calibration - where measurement uneertainty
Uncertainty of measurement refers to the doubt must be reported on appropriate certification;
that exists about any measurement; there occurs a • test - if measurement uncertainty is required to
margin of doubt for every measurement. This establish either a "pass" or "fail" condition.
expression of measurement uncertainty raises other
questions: "How large is the margin?" and "How bad Alternatively, information on measurement uncer-
is the doubt?" Henee, in order to quantify uncer- tainty is vital to hold a:
tainty two numbers are required, one being the
SPECIFICATION VERIFICATION
OPERATOR: OPERATOR:
OPERATION OPERATION
Collection - Collection
- Construction - Construction
Characteristics Characteristics
spccification evaluation
Comparison ~
for conformance
Figure 205. The "duality principle": the link between design intent and metrology [BS 8888: 2000.]
• tolerance - where the uncertainty had been control has been established, statistical measures are
previously established, prior to deciding whether adopted. If the metrological process is not inftu-
the tolerance is met (see Figure 206). enced by systematic or random errors, then the
process is said to be behaving "normally" and any
Otherwise one might need to read and under- process output data is valid. Two statistically derived
stand the calibration certificate or written specifica- mathematical expressions are needed to define
tion for a particular testlmeasurement. It is worth whether a process is behaving correctly: these are
noting, that a measurement is not traceable unless the arithmetic mean and its accompanying standard
quoted wiith an uncertainty. deviation. Normally, the arithmetic mean is conve-
niently shortened to mean, this being denoted by the
symbol x (termed "x-bar"). This x value is the mean
Statistical measures of all the values of x and can be derived from the
following expression:
In order to evaluate the test data from an inspection
procedure, to determine whether adequate process
Lower Upper
Specification Specification
Limit: Limit:
I
Specification Zone
[OUTof [OUTof
[IN specification] specification]
specification]
DESIGN/SPECIFICATION
PHASE
VERIFICATlON
PHASE
U U U U
Non-conformance Non-conformance
Uncertainty Conformance Zone Uncertainty Zone
Zone
Figure 206. Comparison of the measurement value with its associated tolerance.
i~l
Xi of the uncertainty of these measurements. Moreover,
knowing how large this spread is enables one to form
where X = arithmetic mean, ~X= sum of X and n = an opinion as to the quality of the inspection pro ce-
number of readings. dure or g.roup of measured data. The customary way
NB Sometimes several readings are taken, which to quanhfy the spread is by utilising the standard
modifies the calculation to deviation - often described by the Greek lower case
letter (J" (sigma). Usually only a moderate number of
measured data is obtained and, in this case, an esti-
mate of the standard deviation can be derived which
is denoted by the letter s, meaning the estimated
where ~fx = the sum of the frequencies of x. standard deviation. In principle the calculation of s
For example in roundness measurement, if 10 for the previous series of LSC roundness polar plots
LSC roundness polar plots were obtained in the would be
course of an inspection procedure - 17, 18,22, 18, 18,
17 + 18 + 22 + 18 + 18 + 19 + 21 + 19 + 18 + 20
19,21,19,18 and 20 /-Lm respectively, then the value x (/-Lm) = 19 (mean)
would be
The next step from the calculated mean is to find the
~x = 17 + 18, + 22 + 18 + 18 + 19 + 21 + 19 + 18 difference between each successive readingj this is
+ 20 (/-Lm) obtained in the following manner (by making the
= 190/-Lm mean LSC value of 19 /-Lm equate to zero):
Therefore -2 - 1 + 3 - 1 - 10 + 20 - 1 + 1
Harmonics/Filtering
Definition of measurement Reconstruction - component geometry
Probe/Stylus type
StyluslProbe error correction
Reference Artefacts
Location and plane
Probe/Stylus lenglh
Deformation compensation
Sampling rale
CUI-off/window
Temperature compensation
Datum sclection Correction - geometrie imperfection
Sampling algorilhm
Calibralion proeedure
Skid/Skidless operalion
----- --------
Figure 207. "Cause-and-effect" (6M) categorisation for measurement uncertainty - generalised causation - in surface texture and roundness instruments. [Adapted fram Stout, et al.l
Quality and calibration techniques
• imported uncertainties - any metrological instru- Table 20. Determination of measurement uncertainty
ment has its own uncertainty and this affects the
subsequent measurements taken; Step Procedure
NB If an instrument has not been previously cali- Decide what you need to find out from your
brated, then in this condition it will exacerbate any measurements. Decide wh at actual measurements and
future measurements taken. calculations are needed to produce the final result
2 Carry out the measurement needed
• operator skill - occasionally certain measure-
ments rely on the operator's skill and judgement, 3 Estimate the uncertainty of each input quantity that feeds
into the final result. Express all uncertainties in similar
with some operators being more efficient and
terms (see following text)
reliable than others; for example, when timing a
trial with a stop watch the level of uncertainty 4 Decide whether the errors of the input quantities are
depends upon the operator re action time; independent of each other, but if not then additional
calculations/information is required
• sampling concerns - any measurements obtained
must be representative of the process being 5 Caiculate the result of your measurement and include
assessed. known corrections from previous calibration, ete.
6' Find the combined standard uncertaintyfrom each
NB As examples of these sampling issues, any individual aspect
temperature measurement should be assessed dose
to the item being monitored and not away from its 7' Expressing uncertainty in terms of coverage factor,
together with a size of uncertainty interval and, state
local thermal environment. When selecting sampies confidence level
from the production line, ensure that they do not
originate in the initial "start-up" batch run, nor that S' Write down the measurement result and its uncertainty,
they are obtained from a mixed stillage from two stating how both were obtained
separate production processes.
a To be discussed later in more detail in this section.
• Metrological environment - the measuring instru- Source: Beginner's G.U.M. Bell/NPL, 2000.
ment can be significantly influenced by either the
component being measured or variations in tem-
perature, humidity, air pressure, possible vibra-
tional effects and many more conditions.
• Type B evaluations - uncertainty estimates
NB The overall measurement uncertainty will be obtained from any other relevant information,
affected by the individual uncertainties, and where such as from calibration certificates, manufac-
the error is known - that is, from a calibration turers' specifications, published information, past
certificate - a correction can be applied to the result experience or just common sense.
of this measurement.
NB It is tempting to think that Type A uncertainties
occur by random processes and Type B uncertain-
Calculation of measurement uncertainty ties result from systematic factors, but this logic is
somewhat questionable.
Prior to the calculation of measurement uncertainty, Table 20 attempts to illustrate how to use infor-
initially the sources of uncertainties need to be mation from both Type A and Type B evaluations for
identified. Once this task has been performed then an overall estimate of uncertainty.
an estimate of the size of the uncertainty from Any contributions to uncertainty must be ex-
each source must be established. Lastly, each of the pressed in the same units before they are combined,
individual and contributory uncertainties is then furthermore having matching levels of confidence.
combined to produce an overall figure for the whole The contributing uncertainties and their respective
uncertainty. There are two methods used to estimate confidence levels need to be uniform and this allows
uncertainties: these are termed either Type A or Type them to then be converted into standard uncertain-
B evaluations, and in many instances uncertainty ties. Plus or minus one standard deviation is the
evaluations of both types are required, their identi- margin for a standard uncertainty; moreover it also
fication being according to the following: gives information on the uncertainty of an average
and not just the spread of these values. It is normal
• Type A evaluations - estimates of uncertainty by to quote standard uncertainty using the symbol u,
statistical techniques, normally from repeated or as u(y), this latter term being the standard uncer-
readings; tainty in y.
"Type Aevaluation": standard Addition and subtraction: summation in
uncertainty calculation quadrature
Once aseries of measurement readings has been The most elementary case for this technique is
x
obtained for a "Type A evaluation", the (mean) where the sum of aseries of measured values - by
value and s (estimated standard deviation) can be either addition and subtraction - is calculated. By
calculated. From this set of readings the estimated way of illustration of the summation by quadrature
standard uncertainty u of the mean can be calcu- method, if it is required to determine the total height
lated from the following: of a group of "wrung-together" gauge blocks of
differing individual sizes, then the standard uncer-
u = s/--Jn tainty of each gauge block could be represented by
the notation a, b, c, etc. The known (measured)
where n = number of measurements taken. values are then found by the combined standard
uncertainty technique, by squaring the individual
uncertainties, adding them together, then taking the
square root of the total, as follows:
"Type 8 evaluation": standard
uncertainty calculation Combined standard uncertainty
V2
P=-
R NB A specific value of the coverage factor (k) will
introduce a particular confidence level for the
expanded uncertainty.
In this case the relative uncertainty u(P)IP in the In particular, if the overall uncertainty is scaled
value of power would be given by by utilising a coverage factor k = 2 to obtain an
approximate level of confidence of 95%, the k = 2
u(P) value is acceptable when the combined standard
P uncertainty tends to be normally distributed. Some
typical coverage factors for normal distributions are
In general, in any multi-step calculations the
procedure for combining standard uncertainties
k = 1 for a confidence level of around 68%;
k = 2.58 for a confidence level of around 99%;
in quadrature can be achieved in multiple steps,
utilising the relevant form for addition, multiplica-
k = 3 for a confidence level of around 99.7%.
tion, ete., at each step. For complicated formulae the Other less popular distribution shapes have a
combination of standard uncertainties is more com- different range of coverage factors. Alternatively,
prehensively discussed elsewhere (e.g., the UKAS whenever an expanded uncertainty is quoted, the
Publication M 3003). standard uncertainty can be found by reversing the
process, namely dividing this uncertainty by an
appropriate coverage factor. On calibration certifi-
Correlation cates the quoted expanded uncertainty, if expressed
properly, can be "interrogated" to obtain the
The equations required to calculate the combined required standard uncertainties.
standard uncertainties above are only valid if the When expressing the measurement uncertainty,
input values for standard uncertainties are not inter- it should be exacting in its definition, allowing no
related or correlated. Correlation refers to the ques- misinterpretation. To achieve accurate uncertainty
tion of whether all the uncertainty contributions are definitions, several important factors need to be
independent. Namely, could a large error in one mentioned:
input measurement cause a similar sizeable error
in another? Further, might some outside environ- • measurement result and uncertainty figure - an
mental inftuence such as temperature create a arte fact was 300 mm ± 1 mm;
similar effect simultaneously on several aspects of • coverage factor and confidence level - recom-
uncertainty, which are either easily established or mended wording to minimise confusion is: "The
require further investigation by to the metrologist? reported uncertainty is based on a standard
In many instances these individual errors are uncertainty multiplied by a coverage factor k = 2,
independent, but where they are not additional providing a level of confidence of approximately
calculations are required. 95%";
• description of how uncertainty was estimated -
reference to the appropriate documentation.
Coverage factor k
In the previous discussion on uncertainty the
components were invariably scaled to obtain the Analysis of uncertainty: Huncertainty
combined standard uncertainty. This result of the budgets"
calculations for combined standard uncertainty may
be thought of as equivalent to "one standard devia- To facilitate the process of calculating uncertainty, it
tion", but it may be necessary to obtain the overall is often helpful to summarise the uncertainty
uncertainty expressed in terms of a different level of analysis - uncertainty budget - in a spreadsheet, as
confidence, typically the 95% limit. Such rescaling indicated in Table 21.
InClustrial metrology . .
Another approach, which is similar in concept to measurement uncertainty is small when compared to,
that depicted in Table 21, is to establish the applica- say, the inspected diametral tolerance, then the
tion of uncertainty budgets using spreadsheets, as metrology equipment can be used with confidence for
depicted in Table 22. Assuming that the input quan- the stated inspection procedure. In the case cited
tities have been set, the next procedure is to calculate above for the uncertainty budget (Table 22) for the
the variation limits (Xi estimates), uncertainty con- metrology instrument, the analysis illustrates that
tributions, and then to set up an uncertainty budget. around 50% of this "budget" is accounted for by tem-
This can be achieved in several steps, as follows: perature factors alone. Because of the large impact
that temperature influences have on the measurement
• calculation of estimates - based, in this case, on uncertainty for any measurements on the shop floor,
ambient conditions, materiallproduct specifica- they must be "corrected back" to 20°e. However, cor-
tions and possible variation limits that are calcu- recting for temperature within the production shop
lated for each input quantity; may lead to unforeseen practical problems being
• application of distribution factor - type of distri- encountered. The temperature on the shop floor could
bution is selected (depending on the probability vary during the working day as dimensional mea-
that the result lies within the prescribed limits) surements occur. The recorded thermal history may
for a rectangular distribution (100%) or normal also not be correct during this time, because any ther-
distribution (99.73%). mometer readings may not be accurate, or even some
NB As an alternative to complex calculations, the uncertainty may exist concerning the actual value for
following correction factors can be used: the coefficient of linear expansion for the workpiece
• rectangular distribution: multiply the limit by material, which leads to dubious inspection pro-
0.7; cedures. These uncontrolled factors of inadequate
• normal distribution (3s): multiply the limit by temperature correction mean that more generous
0.5. limits are necessary to take into account the variabil-
Owing to the fact that in Table 22 there is no corre- ity introduced because of such temperature influ-
lation between the uncertainty components, the com- ences. Here, the most obvious way to mitigate the lack
bined standard uncertainty is expressed in the form of temperature control and its adverse effect on the
of a standard deviation. In this case, the combined measurement uncertainty is to undertake final
uncertainty (UJ, which was established at 2.29 j.Lm, inspection in a temperature-controlled environment
will need to be multiplied by a coverage factor of k = that is as dose as practicable to that of 20°e.
2, to ensure a 95% probabilitythat the measured result Thermal-induced measurement uncertainties
willlie within the uncertainty band. The metrology during metrological inspection, notably the coeffi-
instrument in this case, which had a manufacturer's cient of linear expansion workpiece issues, become
stated specified accuracy of 2 j.Lm, here had a mea- critical factors at the highest levels of accuracy. In
surement uncertainty of 4.58 j.Lm when used to calibration laboratories where thermal influences
inspect shafts under workshop conditions. In any must be adequately controlled in order to minimise
uncertainty budget calculations the objective is to temperature-induced errors into measurement, the
ascertain whether the measured result will be ade- three greatest single contributors in uncertainty
quate for its intended purpose. For example, if the components are:
Repeatability A 1.00
Variation of zero A 1.00
Indication error B 1.00 0.6 0.60
Flatness B 0.60 0.5 0.30
Straightness B 0.60 0.5 0.30
Parallelism B 1.00 0.5 0.50
Ambient tempo B 0.30 0.7 0.21
Temperature diff. B 1.40 0.7 0.98
Comp. form error B 2.00 0.6 1.20
Combined uncertainty U, 2.29
Expanded uncertainty U= 2x U, 4.58
Where
calibration of material thermometers - ensuring demands are for this specification. By way of illustra-
that these instruments (various types of temper- tion, sometimes a specification may incorporate
ature measurement devices) are thermally error- factors such as "attributes" (non-measurable enti-
mapped; ties) - visible appearance, interchangeability, electri-
2 actual workpiece temperature is established - as cal connectivity, etc. - which have no actual bearing
this will have a large influence on the coefficient on the measurements previously taken, but can
of linear expansion (which must also be known); impinge on the whole uncertainty problem.
3 air temperature reading errors must be known -
due to air convection currents (lamellar air flowl
air turbulence/hot -, or cold-spots within the Reducing measurement uncertainty
room, etc).
It is essential to remember that it is just as important
Other environmental factors such as humidity and to attempt to minimise uncertainties as it is to quan-
air pressure can also have a significant influence on tify them. Good working practices will help to
the measurement uncertainty, particularly if the reduce these measurement uncertainties, which
light path of laser-based equipment is employed in might include the following:
the calibration/measurement procedure.
In the previous tabulation and discussion of mea- • calibration of instruments (or have them cali-
sure me nt uncertainty, it was important that the brated bya third party) - then applythose calibra-
correct conclusions were drawn from these results, tion corrections which appear on the certificate;
which is of great significance when deciding if the • compensating for any corrections - make adjust-
values fall within, on or outside the specification ments for any other significantly known errors;
limit. If both the result and its accompanying meas- • ensuring measurements are traceable to national
urement uncertainty fall inside the specification standards - employing calibrations that offer
limits, then the process can be deemed to be com- traceability via an unbroken chain of measure-
pliant, in that the operation will be capable of sus- ments to the relevant standard (see Figure 199);
taining efficient measurement and process control. • selecting the optimum metrology equipment -
For non-compliance to occur, neither the result nor normally they would encompass a calibration
any part of the uncertainty band will fall within the facility with minimum uncertainty of measure-
specified limits. In cases where neither the result nor ment;
part of the uncertainty band is either completely • repeating and checking measurements - occa-
inside or outside the limits, then a dilemma occurs, sionally allow someone other than the usual
as no firm conclusion about the compliance state can inspector to repeat these readings, or utilise a
be made. Prior to stating the compliance with a spec- different method of assessment to ensure validity
ification, it is always advisable to check what the of the results;
• checking calculations and transcription of results artefacts. Due to the fact that most surface texture
- ensuring that results are substantiated and are measuring instruments have a wide range of operat-
correctly written; ing conditions and usage, the net result is that more
• utilising uncertainty budgets - the "budget" will than one type of artefact has been developed to cater
identify where the most significant uncertainties for these demands. The current standard relating to
occur, so that they can be minimised; surface texture calibration (ISO 5436-1: 2000) con-
• awareness of problems in "calibration chains" - at siders five general cases of artefact having several
every step in the chain, uncertainty can increase. versions of each type - the first four initially being
discussed below. A general consideration for any
NB Surface texture measuring instrument un- instrument calibration is that its profile should cor-
certainties covered in the Measurement Good res pond to the surface that is to be measured. In more
Practice Guide no. 37 by the NPL (Chapter 8) - see general terms, these arte facts fulfil the following
References. assessment criteria, namely, Type A calibration stan-
Utilise good working practices in measurements, dards will assess the instrument's vertical magnifica-
such as by following equipment manufacturers' tion factor, but do not give information with regard
instructions operated by using experienced and rele- to instrument calibration in the scanning axis; this
vantly trained personnei; checking and validating latter point of scanning is dealt with by the Type C
software (if employed) to ensure it operates satisfac- artefact. Furthermore, it is important to check the
torily; ensuring that any calculations in the "round- instrument's overall calibration and that the Type D
ing" of measurement values is correct, ensuring that artefact has been produced to assess the ability to
good records ofboth measurements and calculations measure and calculate a surface texture parameter.
are produced at the time of metrological inspection. Finally, the Type Bartefact checks and ensures that
Lastly, keep a written account of any other relevant the selected stylus performs to specification. In order
additional information, as this may be useful if at a to determine whether any surface texture instrument
later stage these results are ever called into doubt. performs adequately, at least four previously cali-
Extra factors need to be considered in any deal- brated and traceable types of artefact need to be
ings with uncertainty issues, particularly if they have available for this task. Hence, these Type A-to-E sec-
any one or a combination of those listed below: ondary calibration standards need to have the rele-
vant current calibration certification to a known
• when using statistics for very small data sets - standard. Such secondary artefact calibration can be
normally considered to be less than about 10; achieved by several means, either using interferome-
• if one uncertainty component is considerably try or by an alternative stylus instrument, which
larger than all the others involved in the "uncer- itself has been calibrated to a traceable standard in
tainty budget"; an "unbroken and documented chain of calibration"
• if just some inputs to the uncertainty calculation to the primary standard (Figure 199), this traceabil-
are correlated; ity being a major requirement of ISO 9000: 2000.
• when the distribution or spread has an unusual These surface texture calibration artefacts have a
shape namely, that it is not "normally distributed"; restricted range, relating to their own individual
• if the uncertainty has been obtained for other characteristics and to those of the instrument to be
than a single result, that is, by fitting a curve or calibrated, as listed in Table 23.
line to a number of points to obtain the required Each type of surface texture artefact will now be
information. briefly reviewed.
The calibration of surface texture instruments prin- The first artefact illustrated in this subgroup is Type
cipally relies on the use of secondary calibration Al (Figure 208a), featuring a wide calibrated groove
Quality and calibration techniques
Table 23. Surface texture artefact types, description and be assessed perpendiculady from the upper mean
applications line to the mid-point of the lower mean line. A
significant number, not less than five, of evenly
Type Artefact description Application: distributed traces shall be taken.
A Depth measurement Calibration of the vertical
profile - having a known Type A2: wide grooves with rounded bottoms (Figure
depth with wide grooves
208c)
B Tip condition Ca libration of the stylus tip
measurement condition - having various
Here (Figure 208c) the surface texture depth stan-
depths and widths and
narrow grooves
dard is comparable to Type Al, with the obvious
difference in their visual appearance being the
C Spacing measurement Calibration of vertical profile
rounded groove, rather than flat bottomed. The
- under certain conditions
artefact can also be utilised radius must be sufficiently large enough to be insen-
calibrating horizontal profiles sitive to either the shape or condition of the stylus
tip, or both. Once again, a significant number of
D Roughness Overall calibration of these
measurement instruments surface traces is demanded - at least five - which are
taken across the arte fact and these are distributed
E Profile coordinate Calibration of instrument - for
measurement its profile coordinate system
evenly over the measuring window.
3w
Figure 208. Depth measurement standards (Type Al and tip condition measurement standards (Type B). [Source: ISO: 5436-1: 2000.1
\ 3 r =stylus path
2
Key:
Figure 209. Calibration artefact Type 83. [Source: ISO 5436-1: 2000.]
Type B3 (Figure 209) instruments. The Type B3 arte fact has a sharp razor
bl ade, but even here a finite radius appears at the
The artefact shown here represents a knife edge artefact's edge, as shown by the magnified view in
having a fine protruding edge, the radius and apex Figure 209.
angle of which is shown, being both smaller and
narrower than that of the stylus under test. The
condition of the stylus can be established by
traversing the stylus over the arte fact and recording Spacing measurement artefacts
the surface profile, as schematically depicted in the (Figure 21 Oa-d)
main diagram. This type of stylus calibration tech-
nique can only be employed with low traversing Artefacts of this type of design are mainly used to
speeds and for direct surface texture profiling calibrate vertical profile components; however, an
(a) Type Cl calibration artefact
r
Psm
l
-~.
Figure 210. Calibration artefacts for spacing measurement. [Source: ISO 5436-1: 2000.]
alternative application for them is to calibrate these parameters were selected to ensure that the
the horizontal features based on the condition attenuation by either the stylus or filter is negligible.
that the groove spacing will be maintained within As previously mentioned, a significant number of
acceptable limits of tolerance for this purpose. traces are advisable, the minimum number being 12,
With spacing measurement artefacts, the grooves which are evenly distributed across the measure-
must be both consistent and repetitive and would ment window. This assessment strategy allows the
normally come in a variety of profile shapes (Figure parameters to be calculated according to the appro-
210a-d). priate ISO standard.
The Type Cl artefact has sine wave profile grooves This Type C2 arte fact has regularly spaced grooves
that are characterised by Rsm and Ra. The values for based on the profile of an isosceles triangle, enabling
both Rsm and Ra parameters to be assessed. The
(a) Type Dl calibration artefact, undirectional irregular
groove profile geometry values selected here are profile
such that negligible attenuation occurs by either the
stylus or filter. Once again, a significant number of
traces are required, the minimum being 12, these
being evenly dispersed over the measurement
window. The surface texture parameters are calcu-
lated according to the relevant ISO standard.
Type D2 - circular ir regular profile (Figure 21lb) Profile coordinate measurement artefact
The Type D2 artefact (Figure 211 b) is characterised (Figures 272 and 2 73)
by Ra and Rz having irregular profiles repeated
every SAc in the radial direction. The profile shape Type Ei (Figure 212)
is constant normal to the measuring direction of the
artefact, in the circumferential direction. At least 12 This Type EI artefact measurement standard is char-
traces are required that are evenly distributed over acterised by radius and Pt. The radius of the sphere,
the measuring window and, as before, the parame- or hemisphere as depicted in this instance, should
ters should be calculated according to the appro- be sufficient to allow the stylus tip to remain in
priate ISO standard. contact with the convex surface profile and not foul
on the stylus's stern during its measurement travel.
Prior to calibration assessment the stylus tip should
be positioned symmetrically either side of the
highest point of the intended trace.
Hemisphere
Range
r/
of Stylus Length
gauge
eosin, OIT.,
I -Lcorrected
-r- - - - - ---
------
----------- --
---- - ~
Known hemisphere
(e.g.,UKAS)
Radius change
of stylus - if
damaged
Figure 212. Type E1 profile coordinate measurement artefact for gauge and stylus calibration using a "qualified" hemisphere. ((ourtesy of
Taylor Hobson/ISO 5436-1: 2000)
Quality and calibration techniques
Prism
Figure 214. Photomicrograph taken on an electron microscope of a Figure 21 S. SEM photomicrograph illustrating catastrophic damage
conical diamond stylus with a radius tip of 5 fLm. [(ourtesy of to the tip of a stylus. [(ourtesy of Hommelwerke, GmbH.]
Hommelwerke GmbH.]
of styli is depicted in Figures 214 and 215, respec- avoid the potential "worst case" situation that is
tively. In Figure 214 the tip is in excellent condition shown in Figure 216, where contact could be made
and the 5 f.Lm tip radius is intact. Conversely, in along the stylus flank, rather than at the tip. The tip
Figure 215 the tip has suffered catastrophic damage, damage as shown in the lower diagram in Figure 216
through misuse or perhaps because of inappropriate will not fully enter the valley and will foreshorten the
protection -left unprotected without the skid and its peak height as it traverses across the surface, leading
accompanying cover - resulting in a potential condi- to a lower recorded Ra reading under this condition.
tion for accidental damage. The uninformed user This unintentional error in the required surface
may not have noticed this damage, which may not be texture parameter could have major repercussions in
visually apparent until high optical magnification is service, or at best will allow substandard/scrap parts
employed. Therefore with the stylus tip in this poor to enter the supply chain. Clearly, there is a require-
state, the operator is currently unaware that false me nt to prevent these unanticipated and undesirable
readings are being introduced into the measurement measurement/quality problems from occurring;
cyde. This stylus tip condition (Figure 215) is dearly with systematic and regular calibration their likeli-
unacceptable, which is why it is important to hood is significantly diminished.
periodically check - via calibration artefacts - that
the tip is in perfeet condition. This calibration pro-
cedure should, as aminimum, be undertaken at least
once per day. Ideally, calibration needs to be part of 6.6 Calibration: roundness
the measurement strategy and its frequency adjusted
according to:
Roundness-testing instruments are generally of two
• conditions of inspection frequency - many read- basic configurations, as depicted in Figure 112.
ings and components to be assessed, necessitates Instrument calibration consists of some general
more frequent calibration routines to be under- testing procedures and the use of several artefacts to
taken; assess the equipment's capabilitity. The types of
• critical nature of these components - high accu- testing regime to be undertaken might normally
racy, more calibration and vice versa; indude the following:
• other unusual metrological conditions - which
might degrade the stylus performance during the • spindie - checking with a previously calibrated
measurement routine. glass sphere or hemisphere;
The ramifications of a damaged stylus on the • stylus deflection - using an appropriate set of cali-
recorded surface texture result can be gleaned from brated gauge blocks, or utilising the so-called
the schematic diagrams shown in Figure 216. Here, "flick-standard";
both aperfect and damaged stylus is illustrated • stylus-to-component alignment - using the "crest-
traversing across a calibrated surface. In reality, ing standard";
this standard should have a wider induded angle • column straightness - employing a calibrated
between the peaks (see Type B2, Figure 208d) to cylindrical square;
90° conical
stylus Stylus displacement Recorded Ra
Point of
motion
ofstylus
Recorded Ra
with fractured
stylus
90° calibrated
Standard
--~
,....---- ---
Ra - Standard->!_ _ __
Figure 216. Effeet that a damaged/worn stylus plays in influeneing the Ra value from the ealibrated standard.
• column squareness - utilising the same calibrated • variability in the user's interpolation of trace
cylindrical square. position on polar graph (for manual "fitting"
techniques only).
NB In the case of the latter two column checks, these
are only undertaken if the instrument has an appro- NB This latter uncertainty is a human-induced
priate alignment column. error and is not strictly speaking an instrument cali-
Some of the known sources of uncertainty in bration error.
roundness measurement are the result of the
following factors:
• horizontal and vertical fluctuations of the instru- Spheres and hemispheres: spin die
ment's spindle path from one trace to the next; assessment
• variability due to stylus type and its length;
• general misalignments in the stylus column to A hemisphere can be employed to check the round-
that of the spindle axis; ness measuring instrument in one of three ways,
• non-uniformity of recorded displayed profile; these are:
InClustrial metrology , .
(i) Verification - a previously calibrated hemisphere made to coincide with a similar mark on the machine,
is measured on the instrument being tested. If the equating to both their datum (zero) positions. On
differences fall within the limits, then the instrument sophisticated instruments, this known error at specific
is accepatable for further use; angular orientations means that a software correction
NB Prior to such calibration work, the instrument can be applied to minimise such errors. Spheres and
must have previously been calibrated for gain by hemispheres used to assess the performance of round-
using a "flick-standard" - see following pages. ness measuring instruments, are usually round to bet-
ter than 250 nm and have a calibration unccertainty of
(ii) Secondary calibration - a previously calibrated ±10 nm. To achieve sphere calibration, a special preci-
hemisphere is measured on the instrument being sion indexing fixture has to be manufactured (Figure
tested. The result from the instrument is compared 217; see the appendix for a schematic view).A displayed
to the known result. These differences are stored in profile is made with the spherical artefact in this posi-
the instrument and are used to correct subsequent tion averaged over four complete revolutions), then via
measurements (software correction); the indexing fixture it is indexed clockwise by 360/n
NB The instrument must have previously been cali- (where n in this case is 10). Once again, four artefact
brated for gain by the "flick-standard". revolutions are undertaken and recorded, with a total
(iii) Primary calibration - of spindie errors. of 11 (36° interval) indexings being carried out to
return to the original angular datum fixture position
Regardless of the equipment configuration prior (Reeve method). It is normal practice to obtain three
to any instrument calibration, the artefact should be orthogonal planes on the calibration sphere at 90°.
centred; on some instruments they utilise automatie Rather than a glass sphere artefact being supplied with
procedures to align the work axis to the table spindie, the instrument (Figures 217 and 218), the more usual
while others require manual centring and levelling. In item is a glass hemisphere, which has its roundness cal-
order to ensure consistency and repeatability in the cal- ibrated at a 3 mm offset from the equator. In any cali-
ibrated data, it is necessary to orient the artefact to that bration assessment it is important to record the angle
of a known angular position on the instrument. This (8) between the stylus arm and the tangent to the arte-
artefact orientation can be undertaken by its "witness fact at the point of contact. This angle is normally set
mark" which denotes the zero angular position; this is at 0° for a sphere measured at its equator but for
.. .
Figure 217. Calibrating a "test sphere" with a special-purpose Figure 218. Calibrating a roundness-testing machine using a glass
indexing fixture on aprecision roundness-testing instrument. sphere, to 28 nm departures from roundness. (Courtesy of Taylor
((ourtesy ofTaylor Hobson.) Hobson.)
Quality and calibration techniques
hemispheres it can be both angled and offset (3 mm) Gauge blocksl"fIick-standard": stylus
with respect to the equator (see Appendix C, Figure
242). (Figure 218). deflection
This offset correction for 0 is a useful tip to note
when assessing aprecision workpiece on a round- Stylus deflection calibration, for accuracy and sensi-
ness instrument that has not been recently cali- tivity of the probe and its associated lever arm
brated. If a significant "error spike" appears on the length, can be established by utilising either a set of
polar trace, its origin can be established by simply calibrated gauge blocks and their accompanying
rotating it through 90°; if it does not disappear then optical flat (Figure 219, inset photograph), or by
the error is in the instrument's spin dIe. using a "Flick-standard" (Figure 220). In the former
Gauge
blocks
and
optical
flat
Table
Gauge blocks
Optical flat
I I I I
I II I over gauge
blocks
I I I I
2.5mm 2.8mm
1 I
Two gauge blocks:
3mm
Figure 219. Calibration of roundness instrument employing optical flat with gauge blocks. [Photograph courtesy ofTaylor Hobson.]
InClustrial metrology , .
Measured step = X - Y = Z
Gauge block step = C
Calibration factor = C/Z = F
The general artefact configuration of gauge
blocks with their associated optical flat arrangement
for the calibration of stylus deflection can be
enhanced by employing the reduction lever principle (b) Flick standard and centring iris on instrument
are illustrated in Appendix C, Figure 241. For ultra-
high precision instruments the conventional gauge Figure 220. A "flick standard" and its amplitude speetrum, being
blocks and optical flat arrangement have to be used to assess a roundness instrument.
mechanically magnified by areduction lever
(Appendix C), typically obtaining magnifications of
20:1. This arrangement can produce a total uncer- wave numbers less than 75 upr contribute to the
tainty budget on gauge block steps to <0.016%, this signal, while the individual wave number amplitudes
being equivalent to <3.2 nm on a step height of are quite low if compared to the 12 /-Lm form devia-
2/-Lm. tion. Any calibration work has to be undertaken in
For calibration of stylus deflection on either a suitable measurement range for the full form devi-
longer stylus arms or with earlier roundness testing ation, although the actual calibration is dependent
equipment featuring analogue-based instrumenta- upon the individual wave amplitudes, hence the
tion, the flick-standard can be successfully utilised signal-to-noise ratio (SNR) tends to be quite low for
(Figure 220). This artefact is designed around a such flicks.
precision cylinder with a small flat on the peripheral It has been suggested that a new form of cali-
face (Figure 220b). The standard artefact has a cali- bration standard will improve data capture and
brated flat on its periphery, which when rotated in response, based on a spatial embodiment of the
contact with the stylus tip (Figure 220b), gives a superposition of several sinusoidal waves, termed a
notable "flick" on the displayed profile (Figure 220a), multi-wave standard (MWS). This waveform artefact
which equates to the calibration value - if instru- can be reproduced around the cylindrical circumfer-
ment calibrated is within its range. It has been ence, whereas the generatrices should be straight
reported that such flick-standards have a major lines without form deviations as these act to lower
dis advantage such as a small dynamical conte nt for the influence of potential variance of differing axial
larger wave numbers. For example, the amplitude of sections on the prospective result (Figure 221). Such
the signal of a typical "flick" having a <1>20 mm arte fact geometry has been termed "R-type MWS"-
cylinder with a flatness depth of 12 /-Lm has no the "R" denoting roundness, with the waves being
significant contributions from larger wave numbers reproducible both for internal and external cylindri-
other than at 75 upr (undulations per revolution) cal artefacts. Hence, these internal "R-MWS" arte-
(see Figure 220a). For this calibrated artefact all the facts are the first internal calibration standards.
(a) Displayed profile of peripheral form profile of multi-wave standard arte fact and its integrating fre-
MWS artefact quency-space analysis, when compared to the con-
Scale:
ventional flick-standard, exhibits a much higher
stability under test, inferring improved transfer sta-
bility of calibration to the end-user.
Cresting standard
Yet another artefact that is utilised for assessment of
angular offsets (arcuate uncertainty) produced by
spherical stylus tips on roundness instruments is
the so-called "cresting standard". "Cresting" is align-
ment of the stylus to the axis of rotation of the
instrument (Figure 222a-c). An incorrect stylusl
component contact causes a certain amount of noise,
which is included with the measurement data.
However, this stylus and component geometrie
relationship will not normally significantly influence
the filtered results.
(b) Corresponding MWS amplitude spectrum The results of the measurement taken can be
influenced in the following three ways:
4
Errors in peak-to-valley measurements (Figure
222d) - this is probably the least significant error
introduced by poor "cresting" and its value is of
the order of: 1 - cos a (where a is the angular
offset) . Typically, with diameters of components
of approximately 10 mm and the instrument
"crested" within 0.5 mm, a is 5.7° and this will
. relate to (1 - cos a) = 0.005, that is, introducing
I
_ ill:onent/Artefact
~StylUS
I Rotation
-$-
(e) Errors in absolute radii
Cresting standard
Calibrated.
diameter
Column straightness and squareness One major problem when assessing any straight-
ness/squareness alignment is termed "coning
Many of the more sophisticated roundness instru- error". This coning error is principally the result of
ments are equipped with a straightness column (see the initial set-up.
Figures 113, 114 and 122 for typical machine con-
figurations). In order to calibrate the alignment
(straightness and squareness) of this column with
respect to the spindie axis, most notably for rotating 6.7 Probing uncertainty:
table instruments, a cylindrical square is employed.
These "squares" can be purchased in a number of
roundness and form
lengths, typically 500 mm, 1000 mm and 2000 mm.
The smallest of these artefacts has an LSC round- One method to obtain more discrimination in
ness of better than 0.25 fLm and the largest less than roundness assessment and at the same time reduce
0.5 fLm. In Figure 223 is depicted one of the shortest measuring uncertainty is to be able to calculate an
cylindrical squares. estimate of how much a measured result may vary
Quality and calibration techniques
6.8 Nanotechnology
instrumentation: now and
in the future
Figure 223. Aprecision artefact - "cylindrical square" - being
employed to calibrate column straightness/squareness on rotating-
table roundness instrument. ((ourtesy of Taylor Hobson.) The term nanotechnology was first introduced in
1974 by Professor Taniguchi to describe production
tolerances and finishes within the nanometric range.
from the true value. This uncertainty may be the His graphical representation of achievable machin-
consequence of a number of factors, not least of ing accuracies (Figure 198) was extrapolated into the
which are operator inftuence and environmental future and has been shown to be a remarkably accu-
conditions. For example, if collecting a greater data rate prediction of what came to pass (Table 18).
density - perhaps acquiring 800 instead of eight data Taniguchi quite correctly concluded that by the mid-
points on a roundness profile - an industrial 1990s some metrological instrumentation would
company can reduce its measuring uncertainty, as be consistently operating in the region of between
illustrated in Figure 224a. 100 um and 1 um. This has meant that highly sophis-
At one extreme, today's scanning instruments ticated instruments would need to be developed and
can read hundreds or thousands of points in the time that further exploitation of surface and roundness
it takes a co ordinate measuring machine (CMM) technologies would be even more exacting in the
with its associated touch-trigger probe to check future. Nanotechnology encompasses more than
around six data points. By way of illustration, a high- simply highly accurate and precise metrology equip-
speed scanning probe can measure a <1>150 mm bore ment, as many micro-miniaturised components and
in around 10 seconds, taking over 800 measuring assemblies today are fabricated as integral nano-
points in the process. To press the point still further, metric devices. Physics, chemistry, biology, engi-
if a 30-second scan of a <1>50 mm boss is taken this neering, materials science and other disciplines
results in approximately 3000 measuring points on meet at the atomic scale.
the component feature. However, if a CMM is
equipped with a scanning head, it can achieve equiv-
alent levels of operational performance, to that of Instrument performance
high-speed scanning probes. If the measurement
involves the assessment of a near-perfect compo- Instrument characterisation falls into a number of
nent, the number of probing points and their loca- categories, although it is possible to list them by
tions become somewhat irrelevant to the calculation three variables:
(a) Uncertainty depending on the number of points measured
10 >200 >2000
Number of points
measured (log seale)
(b) Significant form measurement errors occur with just four recorded points taken, but true
contour assessed when continuous probing occurs
Geometrie uneertainty
of position - produet of Maximum
few points taken Inseribed
Minimum CircIe (MIC)
Cireumseribed
CircIe (MCC)
Single
points
Sequenee of Roundnessl
Seanned points (eontinuous
probing)
Figure 224. Probing uncertainty arises if tao few point are taken on roundness parts. (After Knebel!American Machinist, 1999.)
(a) Feature and scale of instrument techniques
Macro
ATOMICTYPE
INSTRUMENTS
Glossmeter
Milli
SEM (1970)
STYLUS CONTACT
INSTRUMENTS OPTICAL
INSTRUMENTS
Diffraction
SEM (1990)
SPATIAL
Micro
Nano
HEIGHT
Nanosurf
AFM / STM (1990)
Macro
Conventional
Milli engineering
QUANTIFY
% INFORMATION
VISUALISE ~ ~ Metrology
% INFORMATION ,./ ~ ~ ~ / ~ calibration
ACTUAL
TREND Jt~/ DESIRED gap
TREND
297
AppendixA Ra
1
= -
Ir
f Ir
Z(X) I dx (units ofm)
Previous and some current surface texture parameters 0
In Chapter 1 the current parameters were discussed The Ra parameter would be primarily used in app1i-
relating to ISO 4287: 1997; here their immediate cations to monitor a production process, where a
predecessors and some current ones are mentioned gradual change in the surface finish was anticipated,
at some length, as many companies still require for example, due to too1 wear in the cutting process.
information relating to these previously valid para- There are a number of conditions that must be
meters for surface texture assessment. met for Ra to be utilised satisfactorily:
Prior to a discussion on the previous methods of
obtaining roughness data from a surface texture • the Ra va1ue over one sampling length represents
trace, a brief review of these surface texture para- the average roughness. The effect of a single
meters will allow a greater understanding of how, spurious non-typical peak or valley within the
where and why they are applied to gain an insight profile's trace will be averaged out and, as such,
into methods of classifying surface conditions. In has on1y a small inftuence on the Ra value;
essence, surfaces that are manufactured can be • it is usual to take assessments over several
produced in a myriad of ways, with surface rough- consecutive sampling lengths and then to accept
ness parameters being historically developed to fulfil the average as the Ra value. The evaluation length
specific commercial and industrial needs. This has contains several sampling lengths (Figure 18a);
meant that a considerable number of surface this ensures that the Ra value is typical of the
descriptors, as they are sometimes known, have surface under test;
occurred, resulting in a frequently quoted term, • an Ra value alone is meaningless, unless quoted
"parameter rash", coined some years ago by with the metre cut-off (AC), or if this can be
Professor David Whitehouse. Many of these para- assumed. Repeatability of the Ra value will only
meters are utilised only by particular specialist occur at an identical cut-off length;
industries. Generally, they can be broken down into • where a dominant surface texture pattern occurs
distinct groups: (lay), then Ra measurement is undertaken at 90°
to this direction;
• amplitude parameters - which are measures of • that Ra does not provide information as to the
the vertical characteristics of the surface devia- shape of either the profile or its surface irregu-
tions; larities. Different manufacturing processes will
• spacing parameters - measures of the horizontal produce divergent surface finishes; therefore it is
characteristics of the surface deviations; normal procedure to quote the actua1 production
• hybrid parameters - which are some combination process along with its expected Ra numerical
of amplitude and spacing parameters; value(s);
• statistical parameters - amplitude heights treated • Ra offers no distinction between peaks and
as statistical data sets. valleys on the surface trace;
• assuming that the Ra numerical value has not
been computed, requiring determination from a
graph previously made of the surface, this can be
Amplitude parameters simply undertaken using suitable software, or
previously in a more basic form by a planimeter.
Ro: arithmetical mean roughness Figure 227 graphically depicts this Ra problem
and illustrates the fact that the workpiece's Ra
The classification of the relative roughness of numerical value alone (as has already been men-
surfaces was developed in England and was termed tioned) is not only meaningless but can, under
centre line average (CLA), while in the USA its equiv-
certain conditions of incorrect interpretation, cause
alent term was the arithmetic average (AA). The catastrophic consequences. This identical Ra value
derivation of Ra is graphically illustrated in Figure shows three potential in-service conditions (Figure
18(b) (see Chapter 1). Mathematically, Ra is the 227: (a) bearing surface; (b) intermediate surface;
arithmetic average value of the departure of the and (c) locking surface; all having an Ra of 4.2 f.lm
profile from the centre line throughout the samp1ing in these examples. In case (a) this surface might
1ength. Determination of Ra is normally computed prove ideal for a "light" bearing application, perhaps
by the software but can be derived using the where some local oil retention was necessary to
following formu1a: reduce its frictional characteristics; whereas case (c)
(a) (b) (c)
fT, f
lr
surface condition and leading to the selection of a
surface with locking state (c) - this would drastically Rq = - Z2(X) dx (m)
Ir 0
shorten the component's life under highly stressed
states. Therefore, using such a parameter and only The reason why both Ra and Rq roughness average
quoting its numerical value in isolation, without parameters were adopted was, in the main, his-
further specifying the other mutually related torical. The Ra surface descriptor is simpler to esti-
descriptors to quantify the surface condition, can mate from the profile recording and as a result
later lead to disastrous consequences. Incorrect use was initially adopted before roughness-measuring
or interpretation by a designer or metrologist of any instruments became more popular. Instrumentally,
surface descriptor could result in, at best, the part Rq has the advantage of simplicity, as phase effects
being totally inappropriate for its current applica- in the electrical filters become of comparatively less
tion - causing poor reliability and, at worst, leading importance and can be disregarded, although they
to catastrophic failure. inftuence the arithmetic average somewhat and
cannot be ignored.
What can be seen in many of the amplitude para-
Rq: root mean square meters is that there is no fixed relationship allowing
conversion from Ra to Rq, as it would depend solely
An alternative method of calculating the average on the shape of the profile. For many production
roughness of a surface is to use statistical tech- processes the Rq value of the surface would be at
niques, such as the root mean square (rms). The rms least 10% greater than its equivalent Ra. In general,
can be obtained by squaring each value, then taking a reasonable approximation of the ratio Ra :Rq =
the square root of the mean. For example, the arith-
1:1.1, but care must be taken with this conversion
metic average of four values, a, b, c and d, would be:
factor as some surface topographies can introduce
an error. As an example of the misleading ratio
(m) effect, the case of a lapped surface has an asymmet-
4 rical profile (i.e., with deep valleys and rounded
crests) - the Ra:Rq ratio can increase to 1:1.5.
When compared to the arithmetic average, rms has
the effect of giving extra weight to higher values, as
shown by the following three groups of values:
Ht, Htm, Hv, Hz, Hmox, Hpand Hpm: peak • Rt is directly affected by the presence of dirt and
scratches, because there is no "averaging effect";
and valley heights • if the slope of the profile is ignored, then there is
no ambiguity as to which are the highest and
Occasionally, it is useful to specify the maximum lowest slopes.
roughness (peak-to-valley) height, rather than Ra,
which gives the me an height. Typical of one of the The symbol Rmax (Figure 228) is the vertical
maximum roughness descriptors is Rt; this para- distance between the highest and lowest points of a
meter correlates to a tactile assessment of the sur- profile within the sampling length, but because of its
face when handled. Rt equates to the German term sensitivity to scratches, ete., it is more usual to take
for roughness depth - Rauhtiefe - being the highest the mean - Rtm - of the five individual (consecutive)
and lowest points of the profile within the evalua- sampling lengths (Figure 228). In Germany, Rtm
tion length, measured perpendicular to the ordinate equates to RZ(D1N)' whereas elsewhere around the
lines on the profile chart (see Figure 228). Some world RZ(ISO) is a different parameter, as described
points worth mentioning relating to the Rt para- later in this section.
meter are that Rp is illustrated in Figure 228, which is another
height term, being the maximum height of the
• with the definition of Rt the centre line does not profile above the centre line within the sampling
occur; length. As the Rp value tends to be extremely sensi-
• the value of Rt is determined over the evaluation tive to large profile peaks within the sampling
length; length, the information is not too reliable and as a
Rmax2
Rmax4 RmaxS
_ RmaxI!
Rp Rt
L L L
L 1--------------1
Evaluation Length J
Rmax= maximum peak-to-valley height within the sampling length L.
Rt = vertical height between the highest and lowest points of the profile within the
evaluation length
Rtm =Mean value of the Rmax of five consecutive sampling lengths.
Rp = Height of the highest point of the profile above the centre line within
sampling length L.
Rpm =Mean value of the Rp of five consecutive sampling lenghs.
Figure 228. Derivation of some peak parameters.
result should be used with care. Due to this uncer- RZrJIS): 1O-point height
tainty introduced by "stray" dominant peaks using
Rp, the "me an levelling depth" parameter Rpm offers Although the Rz 01S ) or RZ(ISO) parameter has now
a more consistent alternative. This latter surface been deleted from the latest ISO standard (ISO 4287:
roughness descriptor is the mean value of the level- 1997), it has been included in this discussion as there
ling depths of five consecutive sampling lengths, are still many engineering drawings in existence that
quantified by the following equation: utilise this surface texture descriptor. The Rz 01S )
parameter averaged the peak-to-valley values, which
had the effect of reducing the influence of either a
spurious irregularity or a scratch. As its name
suggested, it was derived from 10 points within the
or sampling length (i.e., being a German-based stan-
1 5
dard the letter "z" was derived from the German;
Rpm = - 2: Pi Zehn Punkt Höhe which equates to "lO-point
5 i=1 height") and is the mean distance between the five
highest and lowest peaks and valleys, respectively,
This Rpm term gives reliable information on the measured perpendicularly to a base line (see Figure
profile's shape and can indicate whether the part 229). RZ(JIS) was determined using the following
in question might be suitable for wear-resistant equation:
applications. Due to Rpm being used to determine
the functionality of a surface, it is often used in Rz 01S ) = (ZPI + ZP2 + ZP3 + ZP4 + ZPs)
tribological applications, for example, bearings,
for establishing interference/shrink fit component - (Zv 1 + ZV 2 + ZV3+ ZV 4 + ZV s) + 5
behaviour, sliding surfaces, or surface treatment
analysis - prior to coatings. Small values of Rpm
are characterised by surface topography having Rz01S) =.51 [ ~Pi
5
+ ~ Vi
5 1
wide peaks and narrow valleys, while large Rpm
values indicate a sharp-pointed profile (i.e., "spiky The five peaks and valleys can be located
surfaces"), this latter surface obviously having anywhere across the sampling length, unlike R(DIN)'
considerably worse wear resistance than the former allowing it to be utilised for short surface lengths,
topography. whereas the alternative R(DIN) would be inappro-
priate because significant peaks or valleys per cut-
off length are not present. RZ(JIS) suffers from the
I SAMPLING/CUT-OFF LENGTH I
~f---------~
Figure 229. The 10-point Rz parameter derivation.
limitation that if a number of peaks and valleys Hence by this criterion local peaks e and f (Figure
occurred condensed within the cut-off length they 230a) would be accepted; conversely, the smaller
would be unrepresentative of the whole surface peaks a, b, c and d would be ignored. This decision
and will have influenced the average condition to ignore sm aller local peaks is concurrent with the
over the profile. The cent re line (i.e., Figure 229) is practical significance of these minor profile irregu-
only used as a reference direction from which peak larities, although it does ignore the fact that the crest
and valley measurements are made, although the of a profile peak should be retained in the surface
same result can be achieved if measured from any assessment. What has been said for local peaks is
line inside or outside the profile, but parallel to also true for profile valleys and their associated
the centre line. Rz01S ) lent itself to assessment from local valleys.The roughness amplitude is important
the graph, needing only 10 direct linear measure- for surface assessment for many applications. The
ments. Further, there was no ambiguity in defining spacing of these roughness peaks has importance
the maximum peak, or valley (Zp\ or Zv\); however, too, particularly on rolled sheet steels, etc., where the
prior to determining which were the peaks, ZP2 to control of surface texture is essential to obtain
ZPs' and valleys, ZV2 to ZV s' it was necessary to define uniform lubrication as the sheet is either pressed or
what constituted a peak or valley. A slight digression drawn to minimise scoring and its influence on the
here might be in order to establish how and in what final paint or plating finishes. The value of the Ra
manner peaks and valleys can be established. parameter alone is not sufficient to specify the
differing types of texture obtainable from the rolling
process. Peak spacing control gives improved bond-
Peaks and peak counting ing of finish treatments with better uniformity while
reducing the tendency to cracking during drawing
From a profile graph, if an attempt is made to or forming operations. With our eyes being very
measure a parameter such as the example shown in sensitive to differences in appearance, some plastic
Figure 229, or to count the number of peaks and parts are plated to enhance their cosmetic appear-
valleys within the sampling length, the question ance. When identical parts have been produced at
arises: "What constitutes a peak or valley?" Figure two factories, if their average peak spacings (peak
230(a) illustrates the dilemma associated with peaks; counts) are not similar they may not be a visual
in this example two areas of material project above match. Moreover, peak spacing is often a significant
the mean line, area A between points C and D, factor in the frictional performance of surfaces for
plus area B between points E and F - these can be automobile brake drums.
termed profile peaks. In this example within area A
are superimposed a number of minor peaks a-f,
termed "local peaks". Are these to be regarded as Spacing parameters
separate peaks and included within the assessment?
It might be said that such local peaks, being of low To the eye the visual presentation of a surface is a
amplitude, can be discounted because they are non- combination of its profile depth and peak spacing.
repeatable and are not really part of the surface Even when a surface has the same Ra value, the
topography, resulting from factors such as instru- appearance can be markedly different. The number
ment instability, vibration or debris on the surface. of peaks within the sampling length becomes a
Whatever the cause for these minor peaks, once the controlling factor where visual appearance is crit-
surface is in service and a tribological action occurs, icaI. Establishing the type of peak from the surface
then various smaller local peaks will be worn away is important. Peaks can be established in a number
before any significant effect occurs to the surface's ofways:
performance. As a result of the last statement, the
question raised is: "Should local peaks be profile peaks are normally established if their
neglected?" Taking the case of local peak f in Figure profile crosses the centre line twice; thus the
230(a), it is almost of comparable height to the actual peaks are half these numerical values. An
highest peak and, as such, should not be ignored. example of counting peaks is shown in Figure
Guidelines based on this criterion for inclusion of 230(b), where a, b, c and d represent two peaks;
local peaks have been proposed: when a peak's 2 establishment of "local peaks" provided they
height measured from the smallest adjacent local exceed a certain height; in this example there
valley is not less than 1% of the maximum height of were seven, namely A, B, C, D, E, Fand G;
the profile peak to the valley, measured from the 3 the number of peaks similar to profile peaks pro-
mean line (i.e., height h in Figure 230a must not be jecting above a reference level at height Y can be
less than 1% of Rp + Rv). determined by halving the number of tim es the
(a) Local and profile peaks
d abc e f
Rp
Rv
Figure 230. The influence of local and profile peaks when peak counting. ((ourtesy of Taylor Hobson.)
profile crosses this reference line; in this case In the first case, the counting of these profile
crossings at e, f, g, h, i, j, k and I give a count of four. peaks is termed high spot count (HSC; see Figure
4 The number of peaks which project through a 231a), whereas the peaks counted by the second,
selectable band centred around the mean line can third and fourth cases are known as peak counts
be established; typically, when the profile projects (Pc), but to minimise any ambiguity it should be
below the reference level at m, then above the stated what represents a peak's definition in our case.
upper level at e, crossing this level twice at fand Pc is normally determined over the greatest assess-
h, this represents just one peak. ment length possible; that is:
(a) High spot count (HSC)
Selectable of slice level Depth of slice level
1 Count 2 Count 3 Count 4 Count 5 Count 6 Count 7 Count
, I
If.=f--------~~~-~--------,p.j
Samplinglcut-off length I
L --~-~--c:=-j
Samplinglcut-off length I
Figure 231. Spacing parameter derivation: high spot count and mean spacing.
Material ratio
curve
100 (bi + bÜ.fu + b 41
L
Sampling length
o 100
---co-
Mr%
Figure 232. Representation ofthe material ratio/Abbott-Firestone curve. ((ourtesy ofTaylor Hobson.)
either of the contact surfaces that is higher than the fraction and p, the profile depth. This Tp parameter,
film of lubrication will penetrate through this superseded by Pmr (although it simulates wear
medium, resulting in physical contact with its asso- effects) is only an approximate substitute for true
ciated mating surface. Such contact will introduce running-in tests, this is because:
friction, thermal increases and premature bearing
wear. Thus any surface having too many inappro- • the bearing ratio is only a fraction of the actual
priate peaks will not be as effective as a bearing, length and not representative of a surface area;
when compared to one having low peaks and deep • estimation of the bearing area is obviously estab-
valleys. lished from a predetermined and short cut -off
The material ratio curve, namely Pmr, Rmr and length - ignoring gaps that could result from
Wmr, for primary, roughness and waviness profiles, waviness and form errors;
respectively, or the Abbott-Firestone curve (as it was • Pmr, being a theoretical value, by its very nature
previously known and denoted as Tp ' but often relates to an unloaded surface, whereas in reality
written as tp )' can be expressed as a percentage of the actual surface may undergo elastic deforma-
the evaluation length at a predefined depth below tion;
the highest peak. It can be determined by the • practical in-service conditions mean that two
following expression (see Figure 232): contacting surfaces are involved and each specific
surface's features contribute to overall wear;
• induced wear is often accompanied by bulk or
Pmr (%) plastic flow of bearing material, with the result
that the geometrical concept of crests being
neatly truncated by an arbitrary line drawn
through them is impractical and unrealistic.
75%
reality the effect of a single peak on a surface's in- pIe, a 5% reference line (Figure 233c) testifies that
service function has litde significance. In order to the top 5% of the profile is not included as part of
minimise the effect of a single peak on the material the calculation for the material ratio. Selection of the
ratio curve, an artificially induced reference line is zero line beneath the highest measurable peak will
chosen to shift the line below this highest peak as be dependent on the topography of the associated
depicted in Figure 233(a and b), this being expressed peaks in the profile, but industrial practice suggests
as a material ratio percentage. Specifying, for exam- the reference level is set between 2% and 5%.
The inftuence of filtering on the preselected From the idealised profile traces and their accom-
depths through the profile will be an important panying material ratio curves illustrated in Figure
factor in modifying the material ratio curves, as 233, it is possible to visualise whether a surface is
will the measuring length selected. Terms such as either a "bearing type" or "locking type" of surface.
micra-material and macra-material ratias relate to Furthermore, pre-selecting a zero reference line at
the filtered or unfiltered (total) roughness profiles, some predefined depth below the highest peak will
respectively. Normally the filtered parameter is show the anticipated wear pattern or likely asperity
preferred, because it eliminates the effects of wavi- (peak) collapse under predefined in-service condi-
ness in the measured profile. Filter distortion of the tions. This level of peak attrition by tribological
measured profile can introduce erroneous results; action or through plastic deformation may be an
this is particularly a problem when plateau-type important factor relating to its functional operation,
surfaces occur. Typical of these are sintered, honed, anticipated usefullife and subsequent reliability.
plasma-coated, ceramic and chrome finishes. Some
apparent confusion has arisen when measuring
these plateau-type surfaces, as to whether a mechan- Parameters derived (rom
ical form of filtering is preferred, via the use of a skid
to minimise the effect that waviness can play in Abbott-Firestone/material ratio curve
inftuencing the shape of the material ratio curve. (ISO 13565: 1996 - Parts 1 to 3)
Some of the literat ure categorically states that skids
should be utilised for these plateau-type surfaces, The standard denotes several surface parameters
while others are equally adamant that a skidless relating to the functional behaviour of highly
mode of operation is preferable, particularly when stressed surfaces, namely lubricating, sealing and
quantifying secondary machined powder metal- rolling faces. Being derived from the material ratio
lurgy surfaces. Powder metallurgy and many scored curve (Figure 234), these parameters not only char-
surfaces are affected by filtering, particularly via acterise the profile's roughness but also the shape of
"overmodulation", necessitating the use of a "phase- the profile. These derived parameters include:
corrected" filter (ISO 11562: 1996). Regardless of
which skid technique is employed, topographical • Rk - core roughness depth;
filtering of plateau-type surfaces to remove waviness • Rpk - reduced peak height;
effects is important; further, as has been mentioned • Rvk - reduced valley depth;
earlier, it is also strongly inftuenced by the selected • Mr1 - peak material ratio;
measuring length for the surface under test. These • Mr2 - valley material ratio;
conditions of surface determination should appear • Al - material filled profile peak area;
with the surface texture symbol (at the appropriate • A2 - lubricant filled profile valley area;
position - see Figure 3). • Va - oil retention volume.
Previously, no standardised measurement condi-
tions for the assessment of Tp existed; this parameter The material ratio curve is broken down into a
has of late become of less importance with the series of straight lines comprising three parts to
advent of newer parameters such as; Rk, Mr1 and calculate the "Rk family" of parameters - the k repre-
Mr2 - this will be discussed in more detail shortly. sents the word "kerne!", meaning core:
o Mr120 40 60 80
Mr
2100 (%)
Figure 234. Derivation of the kernal roughness depth, Le., depth of roughness core profile, Rk. ((ourtesy of Taylor Hobson.)
• profile peak area - Rpk; Plateau-like surfaces, when measured, can be repre-
• co re roughness area of the profile - Rk; sented by peak height, whereas the valleys' depths
• profile depth area - Rvk. are only a means of establishing the character of its
respective roughness profile. The functional behav-
Such parameters are exdusively utilised for ob- iour of a component is not only decided by its rela-
taining the roughness profile of plateau-like (asym- tive "global" roughness, as indicated by an equivalent
metrical) surfaces with the digital valley suppression Ra value, but also by the profile's surface structure.
filter (ISO 11562: 1996). The derivation of the Rk
parameter is depicted in Figure 234. It is necessary to
find the tangency points for the minimum slope (the The average (RJ.a) and RMS profile
turning point) from the "S-shaped" material ratio
curve, delineated here by the verticallines at Mr1 and (RJ.q) slopes (ISO 4287: 1997)
Mr2. These tangency points relate to the 0% and
100% material ratio lines, being equatable to heights Figure 235 illustrates how the parameters RLla and
Rpk (for peaks) and Rvk (for valleys), respectively. RLlq are derived. Expressly, the parameter RLla is
The Rk zone represents the depth of core roughness, derived from the average slope of a filtered profile
as it is in the vicinity where the profile has the densest relative to the mean line of the trace. Its derivation
bearing region. The locations of both Mr1 and Mr2 can be established by dividing the profile peak in
relate to the material ratios at the top and bottom of question into smaller portions, then numerically
the roughness core, respectively. These values can be averaging the slope for each portion, as indicated in
used to determine still other parameters, such as the enlarged detail of the peak shown in Figure 235.
the "oil retention volume", derived from the Rvk Calculation of RLla can be found from the following
and Mr2 relationship (Va, which relates to the shaded formula:
triangular area A2 in Figure 234), principally used by
the automotive industry. The material ratio curve Va
can be described in terms of the area below the co re RLla 1
= -. 2: I-'
n
n i~l
Lly-I
Llx i
roughness (Mr2) and the demarcation of the 100%
material line. The numerical value of Va can be
where n represents the number of ordinates.
expressed by
Rather than taking individual numerical average
Rvk(lOO - Mr2) values for profile slopes within the sampling length
Va = ---'-------'- (as in the case of RLla), the root mean square "RMS
200 profile slope" (RLlq) can be calculated. A bonus of
utilising the RMS - RLlq - value is that it offers
Rpk - reduced peak height - is illustrated in
increased sensitivity to extreme values, unlike that
Figure 234, being the height of the top portion of the
surface profile positioned above the core profile. Jf a of the numerical method of determination using
small value of Rpk occurs, this characteristic would RLla, which tends to minimise their influence.
represent good wear resistance or its "running-in"
behaviour. The magnitude of Rpk is indicated by
triangular area Al' whose height is equal to Rpk and RLlq = JUr) fr [e(x) - eF dx
with a base of Mrl. By utilising such areas the effect
of a spurious peak in the profile trace becomes where
minimised. At the lower portion of the material ratio
curve the height Rvk represents the depth of the
lowest part of the profile, with valleys extending
below the core profile. This parameter has an oil-
e= Ur) fr e(x) dx
Figure 235. Derivation of the parameters average (~a) and RMS (~q) profile slopes. (Courtesy of Taylor Hobson.)
Figure 236(a) indicates how Aa is derived, wh ich is Whenever a complex profile occurs - this being
the average wavelength of the surface profile. The an amalgamation of several different wavelengths -
parameter Aa should not be confused with the then the average wavelength of these "weighted
"spacing parameter" Sm - this being the me an peak- components", according to their amplitude, can be
to-peak spacing within the profile's length when represented by Aa. In Figure 236(a) the roughness
peaks exceed a certain threshold, whereas Aa con- profile is illustrated for three surfaces. If a large
siders all the "components" of the surface profile, average roughness (Ra) is present, but having a sm all
namely, the wavelength in conjunction with the slope (Rßa) - as in the case of the top trace - this
amplitude (its peak-to-valley height) -although if a indicates a wavy type of surface having a large Aa
profile has a significant sinusoidal profile of pre- value. Conversely, if the magnitude of roughness
dictable periodicity, under these conditions Aa will decreases but the slope increases, the surface be-
approach that of the peak-to-valley spacing repre- comes rougher but less wavy, as indicated by the
sented by Sm. middle trace, or as indicated in the bottom trace
The average wavelength (Aa) surface descriptor where the roughness has been superimposed onto
can be determined as follows: waviness. The visual appearance of a surface may
(a) Average wavelength (Aa)
Aa= 8
Aa= I
Aa=4
e e
e
e
(b) RMS profile wavelength (Aq)
Figure 236. Average (Aa) and RMS (Aq) profile wavelengths. ((ourtesy ofTaylor Hobson.)
vary from that of a highly polished and reflective one of surfaces - an important factor for automobile
to matt surfaces, but they can be compared using the bodies. '\q can be utilised in tribological situations
'\a parameter. where very closely spaced roughness irregularities
The RMS profile wavelength ('\q) can be visu- of the surface te nd to be of relatively small ampli-
alised in Figure 236(b) and is a measure of the spac- tude and rapidly wear away in service - such as for
ings between local peaks and valleys, taking into a bearing application. Since these irregularity ampli-
account their relative amplitudes and individual tudes are quite small, any changes in the overall Ra
spatial frequencies. Its derivation can be established value during running-in are also small, with the
from shorter wavelengths disappearing and resulting in
more pronounced changes in the average wave-
27TRq length. Of more practical importance is the use of
'\q=~~
RLlq the average wavelength as a means of directly moni-
toring the manufacturing process. For example, in a
As in the case of the slope parameter RLlq, this continuous outside-diameter turning operation of
equivalent wavelength parameter ('\q) is more sensi- high-quality finishing, the average wavelength
tive to extreme values than either the RLla or '\a, these directly relates to the feedmarks promoted by the
being for average slope and wavelengths, respec- residual effects of the partial tool geometry as it
tively. passes along the workpiece. If the machine tool
The '\a parameter is particularly useful in sheet settings are incorrect, the values of both '\a and '\q
steel applications where the average wavelength is a will dramatically change, even though the Ra or
measure of the openness or closeness of the texture similar height parameter may not alter significantly.
and correlates weIl with the cosmetic assessment Similarly, for most grinding operations the para-
. AppendixA
Table 24. Comparison of aetual lca and Ra values from measure- cutting process. The resultant surface profile for the
ments made on aseries of speeimens bored hole would depict the interactions from the
boring bar deformations and any harmonie oscilla-
Production proeess lca(/J.m) Ra (/J.m) tions. This boring bar motion reflected in the profile
trace would exhibit low average profile height, but
Planning 400 17.8 with a large range of height values.
Fine cut planing 440 5.1 Surface texture data can be statistically manipu-
Multiple-tooth milling 1300 5.1 lated, beginning with the profile trace's height or
Fly-eut milling 300 2.2
amplitude distribution curve - this being a graph-
00 turning 100 1.7
Oiamond turning 37 0.3
ical representation of the distribution of height ordi-
Eleetro-erosion 340 10.1 nates over the total depth of the profile.
Eleetro-sinking 57 1.8 The characteristics of amplitude distribution
Surfaee grinding 77 0.95 curves can be defined mathematically by several
Cireumferential grinding 33 0.55 terms called "moments"; these are:
Plunge grinding 43 0.17
Honing 19 0.07 • arithmetic average 01 the profile - the first
moment (mI);
• profile height variance - the second moment
meter Aa or Aq has a direct relationship to the (m2);
average grit size, hence by monitoring the average • skewness - the third moment (m3);
wavelength this will provide relevant information • kurtosis - the fourth moment (m4).
relating to when the wheel must be redressed to
maintain its surface quality.
In Table 24 are shown the Aa values taken using Arithmetic average of the profile
sampies from a range of production processes. This
table illustrates that surfaces generated by a variety The first moment (mI) can be found from the
of production methods having similar Ra values expression
(fine cut planing and multiple tooth milling, or alter-
(~)~Yi
natively turning and electro-sinking) can exhibit
considerably differing values of Aq. This enables the ml = y=
n I~l
metrologist or manufacturing engineer to assess a
surface under test with considerably more dis er im-
ination than might otherwise be the case if only the
Yi
where is the height ordinate and n is the number
of ordinates.
Ra value alone had been used. NB By definition, the mean height of a filtered
profile equates to zero.
Statistica/ parameters
The amplitude distribution curve (Figure 237) Profile height variance
represents the comparative total heights over which
the trace achieves any selected range of heights The formula for the second moment (m2) is
above or below the centre line. One can deal with
this amplitude or height data statistically, in the
same mann er as one might physically measure
m2 = R q2 = (~)~ (yy
n Fl
anthropometrie data such as a person's average
stature, within a specific population range. As with NB The variance gives an indication of the profile
the statistical dispersion of population stature, engi- range heights, its square root being the standard
neering surfaces can exhibit a broad range of profile deviation of the amplitude distribution curve or its
heights. roughness parameter Rq.
For example, a boring operation with a relatively
long length-to-diameter ratio may cause deflection
(elastic deformation of the boring bar) and occa- 5kewness (Rsk) -1504287: 7997
sion the cutting insert to deflect, producing large
peak-to-valley undulations along the bore (wavi- Skewness is a measure of the asymmetry of the
ness). Superimposed onto these longer wavelengths amplitude distribution curve; alternatively, this can
are small-amplitude cyclical peaks (periodie oscilla- be expressed another way, as the symmetry about
tions) indicating vibrations resulting from the the mean line (see Figure 237a). If symmetry occurs
then Rsk equates to zero, but an unsymmetrical iron surface topography, having comparatively large
profile gives rise to a skewed curve (see Figure 237b numerical values of negative skewness. The surface
and c). The bias of Rsk depends upon whether the is sensitive to extreme ordinate values within the
bulk of the material is above or below the mean line. profile under test; this is due to Rsk being a function
In the case of Figure 237(b), the bulk of material of the cube of the ordinate height. As a result of this
occurs below the mean line - promoting a "locking" peak sensitivity, it is a hindrance when attempting
type of surface. Conversely, in the case of Figure to inspect plateau-type surfaces.
237(c), the majority of material is present above the Skewness is the third moment (m3) of the ampli-
mean line - representing a "bearing" or plateau tude distribution curve and can be expressed in the
surface. Such skewness bias enables a metrologist to following manner:
distinguish between two profiles having identical Ra
values but divergent shapes and hence considerably
different in-service applications. A numerical value m3 = Rsk = (~(
1 3)
Rq)
(!) !
n i=l
(yy
can be given to Rsk and in the case of Figure 237(b)
the "positive skewness" may eventually obtain an The shape or "spikeness" of the amplitude distri-
adequate bearing surface, although it is unlikely to bution curve can also relay useful information about
have oil-retaining abilities. This type of surface can the dispersion or "randomness" of the surface profile
typically be exploited for adhesive bonding applica- which can be quantified by means of a parameter
tions. The surface characterised by Figure 237(c) known as kurtosis (Rku).
might occur in the cases of porous, sintered or cast
Amplitude
distribution
curve
(c) "Bearing" surface temperature
Figure 237. How surface texture topography influences the amplitude distribution curve.
· AppendixA
Kurtosis (Rku)<3
Amplitude
distributioll
Figure 238. Variation in surface topography influences the shape and height of the amplitude distribution curve.
Kurtosis (Rku) -ISO 4287: 1997 By definition, Rku is the fourth moment of the
amplitude distribution curve (m4), being the relative
"sharpness" of the curve. The amplitude distribution
The surface parameter skewness (Rsk) is not sensi- curve shown in Figure 238(b) indicates smaller and
tive if the profile's "spikes" are distributed evenly less pronounced condensed peaks and valleys than
both above and below the mean line. Another term, that of the larger, more widely spaced "spiky" peaks
kurtosis (Rku), has this ability (see Figure 238a). and valleys illustrated in Figure 238( c). As a result of
Kurtosis provides a means of measuring the sharp- these topographical profile trace differences in peak
ness of the profile, with a "spiky" surface exhibiting and valley height and their density distribution, the
a high numerical value of Rku (Figure 238c); alter- Rku shape changes, as will their respective numer-
natively, a "bumpy" surface topography will have a ical values, as indicated in Figure 238(a).
low Rku value (Figure 238b). As a consequence of Due to the fact that Rku is a function of the fourth
this ability to distinguish variations in the actual power of its profile ordinates, it has extreme sensi-
surface topography, Rku is a useful parameter in the tivity to variations in peaks and valleys within the
prediction of in-service component performance profile trace under test. Due to Rku sensitivity, in
with respect to lubricant retention and subsequent practice it can be difficult to apply to the analysis of
wear behaviour. surface texture. As has already been mentioned,
kurtosis - being the fourth moment of the ampli- This completes the review of just some of the
tude distribution curve (m4) - can be calculated in previous and current surface texture parameters, but
the following manner: it is by no means an exhaustive list of those previ-
ously utilised, as many industries have developed
m4 = Rku = (~)4)
(Rq
(~)
n
~ (yy
,=!
their own parameters for specific industrial or
research-based requirements.
(a) Lines of constant slope (arctan Smax) and Iines of constant radius (Rmin) in
amplitude-wavelength space
yL
~ lA 10
E
x E
w 100
"
"0 E 10
Z "-
Ci
E
«
100
10
E
c:
0.1
0.01
0.1 10 100 I1 10 100 I1 10 100 1000
nm mm
Su rface wavelength
Log Rs
Amplitude.........--I----f._--,.4---,
r /2 -+-f-l---,.L,+-I--+-
I
2rh Rh
Log Surface Wavelength
Figure 239. Basis for the Stedman diagrams. [Sourees: Stedman, 1987, 1990; Franks, 1991.]
(a) Stedman diagram: range and resolution
Cmax :sharpest curvature; Zmin : smallest height difference;
8max :steepest slope; Amin :shortest wavelength;
Rp :Iargest height difference; Amax :longest wavelength
I /Cmax //8max
Rp/2 I / ///
- ---I------~VQ~~"T7::~
I
Log A I
I
i~~88&~
1/X)<X)<x~<~<~,(';
1 mm
l~m
rmax:5~m Zmin:5~m
1m
Figure 240. Stedman diagrams for instrument assessment of comparative performance. [Source: Stedman (bl. 1987.]
features of the particular instrument in question to this a110wing acceptable measurements to be made.
be found, namely height, surface wavelength, slope In a similar manner the vertical range (Rv ) and reso-
and curvature, which can be represented at any lution (r) restrict amplitudes, with the horizontal
potential scales within an individual uncomplicated range (Rh) and resolution (rh) restricting the wave-
chart of AW space. lengths that can be measured. For other classes of
If one considers the instrument or probe interac- profilometers typified by those based on optical or
tion with the sinusoidal profile, it fo11ows that most other non-contact probes, analogous limit lines can
instrument parameters enforce limits on the sine be derived. For example, the numerical aperture of
wave ranges that can be reliably measured. By way an objective through which a beam is focused to
of illustration, the tip radius (R s ) of a stylus must not form an optical probe will limit the maximum slope
exceed Rmin of a sine wave that is to be drawn. Rs can that can be sensed.
be plotted as a limit line of slope 2 in low AW space, In a co11ective sense, these limit lines will define
with only sine waves to the right of the limit line a polygonal zone, within which a11 the conditions for
being measurable. The slope errors (Sd) of a datum acceptable measurement are satisfied (see Figure
or reference slideway should idea11y not be greater 239b). This bounded profile can be taken as the
than Smax of any sine wave to be measured. The Sd working zone for the instrument in question, being
plots as a limit line of unit slope, with values above referred to as its AW map.
Comparison of instruments in AWspace that links both specification and function to its
manufacture and metrology.
It is possible to compare a diverse range of instru-
ments in AW mapping space. In a single scan it is
possible to show the preset magnification and scan AWanalysis: high er-order assessment
length for a selected probe or stylus that is con-
strained within the area of AW space, being only The AW analysis for instrument performance previ-
sensed to a particular location of the overall AW ously described can suggest limit lines that delineate
map. Moreover, a more in-depth AW mapping appli- sharp boundary attributes between a "go" and "no
cation might show the effects of setting different go" situations. Often in practice, such boundaries
magnifications and filters, together with other oper- tend to be "fuzzy" and this anomaly can be resolved
ating conditions for a single instrument. Such by higher-order analysis that can quantify this
detailed maps can be an important insight to the b~undary fuzziness as error contours. This strategy
user and can be incorporated in the instrument's wIll enable AW maps to be realised, having closed
manual. Further, it can display the appropriate contours for different levels of uncertainty. Thus, AW
conditions currendy set up for the instrument in the maps can provide a unifying link between the work-
computer's software. piece specification, its surface function, production
processes and subsequent metrological assessment,
hence playing a vital role in quality assurance.
AWspace: surface function and quality Moreover, these AW analysis tools are a vehicle in
presenting complex information in a succinct
assurance manner.
Yet another facet of this important technique of AW
mapping is that surface texture requirements can be
expressed by appropriate analysis of the function of References
a surface. For example, a mirror's optical specifica-
tion could be converted to AW limits by considera- Franks, A. Nanometric surface metrology at the National Physical
Laboratory.Nanotechnology 2,1991,11-18.
tion of diffraction theory and geometrical optics, Stedman, M. How to compare different surface texture measuring
plus the dimensions of the mirror would define lllstruments. Quality Today, April 1990, 35-36.
AW space relevant to the function of the mirror. Stedman, M. Basis for comparing the performance of surface
The application of surface metrology within the AW measuring machines. Precision Engineering 9(3), 1987a, 149-
window can be a route to quality assurance. The 152.
Stedman, M. Mapping the performance of surface-measuring
capabilities of the production processes - grinding, instruments. Proceedings of SPIE, 803, 1987b, 138-142.
lapping and polishing - can also be mapped, with Thomas, T.R. Rough Surfaces (2nd Edn.). Imperial College Press,
AW analysis being utilised as the unifying concept 1999.
AppendixC
Surface texture and roundness: calibration diagrams and photographs
* Major lever length can be accurately set and rneasured to ±0.05 rnrn. This could produce a 0.04% uncertainty in step at the
stylus
**Minor lever length can be set using gauge blocks to an accuracy of ± the uncertainty in the blocks (typically <±0.0001 rnrn),
producing a possible error of 0.001 %.
NB: Total uncertainty budget on actual step generated is ±O.16% (±0.16% (±3.2 nrn on a 2rnrn step height on gauge blocks).
B C
I
I
I
I
I
A/20=B+C/2
I I
127 mm*
~--------------------------------------------------------~~
~ l 16.35 mm*
[;:0.1
Figure 241. The traceable magnification and calibration on surface texture/roundness instruments using the "reduction lever principle".
((ourtesy of Taylor Hobson.)
(a) ,-----_--,
Indicator Indicator outputs
11 8 = R(8) + B(8)
Workpiece
Rotary
table 12 8 = -R(8) + B(8)
Toroidal shaped
stylus
GJass hemisphere
Rotary tahle
Kinematic location
spheres
72 °, or 36°
indexing
Geneva catch
plate
-t:::=-- - - - --<::::r--
Gauge Gauge
direction direction
I
--,---
'"
Position 2: Invert
Position 1: Normal -
Gauge: Reversed
Gauge: Normal
-I + C
1+ C
Air Material
~ --=:::::I-
Gauge Gauge
direction direction
-I - C -I + C
Material Air
Twin-trace bisector: -I
Algebriac addition Bisector
= -instrument error
oftraces : -2 1
Note: The air / material
!"elationship is reversed
Figure 244. Calibration a roundness instrument for component or instrument uncertainty. (Courtesy of Taylor Hobson.)
AppendixC
Roughness
data
information
Figure 246. A range of three calibration standards for checking electronic stylus surface texture instruments [Courtesy of Rubert & Co.].
InClustrial metrology . .
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76 90.0 83.0 95.5 90.0 83.5 1556 96 76.0 91 .8 80.4 68.9 58.9 231 179 216 102 . 46 831 756 47.0 18.7 84.5 61 .0 133.3 103 80 :::l
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70 86.5 78.5 94.0 86.0 77.5 1076 972 90 68.0 89.9 76.4 62.8 98.5 55.2 201 157 185 89 40 797 73.6 43.0 12.6 81.0 55.5 ' 30.7 97 75
69 88.0 78.0 : 93.5 85.0 76.5 1004 946 ' 69 84.0 89.5 75.8 61.8 98.0 54.6 196 164 180 86 39 79 I 73.3 42.3 116 80.0 54.5 30.3 '961 . 74
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87 85.0 76.1 92.9 83.6 74.2 900 895 67 61 .0 86.9 744 59.8 96.5 534 188 146 172 64 37 78.0 72.7 41 .0 9-6 79.0 NA 53.0 29.5 94 ' 72
88 84.5 75A 92.5 82.8 73.3 865 870 NA 77.4 12.3 40.3 8.6 78.5 100 52.0 29.1 93 . 72
86 59.0 86.6 73.8 58.8 955 52.8 164 145 169 83 36
65 83.9 74.5 92.2 81.9 72.0 832 846 739 85 57.5 86.2 73.1 578 94.5 523 180 142 165 82 35 76.9 72.0 39.6 7.6 78.0 99.5 51.5 28.7 92 71
84 83.4 73.8 91 .8 81.1 71 .0 600 822 722 84 58.0 87.9 72.4 58.8 940 51 .7 176 140 162 81 34 76.3 71.7 39.0 66 77.0 99.0 50.5 28.2 91 · 76
63 82.8 73.0 ' 91 .4 80.1 69.9 772 799 706 83 54.0 87.6 718 55.8 93.0 51 1 173 137 159 80 33 75.7 71.4 36.3 5.6 76.5 98.8 495 27.8 90 69
62 82.3 722 91.1 79.3 68.8 746 776 688 82 52.5 87.3 71 . I 64.8 92.0 50.6 170 135 156 77 32 75.2 71 .0 37.6 4.6 76.0 98.5 48.5 27.4 89 , 69
61 61.8 71.5 90.7 78.4 67.7 720 754 · 670
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79 47.5 68.3 69.1 51.8 89.5 48.9 161 128 147 70
58 80.1 69.2 89.3 75.7 84.3 6S3 690 615 338 28 73.0 69.3 34.5 NA 73.5 97.0 45.0 25.5 86 : 66
78 46.0 86.0 68.4 50.8 68.5 48.4 158 126 144 69
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56 ' 79.0 87:7 86.3 73.9 62.0 613 650 . 577 313 33.0 72.5 96.3 43.5 : 24.5 84 65 ~
76 NA 42.5 85.3 67.1 48 8 87.0 47.3 152 ' 122 139 67 26 72.0 69.0
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54 78.0 681 87 .4 72.0 59 .8 577 643 292 24 32.0 71.0 95.5 41 .5 24.0 82, 64
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71 97,4 345 83,7 63.7 43.8 '00 82.5 '4.8 141- 112 127 62j 21 69.0 87.5 29.5 69,5 945 390 22.5 81 62
SO 75.9 631 65.5 68.5 55.0 513 542 461 255
70 96.6 32.5 83.' 83. 1 42.8 99.5 815 443 139 110 125 61 20 68.5 67.3 29.0 68.5 943 380 220 60 61
49 75.2 621 65.0 67.6 53.8 49J1 . S26 469 246
69 96.2 31 .0 83.0 62.4 41,8 99.0 81 .0 43.8 137 109 ,23 60 19 68.0 67.0 28.5 88.0 94.0 375 , 21.5 79 61
46 74.7 614 84.5 86.7 52.5 464 510 , 455 238 78 60
86 956 29.5 82.7 61.7 408 98.0 60.0 433 135 '07 '21 59 18 67.0 66.5 27.5 675 935 36.5 ' 213
47 74,1 60,6 83.9 65.6 51 .4 471 495 ' 443 229
67 95.1 28.0 82.4 61 .0 39.8 91.5 79.0 428 133 106 119 58 17 88.5 66.3 27.0 61.0 93.0 35.5 ' 210 78 60
46 736 60.0 83.5 84.8 SO.3 458 460 432 n1 77 ' i 5~
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65 93.9 25.0 81 .8 59.7 37.7 96.0 715 416 129 102 116 56 15 65.5 65.5 25.5 65.5 92.5 34.0 20.0
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41 70.9 56.2 80.8 60.4 44,3 402 414 381 198
61 91 .7 19.0 605 57.0 33.7 935 74.0 400 122 96 108 11 63.5 843 23,0 63.5 91 .0 30.5 . 73 57
40 70.4 55.4 80.4 59.5 43.1 392 402 371 162
60 91.1 17.5 60.1 56.4 32.7 93.0 73.0 395 120 95 107 , 10 63.0 64.0 220 62.5 90.5 29.5 72 57
39 689 54.6 79.9 58.6 41.8 382 391 362 177 11 ; 57 ,
59 90.5 16.0 79.8 567 31 .7 925 720 390 116 84 106 9 62,0 83,8 21.5 62.0 90.3 29.0
38 694 53.8 79.4 57.7 40.8 372 380 353 171 I . ' 71
58 90.0 14.5 79.5 55,0 30.7 920 71.0 38.6 , '17 92 104 I 8 615 83.,5 20.5 6'5 900 28.0 56
37 68.9 531 78.8 56.8 39.6 363 370 344 186 56 ,
57 89.4 13.0 79.2 54,4 29.7 9 1.0 70.5 36.' : 115 91 103 7 61.0 63.0 20.0 61 .0 89.5 27.0 10
36 86.4 52.3 78,3 55.9 38.4 354 360 336 161
58 98.8 11 .5 78.8 53.1 28.7 905 695 37.7 114 90 101 8 60.5 62.8 195 60.5 69.3 26.0 . 69 55
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67.4 SO.8 77.2 54.2 .1 338 319 152 55 88.2 10.0 78.5 53.0 27.7 90.0 885 37,2 112 89 100 z 5 60.0 625 185 60.0 89.0 25.5 69 55
34 342
149 84 87.7 8.5 78.2 52.4 26,7 89.5 880 36.8 111 87 4 59.5 620 180 59.0 88.5 24.5 69 55
33 66.8 SOO 76.6 53.3 34.9 327 33. 311 ~A
53 87.1 7.0 77.9 51 .7 25.7 89.0 67.0 36.3 110 66 3 590 61.8 17.0 585 880 23.5 . 68 54
32 86.3 49.2 76.1 52.1 33.7 318 326 301 146
NA 52 66,5 5.5 77.5 51 .0 24.7 98.0 86.0 35.9 109 85 2 580 61 ,5 16,5 58.0 87.8 23.0 68 54
31 65.8 48.4 75.6 51 .3 32.5 310 318 294 141 68
SI 86.0 4.0 77.2 SO,3 237 87.5 65.0 35.5 108 84 1 57,5 6 1.0 16.0 57.5 87,5 220 54 '
30 85.3 47,7 75.0 SO.4 31 .3 302 311 286 92,0 138
SO 85,4 2,5 76.9 49.7 227 87.0 84.5 350 '07 83 t 0 57,0 60,S 15.0 570 87.0 210 67 53 1
29 84.8 47.0 74.5 49.5 30.1 294 304 279 91.0 135
28 64.3 46.1 73.9 46.6 28.9 286 297 271 90,0 131
27 83.9 452 73.3 47.7 27.8 279 290 264 99,0 128
26 83.3 44.6 72.8 46.8 26.7 272 284 258 88.0 125
25 628 438 72.2 45.9 25.5 266 278 253 87 ,0 123
24 624 43. 1 71.8 45.0 24.3 260 272 247 86.0 119
23 62.0 42.1 71.0 44.0 23.1 254 266 243 84.5 117
22 6'-5 41 .6 70.5 43.2 22.0 248 261 237 83.5 115
21 61.0 40.9 69.9 42.3 20.7 243 256 231 82.5 112
V Z
valley fluid retention index 78 Zerodur: thermally stable material 63,65,
van der Waals force 123,127 292