Formulation Guide Personal Care and Cosmetics EN
Formulation Guide Personal Care and Cosmetics EN
Formulation Guide Personal Care and Cosmetics EN
Formulation Guide
CONTENT
BODY TREATMENT
Shower Gels 12 - 21
FACE TREATMENT
Shaving products 64 - 67
HAIR TREATMENT
Shampoos 68 - 73
OTHER
LIQUID
HAND SOAPS
Liquid hand soap is a product formulated to wash and clean hands.
It belongs to the group of common dirt removers in commercial and
industrial cleaning processes. Liquid hand soaps are the most widely
used products in cleaning sector.
On one square centimeter of the skin there are plenty of various bac-
teria. All these germs are transferred every day from human to human
when shaking hands, holding on to the handles in public transport, to-
uching coins and banknotes that come into contact with hundred of
hands a day.
Only proper hand hygiene will protect us against dangerous germs and
bugs. That is the reason why hands should be oftently washed with the
usage of an appropriate designed formulations.
Cocamidopropyl Betaine ROKAmina K30 7.00 surfactant PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.00 re-oiling agent
C Citric Acid q.s. pH modifier Cocamidopropyl Betaine ROKAmina K30 7.00 surfactant
APPEARANCE visual method clear, homogenous liquid APPEARANCE visual method bright-yellow gel
VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 - 6000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 2500 – 5000
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. Add ingredients from phase A to warm water (50-55°C). 4. If necessary, add Sodium Chloride to adjust the viscosity. 1. Add ingredients from phase A to the warm water (45- 5. Add Sodium Chloride to adjust the viscosity. NOTE.
Mix until homogenous solution is obtained. NOTE: it is very important to equilibrate a sample at 50°C). Mix until uniform. Add salt (not in one go) – after addition of each portion
25°C for at least one hour to get an accurate viscosity mix well.
2. Cool the batch down to at least 35°C. 2. Cool the batch down to at least 35°C.
measurement.
6. Control the pH range – if necessary, add citric acid. Mix
3. Add parfum and Cocamidopropyl Betaine during 3. Add fragrance, PEG-7 Glyceryl Cocoate and colorant
5. If necessary, adjust pH by Citric Acid to 4.8 – 5.5. well after adjustment.
mixing. Mix until homogenous solution is obtained. during mixing. Mix until uniform.
7. Control viscosity if necessary, add Sodium Chloride.
4. Add slowly Cocamidopropyl Betaine during mixing.
Mix until uniform.
Ehylhexyl Glycerine,
1.00 preservative
Phenoxyethanol
Sodium Hydroxide
D q.s pH modifier
(30% solution)
APPEARANCE visual method black, viscous gel APPEARANCE visual method yellow liquid
VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 20°C 15000 – 20000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 - 5000
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. Pour the warm deionized water (40-50°C) into the main 3. Add phase B to phase A. Mix until homogenous 1. Into the large vessel (big enough to provide adequate 4. Adjust pH to 8.5 – 9.0 by using Citric Acid. Mix well
vessel and add the Acrylates/C10-30 Alkyl Acrylate solution is obtained. Cool the batch down to 30°C. mixing while preparing batch) pour deionized water. after adjustment.
Crosspolymer. Start mixing when the agent is completely When the batch is around 30°C, add preservative,
2. Add ingredients from phase A to the vessel while mixing. 5. Add fragrance, preservative and Cocamidopropyl
wetted. Mix until the homogenous solution is obtained. Activated Charcoal and fragrance. Mix for 20 – 30
Heat up to 70 – 75°C. Mix until homogenous solution Betaine. Mix until homogenous solution is obtained.
minutes with slow agitation. If necessery, homogenise
2. Combine ingredients from phase B in a separate vessel. is obtained.
for 1-2 minutes. 6. If necessary, add Sodium Chloride to adjust the viscosity.
Heat up to 60°C with gentle agitation. Mix until
4. Readjust the final pH to 5.5 – 6.5 with additional 3. Cool the batch down to at least 35°C. NOTE: it is very important to equilibrate a sample at
homogenous solution is obtained.
Sodium Hydroxide (30%) if necessary. 25°C for at least one hour to get an accurate viscosity
measurement.
Ehylhexyl Glycerine,
1.00 preservative
Phenoxyethanol Cocamide DEA ROKAmid KAD 0.50 surfactant
APPEARANCE visual method clear yellowish gel APPEARANCE visual method light-green, viscous gel
VISCOSITY [cP] Brookfield LV, spindle 34, speed 4.0 RPM, T: 25°C 3000 – 6000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 3.0 RPM, T: 25°C 2000 - 5000
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. Heat up the water to (40-50°C) and add the ingredients 3. Add Sodium Chloride to adjust the viscosity. NOTE. 1. Combine ingredients from phase A. Mix until uniform. 3. Add Sodium Chloride while mixing. Mix until uniform.
one after another in the order from the table above. Add salt (not in one go) – after addition of each
2. Add phase B ingredients. Mix until uniform. 4. Control viscosity and pH.
portion mix well.
2. Before adding a parfum cool the mixture down to room
temperature and add the rest of ingredients.
SHOWER
GELS
Shower gels are designed to remove dirt, tallow and impurities of the
epidermis, as well as prevent its drying. Products of this type should also
adequately moisturize and nourish the skin.
There are plenty of different shower gels available on the market such as:
• pearly / transparent / coloured products,
• traditional / mild products,
• designed for babies / people with sensitive skin,
• moisturising products.
and many others, although there are general requirements for this type
of cosmetics.
Sodium Benzoate,
0.60 preservative
Sodium Lauroyl Sarcosinate ROKAtend LS 20.00 surfactant Potassium Sorbate
PEG-120 Methyl PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.50 re-oiling agent
B 0.50 thickening agent
Glucose Dioleate
APPEARANCE visual method viscosus, pearl gel APPEARANCE visual method clear, viscosus gel
VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 – 6000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 – 6000
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. Add ingredients from phase A to the hot water (70-75°C). 5. Add pearling agent. Mix until uniform. 1. Add ingredients from phase A to the warm water (55-60°C). 5. Add Sodium Chloride to adjust the viscosity. NOTE.
While mixing add ingredients one after another in the Mix until uniform. Add salt (not in one go) – after addition of each portion
6. Add Sodium Chloride to adjust the viscosity. NOTE.
order from the table above. Mix until uniform. mix well.
Add salt (not in one go) – after addition of each portion 2. Cool the batch down to at least 50°C.
2. Cool the batch down to at least 50°C. mix well. 6. Control the pH range – if necessary, add Citric Acid.
3. Add PEG-120 Methyl Glucose Dioleate and PEG-7
Mix well after adjustment.
3. Add PEG-120 Methyl Glucose Dioleate during mixing. 7. Control the pH range – if necessary, add Citric Acid. Glyceryl Cocoate during mixing. Mix until uniform.
Mix until uniform. Cool the batch down to at least 35°C. Mix well after adjustment. Cool the batch down to at least 35°C.
4. Add fragrance and Coco Betaine during mixing. Mix 8. Control the viscosity, if necessary add Sodium Chloride. 4. Add fragrance and Cocamidopropyl Betaine during
until uniform. mixing. Mix until uniform.
APPEARANCE visual method white viscous gel APPEARANCE visual method black-gold gel
VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 6000 – 9000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 6.0 RPM, T: 25°C 8000 – 15000
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. Pour the warm deionized water (40-50°C) into the 4. Add phase B to main vessel. Mix until homogenous 1. In a main vessel combine ingredients from phase A 3. Combine ingredients from the phase B and mix until
main vessel and add the Acrylates/C10-30 Alkyl Acrylate solution is obtained. If needed, homogenise for 2-3 by adding Xanthan Gum to Glycerin and mixing until uniform. Control the pH range – if necessary, add
Crosspolymer. Start mixing when the agent is completely minutes. homogenous solution is obtained. Then, take 2.5 g of Citric Acid.
wetted. Mix until the homogenous solution is obtained. water from phase A to a separate beaker add Polyqu-
5. Combine ingredients from phase C in a separate vessel. 4. Add phase B to phase A and mix well. Cool the batch
2. Add Sodium Hydroxide. Mix until homogenous solution Heat up to 40°C with gentle agitation. Mix until aternium-7 and mix them well.
down to 30°C and homogenise for 2-3 minutes.
is obtained. homogenous solution is obtained. 2. Add the rest of warm water (50-55°C) from phase A
3. Combine ingredients from phase B in a separate vessel. 6. Add phase C to the main vessel. Mix until homogenous to the main vessel and homogenise for 1-2 minutes.
Add Xanthan Gum to Glycerin – mix until homogenous solution is obtained. Cool the batch down to 30°C. At the and of preparation, mix the solutions, add
solution is obtained. Add warm water (40-50°C) and preservative and homogenise for 2-3 minutes.
7. Add fragrance and preservative. Mix gently until
Polyquaternium-10. Mix until homogenous solution is
homogenous solution is obtained.
obtained. If necessery, homogenise for 2-3 minutes.
Xanthan Gum 0.90 viscosity modifier Xanthan Gum 0.90 viscosity modifier
Ammonium Laureth Sulfate SULFOROKAnol A325/1 24.00 surfactant PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.00 surfactant
Activated Charcoal 0.01 pigment Cocamidopropyl Betaine ROKAmina K30K 3.40 surfactant
Sodium Benzoate,
0.30 preservative
Potassium Sorbate
APPEARANCE visual method black clear gel APPEARANCE visual method colorless clear gel
VISCOSITY [cP] Brookfield LV, spindle 34, speed 6.0 RPM, T: 25°C 6000 – 15000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 6.0 RPM, T: 25°C 7000 – 15000
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. In a main vessel combine ingredients from phase A 3. Combine ingredients from the phase B and mix until 1. In a main vessel combine ingredients from phase A. 3. Add phase B to phase A and mix well. Cool the batch
by adding Xanthan Gum to Glycerin and mixing until uniform. Control the pH range – if necessary, add Add Xanthan Gum to glycerin – mix until homogenous down to 30°C and homogenise for 2-3 minutes.
homogenous solution is obtained. Then, take 2.5 g of Citric Acid. solution is obtained. Then, pour warm water (50-55°C)
water from phase A to a separate beaker add from phase A to the main vessel and mix. Add
4. Add phase B to phase A and mix well. Cool the batch
Polyquaternium-7 and mix them well. preservative. Homogenise for 2-3 minutes.
down to 30°C and homogenise for 2-3 minutes.
2. Add the rest of warm water (50-55°C) from phase A to 2. Combine ingredients from the phase B and mix until
the main vessel and homogenise for 1-2 minutes. At uniform. Control the pH range – if necessary, add Citric
the and of preparation, mix the solutions, add Acid.
preservative and homogenise for 2-3 minutes.
CI 77000,
0.02 pigment
Acrylates Crosspolymer Urea 0.50 active
Sodium Benzoate,
0.30 preservative
Potassium Sorbate
APPEARANCE visual method gold scintillating gel APPEARANCE visual method transparent, viscous gel
VISCOSITY [cP] Brookfield LV, spindle 34, speed 6.0 RPM, T: 25°C 7000 – 15000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 3.0 RPM, T: 25°C 2000 - 7000
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. In a main vessel combine ingredients from phase A. 3. Add phase B to phase A and mix well. Cool the batch 1. Combine ingredients from phase A. Mix until uniform. 3. Add Sodium Chloride while mixing. Mix until uniform.
Add Xanthan Gum to glycerin – mix until homogenous down to 30°C and homogenise for 2-3 minutes.
2. Add ingredients from phase B while mixing. Mix until
solution is obtained. Then, pour warm water (50-55°C)
uniform.
from phase A to the main vessel and mix. Add
preservative. Homogenise for 2-3 minutes.
2. Combine ingredients from the phase B and mix until
uniform. Control the pH range – if necessary, add
Citric Acid.
SHOWER OILS
& BODY WASH
EMULSION
Shower oils and body wash emulsions are suitable for dry and very dry
skin. They gently cleanse and at the same time renew the lipid layer of
the skin.
Shower oils turn into foam when exposed to water what brings a pleasant
feeling to the skin.
They are oftently recommended for washing sensitive, dry skin, but in
winter shower oils will be useful for any skin. They grease it well, rebu-
ild protective film strained by winter conditions, prevent moisture loss,
smooth, soften, nourish and strengthen. They are very delicate, so using
them brings a real pleasure.
After bathing, the skin is lightly dry by a towel with no need to lubricate
it with a moisturizer, because it is slightly oily.
22 Shower oils & body wash emulsion Personal Care - Formulation Guide 23
SHOWER AND BATH OIL [KD-115] MILD BODY WASH EMULSION [KD-80]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION
Phenoxyethanol, Methylparaben,
D 0.80 preservative
Ethylparaben, Propylparaben
Procedure: Procedure:
1. In a main vessel combine ingredients from phase A 3. Add ingredients from phase B to phase A while mixing. 1. In a main vessel combine ingredients from the phase A. 6. Add C into A, stir well with hand stirring, keep A/B at
and mix until uniform. Mix until uniform. 75-80°C. Homogenize with 2000-3000 RPM, 90 sec.
2. Add Xanthan Gum to Glycerin - mix until homogenous
2. Combine ingredients from phase B in a separate vessel solution is obtained. 7. Cool the batch down to 50°C. Add phase D ingredients
and mix until uniform. while mixing. Homogenize with 2500-3500 RPM, 90 sec.
3. Add the phase B components to phase A while mixing.
Mix until uniform. 8. Cool the batch down to 25°C. Add phase E ingredients
while mixing. Homogenize with 2500-3500 RPM, 30 sec.
4. In a separate vesselI combine ingredients from the
phase C.
5. Heat phase A and C to 75-80°C.
24 Shower oils & body wash emulsion Personal Care - Formulation Guide 25
BODY EMULSION [KD-81]
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION
Phenoxyethanol, Methylparaben,
B 0.80 preservative
Ethylparaben, Propylparaben
PEG-7/PPG-2
ROKAnol GA7LAW 1.00 emollient
Propylheptyl ether
pH 5.0 – 7.0
Procedure:
1. In a separate vesselIs combine ingredients from phase 5. Cool the batch down to 25°C. Add phase D ingredients
A, B and C. while mixing. Homogenize with 2500-3500 RPM,
120 sec.
2. Heat phase A and B to 75-80°C.
3. Add B into A, stir well with hand stirring, keep A/B at
75-80°C. Homogenize with 2000-3000 RPM, 120 sec.
4. Cool the batch down to 50°C while mixing. Add phase C
ingredients while mixing. Homogenize with 2500-
3500 RPM, 120 sec.
26 Shower oils & body wash emulsion Personal Care - Formulation Guide 27
Body Treatment
INTIMATE
HYGIENE
The intimate woman place is a unique ecosystem which is inhabited
by over 100 species of microorganisms. Among them are the bacteria,
whose metabolic product like lactic acid protects the vaginal environment
from pathogens. Because of that the pH of intimate area is below 4.5.
B Sodium Laureth Sulfate SULFOROKAnol L227/1 18.00 surfactant B Sodium Laureth Sulfate SULFOROKAnol L227/1 18.00 surfactant
PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.00 surfactant PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.00 surfactant
D Coco Betaine ROKAmina K30B 8.75 surfactant D Coco Betaine ROKAmina K30B 8.75 surfactant
APPEARANCE visual method bright-yellow gel APPEARANCE visual method light-yellow gel
VISCOSITY [cP] Brookfield LV, spindle 34, speed 6.0 RPM, T: 25°C 1000 – 7000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 6.0 RPM, T: 25°C 1000 - 7000
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. In a main vessel combine ingredients from phase A. 4. Add slowly Coco Betaine while mixing. Mix until uniform. 1. In a main vessel combine ingredients from phase A. 4. Add slowly Coco Betaine while mixing. Mix until uniform.
Mix until uniform. Mix until uniform.
5. If nesesery, adjust pH by Lactic Acid to 4.0 – 4.5. 5. If nessesery, adjust pH by Lactic Acid to 4.0 – 4.5.
2. Add ingredients from phase B. Mix until uniform. 2. Add ingredients from phase B. Mix until uniform.
3. Add parfum while mixing. Mix until uniform. 3. Add parfum while mixing. Mix until uniform.
Coco-Glucoside,
B 0.50 surfactant
Sodium Laureth Sulfate SULFOROKAnol L227/1 12.00 surfactant Glyceryl Oleate
APPEARANCE visual method transparent gel APPEARANCE visual method transparent gel
VISCOSITY [cP] Brookfield LV, spindle 34, speed 6.0 RPM, T: 25°C 1000 – 7000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 6 RPM, T: 25°C 2000 – 7000
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. In a main vessel combine ingredients from phase A. 3. Add Parfum while mixing. Mix until uniform. 1. Combine ingredients from phase A. Add ingredients 3. Add Coco Betaine while mixing. Mix until uniform.
Add ingredients from phase A to warm water (40-45°C). from phase A to warm water (40-45°C). Mix until
4. Add slowly Coco Betaine while mixing. Mix until uniform. 4. If necessary, adjust pH by Lactic Acid to 4.0 – 4.5.
Mix until uniform. homogenous solution is obtained. Cool the batch
5. If necessary, adjust pH by Lactic Acid to 4.0 – 4.5. down to at least 30°C.
2. Add ingredients from phase B. Mix until uniform. Cool
the batch down to at least 30°C. 2. Add parfum while mixing.
MEA Lauryl Sulfate ROSULfan M 18.00 surfactant Magnesium Laureth Sulfate EXOsoft MGB 25.00 surfactant
B Coco Betaine ROKAmina K30B 6.00 surfactant Lactic Acid q.s. pH adjuster
C Lactic Acid q.s pH adjuster Coco Betaine ROKAmina K30B 8.00 surfactant
APPEARANCE visual method bright-yellow gel APPEARANCE visual method transparent gel
VISCOSITY [cP] Brookfield LV, spindle 34, speed 6 RPM, T: 25°C 2000 – 7000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.0 RPM, T: 25°C 1000 - 4000
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. Combine ingredients from phase A. Add ingredients 3. If necessary, adjust pH by Lactic Acid to 4.0 – 4.5. 1. Combine ingredients from phase A. Add ingredients 3. Add slowly Coco Betaine and parfum while mixing. Mix
from phase A to water (25-30°C). Mix until homogenous from phase A to water and heat to 50°C. Mix until until uniform.
solution is obtained. homogenous solution is obtained.
2. Add slowly Coco Betaine and parfum while mixing. 2. Cool the batch down to at least 30°C.
Mix until uniform.
Disodium Laureth
Glycerin 1.00 moisturising agent EXOsoft L3/40 4.00 surfactant
Sulfosuccinate
PEG-7 Glyceryl Cocoate ROKAcet KO300G 0.50 surfactant B Panthenol 0.10 active
APPEARANCE visual method pearly gel APPEARANCE visual method bright-yellow liquid
VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 - 8000 STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure:
Procedure: 1. In a main vessel combine ingredients from phase A. 3. Add Cocamidopropyl Betaine and parfum during
Add ingredients from phase A to warm water (40-45°C). mixing. Mix until uniform.
1. In a main vessel combine ingredients from phase A. 3. Add ingredients from phase C and D during mixing. Mix until uniform.
Add ingredients from phase A to warm water (40-45°C). Mix until uniform. 4. If nessesery, adjust pH by Lactic Acid to 4.0 – 4.5.
Mix until uniform. 2. Add PEG-120 Methyl Glucose Dioleate and Panthenol.
Mix until uniform. Cool the batch down to at least 30°C.
2. Add ingredients from phase B. Mix until uniform. Cool
the batch down to at least 30°C.
SKIN CARE
PRODUCTS
Skin Care Products are a big group of cosmetics which are available in
many different categories. Generally each skin care product like balm,
moisturiser or lotion should provide to the skin sufficient nourishment
as well as protection.
In the beauty market there are plenty of brands and products to choose
from. Selection of the suitable product should be connnected with the
skin type and it’s compatibility.
In terms of oily skin, light weight lotion are recommended. In case of dry,
mature skin, moisturiser with a thicker consisitency should be chosen.
Night creams will generally be thicker than a day cream.
A Aqua 2.50 emulsion stabilizer A Cetearyl Alcohol EXOalc 1618 flakes 4.00 emulsion stabilizer
Glyceryl Stearate,
1.50 emulsifier
PEG-100 Stearate Stearic Acid 1.50 rheology modifier
B Aqua 78.35 solvent PPG-15 Stearyl Ether ROKAnol SP15L 8.00 emollient
Phenoxyethanol, Methylparaben,
C 1.00 preservative
C Carbomer 0.30 rheology modifier Ethylparaben, Propylparaben
PPG-15 Stearyl Ether ROKAnol SP15L 1.00 emollient D Parfum 0.50 fragrance
Phenoxyethanol, Methylparaben,
D 1.00 preservative
Ethylparaben, Propylparaben
APPEARANCE visual method white emulsion APPEARANCE visual method white emulsion
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. In a separate vessel combine ingredients from phase 3. Cool the batch down to 50°C while mixing. Add 1. In a separate vesselI combine ingredients from phase 4. Cool the batch down to 50°C while mixing. Add phase C
A, B and C. Heat the phase A and B to 75-80°C. ingredients from phase C and D while mixing. A and B. ingredients while mixing. Homogenise with 2500-3500
Homogenise with 2500-3500 RPM, 120 sec. RPM, 90 sec.
2. Add A into B, stir well with hand stirring, keep A/B at 2. Heat phase A and B to 75-80°C.
75-80°C. Homogenize with 2000-3000 RPM, 120 sec. 4. Cool the batch down to 25°C. Add phase E while 5. Cool the batch down to 25°C. Add phase D ingredients
3. Add A into B while mixing, keep A/B at 75-80°C.
mixing. Homogenize with 2500-3500 RPM, 120 sec. while mixing. Homogenise with 2500-3500 RPM, 30 sec.
Homogenise with 2000-3000 RPM, 120 sec.
Glyceryl Stearate,
A 2.50 emulsifier
PEG-100 Stearate
Acrylates/C10-30 Alkyl
D 0.20 rheology modifier
Acrylate Crosspolymer
Phenoxyethanol, Methylparaben,
E 0.80 preservative
Ethylparaben, Propylparaben
pH 5.0 – 7.0
Procedure:
1. In a separate vesselI combine ingredients from phase 4. Heat phase A and B to 75-80°C.
A and B. 5. Add A into B while mixing, keep A/B at 75-80°C.
2. Add slowly phase D ingredients to phase B while mixing. Homogenise with 2000-3000 RPM, 120 sec.
Mix until uniform. 6. Cool the batch down to 50°C while mixing. Add phase E
3. In a separate vesselI combine ingredients from phase C. ingredients while mixing. Homogenise with 2500-3500
Mix until uniform. Add slowly phase C ingredients to RPM, 90 sec.
phase B while mixing. Homogenise with 2000-3000 7. Cool the batch down to 25°C. Add phase F ingredients
RPM, 90 sec. while mixing. Homogenise with 2500-3500 RPM, 120 sec.
FACE CARE
PRODUCTS
Face Care Products are basic care cosmetics for every woman. Facial
skin is our business card, that is why we should take care of it as best as
possible. Today’s Face Care Cosmetics are multi-tasking, but they also
meet the needs of skin living under strong oxidative stress, which can
lead to loss of collagen and elastin. There are many types of Face Care
products, so it’s worth knowing their purpose and application.
During the day, our skin has different needs than at night, hence the
need to use a different day and night care products. The face care pro-
ducts for the day have a protective function against harmful external
factors. The consistency of the day cosmetic is much lighter than the
night one. Many day cosmteics also have a small UV filter that protects
from sunlight. The night cosmetic is designed to regenerate and nourish
the face. The skin regenerates quickly at night, which is why the cosme-
tic applied during the evening care ritual should contain many nutrients.
Benzyl Alcohol,
Ethylhexylglycerin, 1.00 preservative Aqua 50.20 solvent
Tocopherol
Ethylparaben, Methylparaben,
1.00 preservative
Phenoxyethanol,Propylparaben
Procedure:
Procedure:
1. In a main vessel heat all ingredients to 75-80°C and Gum, Glycerin and warm water (50°C). To obtain
1. Pour the warm deionized water (40-50°C) in to the 3. Add phase B to phase A. Mix until homogenous solution do the same with phase B. homogenous solution, homogenize for 1 min.
main vessel and add the Acrylates/C10-30 Alkyl Acrylate is obtained. Cool the batch down to 30°C.
Crosspolymer. Start mixing when the polymer is com- 2. Pour the hot water form phase B into phase A, mix 4. Combine ingredients from the phase D and mix until
4. When the batch temperature is around 30°C, add pre- well (avoid cooling) and homogenise for 5 minutes. uniform. If necessary, add Citric Acid.
pletely wetted. Mix until the homogenous solution is
servative, Propylene Glycol and fragrance. Then, start cooling the formulation and repeat homo-
obtained. 5. Add phase D and B to main vessel (phase A) and mix
5. Readjust the final pH to 5.5 - 6.5 with addition of genization at 60°C. Do the same at 40°C.
2. Combine ingredients from phase B in a separate vessel. for 5 min, then homogonise for 1 min.
Sodium Hydroxide (30%) if necessary. 3. At the same time, prepare phase C by mixing Xanthan
Heat up to 60°C with gentle agitation. Mix until homo-
genous solution is obtained.
PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.50 re-oiling agent Sodium Lauroyl Glycinate ROKAtend GL 10.00 surfactant
Glycerin 1.00 moisturising agent Sodium Lauroyl Sarcosinate ROKAtend LS 30.00 surfactant
Sodium Lauroyl Sarcosinate ROKAtend LS 34.70 surfactant Propylene Glycol 3.00 solvent
Ehylhexyl Glycerine,
1.00 preservative
Phenoxyethanol PEG-7 Glyceryl Cocoate ROKAcet KO300G 1.60 re-oiling agent
Cocamide DEA ROKAmid KAD 0.50 surfactant Citric acid 0.40 pH modifier
pH 6.0 - 7.5
pH 6.0 - 7.5 (water phase)
STABILITY 1 month st 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. Add ingredients from phase A to the warm water (40-5°C). 3. Control the pH range – if necessary, add Citric Acid. 1. Add ingredients from phase A to the warm water 3. Control the pH range – if necessary, add Citric Acid.
Mix until uniform. Mix well after adjustment. (40-50°C). Mix until uniform. Mix well after adjustment.
2. Then, cool the mixture down to room temperature 2. Then, cool the mixture down to room temperature 4. Add Sodium Chloride to adjust the viscosity. NOTE.
before adding a preservative and add the rest of before adding a preservative and add the rest of Add salt (not in one go) – after addition of each portion
ingredients. ingredients. mix well.
Sodium Benzoate,
0.60 preservative
Potassium Sorbate Disodium Laureth
EXOsoft L3/40 5.00 surfactant
Sulfosuccinate
APPEARANCE visual method viscous pearling gel clear, blue viscous gel with
APPEARANCE visual method
suspended air bubbles
pH 4.8 – 5.5
pH 5.0 – 6.0
VISCOSITY [cP] Brookfield LV, spindle 34, speed 4.0 RPM, T: 25°C 6000 - 9000
STABILITY 1 month at 5°C, RT, 40°C confirmed
STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure:
Procedure:
1. Pour the warm deionized water (40-50°C) in to the 3. Add phase B to phase A. Mix until homogenous solution
1. In a main vessel combine ingredients from phase A. 3. Add phase B to phase A. Mix until homogenous solution main vessel and add the Acrylates/C10-30 Alkyl Acrylate is obtained. Cool the batch down to 30°C.
Add Xanthan Gum to Glycerin - mix until homogenous is obtained. Cool the batch down to 30°C. Crosspolymer. Start mixing when the polymer is
4. When the batch temperature is 30°C, add preservative,
solution is obtained. Add warm water (40-50°C) and completely wetted. Mix until the homogenous solution
4. Adjust pH to 4.8 – 5.5 by using Citric Acid. Mix well fragrance and Sodium Hydroxide. Mix for 20 minutes
preservative. Mix until homogenous solution is obtained. is obtained.
after adjustment. with slow agitation.
Homogenise for 2-3 minutes.
5. Add ingredients from phase C. Mix until homogenous 2. Combine ingredients from phase B in a separate vessel.
5. Readjust the final pH to 5.0 - 6.0 with addition of
2. Combine ingredients from phase B. Add ingredients Heat up to 30°C with gentle agitation. Mix until homo-
solution is obtained. Sodium Hydroxide (30%) if necessary.
from phase B to warm water (40-45°C). Mix until genous solution is obtained.
homogenous solution is obtained.
Helianthus Annuus
Betaine 2.00 active 5.00 emollient
Seed Oil
Cocamidopropyl Betaine ROKAmina K30 3.00 surfactant Magnesium Aluminum Silicate 0.10 rheology modifier
Phenoxyethanol, Methylparaben,
D 0.50 preservative
Ethylparaben, Propylparaben
APPEARANCE visual method pink gel
VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 18000 - 22000
E Parfum 0.30 fragrance
STABILITY 1 month at 5°C, RT, 40°C confirmed
Cellulose acetate 0.35 abrasive
Procedure:
1. Pour the deionized water (25-30°C) into the main 3. Add slowly phase B to phase A while mixing. Mix until emulsion with scrub
APPEARANCE visual method
vessel and add the Acrylates/C10-30 Alkyl Acrylate uniform. particles
Crosspolymer. Start mixing when the polymer is
4. Add Preservative, Cocamidopropyl Betaine and parfum pH 5.0 – 7.0
completely wetted. Mix until the homogenous solution
while mixing. Mix until uniform.
is obtained. Homogenise for 1-2 minutes. STABILITY 1 month at 5°C, RT, 40°C confirmed
Phenoxyethanol, Methylparaben,
0.50 preservative
Ethylparaben, Propylparaben
pH 5.0 – 7.0
Procedure:
1. In a main vessel combine ingredients from the phase B. 4. Add A into B, while mixing, keep A/B at 75-80°C.
Add Pentylene Glycol, Betaine to the water. Add Homogenise with 2000-3000 RPM, 120 sec.
Magnesium Aluminum Silicate while mixing. Homogenise
5. Cool the batch down to 50°C while mixing. Add phase C
with 2000-3000 RPM, 5-6 min.
ingredients while mixing. Homogenise with 2500-
2. In a separate vessel combine ingredients from the pha- 3500 RPM, 120 sec.
se A.
6. Cool the batch down to 25°C.
3. Heat phase A and B to 75-80°C.
MAKE UP
REMOVERS &
MICELLAR FLUIDS
Eye Make-up Remover and micellar fluid products are intended to help
easily remove make-up that has been applied. They help to remove the
applied color and to make sure it easily wipes off using a tissue.
Makeup removal should be part of our daily skin care ritual because it is
healthy for skin.
• washes away cosmetics, impurities and dirt from the surface of our
skin, which could lead to irritation or cause our skin to age more rapidly
• reduces the risk of developing pimples, redness, blackheads and other
types of blemishes
• promotes cellular renewal by eliminating dead skin
• stimulates skin’s microcirculation due to the massage action
• lets our skin breathe
APPEARANCE visual method clear colorless liquid APPEARANCE visual method transparent liquid
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure:
Procedure:
1. Heat up the water to 40-50°C and add the ingredients
one after another in order from the table above. 1. In a main vessel combine ingredients from phase A 4. Add phase B to phase A and mix well.
and heat up to 65-70°C.
2. Before adding a parfum cool down the mixture to room 5. Cool the batch down to at least 30°C while mixing.
temperature and add the rest of ingredients. 2. Combine ingredients from phase B in a separate vessel
and mix until uniform.
3. Add Citric Acid if necessary.
3. Cool the batch down to at least 50°C while mixing.
APPEARANCE visual method transparent liquid APPEARANCE visual method transparent liquid
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure:
Procedure:
1. In a main vessel combine ingredients from phase A and 4. Combine ingredients from phase D in a separate vessel
heat up to 65-70°C. and mix until uniform. 1. Combine ingredients from phase A. Add ingredients 2. Add Sodium Lauroyl Sarcosinate. Mix until uniform.
from phase A to hot water (75-80°C). Mix until homo- Cool the batch down to at least 30°C.
2. Add Xanthan Gum to Glycerin - mix until uniform. Add 5. Add ingredients from phase C, D and E to phase A
genous solution is obtained. Cool the batch down to
phase B to phase A while mixing. Mix until uniform. while mixing. Mix until uniform. 3. If necessary, adjust pH by Citric Acid to 5.0 – 7.0.
at least 50°C.
3. Cool the batch down to at least 50°C.
Phenoxyethanol, Methylparaben,
0.80 preservative
Ethylparaben, Propylparaben
PEG-7/PPG-2
F ROKAnol GA7LAW 2.00 emollient
Propylheptyl ether
APPEARANCE visual method transparent liquid APPEARANCE visual method white emulsion
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. Combine ingredients from phase A. Add ingredients 2. Add ingredients from phase B. Mix until uniform. Cool 1. In a separate vesselI combine ingredients from phase 5. Add A into B, stir well with hand stirring, keep A/B at
from phase A to hot water (75-80°C). Mix until homo- the batch down to at least 30°C. A, B and C. 75-80°C. Homogenise with 2000-3000 RPM, 120 sec.
genous solution is obtained. Cool the batch down to
3. If necessary, adjust pH by Citric Acid to 5.0 – 7.0. 2. Add slowly phase D ingredients to phase B while mixing. 6. Cool the batch down to 50°C while mixing. Add phase E
at least 50°C.
Mix until uniform. ingredients while mixing. Homogenise with 2500-
3500 RPM, 90 sec.
3. Add slowly phase C ingredients to phase B while mixing.
Homogenise with 2000-3000 RPM, 90 sec. 7. Cool the batch down to 25°C. Add phase F ingredients
while mixing. Homogenise with 2500-3500 RPM, 90 sec.
4. Heat phase A and B to 75-80°C.
SHAVING
PRODUCTS
Shaving products are intended to be used to assist in the removal of
unwanted body hair. Those products have to guarantee the ease and
effective shaving for both women and men. Cosmetic category called
“shaving products” beside of typical shaving product include cosme-
tics such as shaving soaps and creams as well as pre- and after shaving
lotions.
The performance of the cream serves as the ultimate test for the formu-
lation and indicates whether the correct blend of ingredients and con-
centrations has been used. In addition, shaving creams often contain
ingredients including: botanicals, essential oil derivatives, chelators, pre-
servatives and other chemicals. Besides modulating performance, these
ingredients can add antiseptic qualities, serve as skin toners, increase
shelf life, etc. but more importantly, they make each formulation unique.
Acrylates/C10-30 Alkyl
0.40 rheology modifier
Acrylate Crosspolymer
Starch Hydroxypropyltrimonium
0.10 conditioner
Chloride
Phenoxyethanol,
0.80 preservative
Ethylhexylglycerin
pH 4.5 – 5.5
Procedure:
1. In a separate vessel combine ingredients from phase A. 2. Homogenise with 2000-3000 RPM, 90-120 sec.
Add slowly Acrylates/C10-30 Alkyl Acrylate Crosspolymer
3. Add phase C ingredients while mixing. Homogenise
to water while mixing. Mix until uniform. Add other
with 2000-3000 RPM, 90-120 sec.
phase A components.
SHAMPOOS
Shampoo is a basic hair care product representing the largest segment
of hair care cosmetics. Typically, hair products are in the form of a visco-
us liquid, that is used for cleaning hair with some exception of waterless
solid form such as bar.
Disodium Laureth
Disodium Laureth EXOsoft L3/40 2.50 surfactant
EXOsoft L3/40 4.00 surfactant Sulfosuccinate
Sulfosuccinate
APPEARANCE visual method turbid gel APPEARANCE visual method viscous, pearl gel
VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 1500 - 5000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 - 6000
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. Add ingredients from phase A to the hot water (70-75°C). 4. Add fragrance, Cocamidopropyl Betaine and preservative
1. Add ingredients from phase A to the hot water (70-75°C). 5. Add PEG-120 Methyl Glucose Dioleate during mixing.
While mixing add ingredients one after another in the during mixing. Mix until uniform.
Mix until uniform. Cool the batch down to at least 35°C.
2. While mixing add ingredients one after another in the order from the table above. Mix until uniform. NOTE.
5. Add pearling agent. Mix until uniform.
order from the table above. Mix until uniform. 6. Add fragrance, preservative and Cocamidopropyl Betaine Add Polyquaternium-10 and mix untill homogenous
during mixing. Mix until uniform. liquid is obtained. Add the rest of the phase A components. 6. Add NaCl to adjust the viscosity. NOTE. Add salt (not
3. Cool the batch down to at least 50°C.
in one go) – after addition of each portion mix well.
2. Cool the batch down to at least 50°C.
4. Control pH range. If necessary, adjust pH by Citric Acid
7. Control the pH range – if necessary, add Citric Acid.
to 5.0 – 7.0. 3. Add PEG-120 Methyl Glucose Dioleate and PEG-7
Mix well after adjustment.
Glyceryl Cocoate during mixing. Mix until uniform.
Cool the batch down to at least 35°C. 8. Control the viscosity if necessary, add Sodium Chloride.
B Aqua 13.00 solvent Ammonium Laureth Sulfate SULFOROKAnol A325/1 35.00 surfactant
Citric Acid 0.20 pH modifier Ammonium Lauryl Sulfate ROSULfan A 15.00 surfactant
Ehylhexyl glycerine,
1.00 preservative Cocamidopropyl Betaine ROKAmina K30 5.00 surfactant
Phenoxyethanol
APPEARANCE visual method viscosus milky gel APPEARANCE visual method bright-green clear liquid
VISCOSITY [cP] Brookfield LV, spindle 34, speed 3.0 RPM, T: 25°C 9000 - 11000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 2000 - 5000
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. In a main vessel combine ingredients from the phase A. Add the rest of the phase B components. Mix until uni- 1. During mixing add Citric Acid and polyquaternium-10 4. Add parfum and Cocamidopropyl Betaine during mixing.
Add Xanthan Gum to Glycerin - mix until homogenous form. to warm water (40-45°C). Mix until homogenous solution Mix until homogenous solution is obtained.
solution is obtained. Add warm water (50-55°C) and is obtained.
3. Add phase B to phase A. Mix until homogenous solution 5. If necessary, add Sodium Chloride to adjust the viscosity.
Microcrystalline Cellulose. Mix until homogenous solution
is obtained. Cool the batch down to 30°C. 2. Add ingredients from phase A to warm water (40-45°C).
is obtained. Homogenise for 2-3 minutes. 6. Control pH range – if necessary, add Citric Acid. Mix well
While mixing add ingredients one after another in the
4. When the batch temperature is 30°C, add parfum and after adjustment.
2. Combine ingredients from the phase B. During mixing order from the table above. Mix until uniform.
preservative. Mix until uniform.
add Citric Acid and Polyquaternium-10 to warm water
3. Add phase B to phase A. Mix until homogenous solution is
(50-60°C). Mix until homogenous solution is obtained.
obtained. Cool the batch down to 35°C.
PRODUCTS
DEDICATED
TO BABIES
The skin of infants, babies and children require special treatment. Each
product form this category has to be developed in a way to support
the natural functions of the skin. Carefully selected ingredients work to-
gether and strengthen each other, making cosmetics very effective in
contact with even the most delicate, sensitive and problematic skin.
Cosmetic products dedicated to babies must be safe for the health of in-
fants and should only contain ingredients that are non-toxic; potent aller-
gens or substances with endocrine disrupting activity should not be present
and preservatives should be used at their lowest effective concentrations.
Detailed recommendations for baby creams and lotions were agreed by
experts in the field to provide guidance to manufacturers and safety asses-
sors.
APPEARANCE visual method clear, light-yellow gel APPEARANCE visual method transparent, viscous gel
VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 1500 - 5000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 - 9000
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. Combine ingredients from phase A. Add ingredients 4. Add parfum and Cocamidopropyl Betaine during 1. In a main vessel combine ingredients from the phase A. 3. When the batch temperature is 35°C, add Cocami-
from phase A to warm water (55-60°C). Mix until mixing. Mix until uniform. Add Xanthan Gum to Glycerin - mix until homogenous dopropyl Betaine during mixing. Mix until uniform.
homogenous solution is obtained. solution is obtained. Add warm water (50-55°C). Mix
5. If necessary, adjust pH by Citric Acid to 5.0 – 5.5. 4. Control the pH range – if necessary, add Lactic Acid.
until homogenous solution is obtained. Homogenise
2. Add PEG-120 Methyl Glucose Dioleate during mixing. Mix well after adjustment.
for 2-3 minutes.
Mix until uniform.
2. Add the phase B components. Mix until uniform. Cool
3. Cool the batch down to 35°C.
the batch down to 35°C.
Disodium Laureth
B EXOsoft L3/40 2.00 surfactant
Sodium Benzoate, Sulfosuccinate
0.50 preservative
Potassium Sorbate
Coco-Glucoside,
0.50 surfactant
B Sodium Lauroyl Sarcosinate ROKAtend LS 4.00 surfactant Glyceryl Oleate
PEG-120 Methyl
C 0.50 thickener D Cocamidopropyl Betaine ROKAmina K30 6.00 surfactant
Glucose Dioleate
APPEARANCE visual method hazy, viscosus gel APPEARANCE visual method bright-yellow, viscous gel
VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 - 9000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 2000 - 8000
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. Combine ingredients from phase A. Add ingredients 3. Add PEG-120 Methyl Glucose Dioleate while mixing. 1. Combine ingredients from phase A. Add ingredients 4. Add Cocamidopropyl Betaine during mixing. Mix until
from phase A to warm water (55-60°C). Mix until Mix until uniform. Cool the batch down to at least 30°C. from phase A to warm water (55-60°C). Mix until uniform.
homogenous solution is obtained. Cool the batch homogenous solution is obtained. Cool the batch
4. Add Cocoamidopropyl Betaine while mixing. Mix until 5. If necessary, adjust pH by Lactic Acid to 4.8 – 5.3.
down to at least 50°C. down to at least 50°C.
uniform.
2. Add ingredients from phase B durin mixing. Mix until 2. Add ingredients from phase B. Mix until uniform.
uniform.
3. Add PEG-120 Methyl Glucose Dioleate during mixing.
Mix until uniform. Cool the batch down to at least 30°C.
Sodium Benzoate,
0.50 preservative
Disodium Laureth Potassium Sorbate
B EXOsoft L3/40 5.50 surfactant
Sulfosuccinate
APPEARANCE visual method transparent liquid APPEARANCE visual method light-yellow liquid
STABILITY 1 month at 5°C, RT, 40°C confirmed VISCOSITY [cP] Brookfield LV, spindle 34, speed 10 RPM, T: 25°C 1000 - 3000
Procedure:
1. Combine ingredients from phase A. Add ingredients 4. Add Cocamidopropyl Betaine during mixing. Mix until Procedure:
from phase A to warm water (45-50°C). Mix until uniform.
homogenous solution is obtained. 1. Combine ingredients from phase A. Add ingredients 3. Add Cocoamidopropyl Betaine during mixing. Mix
5. Readjust the final pH to 5.0 - 6.5 with additional Lactic
from phase A to warm water (50-55°C). Mix until until uniform.
2. Add Disodium Laureth Sulfosuccinate during mixing. Acid.
homogenous solution is obtained. Cool the batch
Mix until uniform.
down to at least 50°C.
3. Add PEG-120 Methyl Glucose Dioleate during mixing.
2. Add ingredients from phase B while mixing. Mix until
Mix until uniform. Cool the batch down to at least 30°C.
uniform. Cool the batch down to at least 30°C.
A Aqua 71.35 solvent PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION
B Ammonium Laureth Sulfate SULFOROKAnol A325/1 15.00 surfactant Glycerin 2.00 moisturising agent
APPEARANCE visual method light-yellow liquid APPEARANCE visual method light-yellow gel
VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 1000 - 3000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 1000 - 4000
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. Combine ingredients from phase A. Add ingredients 3. Add PEG-120 Methyl Glucose Dioleate and Coco- 1. Combine ingredients from phase A. Add ingredients 4. Add phase C to the main vessel while mixing. Mix until
from phase A to warm water (50-55°C). Mix until Glucoside, Glyceryl Oleate during mixing. Mix until from phase A to water (30-35°C). Mix until homogenous uniform.
homogenous solution is obtained. uniform. Cool the batch down to at least 30°C. solution is obtained. Cool the batch down to at least 30°C.
5. Add Cocoamidopropyl Betaine while mixing. Mix until
2. Add ingredients from phase B durin mixing. Mix until 4. Add slowly Coco Betaine during mixing. Mix until 2. Add ingredients from phase B. Mix until uniform. uniform.
uniform. uniform.
3. Combine ingredients from phase C in a separate vessel. 6. If necessary, adjust pH by Lactic Acid to 4.8 – 5.2.
Add Parfum to Polysorbate 20 - mix until uniform.
PHASE INCI NAME BRAND NAME CONCENTRATION [%] FUNCTION A Aqua up to 100 solvent
Sodium Benzoate,
0.50 preservative
Potassium Sorbate Benzophenone-4 0.05 UV filter
PEG-7 Glyceryl Cocoate ROKAcet KO300G 0.50 surfactant B Ammonium Laureth Sulfate SULFOROKAnol A325/1 30.00 surfactant
C Cocamidopropyl Betaine ROKAmina K30 6.00 surfactant PEG-7 Glyceryl Cocoate ROKAcet KO300G 0.50 surfactant
APPEARANCE visual method transparent liquid APPEARANCE visual method pearl, light-blue gel
VISCOSITY [cP] Brookfield LV, spindle 34, speed 12 RPM, T: 25°C 1000 - 4000 VISCOSITY [cP] Brookfield LV, spindle 34, speed 2.5 RPM, T: 25°C 3000 - 8000
STABILITY 1 month at 5°C, RT, 40°C confirmed STABILITY 1 month at 5°C, RT, 40°C confirmed
Procedure: Procedure:
1. Combine ingredients from phase A. Add ingredients 4. Add Sodium Chloride during mixing (Add small 1. In a main vessel combine ingredients from phase A. 4. Add slowly Cocoamidopropyl Betaine while mixing.
from phase A to water (55-60°C). Mix until uniform. portions and dissolve). Heat up to 55-60°C. Mix until uniform. Mix until uniform.
Cool the batch down to at least 50°C.
5. If necessary, adjust pH by Lactic Acid to 4.8 – 5.3. 2. Add Ammonium Laureth Sulfate. Mix until uniform. 5. Add ingredients from phase E. Mix until uniform.
2. Add PEG-120 Methyl Glucose Dioleate during mixing.
3. Add ingredients from phase C. Mix until uniform. Cool 6. Add Sodium Chloride while mixing (Add small portions
Mix until uniform. Cool the batch down to at least 30°C.
the batch down to 30°C. and dissolve).
3. Add Cocamidopropyl Betaine and Parfum during
mixing. Mix until uniform.