Polycold Maxcool Series
Polycold Maxcool Series
Including Models:
MaxCool 4000H
MaxCool 2500L
214072 Revision B
Polycold Cryochiller
Installation and Operation Manuall
Information provided within this document is subject to change without notice, and although believed to be
accurate, Brooks Automation assumes no responsibility for any errors, omissions, or inaccuracies.
AcuLigner™, Align™, AquaTran™, AutoTeach™, ATR™, AXM™, Basic Blue™, BiSymmetrik™,
CenterSmart™, Cool Solutions™, Crate to Operate™, e-RMA™, e-Spares™, e-Volution™, FastRegen™,
FIXLOAD™, FrogLeg™, InLigner™, InCooler™, Interface™, Jet Engine™, LowProfile™, M2 Nano™,
Mini-Ion™, PASIV™, PowerPak™, PerformanceBlue™, PowerTools™, QuadraFly™, Radius™, Radient™,
Radient Express™, Reliance™, Reliance ATR™, RetroEase™, SCARA™, SmartPM™,
SPOTLevel™, Synetics™, The New Pathway to Productivity™, Time Optimized Trajectory™, Time Optimal
Trajectory™, Time Optimized Path™, TopCooler™, TopLigner™, Ultimate Blue™, VAC-407™, VacuTran™,
Vacuum Quality Monitor™, VQM™, Vacuum Quality Index™, VQI™, and the Brooks logo are trademarks of
Brooks Automation, Inc.
AcuTran®, AquaTrap®, Conductron®, Convectron®, the Cool Solutions logo, Cryodyne®, Cryotiger®,
Cryo-Torr®, Fusion®, GOLDLink®, Granville-Phillips®, Guardian®, GUTS®, Helix®, Jet®, Leapfrog®,
MagnaTran®, MapTrak®, Marathon®, Marathon 2®, Marathon Express®, Micro-Ion®, MiniConvectron®,
On-Board®, Polycold®, Razor®, Simplicity Solutions®, the Simplicity Solutions logo, Stabil-Ion®, TrueBlue®,
TurboPlus®, Vision®, Zaris®, and the Brooks Automation logo are registered U.S. trademarks of Brooks
Automation, Inc.
Corporate Headquarters
15 Elizabeth Drive, Chelmsford, MA 01824 USA
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Installation and Operation Manual
Contents
Introduction
Using This Manual . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-1
System Illustration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-2
System Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-3
Definitions: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-3
About the Polycold MaxCool Cryochiller . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-3
Polycold Cryochiller Versions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-4
Theory of Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-4
Water Vapor Capturing in High Vacuum Systems . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-5
Minimizing Oil Backstreaming From Diffusion Pumps . . . . . . . . . . . . . . . . . . . . . . . . . . .1-6
Heat Removal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-7
Polycold Cryochiller System Components . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-8
Polycold Cryochiller Component List . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-8
Polycold Cryochiller Views. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-10
Regulatory Compliance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-13
Declaration of Conformity (DOC). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-13
Declaration of Incorporation (DOI). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-14
Disclosure Table, EIP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-15
Limited Warranty . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1-16
Safety
Explanation of Hazard Alerts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-1
Safety Text . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-1
Safety Icons . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-1
Signal Words and Color. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-2
Alert Example . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-2
Use of Notes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-2
General Guidelines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-3
Safety Labels and Safety Label Identification. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-4
Label Identification and Location . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-4
Safety and Operational Interlocks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-9
Cryochiller Lockout/Tagout . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-12
Mechanical Hazards . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-12
Electrical Hazards. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-14
Thermal Hazards . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2-15
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Installation and Operation Manual
Installation
Installation Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-2
Installation Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-3
Component Description . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-3
Installing a Refrigeration Unit to Meet ASHRAE Requirements . . . . . . . . . . . . . . . . . . . 4-3
Inspect and Unpack the Polycold Cryochiller . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-4
Move to Location. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-7
Remove the Compressor Hold-Down Nuts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-9
Connect the Cooling Water . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-10
Connect Electrical Power . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-13
Input Power Transformers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-16
Install the Cryosurface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-17
Install the Feed-Through and Cryocoil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-17
Install a Cryobaffle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-19
Install the Refrigerant Lines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-19
Guidelines for Refrigerant Lines. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-20
Route and Install the Refrigerant LInes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-21
Install Parker UltraSeal Compatible Couplings (Standard Fitting) . . . . . . . . . . . . . . . . . 4-24
Install Cajon VCR Couplings (Optional Fitting) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-25
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Installation and Operation Manual
Interfacing
General Interface Information. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-1
General Interface Rules. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-2
RS-232 Interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-2
Gauge Relay (J4) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-3
Human Machine Interface - HMI. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-4
Navigation Keys . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-4
Cool/Standby/Heat Keys . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-4
Remote Key . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-4
OK LED . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-4
Fault LEDs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-5
Reset Button . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-5
HMI Display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-5
HMI Home Screen Display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-6
HMI Top Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-7
System Status . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-8
Configuration Page 1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-9
Configuration Page 2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-10
Control Parameters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-11
Set Comm Parameters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-12
Basic Service . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-13
Ethernet . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-14
Profibus . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-15
DeviceNet . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-16
24V DI/DO Remote Interface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-17
24 V DI/DO Single Circuit Non-Isolated. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-20
24 V DI/DO Dual Circuit Non-Isolated . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-21
24 V DI/DO Single Circuit Isolated . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-22
24 V DI/DO Dual Circuit Isolated . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-23
24V DI/DO Remote Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-24
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Installation and Operation Manual
Operation
Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-1
System Components. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-2
Local Controls and Indicators . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-3
HMI Keypad . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-3
LED Status Table . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-5
Single Circuit Modes of Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-5
Standby . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-5
Cool . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-6
Cool Mode Selection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-6
Defrost . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-6
Defrost Mode Selection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-6
Dual Circuit Modes of Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-7
One Circuit Standby and One Circuit Cool. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-7
One Circuit Defrost and One Circuit Cool . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-7
One Circuit Defrost versus One Circuit Standby . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-7
Compressor Safety Chain . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-7
Polycold Cryochiller Startup . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-8
System Boot/Power-Up . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-8
Compressor Startup . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-9
Alternate Compressor Startup . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-9
Operating the Polycold Cryochiller with a Cryocoil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-9
Start and Cool the System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-9
Defrost the Cryocoil . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-10
Operating the Polycold Cryochiller with a Cryobaffle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-11
Standby and Cool Modes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-11
Defrost the Cryobaffle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-11
Host Commands
Command Group Listing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-1
Command Format . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-2
Command Format . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-2
Response Format. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-2
Command Terms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-3
32 Bit Numbered Bitfield . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-3
Checksum Calculation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-4
Excel Macro for Checksum Calculation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-5
Example of Interface Usage:. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-6
Example of a Get Host Command . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-6
Example of a Set Host Command . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-6
Set Command Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-7
Security Levels . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-7
Example of Security Level . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-8
Command Listing Format . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-8
ABC_DEF Description of the Command . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-8
Commonly Used Host Commands . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7-8
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Contents Polycold Cryochiller
Installation and Operation Manual
Configuration
About System Configuration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-1
Power Management - Cylinder Unloading . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-2
Power Management in Standby Mode . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-2
Power Management in Cool Mode. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-2
Mode Selection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-3
Standby . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-3
Cool Mode Selection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-3
Defrost Mode Selection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-3
Alternate Thermocouple Control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-3
External Vacuum Control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-4
Set Point Relays . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-4
Remote Control Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8-4
Preventive Maintenance
Preventive Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-1
Preventive Maintenance Schedules . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-2
Troubleshooting
Troubleshooting Techniques . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-1
Define the Problem . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-1
Contacting Authorized Service. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-1
Troubleshooting Tables . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-2
Fault Reporting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-2
HMI and Observed Errors . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-3
Power Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-3
Communication Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-3
Compressor Motor Troubleshooting. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-4
Fan Fault Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-5
Pressure Related Troubleshooting. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-6
Temperature Related Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-7
Performance Related Troubleshooting. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-9
Date or Time Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10-9
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Polycold Cryochiller Contents
Installation and Operation Manual
Appendices
Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-1
Appendix A: Contact Brooks Information. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-1
Customer Support Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-2
Appendix B: Lifting Rings (Optional). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-3
Appendix C: CB2 Excepted Wiring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-5
Appendix D: Remote EMO . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-6
EMO Status . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-6
EMO Remote Control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-6
Remote EMO Connector Wiring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-7
Appendix E: Water Vapor Cryotrapping . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-8
Cryosurface Pumping Efficiency . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-8
Appendix F: Feedthroughs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-10
About Feedthroughs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-10
Appendix G: Zero Line Loss Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-13
Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-13
Appendix H: Rapid Balance Pressure Check . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-19
Static Pressure versus Rapid Balance Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-19
Rapid Balance Pressure Check Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-19
Appendix I: Disconnect, Packing, and Shipping Instructions. . . . . . . . . . . . . . . . . . . . . . . . . .12-20
Packing Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-21
Appendix J: Material Safety Data Sheets - MSDS. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-21
MSDS - Refrigerant Gas . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-22
MSDS - POE Solest Oil LT-32 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-29
Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
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Contents Polycold Cryochiller
Installation and Operation Manual
Brooks Automation
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Polycold Cryochiller
Installation and Operation Manual
1 Introduction
This product is intended for use by industrial customers and should be serviced only by Brooks or
Brooks trained representatives. The manuals and related materials are provided in English at no charge
and are intended for use by experienced technicians. It is the responsibility of the user to obtain and
assure the accuracy of any needed translations of manuals. If you require assistance please contact
Brooks service department. Contact information can be found at: www.brooks.com.
This manual provides information for a wide variety of Polycold Cryochiller configurations. Some of the
features that are shown are optional and may not be installed on your system. Refer to Brooks Automa-
tion sales literature to determine what items are optional.
There may be additional installation, maintenance, troubleshooting, and repair information in other
manuals which may affect the settings or operation of the Polycold Cryochiller. When integrated in a
system, the Polycold Cryochiller may be set to system specifications. Before adjusting or changing set-
tings, consult the appropriate system documentation.
All documents that are referenced in this manual refer to documents of the latest revision as of the pub-
lication date of this manual. Brooks Automation Technical Support issues Technical Support Bulletins
(TSBs) to notify the owners of record of any field retrofits.
Pressures are stated as gauge (i.e., psig) not absolute. Psig is pounds per square inch gauge and kPa
is Kilopascals gauge. kPa = 6.895 x Psig. bar = Psig ÷ 14.5
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Introduction Polycold Cryochiller
System Illustration Installation and Operation Manual
System Illustration
Circuit 1
Lift Rings (optional) Refrigerant
Lines
Feed (left)
Return (right)
EMO Switch
(optional)
(optional)
Circuit 2
HMI Refrigerant
Display Lines
and Feed (left)
Keypad Return (right)
Communications
Panel
Circuit
Breakers
Power In
Water In / Out
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Polycold Cryochiller Introduction
Installation and Operation Manual System Summary
System Summary
Definitions:
Refrigeration Unit: The device that compresses, cools, and pumps the refrigerant through the refrig-
erant line and cryosurface.
Refrigerant Line: Typically an insulated bundle that contains feed and return hoses that transfer refrig-
erant between the Polycold Cryochiller refrigeration unit and the cryosurface.
Cryosurface: The cold element that is installed in the customer's vacuum chamber. Cryosurfaces are
usually shaped as a coil to capture water vapor or as a baffle to capture backstreaming oil.
The MaxCool Cryochiller is a closed loop cryogenic refrigeration system with many applications. It is
frequently used to capture water vapor and other condensable substances by freezing them onto a cold
surface such as a cryocoil (Meissner trap) or chevron baffle. This Cryochiller is also used to cool and
heat objects such as electrostatic chucks used in semiconductor wafer processing.
The Polycold MaxCool Cryochiller consists of a refrigeration unit, refrigerant line set, and a cryosurface
with cryogenic feedthrough. The refrigeration unit can pump cold or hot refrigerant in a continuous loop
through the refrigerant lines and cryosurface. The innovative cryogenic refrigeration process in the
Polycold Cryochiller uses patented refrigerant mixtures and patented control processes developed by
Brooks Automation Polycold Systems.
Some configurations include advanced controls that reduce power consumption. Models are available
that control two independent circuits, providing greater design flexibility for vacuum systems such as
two cryocoils or one cryocoil and one cryobaffle. All models include both local and remote operation.
Optional features can be selected to add advanced performance and remote communications features
that enhance productivity and add convenience. Some of these optional features include:
• Additional sound attenuation
• Compliance with SEMI S2 and F-47 standards
• Process heating
• Ethernet, Profibus, DeviceNet, or 24V DI/DO remote interfaces
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Introduction Polycold Cryochiller
Theory of Operation Installation and Operation Manual
The Polycold Cryochiller is manufactured in different models and configurations to fit a variety of appli-
cations. Table 1-1 shows the currently manufactured Cryochiller model numbers and their description.
Contact Brooks Sales for optional configurations.
Configuration Description
MaxCool 4000H Optimized for maximum water vapor cryopumping speed and maxi-
mum vacuum process throughput (formerly XC-8800 HC)
MaxCool 2500L Optimized for minimum water vapor partial pressure and maximum
vacuum process quality (formerly XC-8800 MT)
Theory of Operation
The Polycold MaxCool Cryochiller employs a patented non-flammable HCFC-free refrigerant mixture in
an auto-refrigerating cycle (ARC) cooling process to provide operating temperatures from -80°C to
-150°C.
This process, which is thermodynamically more efficient than a multistage cascade process, combines
all of its refrigerants into a single multi-component stream circulated by one compressor.
The advantages of the mixed refrigerant ARC cooling process are reduced system complexity, more
favorable operating conditions, lower maintenance, and greater reliability.
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Polycold Cryochiller Introduction
Installation and Operation Manual Theory of Operation
Water vapor can be up to 95% of the residual gas in high-vacuum chambers and is typically the most
reactive contaminant in such systems. The exceptionally high water vapor pumping speed provided by
the Cryochiller greatly increases product throughput and produces higher film quality, better adhesion,
and more reproducible deposition.
When capturing water vapor in high vacuum systems, the cryosurface is normally a coil. A rapid inter-
change between the cold and defrost states frees up valuable cycle time and increases product
throughput.
As the vacuum chamber begins the pump down sequence, the pre-programmed Polycold Cryochiller
can exit the Standby mode and quickly cool the cryocoil, providing much higher pumping speeds than
traditional vacuum pumps and significantly reducing chamber pump down time.
During the deposition process, the Polycold Cryochiller remains in the Cool mode to greatly reduce
water vapor contamination and increase product yield. During chamber venting, the Polycold Cryo-
chiller quickly heats the cryocoil to defrost and sublime the captured water vapor.
In this application, the cryocoil can be mounted directly in the vacuum chamber so conductance is not
limited by ports, manifolds, valves and baffles. The cryocoil is easy to install and can be adapted to fit
any system. It does not need a high vacuum valve. See Figure 1-3 on page 1-6.
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Introduction Polycold Cryochiller
Theory of Operation Installation and Operation Manual
A
B
Legend:
A. Polycold Cryochiller Refrigeration Unit
B. Refrigerant line
C. Cryogenic feedthrough
D. Vacuum chamber wall
E. Cryosurface
Backstreaming can occur any time oil diffusion pumps are used in high vacuum systems. Hot oil vapor
from a diffusion pump can migrate into the vacuum chamber and contaminate the system.
An optically-opaque cryogenic chevron baffle that is cooled by the Polycold Cryochiller is placed over
the diffusion pump to greatly reduce oil contamination due to backstreaming. This baffle also provides
additional water vapor pumping speed to the vacuum tool. This greatly improves vacuum system clean-
liness and leads to greater product quality and yield. Quick cooling and defrosting is not typically
required for such an application because the cold cryobaffle remains isolated behind a high vacuum
valve whenever the chamber is vented to atmosphere. See Figure 1-4 on page 1-7.
Optically transparent cryobaffles are also available from Brooks Automation Polycold. These baffles are
appropriate for increased water vapor pumping speed in turbomolecular pump applications.
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Polycold Cryochiller Introduction
Installation and Operation Manual Theory of Operation
B C
Figure 1-4: Polycold Cryochiller Used with Optically Opaque Baffle to Minimize Oil Backstreaming
Legend:
A. Polycold Cryochiller Refrigeration Unit
B. Refrigerant line
C. High vacuum valve
D. Cryobaffle
E. Oil diffusion pump
Heat Removal
The Polycold MaxCool Cryochiller is also used in applications requiring high power cooling to temper-
ature as low as -150°C.
There are a wide variety of heat removal applications, but two notable examples include the cooling of
external heat exchangers that chill a gas or a liquid and the cooling of refrigerant-cooled chucks that
control the temperature of semiconductor wafers and other substrates during a manufacturing process
in vacuum. See Figure 1-5.
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214072 Revision B 1-7
Introduction Polycold Cryochiller
Polycold Cryochiller System Components Installation and Operation Manual
B C
D E
Legend:
A. Polycold Cryochiller Refrigeration Unit
B. Refrigerant line
C. Feedthrough
D. Chamber Wall
E. Cool Plate
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Polycold Cryochiller Introduction
Installation and Operation Manual Polycold Cryochiller System Components
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Introduction Polycold Cryochiller
Polycold Cryochiller System Components Installation and Operation Manual
18
17
19
16
2
15
14
13
12
11
10
5 6 7 8
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Polycold Cryochiller Introduction
Installation and Operation Manual Polycold Cryochiller System Components
23
20
22
21
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Introduction Polycold Cryochiller
Polycold Cryochiller System Components Installation and Operation Manual
24
25
Limitations
This product is intended for use by industrial customers and should be serviced only by Brooks or
Brooks trained representatives.
The Installation and Operation manual and related materials are provided in English at no charge and
are intended for use by experienced technicians. It is the responsibility of the user to obtain and assure
the accuracy of any needed translations of manuals.
If you require assistance, please contact Brooks service department. Contact information can be found
at www.brooks.com.
Brooks Automation
1-12 214072 Revision B
Polycold Cryochiller Introduction
Installation and Operation Manual Regulatory Compliance
Regulatory Compliance
The Polycold Cryochiller meets the requirements of the European Union’s Machinery Directive
(2006/42/EC), the Low Voltage Directive (2006/95/EC), and the EMC Directive (2004/108/EC).
Brooks Automation has issued a Declaration of Conformity for units that are used independently from
a system, and the Polycold Cryochiller has a CE mark affixed.
Brooks Automation
214072 Revision B 1-13
Introduction Polycold Cryochiller
Regulatory Compliance Installation and Operation Manual
When the Polycold Cryochiller is supplied for integration into a system, the final integrator is overall
responsible for conformity to the applicable directives and safety systems. When the system has the CE
mark, the Cryochiller becomes an incorporated component and the attached Declaration of Incorpora-
tion applies.
x That this partly completed machinery conforms with the provisions of Electromagnetic
Compatibility Directive 2004/108/EC.
o EN 61000-6-4
o EN 61000-6-2
x That this partly completed machinery fulfills all the relevant provisions of Directive 97/23/EC
(Pressure Equipment Directive).
o PED Category: II
o Conformity Assessment: Module A1
o Notified Body: TÜV SÜD Industrie Service GMBH (NB #0036)
WestendStrasse, 80686, Munchen, Germany
o Standards: EN 378, EN 60204-1, EN ISO 12100-1, -2
x We will transmit, in response to a reasoned request by a national authority, relevant information
on the partly completed machinery, on paper or in electronic form, without prejudice to our
intellectual property rights.
The partly completed machinery must not be put into service until the final machinery into which it is
incorporated has been declared in conformity with the provisions of Directive 2006/42/EC
Signature
Brooks Automation
1-14 214072 Revision B
Disclosure Table, EIP, Polycold Cryochiller Part Number 192189 Revision B
Brooks Automation
214072 Revision B
Polycold Cryochiller
Disclosure Table
February 5, 2013
Installation and Operation Manual
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Mercury Hexavalent Polybrominated Polybrominated
Lead Cadmium
(Hg) Chromium Biphenyls Diphenyl Ethers
(Pb) (Cd)
(Cr(VI)) (PBB) (PBDE)
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O:␜年Ქኂ‛德年ㇱઙᚲဋ൪᧚ᢱਛ⊛㊂ဋ SJ/T11363-2006 屓ቯ⊛㒢㊂ⷐ᳞એਅޕ
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All assemblies listed above comply with China RoHS temporarily allowed exemptions limit from The Key Catalog for Controlling Pollution by Electronic Information
Products (Batch 1)
Brooks Automation
15 Elizabeth Drive
Chelmsford, MA 01824 USA
REVISION HISTORY:
Revision A: 5/15/2012 Initial Release per EC # 57074 L. Case
Revision B: 2/5/2013 Updated product names per EC# 63451 L. Case
1-15
Introduction
Regulatory Compliance
Introduction Polycold Cryochiller
Regulatory Compliance Installation and Operation Manual
Limited Warranty
Limited Warranty
Polycold® Systems Cooling Products, CryoTiger®,AquaTrap®, Polycold Compact Cooler, Repair
Table A
Product New Product Repair Service
Warranty Warranty
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Brooks Automation
1-16 214072 Revision B
Polycold Cryochiller
Installation and Operation Manual
2 Safety
Failure to review the Safety chapter and follow the safety warnings
can result in death or serious injury.
• Do not perform installation, operation, or maintenance proce-
dures until you have read and understand the safety information.
• Follow all applicable facility safety codes
• Read and understand each procedure before performing it.
If additional safety related upgrades or newly identified hazards associated with the Polycold Cryo-
chiller are identified, Brooks Automation Technical Support notifies the owner of record with a Technical
Support Bulletin (TSB).
Safety Text
Safety Icons
• Hazard alerts contain Safety Icons that graphically identify the hazard.
• The safety icons in this manual conform to ISO 3864 and ANSI Z535 standards.
Brooks Automation
214072 Revision B 2-1
Safety Polycold Cryochiller
Explanation of Hazard Alerts Installation and Operation Manual
Alert Example
Type of Hazard
ELECTRICAL SHOCK HAZARD
Contact with electrical power can cause death or serious injury. Cause and Severity
of Hazard
To avoid electrical shock, disconnect the power before trouble-
shooting the electrical components. How to Avoid
the Hazard
Figure 2-1: Components of a Safety Alert
Use of Notes
This manual uses notes to make the reader aware of additional information. Information in notes is not
related to human or equipment safety. A note does not use icons. The following is an example of a Note.
NOTE: Save all shipping materials for future use. If the Polycold Cryochiller is shipped, the original
shipping crate must be used.
Brooks Automation
2-2 214072 Revision B
Polycold Cryochiller Safety
Installation and Operation Manual Explanation of Hazard Alerts
General Guidelines
Unauthorized Service
Operation or service by untrained or unauthorized personnel may
result in personal harm or damage to equipment.
• Only qualified personnel who have received certified training and
have the proper qualifications for their jobs are allowed to trans-
port, assemble, operate, or maintain the Product.
• Only Brooks parts are authorized to be used when configuring or
repairing this system.
Proper Operation
Improper use of the Polycold Cryochiller may cause personal
injury.
• Do not operate the Polycold Cryochiller before it is properly
installed.
• Do not modify connectors or cables.
• Do not operate the unit without all guards and safety devices in
place.
• Do not install or operate the Polycold Cryochiller if it has been
dropped, damaged, or is malfunctioning.
• Do not use the Polycold Cryochiller for any purpose other than
as a cryochiller or damage to the Cryochiller or the equipment to
which it is connected may occur.
Seismic Restraint
The use of the Polycold Cryochiller in an earthquake prone envi-
ronment may cause equipment damage or personal harm.
• The user is responsible for determining whether the product is
used in an earthquake prone environment
• The user is responsible for providing appropriate seismic
restraint in accordance with local regulations.
Brooks Automation
214072 Revision B 2-3
Safety Polycold Cryochiller
Safety Labels and Safety Label Identification Installation and Operation Manual
NOTICE
Do not change or remove the safety labels or equipment identification labels.
Table 2-1 lists the labels that are affixed to the Polycold Cryochiller. These labels alert personnel to haz-
ards on or within the product and provide information about the product.
Figure 2-2 shows the location of each label. To replace a lost or damaged label call Brooks Automation
Technical Support.
Brooks Automation
2-4 214072 Revision B
Polycold Cryochiller Safety
Installation and Operation Manual Safety Labels and Safety Label Identification
Brooks Automation
214072 Revision B 2-5
Safety Polycold Cryochiller
Safety Labels and Safety Label Identification Installation and Operation Manual
Nameplate Label
Part Number: 407168-00 (left or top section)
Qty: 1 (2 label set)
Location: Inside on lower left frame of compressor area
Contains part number, serial number, and specification
information.
Brooks Automation
2-6 214072 Revision B
Polycold Cryochiller Safety
Installation and Operation Manual Safety Labels and Safety Label Identification
Nameplate Label
Part Number: 407168-00 (right or bottom section)
Qty: 1 (2 label set)
Location: Inside on lower left frame of compressor area
Contains specification information
Brooks Automation
214072 Revision B 2-7
Safety Polycold Cryochiller
Safety Labels and Safety Label Identification Installation and Operation Manual
407114-00
407110-00
407112-00
184193
407168
407114-00
Figure 2-2: Locations of Labels on the front side of the Polycold Cryochiller
Brooks Automation
2-8 214072 Revision B
Polycold Cryochiller Safety
Installation and Operation Manual Safety and Operational Interlocks
184193
407114-00
Figure 2-3: Locations of Labels on the back side of the Polycold Cryochiller
The Cryochiller contains the interlocks listed in Table 2-2 and shown in Figure 2-4.
Brooks Automation
214072 Revision B 2-9
Safety Polycold Cryochiller
Safety and Operational Interlocks Installation and Operation Manual
Interlock Function
Circuit Breakers Protective devices that prevent current overload of the com-
pressor motor or control system.
Circuit breakers require manual reset.
High Voltage Interlock The Lockout/Tagout slide bar must be moved to the lock-
out/tagout position with the primary circuit breaker in the OFF
position in order to remove the cover to the high voltage box
and access the interior of the high voltage assembly.
Over Pressure Relief Valve A pressure relief valve vents refrigerant gas when the refriger-
ant circuit pressure exceeds the set point of the valve.
Causes a controlled-release of excess pressure for the refrig-
erant in a manner that avoids an over pressure event.
Valve closes when pressure is reduced to the valve set point.
Compressor Motor Thermo- Detects when the temperature of the compressor on the Poly-
stat cold Cryochiller exceeds a safe temperature and shuts off
power to the compressor motor.
The thermostat automatically resets when the temperature of
the compressor motor thermostat falls to a safe level.
Hazardous Voltage
Overriding interlocks can cause electrical hazards. Direct contact
with hazardous voltage will cause death or serious injury.
• Do not defeat, modify, or disable any of the unit’s safety inter-
locks.
NOTICE
The user may choose to add an Emergency Off (EMO) circuit to the Polycold
Cryochiller and is accountable for that EMO circuit.
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2-10 214072 Revision B
Polycold Cryochiller Safety
Installation and Operation Manual Safety and Operational Interlocks
Main
Circuit
Breaker
Lockout/Tagout
Slide Bar
Provides Interlock for
High Voltage Cover
Over Pressure
Relief Valve
Compressor
Motor Thermostat
(internal to compressor)
Lockout / Tagout
Working with energized equipment may cause electrical shock or
burn and may result in death or serious harm.
• All energy must be removed from the equipment per the sys-
tem’s or the facility’s Lockout/Tagout procedure before servicing.
• If local procedures are not available, follow the procedure for
Lockout/Tagout in OSHA Standard 29CFR 1910.147.
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214072 Revision B 2-11
Safety Polycold Cryochiller
Mechanical Hazards Installation and Operation Manual
Cryochiller Lockout/Tagout
A slide bar that is attached to the high voltage box cover is provided as the Lockout/Tagout device.
When the high voltage box cover is removed, the Lockout/Tagout device is also removed, and Lock-
out/Tagout procedures must be performed on the input power to the Polycold Cryochiller.
Mechanical Hazards
Tip Hazard
This unit has a high center of gravity and may tip when moved
improperly or when left stationary with casters unlocked which may
cause death or personal injury.
To avoid this hazard, follow these precautions:
• Read the user’s manual before moving.
• For smooth hard floors, move by rolling slowly and avoid rapid
acceleration and deceleration.
• Move only on smooth level surfaces that are free of gaps,
grooves, or debris.
• For uneven or soft floors, move using optional hoist rings with
overhead lift
• Do not use casters to move up and down ramps.
• Apply force below center line when moving by hand.
• Lock two front casters when not moving.
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2-12 214072 Revision B
Polycold Cryochiller Safety
Installation and Operation Manual Mechanical Hazards
Trip Hazard
Trip hazard which may cause personal injury exists if the facilities
connections such as power and communications cables, gas and
vacuum lines, for the compressor are not properly routed.
• Route facilities connections and communication cables out of
the way where there is no travel and they do not cause trip haz-
ards
Heavy Object
The Polycold Cryochiller weighs a minimum of 533 kg (1175 lb) up
to a maximum of 544 kg (1200 lb).
Failure to take the proper precautions before moving this unit could
result in personal injury.
• Follow appropriate methods for moving heavy equipment.
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214072 Revision B 2-13
Safety Polycold Cryochiller
Electrical Hazards Installation and Operation Manual
Electrical Hazards
The Brooks Automation Polycold Cryochiller is a hazardous voltage device. It requires a user installed
slow blow circuit breaker that meets, or exceeds, the minimum SCCR rating specified by SEMI S2. See
Electrical on page 3-4.
The proper precautions for operating and servicing electrical equipment must be observed.
Electrical Hazard
Contact with energized equipment can cause electric shock and
result in death or serious injury.
• All electrical energy supplied to the Polycold Cryochiller must be
disconnected from the system according to the facility’s lock-
out/tagout procedure before performing service or maintenance.
• Lockout/Tagout device is provided for use when high voltage box
cover is in place.
• Lockout/Tagout must be provided at the input power source if
high voltage box cover is removed,
• Only a qualified electrician or electrical technician is allowed to
open the Polycold Cryochiller and troubleshoot electrical prob-
lems.
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Polycold Cryochiller Safety
Installation and Operation Manual Thermal Hazards
Thermal Hazards
The condenser and compressor inside the Polycold Cryochiller present thermal hazards.
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214072 Revision B 2-15
Safety Polycold Cryochiller
Chemical Hazards Installation and Operation Manual
Chemical Hazards
The Polycold Cryochiller is supplied with two Overpressure Relief Valves. In the unlikely event that the
relief valves release refrigerant gas, the gas must vent to atmosphere in a well vented area that meets
the minimum room size requirements as specified in ASHRAE-15 and EN-378.
Asphyxiation Hazard
The blend of refrigerant used in the Polycold Cryochiller is non
flammable and non toxic. However, as with any gas, asphyxiation
could occur if concentrated refrigerant gas is inhaled which may
cause death or serious injury.
• Service the Polycold Cryochiller in a well ventilated area as
specified by ASHRAE-15 and EN-378.
Chemical Hazard
Opening the refrigerant circuit or changing valve settings without
following the instructions in this manual could result in release of
refrigerant gas which is considered a green house gas.
• Avoid releasing refrigerant gas to the atmosphere.
• Keep the gas line couplings aligned when making or breaking
coupling connections to prevent leaks due to a sharp bends.
• Review this manual before performing any procedure including
routine operation.
NOTICE
United States and other federal laws require a certified refrigeration technician
(Type 2, High Pressure) perform any procedure that could release refrigerant to
the atmosphere.
This includes:
• Installing the Polycold Cryochiller
• Inspecting procedures
• Disconnecting the refrigerant lines
• Troubleshooting procedures
• Repairing
• Disposing of the unit or charged components
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2-16 214072 Revision B
Polycold Cryochiller Safety
Installation and Operation Manual High Pressure Gas Hazard
Fire Hazard
Cleaning fluids such as isopropyl alcohol may cause fire if used on
hot parts.
• Allow the Polycold Cryochiller to cool before using cleaning flu-
ids.
Brooks Automation
214072 Revision B 2-17
Safety Polycold Cryochiller
Environmental Information Installation and Operation Manual
Environmental Information
NOTICE
The Polycold Cryochiller contains fluorinated green house gases covered by the
Kyoto Protocol.
Refrigerant Gas
A qualified refrigeration technician is required to remove the refrig-
erant from the Polycold Cryochiller.
• When working with refrigerant gas, follow all facility and local
regulatory environmental procedures regarding the storage, han-
dling, and disposal of the gases.
• Refer to the refrigerant Material Safety Data Sheets, MSDS.
Hazardous Materials
Ensure the product has been properly decontaminated before performing any service. Follow the facil-
ity’s decontamination procedures.
Follow all facility and local regulatory procedures for the disposal of hazardous materials. If the compo-
nents are charged with refrigerant, refer to the Material Safety Data Sheets, MSDS, for each refrigerant.
A single Material Safety Data Sheet set for the different blends of gasses is located in Appendix J:
Material Safety Data Sheets - MSDS on page 12-21.
The compressor in the Polycold Cryochiller contains lubrication oil which may be considered a hazard-
ous substance. The MSDS for the POE Solest LT-32 oil is included in Appendix J: Material Safety Data
Sheets - MSDS on page 12-21
Brooks Automation
2-18 214072 Revision B
Polycold Cryochiller
Installation and Operation Manual
Physical Specifications
Height - mm (inch)
1791 (70.5) 1791 (70.5)
(without castors or lifting hooks)
NOTE: All units have cold elements that may be decoupled from the refrigerant lines.
NOTE: Maximum angle of inclination for shipping or handling all units is forty-five degrees (45°).
When moving units using pallet jack or optional casters must be moved on level floors only.
NOTE: All specifications are for the standard product configuration. Specifications can vary for
customized configurations
NOTE: Sound measurements were made on each side of the unit at a distance of 1.0m (39 in) and
at a height of 1.6m (63 in). Measurements taken from each side of the unit did not vary sig-
nificantly. Measurements will vary with the acoustics of the environment.
Brooks Automation
214072 Revision B 3-1
Specifications and Site Preparation Polycold Cryochiller
Physical Specifications Installation and Operation Manual
Dimensions
Dimensions are mm (inches) based on a
standard unit.
Center of gravity based on a unit without
casters.
For a unit with casters, increase vertical
dimension by 76.2mm (3 inches)
For a unit with lift hooks folded down, increase
vertical dimension by 34mm (1.34 inches)
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3-2 214072 Revision B
Polycold Cryochiller Specifications and Site Preparation
Installation and Operation Manual Physical Specifications
Site Preparation
The refrigeration unit should be installed in an environment that meets the following conditions:
• Indoors
• Above ground
• Well ventilated area. Room size must meet minimum requirements of ASHRAE-15 and
EN-378. See Installing a Refrigeration Unit to Meet ASHRAE Requirements on page 4-3.
• Room temperature of 4-38° C (40-100° F)
• Relative humidity of 20-80%, non-condensing
The Polycold Cryochiller must remain vertical while operating. The refrigeration unit is not gravity sen-
sitive and may be placed at any elevation relative to the cryosurface.
Access
Multiple units placed facing each other Figure 3-2: Polycold Cryochiller Service Access
require 914mm (36 inches) front service Units are mm (inches) (not to scale)
access.
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214072 Revision B 3-3
Specifications and Site Preparation Polycold Cryochiller
Electrical Installation and Operation Manual
Electrical
Brooks Automation
3-4 214072 Revision B
Polycold Cryochiller Specifications and Site Preparation
Installation and Operation Manual Electrical
Transformer
Fuse Size Power Input
Tap Setting RLA Amps MCC Amps LRA Amps
Amps kVA
and ID Label
200-3-50/60 55.4 75 160 80 19.2
230-3-50/60 48.3 75 160 80 19.2
35 (see Note 1)
380-3-50 27.2 39 80 17.9
45 (see Note 2)
400-3-50 25.8 39 80 35 17.9
460-3-50/60 25.4 39 80 35 20.2
480-3-60 21.5 39 80 35 17.9
575-3-60 17.9 31.2 64 35 17.8
Note 1: 35Amp breaker is allowable for 380-3-50 setting when nominal voltage is 380V +10% / -5%.
Note 2: 45Amp breaker is required for 380-3-50 setting when nominal voltage is 380V +10% / -10%.
Brooks Automation
214072 Revision B 3-5
Specifications and Site Preparation Polycold Cryochiller
Cooling Water Installation and Operation Manual
Cooling Water
The cooling water supplied to the Cryochiller must meet temperature, flow, and purity requirements.
• Cooling water temperature must be between 13 – 38° C (55 – 100° F).
• Minimum flow rates and water temperatures are shown in Table 3-6.
• Purity requirements are shown in Table 3-7.
Minimum water flow rates are based on requirements to effectively remove heat from the cryochiller
and to reduce risk for scale and corrosion of the condenser. Flow rates below the published minimum
required flow rate can result in scale and corrosion since the risk for these conditions increases with
lower water flow rates and higher outlet water temperatures.
Condenser failures or unit performance issues that occur on units operating at water flow rates that are
lower than the minimum required flow rate in Table 3-6 are not covered by warranty.
Allow for cooling water temperature rise during the summer months.
User is advised to add a filter to the cooling water to remove dirt and abrasives. 100 micron filter is rec-
ommended. Chemical impurities in the cooling water must be compatible with copper. See Table 3-7.
18 (65) 18.2 (4.8) 145 (38.3) 10.3 (1.5) No data 23.2 (79,232)
MaxCool 27.3 (7.2) 145 (38.3)
24 (75) 20.7 (3) No data 23.2 (79,232)
4000H
29 (85) 54.1 (14.3) 145 (38.3) 77.2 (11.2) 3.4 (0.15) 23.2 (79,232)
38 (100) – Max. 54.1 (14.3) 145 (38.3) 77.2 (11.2) 3.4 (0.15) 23.2 (79,232)
13 (55) – Min. 13.6 (3.6) 145 (38.3) 6.9 (1) No data 21.7 (74,109)
18 (65) 18.2 (4.8) 145 (38.3) 10.3 (1.5) No data 21.7 (74,109)
MaxCool 27.3 (7.2) 145 (38.3)
24 (75) 20.7 (3) No data 21.7 (74,109)
2500L
29 (85) 54.1 (14.3) 145 (38.3) 77.2 (11.2) 3.4 (0.15) 21.7 (74,109)
38 (100) – Max. 54.1 (14.3) 145 (38.3) 77.2 (11.2) 3.4 (0.15) 21.7 (74,109)
1
NOTE: Pressure Drop values assume a 3/4-inch (20 mm) standard pipe size.
Maximum working pressure of the unit’s cooling water circuit is 1380 kPa (200 psig).
Brooks Automation
3-6 214072 Revision B
Polycold Cryochiller Specifications and Site Preparation
Installation and Operation Manual Cooling Water
The chemistry of water typically used to cool equipment can vary widely. Multiple different elements,
compounds and ions may be present at the same time. Depending on which chemicals are present,
their amount, and the cooling water temperature, there may or may not be a risk for scaling.
The guidelines listed here are provided to reduce the potential for scale and scale related corrosion.
Whereas scale reduces heat exchanger effectiveness and cause the cryochiller performance to
degrade, scale deposits can result in corrosion that can occur beneath the scale layer. The presence
of excessive amounts of chlorine or chloride can accelerate this type of corrosion.
In addition to scale, the accumulation of micro organisms on heat exchanger surfaces can lead to
corrosion. Even after microbes have been killed by heat of chemical agents, they remain on the
surface and have the same effect as scale.
The specific elements of water quality which are important depend upon your local area and the
minerals and chemicals dissolved in your cooling water. Although your local water supply was used to
fill water into your cooling loop, it is the chemistry of the water circulating through your cooling loop
which is important. In many cases, this is significantly different from the make up of the water originally
filled into the cooling loop.
Best practice for cooling loop maintenance call for periodic sampling (i.e. monthly) and analysis of the
water quality circulating in the cooling loop. When parameters are beyond the limits listed in Table 3-7,
then corrective action is needed to bring them within the limits.
In cases where the cooling water is consistently at risk for scale, a periodic descaling process should
be put in place, such as monthly or quarterly depending on scaling risk. Scale risk typically increases
with water outlet temperature. This risk increases significantly when the compressor is allowed to
operate without any water flow. While such events are expected, if a unit is repeatedly operated
without cooling water, the condenser should be descaled.
Water quality may vary by location. The most common chemical properties and their recommended lev-
els are identified in bold in Table 3-7. Additional properties which may be present in your cooling water
are listed without bold.
Brooks Automation
214072 Revision B 3-7
Specifications and Site Preparation Polycold Cryochiller
Cooling Water Installation and Operation Manual
Chlorides (Cl-) < 100 ppm Higher levels can cause pitting corrosion.
Higher levels accelerates copper leaching by oxidation
Free Chlorine (Cl2) < 0.5 ppm
and dissolution of the metal surface.
Levels higher than 100 ppm increase the risk of copper pitting
Sulphate (SO42- ) < 100 ppm
corrosion.
Resistivity is the inverse of Conductivity.
Electrical Resistivity 2,000 - 100,000 Ω-cm Higher resistivity above 100,000 Ω-cm can result in copper
corrosion.
Hydrogen Sulfide (H2S) < 0.05 ppm Higher levels can lead to corrosion, pitting, and copper fatigue.
Free (aggressive)
< 5 ppm Higher levels can indicate oxidation of metals.
Carbon Dioxide (CO2)
Iron (Fe) < 0.3 ppm Higher levels can increase the risk of galvanic corrosion.
Aluminum (Al) < 0.2 ppm Higher levels can increase the risk of galvanic corrosion.
Manganese < 0.5 ppm Higher levels can increase the risk of galvanic corrosion.
Total Copper (Cu) < 0.3 ppm Higher levels can increase the risk of galvanic corrosion.
HCO3- / SO42- > 1 ppm Lower levels below 1 ppm add risk of copper pitting
Ammonium (NH4+) < 2 ppm Higher levels increase the risk of copper corrosion.
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3-8 214072 Revision B
Polycold Cryochiller Specifications and Site Preparation
Installation and Operation Manual Performance Specifications
Performance Specifications
Table 3-8 lists the performance specifications for the Polycold Cryochiller product family. For additional
information, contact Brooks Automation Polycold Systems.
Maximum load
4000 W at -98 C 2500 W at -120 C
(watts at warmest average temperature)
Notes:
Brooks Automation
214072 Revision B 3-9
Specifications and Site Preparation Polycold Cryochiller
Cryocoils and Refrigerant Lines Installation and Operation Manual
The cryocoil(s) must be specified and sized for the process. Contact Brooks Automation Polycold for
assistance in selecting the proper cryocoil.
Total cryocoil surface area for dual circuit models must be divided between the two circuits. Larger
cryocoils may give faster pumping speeds and can be used in some applications. However, if the heat
load is too great, the cryopump becomes less efficient and may be shut off by a protective device
Test Pressure, bar (psig) 44.4 (644) 44.4 (644) 44.4 (644) 44.4 (644)
Temperature Range +150C to -160C +150C to -160C +150C to -160C +150C to -160C
Note 1 Other refrigerant line lengths and cryocoils may be possible, depending upon performance
requirements.
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3-10 214072 Revision B
Polycold Cryochiller Specifications and Site Preparation
Installation and Operation Manual Cryocoils and Refrigerant Lines
NOTICE
The tubing for the refrigerant lines and cryocoil must be dried prior to installation.
• Perform strength test with dry compressed nitrogen using the appropriate
safety precautions
• After testing, backfill with dry nitrogen and cap the assembly.
• Hydrostatic pressure testing is NOT recommended because it introduces sig-
nificant amounts of water and will void the warranty.
• Lines or coils that are hydrostatically tested must be drained of water and then
baking out at 80 C for at least 12 hours under a dry nitrogen purge.
• A calibrated hygrometer should be used to verify that water vapor concentra-
tion is less than 50 ppm at the end of the bake out process.
Balance Pressure
NOTE: 1 These pressures are for the refrigeration units only. The balance pressure may drop 5-20
psig (35-70 kPa) after installing the refrigerant line and cryosurface and opening the isola-
tion valves.
NOTE: 2
Balance Pressure refers to the pressure of the unit when it is turned off and warmed up
to room temperature. It is the balance of pressure on both sides, the suction side and the
discharge side, of the compressor. When the compressor is running, the unit creates a
pressure difference between the suction and discharge sides of the compressor.
Brooks Automation
214072 Revision B 3-11
Specifications and Site Preparation Polycold Cryochiller
Cryocoils and Refrigerant Lines Installation and Operation Manual
This product does not contain R-22 or any CFC’s or HCFC’s and is in accordance with U.S. EPA law
and EC2037/2000 and EC1005/2009.
All refrigerant used in Polycold's MaxCool Cryochiller products have significant GWP values. Users and
service providers should ensure that refrigerant is not released to the environment at any time. The
refrigerant should be reclaimed and either recycled or destroyed in accordance with international regu-
lations and the current best industry practices.
Calculations of the GWP for the Polycold Cryochiller refrigerant blends, as shown in Figure 3-11, were
calculated in accordance with the European Union's EC Regulation No 842/2006 on Certain Fluori-
nated Greenhouse Gases.
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3-12 214072 Revision B
Polycold Cryochiller
Installation and Operation Manual
4 Installation
General Hazard
Failure to review the Safety section and follow the safety warnings
can result in death or serious injury.
• Do not attempt to perform installation, operation, or maintenance
procedures on the Polycold Cryochiller until you have read and
understand the information in the Safety chapter.
• Read and understand each procedure before performing the
procedure.
This chapter assumes that the user has completed the specification, design, and component selection
process. Refer to the Introduction and Specification chapters for design and specification information.
Brooks Automation
214072 Revision B 4-1
Installation Polycold Cryochiller
Installation Checklist Installation and Operation Manual
Installation Checklist
Use the checklist in Table 4-1 when installing the Polycold Cryochiller. Perform the procedures in the
order shown. Initial and date each procedure as you complete it.
NOTE: Before installing the Polycold Cryochiller, check the specifications and site requirements in
this manual.
10. Check the Refrigerant Lines and Cryosurface for Leaks 4-27
Brooks Automation
4-2 214072 Revision B
Polycold Cryochiller Installation
Installation and Operation Manual Installation Overview
Installation Overview
Before starting installation, review the items in this section to confirm that the installation location meets
the requirements of the Cryochiller and that the proper components have been selected and are avail-
able to perform the installation.
Component Description
Confirm that each of the main components of the Polycold Cryochiller are available for installation.
• Refrigeration Unit
• Refrigerant Line
• Cryosurface; one of two types:
– Coil - for water vapor cryotrapping
– Baffle - usually used to minimize oil back streaming
• Cryogenic feedthrough, which routes the refrigerant lines through the vacuum chamber wall
The following information helps to comply with ANSI / ASHRAE 15-1994 “Safety Code for Mechanical
Refrigeration.”
• ANSI is for the American National Standards Institute.
• ASHRAE is for the American Society of Heating, Refrigeration, and Air Conditioning Engineers.
Normally, the manufacturer provides the type and amount of refrigerant used in the refrigeration unit.
However, Polycold considers their mixtures of refrigerants to be proprietary. Therefore, the following
information complies with the above standards.
• The amount of refrigerant mixture, the minimum room size, and the refrigerant safety group
classification are included next to the refrigeration unit's nameplate.The nameplate is located
on the frame under the lower left front panel or above the water connection panel, lower right
front panel.
• Brooks determined the refrigerant safety group classification of the refrigerant mixture by eval-
uating the safety group classifications of the individual components. This evaluation used ANSI
/ ASHRAE-34 and EN 378.1 as a guide.
• The Polycold Cryochiller is a “direct (refrigeration) system”. It is only intended to be installed
above ground in an industrial environment.
• To comply with the Safety Code for Mechanical Refrigeration, ANSI/ASHRAE-115-2007, the
units should be located in a room no smaller than listed.
• If the minimum room size indicated on the nameplate is not obtainable, the refrigeration unit
must be installed in a “refrigerating machinery room”. Consult local or national building codes
for machinery room requirements.
• See section 9.7.8 of ANSI / ASHRAE 15- 1994 for location requirements.
• Only A1 refrigerants are used on MaxCool systems. According to ASHRAE 15 and EN 378, it
is permissible for the pressure relief valves to vent into the equipment cabinet. This assumes
the unit is installed above ground and in a room that meets the minimum room volume.
Brooks Automation
214072 Revision B 4-3
Installation Polycold Cryochiller
Inspect and Unpack the Polycold Cryochiller Installation and Operation Manual
1
The discharge capacity recommended by Polycold is based on actual relief requirements from the refrigera-
tion system as assessed by these standards. The pressure relief devices on the refrigeration unit are over-
sized. Discharge capacities based on the pressure relief devices are 23.9 pounds of air per minute.
Item Description
General Hazards
The Polycold Cryochiller presents hazards that may cause death
or personal injury.
• Review this manual before performing any procedure. This
includes routine operation of the Polycold Cryochiller.
• Know the information in the Safety Chapter.
• Review the MSDSs that are associated with this tool.
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4-4 214072 Revision B
Polycold Cryochiller Installation
Installation and Operation Manual Inspect and Unpack the Polycold Cryochiller
1. Carefully inspect all surfaces of the shipping containers for signs of damage or stress.
Note that there may be more than one shipping container.
3. Remove strapping and fasteners that hold the cardboard enclosure to the palette.
4. Remove the lower braces from the palette that block the base frame of the Cryochiller.
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214072 Revision B 4-5
Installation Polycold Cryochiller
Inspect and Unpack the Polycold Cryochiller Installation and Operation Manual
NOTE: If the system is exposed to extreme cold during shipping, the balance pressure is reduced
due to the increased condensation of the refrigerant mixture. Refrigerant may take up to 48
hours at room temperature to achieve normal balance pressure and for the pressure gauge
to display the proper reading.
10. Go to the Installation Checklist Table 4-1. Initial and date this task. Go to the next task on the check-
list.
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Polycold Cryochiller Installation
Installation and Operation Manual Move to Location
Move to Location
Item Description
Tools Lift Device to lift, move, and place the unit -See Warning -
Heavy Object below
# 2 Phillips screwdriver
(2) 9/16-inch wrenches
NOTE: If the unit includes the Lifting Ring option, refer to Appendix B: Lifting Rings (Optional) on
page 12-3
If the unit includes casters, refer to 185304, Install Procedure, Caster Option.
Heavy Object
The refrigeration unit weighs more than 522 kg (1150 lb). Failure to
properly lift this device may result in death or serious injury.
• Use a fork lift or crane when lifting or moving the compressor
unit.
• If using lift ring option, refer to Appendix B: Lifting Rings
(Optional) on page 12-3
Refer to Figure 3-1 on page 3-2 and Figure 3-2 on page 3-3 for placement and spacing
requirements.
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214072 Revision B 4-7
Installation Polycold Cryochiller
Move to Location Installation and Operation Manual
NOTICE
If using a fork lift or pallet jack, make sure the forks extend fully through the frame
of the Polycold Cryochiller and completely support both sides of the frame.
Lifting the unit with a forklift or pallet jack without having the forks or jack fully
extended through the Cryochiller frame will damage the frame and void the war-
ranty.
6. Go to the Installation Checklist Table 4-1. Initial and date this task. Go to the next checklist task.
Brooks Automation
4-8 214072 Revision B
Polycold Cryochiller Installation
Installation and Operation Manual Remove the Compressor Hold-Down Nuts
Item Description
1. Use a Phillips-head screwdriver to remove the (4) screws that attach the front lower
panel on the system and remove the panel.
2. Use a Phillips head screw driver to remove the (5) screws that attach the rear lower panel on the
system and remove the panels.
See Figure 4-4.
3. If an optional spare parts kit was ordered, it will be behind the lower front panel of the unit.
Remove the spare parts kit and verify that all of the parts were shipped with the unit.
4. Locate the compressor in the bottom of the refrigeration unit. See Figure 4-3 and Figure 4-5.
Brooks Automation
214072 Revision B 4-9
Installation Polycold Cryochiller
Connect the Cooling Water Installation and Operation Manual
9. Go to the Installation Checklist Table 4-1. Initial and date this task. Go to the next task on the check-
list.
Item Description
NOTICE
Water should be filtered for contaminants and copper reducing microbes.
Brooks recommends filtration to 100 microns and microbiological controls be put
in place in order to supply clean and safe cooling water to your Polycold product.
Failure to provide water of proper specification may void the system warranty.
Brooks Automation
4-10 214072 Revision B
Polycold Cryochiller Installation
Installation and Operation Manual Connect the Cooling Water
NOTICE
If the system is turned on before cooling water has been connected, damage to
the equipment can result.
Verify that cooling water has been connected before turning on power to the unit.
1. Ensure that the water supply for the Polycold Cryochiller refrigeration unit meets the
specifications in Cooling Water on page 3-6
Optional:
Install pressure gauges on the water lines at the refrigeration unit in order to measure the pressure
drop within the refrigeration unit. This will help you adjust the water flow for optimum operation of
the Polycold Cryochiller. It will also aid you in troubleshooting if there are water cooling problems.
See Figure 4-6
It is also recommended to install two parallel input water lines including valves, water filters, and
flow meters. This allows switching water lines and avoiding equipment shutdown during scheduled
maintenance. See Figure 4-6
NOTICE
If using rotameter-type flow meters, their inherent restriction may reduce the
actual flow rate delivered to the refrigeration unit.
Manual
shut-off valves Filters
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214072 Revision B 4-11
Installation Polycold Cryochiller
Connect the Cooling Water Installation and Operation Manual
5. Tighten each water line finger tight until the water line gasket contacts the fitting and then tighten 2
to 3 additional full turns. The number of turns required to tighten the fittings is affected by the thick-
ness of the tape or sealant that has been applied to the threads.
6. Turn the supply and return water lines on. Check for leaks. If water leakage is found, tighten the
leaking fitting an additional 1/4 turn. If water continues to leak at the connection, turn off the supply
and return water lines, disconnect the fittings and check for the cause of the leak.
7. When the water connections are installed, test, and do not leak, go to the Installation Checklist
Table 4-1 on page 4-2. Initial and date this task. Go to the next task on the checklist.
Brooks Automation
4-12 214072 Revision B
Polycold Cryochiller Installation
Installation and Operation Manual Connect Electrical Power
Item Description
Tools Torque Wrench for 3.9 to 4.5 N-m (35 to 40 lb-in) range
... or equivalent for electrical terminal connections
Materials 4-Conductor power cable that meets local electrical code for the volt-
age and amperage of the unit See Table 3-5 on page 3-5.
Connector for power cord to facilities power connection
Cable Strain Relief or Conduit Connector for 49.2mm (1.94 inch)
power access hole
1/4 inch ring lugs
Hazardous Voltage
Contact with energized equipment may cause electric shock and
result in death or serious injury.
• Only a qualified electrician or electrical installer is allowed to
install the power to the Polycold Cryochiller.
1. The location of power input to the Polycold Cryochiller is on the lower right corner of
the front of the unit. There is a 49.2mm (1.94 inch) clearance hole in the outer skin and
a 42.1mm (1.656 inch) mounting hole on the frame for mounting an appropriate sized
strain relief or conduit connector.
2. Route the 4 conductor cable or individual wires through the connection, up the right front leg, above
the cable tray that is attached to the bottom of the shelf that separates the compressor area from
the valve area, and then up to the circuit breaker area.
3. Confirm that the protective grommet or strain relief is in place in the opening below CB1.
4. When using larger cables, the (3) screws that hold the front edge of the upper cable track may be
removed and the track lowered to provide greater access. When completed, replace the (3) screws.
5. If the input power cable is too large to route through the cable tracks or existing cable is too short,
use Terminal Block Accessory and Wiring Kt, p/n 181500.
If using 4-conductor cable that is too stiff to bend in the cable tracks, remove the outer jacket from
the cable after it passes through the strain relief. Optionally, use Terminal Block Accessory and Wir-
ing Kt, p/n 181500.
Brooks Automation
214072 Revision B 4-13
Installation Polycold Cryochiller
Connect Electrical Power Installation and Operation Manual
Cable connects to
customer provided
strain relief
Cable Track
Screws
Conduit connects to
(3 places)
customer provided
conduit connection
Brooks Automation
4-14 214072 Revision B
Polycold Cryochiller Installation
Installation and Operation Manual Connect Electrical Power
9. Tighten each 1/4-20 (M6) terminal screw to 3.9 to 4.5 N-m (35
to 40 lb-in).
10. Connect the ground line of the power cable to the ground stud
using the hardware provided in the fastener sequence. Follow
the stack sequence below and shown in Figure 4-11.
• External star washer
• Terminal lug
• Flat washer - (optional)
• Lock washer - (optional)
• 1/4-20 (M6) Nut
11. Tighten the 1/4-20 (M6) ground nut to 4.5 to 5.1 N-m (40 to 45
lb-in).
12. After the power cable is fully connected, secure the power
cable to the track using cable ties. Holes are provided in the Figure 4-10: Terminal Washer
cable track for inserting the cable ties. Stack Sequence
14. Check the input voltage and compare to the voltage specified
on the system label. Adjust the tap settings, if required, to
accommodate the actual input voltage. See Input Power Trans-
formers on page 4-16.
Brooks Automation
214072 Revision B 4-15
Installation Polycold Cryochiller
Connect Electrical Power Installation and Operation Manual
The Polycold Cryochiller has one of three different transformers installed based on the input power
requested when the unit was ordered. The system is set to a specific input voltage at the factory by
transformer tap settings. These tap settings must be adjusted in the field as required to accommodate
the actual voltage at the installation site.
• Available tap settings are: 200V, 230V, 380V, 400V, 430V 460V and 480V.
• All transformers use the same numbering scheme for tap settings but the taps may be in differ-
ent physical locations on the transformer depending on the transformer that is used.
2. Check the transformer tap settings. Refer to the tap setting sticker on the transformer or Figure
4-12.
3. Rewire the transformer tap settings as required. Refer to Table 3-4 on page 3-4 for tap settings for
your compressor and voltage.
• Remove the protective cover
• Change the input wiring and jumper settings as required
• Replace the protective cover
Figure 4-12: Tap Settings for 230 and 480 Volt Transformers
4. Go to the Installation Checklist Table 4-1. Initial and date this task. Go to next task on the checklist.
Brooks Automation
4-16 214072 Revision B
Polycold Cryochiller Installation
Installation and Operation Manual Install the Cryosurface
Item Description
Tools 2.5 inch Spanner wrench, p/n 810030-07, for the nut on
feedthrough connection
Materials High-vacuum grease - must have an appropriate low vapor
pressure (for optional use on the feed-through's)
O-ring, as required
This section describes how to install the cryocoil or cryobaffle, and refrigerant lines. If these items are
not already selected, then follow the recommendations below.
• Refer to System Summary on page 1-3 and Cryocoils and Refrigerant Lines on page 3-10 for
cryosurface information.
• Refer to Appendix F: Feedthroughs on page 12-10 for feedthrough selection information.
• Contact Brooks Automation Polycold Systems for more information.
NOTE: This task assumes that both a cryosurface and a standard 50mm (2-inch) feed-through
from Brooks Automation Polycold Systems are being installed.
If a cryobaffle or cryocoil and feed-through has been custom-fabricated by a source other
than Brooks Polycold, verify that the part meets the specifications in the section Specifica-
tions and Site Requirements, Cryocoils and Refrigerant Lines on page 3-10.
The feed-through on the Brooks Polycold Systems Cryocoil is designed to be installed from the inside
of a vacuum chamber. This allows removal of the cryosurface when cleaning or servicing the vacuum
chamber.
1. Inspect the feed-through port thickness, hole diameter, and sealing surface. Ensure
that the feed-through port is compatible with the feed-through.
2. Clean the inner and outer surfaces of the feed-through port on the vacuum chamber wall where the
cryosurface feed-through is to be installed.
Brooks Automation
214072 Revision B 4-17
Installation Polycold Cryochiller
Install the Cryosurface Installation and Operation Manual
3. Inspect and clean the O-ring groove and O-ring in the inner flange of the feed-through.
5. From the inside of the vacuum chamber, insert the feed-through into the feed-through port.
6. Tighten the feed-through nut finger-tight and position the cryosurface. If the cryosurface has fasten-
ers, secure them at this time. See Figure 4-13.
7. Verify that no moving parts will hit the cryosurface. Make sure the cryosurface does not touch the
vacuum chamber wall or anything in the vacuum chamber. The cryosurface must be at least 16mm
(5/8-inch) from the vacuum chamber wall to prevent ice bridging. Greater distances are better.
8. Hold the feed-through in place and tighten the nut with the spanner wrench included with the cryo-
surface assembly. Make certain the nut is tight. If the nut is loose, the O-ring will tend to lift from the
vacuum chamber wall when under vacuum.
9. Install a heat radiation shield if the cryocoil is in direct view of a source of heat greater than 50°C.
Position the shield between the cryocoil and the heat source. The shield should be as close as pos-
sible to the heat source and as far away as possible from the cryocoil. The cryocoil traps molecules
best when it has maximum view of the vacuum chamber.
10. Check the vacuum chamber for leaks. If any leaks are found, correct them before proceeding.
11. Go to the Installation Checklist Table 4-1. Initial and date this task. Go to the next task on the check-
list.
Brooks Automation
4-18 214072 Revision B
Polycold Cryochiller Installation
Installation and Operation Manual Install the Refrigerant Lines
Install a Cryobaffle
1. If you are installing a Polycold “CB” type cryobaffle, carefully center it between the
flange bolt holes to assure a good O-ring seal.
3. Make sure the cryosurface does not touch the vacuum chamber wall or anything else in the vacuum
chamber. The cryosurface should be at least 16mm (5/8-inch) away from the vacuum chamber wall
to prevent ice bridging. Note that greater distances are better.
4. Install a heat radiation shield if the cryobaffle is in direct view of a source of heat greater than 50°C.
Position the shield between the cryobaffle and the heat source. The shield should be as close as
possible to the heat source and as far away as possible from the cryobaffle. The cryobaffle traps
molecules best when it has maximum view of the vacuum chamber.
5. Check the vacuum chamber for leaks. If any leaks are found, correct them before proceeding.
6. Go to Installation Checklist Table 4-1. Initial and date this task. Go to the next task on the checklist.
NOTICE
This procedure assumes that refrigerant lines from Brooks Automation, Inc.
Polycold Systems are being installed.
• If installing a refrigerant lines not made by Polycold Systems, verify that the
refrigerant lines meet the required specifications.
• Contact Brooks Polycold for assistance.
NOTICE
Dual-Circuit System
This section assumes both refrigerant circuits are connected at the same time.
It is possible to connect only one refrigerant circuit of a dual circuit system.
• When connecting the second refrigerant circuit, the refrigerant mixture must
be fully drawn back into the unit.
• Contact Brooks Automation Customer Support for more information.
Brooks Automation
214072 Revision B 4-19
Installation Polycold Cryochiller
Install the Refrigerant Lines Installation and Operation Manual
Item Description
For Cajon VCR Silver-plated stainless steel gaskets or unplated nickel gaskets
Style Couplings 1-3/16 inch open end wrench
(Optional) 1-1/16 inch open end wrench
NOTICE
Use of unauthorized or non-standard couplings voids your warranty.
Improper use of, incorrect installation of, over-tightening of, or use of damaged
O-rings in couplings will void your warranty.
NOTICE
O-ring removal tool requires lubrication.
Always clean couplings after using the lubricated tool.
Brooks Automation
4-20 214072 Revision B
Polycold Cryochiller Installation
Installation and Operation Manual Install the Refrigerant Lines
NOTICE
Refrigerant lines should only be bent once.
Re-bending a refrigerant line can cause “work hardening” and fractures and
refrigerant line failure.
1. Use the following considerations to plan the route of the refrigerant line between the
cryosurface and the top of the refrigeration unit:
• The refrigerant line should not be a hindrance or hazard to the movement of personnel.
• The refrigerant line should not hinder access to or maintenance of any equipment.
• Provide at least 32mm (1-1/4 inches) wall thickness of insulation around the feed and return
lines. If the insulation and system are not completely sealed and airtight, water vapor from the
air will accumulate on some of the surfaces and create ice on the refrigerant lines.
• Support the line at mid-length and at three-foot intervals.
Ensure that the line supports do not crush the insulation covering the lines.
Use supports that are at least 100mm (4 inches) wide.
• Do not use supports that make direct contact with the exposed tubes or couplings.
• Do not allow the lines to be vibrated by the application.
• Important.
The feed lines are made of soft
refrigeration copper and have a min-
imum bend radius of 300mm (12
inches).
The brand or type of tape, hangers, Figure 4-14: Minimum Refrigerant Line Bend Radius
clamps, or cradles depends on what
is available and acceptable at the
installation site.
Brooks Automation. Inc. Polycold Systems recommends using a continuous line length from
the refrigerant unit to cryocoil feed-through. Polycold does not recommend or warranty the use
of intermediate fittings.
If your line design has an intermediate set of fittings between the unit and chamber
Brooks Automation
214072 Revision B 4-21
Installation Polycold Cryochiller
Install the Refrigerant Lines Installation and Operation Manual
feed-through, Polycold recommends eliminating these fittings and brazing the tubes together.
If brazing the lines cannot be done, use only approved fittings and support the tubing within
300mm (12 inches) of each side of the intermediate fitting.
If the sealing surfaces are scratched or dented, contact the Brooks Automation Polycold Service
Department.
NOTE: Parker UltraSeal compatible couplings are standard on all Polycold Cryochillers.
Brooks Automation
4-22 214072 Revision B
Polycold Cryochiller Installation
Installation and Operation Manual Install the Refrigerant Lines
connected. These valves cannot be operated when they are at cryogenic temperatures.
10. Locate the refrigerant feed and return fittings on the upper right corner of the front of the refrigera-
tion unit.
Remove the brass blank-off fittings from the feed and return lines using the following procedure.
See Figure 4-16.
a. Use one wrench to hold the fitting on the refrigerant line steady.
b. Use a second wrench to carefully loosen the blank-off fitting from the refrigerant line.
c. Slowly remove the blank-off fittings from the feed and return couplings while listening for
refrigerant leakage.
– A brief hiss of refrigerant gas leakage is OK.
– Continuous escape of refrigerant is NOT OK. Quickly reinstall the blank-off fit-
tings and make certain the isolation valves are closed.
Circuit 1
Feed Return
Lines Lines
Circuit 2
Figure 4-16: Polycold Cryochiller Refrigerant Lines with Standard Ultra Fittings
Brooks Automation
214072 Revision B 4-23
Installation Polycold Cryochiller
Install the Refrigerant Lines Installation and Operation Manual
11. Save the blank-off fittings and store them with the
unit for reinstallation if the refrigerant lines are dis-
connected.
Female Nut
Gland
Male Coupling
Sealing Surfaces
2. Place the gland against the O-ring and male coupling. Make certain the O-ring does not drop out of
the groove
4. Use two wrenches to tighten the coupling. Keep the male coupling stationary with the 15/16-inch
wrench and tighten the nut with the 1-inch wrench. Each wrench must have a length of at least 12
inches (300 mm).
Brooks Automation
4-24 214072 Revision B
Polycold Cryochiller Installation
Installation and Operation Manual Install the Refrigerant Lines
5. Tighten the nut no less than ¼ turn until resistance increases sharply and no further tightening
occurs. The metal o-ring will be crushed into the o-ring groove. Tighten each coupling to 54-80 Nm
(40-60 pound-foot).
NOTE: The Parker fittings are coupled and sealed based on mechanical displacement of the
threaded parts, which results in compression at the sealing surface. Torque values are pro-
vided for customers requiring a measurable value.
6. Go to the Installation Checklist Table 4-1 on page 4-2. Initial and date this task. Go to the next task
on the checklist.
Female Nut
Gland
Sealing Surfaces
Gland
Male Nut
3. Use both wrenches to tighten each coupling no less than ¼ turn until resistance increases sharply
and no further tightening occurs, approximately 54-80 Nm (40-60 pound-foot).
NOTE: The Cajon fittings are coupled and sealed based on mechanical displacement of the
threaded parts, which results in compression at the sealing surface. Torque values are pro-
vided for customers requiring a measurable value.
4. Go to Installation Checklist Table 4-1. Initial and date this task. Go to the next task on the checklist.
Brooks Automation
214072 Revision B 4-25
Installation Polycold Cryochiller
Route Condensate Drain Tube Installation and Operation Manual
Item Description
1. Locate the condensate drain tube. It is visible from the base of the unit and is visible
when the front skirt and rear skirt are removed. See Figure 4-20.
2. Determine if the drain tube should be routed to the front or to the rear of the unit.
3. Be careful to not damage the fitting on the bottom of the drain pan while moving the hose to posi-
tion.
Support the drain pan fitting while carefully moving the drain hose to the desired side of the unit.
4. When the drain hose is in its final position, check the hose for kinks and adjust as required.
5. Route the tubing to a facility waste water drain or to the input line of a condensate pump.
External
Condensate
Drain Tube
6. Go to the Installation Checklist Table 4-1. Initial and date this task. Go to the next task on the check-
list.
Brooks Automation
4-26 214072 Revision B
Polycold Cryochiller Installation
Installation and Operation Manual Check the Refrigerant Line and Cryosurface for Leaks
Item Description
Chemical Hazard
Failure to have a qualified refrigeration technician do all refrigera-
tion work could result in system damage or personal injury.
• Contact a qualified refrigeration technician to perform all refriger-
ant work.
The leak gas used must be dry with a dew point of -80 C or less.
Helium leak checking the refrigerant line and cryosurface is an acceptable alternative to the procedure
specified below if helium leak check equipment and trained helium leak check operators are available.
If helium is used as a leak check medium, only use helium while the compressor is off and ensure that
the pressure in the line and cryosurface during this test does not exceed the lowest refrigerant pres-
Brooks Automation
214072 Revision B 4-27
Installation Polycold Cryochiller
Check the Refrigerant Line and Cryosurface for Leaks Installation and Operation Manual
sure. This is important to assure that helium does not migrate into and contaminate the refrigerant sys-
tem. When the system is off, the lowest pressure is the balance pressure.
During evacuation of the line and coil, after the leak check, it is recommended to purge the line with dry
nitrogen or dry argon that has a dew point of -80 C or less since it can be difficult to pump out pure
helium.
Be aware of false positives created by the armaflex insulation around the line set. The factory installed
tube insulation and flat insulation can produce false positives with some leak check sensors.
Refrigerant
Gas
R134a
Dry
Nitrogen
Gas
Refer to Figure 4-21 and Figure 4-22 for the following steps.
2. Connect the manifold's suction (low pressure) hose to the evacuation valve inside the valve box.
See Figure 4-21.
5. Open the suction valve on the manifold and pressurize the refrigerant line and cryosurface to
70-140 kPa (10-20 psig). This adds refrigerant trace gas to the system.
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Polycold Cryochiller Installation
Installation and Operation Manual Check the Refrigerant Line and Cryosurface for Leaks
6. When the refrigerant line is pressurized, close the suction valve and disconnect the refrigerant cyl-
inder.
NOTICE
Improper pressurization can damage refrigerant lines or system components.
Do not pressurize the refrigerant line and cryosurface above 3100 kPa (450 psig)
with the cryosurface attached to the system. The pressure relief valve may leak
if it is activated.
7. Connect the nitrogen cylinder to the center port of the manifold. See Figure 4-21.
8. Open the suction valve and increase the pressure in the refrigerant line and cryosurface to 1030
kPa (150 psig).
Refrigerant
Gas
R134a
Dry
Nitrogen
Gas
10. Use a halogen leak detector to check each connection in the refrigerant circuits. This includes the
Parker UltraSeal compatible or Cajon VCR couplings, the Evacuation Valve, and all brazed joints.
The couplings have two small access holes on each nut to help find leaks. Cover the lower access
hole with a finger and put the sensor at the higher hole. See Figure 4-23.
NOTE: If there is a large leak and the source cannot be pinpointed without activating the leak
detector, open the manifold's suction valve until the pressure drops to about 345 kPa (50
psig). This should allow detection of the source of the leak.
Brooks Automation
214072 Revision B 4-29
Installation Polycold Cryochiller
Check the Refrigerant Line and Cryosurface for Leaks Installation and Operation Manual
Chemical Hazard
The blend of refrigerants used in the Polycold Cryochiller is non
flammable and non toxic. However, as with any gas, asphyxiation
could occur if concentrated refrigerant gas is inhaled.
• Service the Polycold Cryochiller in a well ventilated area.
• Never add refrigerant to a unit with a leak. Locate and repair any
leaks prior to adding refrigerant or re-charging.
11. If the pressure in the manifold has decreased below 1030 kPa (150 psig), use leak detector soap
and an inspection mirror to locate the source of the leak.
12. If a leak is found, correct the leak using one of the steps below and retest:
• To correct a leak on a Parker UltraSeal compatible or Cajon VCR coupling, follow the steps in
Correct a Leak in a Parker UltraSeal Compatible or Cajon VCR Coupling on page 4-31.
• To correct a a leak on a brazed joint or a valve, contact Brooks Service for assistance.
13. If no leaks are found, verify the manifold pressure is still 1030kPa (150 psig).
14. If the pressure in the manifold stays at 1030 kPa (150 psig), follow these steps:
a. Close the valves on the manifold.
b. Disconnect the equipment from the manifold, but leave the manifold connected to the evac-
uation valve on the refrigeration unit.
15. Go to the Installation Checklist Table 4-1. Initial and date this task. Go to the next task on the check-
list.
Brooks Automation
4-30 214072 Revision B
Polycold Cryochiller Installation
Installation and Operation Manual Check the Refrigerant Line and Cryosurface for Leaks
1. Cover the lower access hole with a finger and apply leak detector soap to the higher
access hole. Observe the higher access hole for at least 2 minutes.
Brooks Automation
214072 Revision B 4-31
Installation Polycold Cryochiller
Evacuate the Refrigerant Line and Cryosurface Installation and Operation Manual
Item Description
Chemical Hazard
Failure to have a qualified refrigeration technician do all refrigera-
tion work could result in personal injury or system damage.
• Have a qualified refrigeration technician do all refrigerant work.
1. Connect the vacuum pump, vacuum gauge, and service manifold. See Figure 4-24.
Figure 4-24: Cold Valve Box Setup to Evacuate Refrigerant Line and Cryosurface
Brooks Automation
4-32 214072 Revision B
Polycold Cryochiller Installation
Installation and Operation Manual Evacuate the Refrigerant Line and Cryosurface
3. On the following valves, remove the solenoid coils and place coil magnets on the valve stems:
See Figure 4-25, Figure 4-26, and Figure 4-27.
• Single Circuit:
VLV5 in the cold valve box
VLV6 in the warm valve assembly.
• Dual Circuit:
VLV5, VLV11 in the cold valve box
VLV6 and VLV12 in the warm valve assembly.
VLV5
Cool Ckt 1
VLV11
Cool Ckt 2
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214072 Revision B 4-33
Installation Polycold Cryochiller
Evacuate the Refrigerant Line and Cryosurface Installation and Operation Manual
Rear
Of Unit VLV6
Defrost Ckt 1
VLV12
Defrost Ckt 2
Front
Of Unit
4. Turn on the vacuum pump and evacuate the refrigerant line and cryosurface to 13Pa (0.1 torr).
NOTE: The vacuum pump should evacuate the refrigerant line and cryosurface to 13Pa (0.1 torr)
within 30 minutes.
If not, there may be a leak which must be corrected.
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Polycold Cryochiller Installation
Installation and Operation Manual Evacuate the Refrigerant Line and Cryosurface
NOTICE
Improper tightening of the refrigerant lines or caps may cause damage or leaks.
Always use correct size wrench
Always use two wrenches when connecting to or installing the refrigerant lines or
cap on the evacuation valve.
• Use one wrench to hold the valve nut.
• Use the other wrench to tighten the fitting or cap.
NOTICE
It is very important to re-install the protective cap and flare nut with bonnet onto
the evacuation valve to prevent refrigerant leaks.
9. Go to the Installation Checklist Table 4-1 on page 4-2. Initial and date this task. Go to the next task.
Brooks Automation
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Installation Polycold Cryochiller
Connect the Refrigerant Line Thermocouples (Type T) Installation and Operation Manual
Item Description
Table 4-3: Complete Thermocouple List for Unit with All Options
Thermo- Customer-
Description Note
couple Installed
TC3 C1 Return
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4-36 214072 Revision B
Polycold Cryochiller Installation
Installation and Operation Manual Connect the Refrigerant Line Thermocouples (Type T)
NOTE: If the refrigerant line was made by someone other than Polycold, make sure the thermo-
couples are properly installed. Refer to Install the Refrigerant Lines on page 4-19.
Thermocouple Thermocouple
Terminal Block Wiring
Pass-Through
1. Locate the low voltage box on the refrigeration unit and remove the terminal access
cover. See Figure 4-29.
To access the pass through, push in on the foam insulation at the left corner of the coolant sup-
ply-return connections and pass the wires behind the sheet metal front panel. Then, pass the wires
behind the interface panel and to the thermocouple terminal block.
3. Locate the external thermocouple terminal block in the low voltage box. See Figure 4-29
Brooks Automation
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Installation Polycold Cryochiller
Connect the Refrigerant Line Thermocouples (Type T) Installation and Operation Manual
4. On the refrigerant line, locate the thermocouple wires labeled COIL IN and COIL OUT.
a. Fold a small piece of tape around each thermocouple wire next to its label.
b. Label the tape “Circuit 1” on the COIL IN and COIL OUT thermocouple wires coming from
the first refrigerant circuit.
c. Label the tape “Circuit 2” on the COIL IN and COIL OUT thermocouple wires coming from
the second refrigerant circuit.
5. Strip about 1/4 inch (6 mm) of insulation from the end of each thermocouple wire.
NOTICE
Do not nick the conductor. The wire may break at the nick from system vibration
and can result in damage to the equipment.
6. Attach the thermocouple wires to their designated locations. See Figure 4-30 and Table 4-3
• The blue-insulated copper wire must be attached to the positive (+) terminal.
• The red-insulated constantan wire must be attached to the negative (-) terminal
• Torque terminal screws to 0.34Nm (3 lb-in).
• Refer to the System Wiring Diagram provided with your system
7. Minimum recommended Thermocouple usage is Coil In and Coil Out for each refrigerant circuit.
Cool plates should also have a Thermocouple.
Additional Thermocouples can be added by the user as desired.
If you are working on a single circuit Polycold Cryochiller, connect the Thermocouple wires as fol-
lows:
• Position # 9: COIL IN
• Position # 10: COIL OUT
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Polycold Cryochiller Installation
Installation and Operation Manual Preliminary Check of the Polycold Cryochiller
If you are working on a dual circuit. Polycold Cryochiller, connect the Thermocouple wires as fol-
lows:
• Position # 9: #1 Line COIL IN
• Position # 10: #1 Line COIL OUT
• Position # 11: #2 Line COIL IN
• Position # 12: #2 Line COIL OUT
8. Go to the Installation Checklist Table 4-1. Initial and date this task. Go to the next task on the check-
list.
Item Description
NOTICE
Do not open the isolation valves at this time or the unit may be damaged.
Follow the instructions that follow in proper sequence to avoid damage to the
equipment.
1. Make sure you have performed all of the tasks up to this point on the installation check-
list.
2. Perform the following tasks before opening the isolation valves on the refrigeration unit: Refer to
Figure 4-31
a. Check the Refrigerant Line and Cryosurface for Leaks
b. Evacuate the Refrigerant Line and Cryosurface
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Installation Polycold Cryochiller
Preliminary Check of the Polycold Cryochiller Installation and Operation Manual
Circuit 1 Circuit 1
Feed Line Return Line
Circuit 2
Return Line
Circuit 2
Feed Line
VLV5
Cool Ckt 1 MV107
Evac Ckt 1
VLV11 *
Cool Ckt 2
MV101
MV102 Hot Gas Feed
Cold Gas Feed
MV103
Common
Return
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Polycold Cryochiller Installation
Installation and Operation Manual Insulate Exposed Refrigerant Tubes and Couplings
3. Open the cold box on the right top panel of the refrigeration unit and locate the red hand valves.
5. Turn each of these hand valves completely counter-clockwise to fully open each valve.
6. Turn each hand valve clockwise 1/4 turn from full open.
The pressure may drop 35-70 kPa (5-10 psig) as the refrigerant mixture enters the refrigerant line
and cryosurface.
13. Go to the Installation Checklist Table 4-1. Initial and date this task. Go to the next task on the check-
list.
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Installation Polycold Cryochiller
Insulate Exposed Refrigerant Tubes and Couplings Installation and Operation Manual
Item Description
NOTICE
Armaflex tape is extremely difficult to remove and makes the feed-through nut
bind when unscrewed and may result in damage to the equipment.
• Do not get Armaflex tape or Armstrong 520 adhesive in the threads of the
feed-through.
Insulate exposed tubes between the refrigeration unit and the refrigerant line insulation:
1. Cut the tubes of insulation so that they will fit snugly between the refrigeration unit and
the refrigerant line's insulation. Cut each tube of insulation lengthwise.
2. Fit a smaller diameter tube of insulation around each exposed tube. Apply adhesive to the length-
wise slits in the insulation. Close the lengthwise slits to form an air-tight seal.
3. Fit the larger diameter tubes of insulation around the smaller diameter tubes of insulation. Seal
each lengthwise slit shut with adhesive. (It is best to stagger the lengthwise seams.)
4. Cover the insulated refrigerant line bundle with a spiral wrap of Armaflex Insulation Tape. Overlap
the previous wrap of insulation tape by at least 1 inch to ensure there are no gaps.
Alternately, cut sheet insulation the same length as the tubes of insulation and wrap the sheet once
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Polycold Cryochiller Installation
Installation and Operation Manual Insulate Exposed Refrigerant Tubes and Couplings
around the refrigerant line bundle, allowing the sheet to overlap 2-3 inches (50-75 mm). Put adhe-
sive on the last 1-1.5 inches (25-40 mm) of the overlapping sheet to secure it in place.
5. Seal both ends of the refrigerant line bundle with tape or insulation tape. Secure the insulation
around the refrigerant line bundle to the refrigerant line's insulation and to the unit's panel. Flare the
tape so that it connects the insulation directly to the Polycold Cryochiller panel.
6. Use the tape or sheet Insulation to insulate all remaining exposed tubes and refrigerant compo-
nents between the refrigerant line insulation and the feed-through.
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Installation Polycold Cryochiller
Insulate Exposed Refrigerant Tubes and Couplings Installation and Operation Manual
Small Diameter
Circuit 1 Insulation on
Refrigerant Refrigerant Line
Lines
Large Diameter
Circuit 2 Insulation on
Refrigerant Refrigerant Line
Lines (with seams offset)
(optional)
Outer Wrap of
Sheet Insulation or
Armaflex Insulation Tape
on Refrigerant Line Bundle
Figure 4-34: Cutaway View A-A Showing Sheet Insulation on Refrigerant Lines at Polycold Cryochiller
Small Diameter
Insulation on
Refrigerant Line
Outer Wrap of
Sheet Insulation or
Armaflex Insulation Tape
on Refrigerant Line Bundle
Figure 4-35: Cutaway View B-B Showing Sheet Insulation on Refrigerant Lines to Cryosurface
7. Cover the exposed tubes between the pre-insulated refrigerant line and the feed-through with a spi-
ral wrap of Armaflex Insulation Tape. Overlap the previous wrap of insulation tape by at least 1 inch
to ensure there are no gaps.
If using sheet insulation, fit the sheet of insulation onto the exposed tubes. Wrap the insulation
around the exposed tubes three times. Put adhesive on the last 1-1.5 inches (25-40 mm) of the
overlapping sheet to secure it in place.
Seal both ends of the insulation with tape to secure the insulation on to the insulation on the refrig-
erant lines and to the feed-through. Do not put the tape closer than 1-2 inches (25-50 mm) to the
threads on the feed-through.
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Polycold Cryochiller Installation
Installation and Operation Manual Insulate Exposed Refrigerant Tubes and Couplings
Figure 4-36: View of Armaflex Insulating Tape on Refrigerant Line Bundle on Polycold Cryochiller
8. Go to the Installation Checklist Table 4-1. Initial and date this task. Go to the next task on the check-
list.
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214072 Revision B 4-45
Installation Polycold Cryochiller
Startup and Test Installation and Operation Manual
Item Description
Electrical Category Type 2 - Equipment is energized. Energized circuits are covered or insulated
The Startup and Test section requires that the Polycold Cryochiller is fully installed and that the vacuum
chamber is operational.
1. Confirm that cooling water is on and flowing properly through the system.
5. Wait for the system to boot up. Boot up takes less than one minute.
When boot up is complete, the system HMI screen displays information.
6. On systems equipped with the EMO, twist the EMO switch clockwise to confirm that it is in the Out
or disengaged position. See Figure 4-39
7. Move the compressor On/Off switch to the ON position. See Figure 4-39
The unit should go to the Standby mode. See Figure 4-40.
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Polycold Cryochiller Installation
Installation and Operation Manual Startup and Test
8. Let the unit stay in the Standby mode for 30 minutes for the "Polycold Stack" to reach operating
temperature. The Polycold Stack is the heat exchangers and other components that are encased
in insulating foam
9. Evacuate the vacuum chamber where the cryosurface is installed to at least 0.01 torr (1.33 Pa)
13. Check the coil inlet and coil outlet temperatures to make
sure that they reach the desired temperatures.
17. For systems with dual refrigerant circuits, repeat steps 9 Figure 4-42: Select Cool Mode
through 16 for channel 2.
18. Go to the Installation Checklist Table 4-1. Initial and date this task. Go to the next task on the check-
list.
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Installation Polycold Cryochiller
Evaluate the Polycold Cryochiller / Place Into Service Installation and Operation Manual
Item Description
Electrical Category Type 2 - Equipment is energized. Energized circuits are covered or insulated
This section requires that the Polycold Cryochiller Startup and Test procedure is complete and the unit
is still running in Standby.
Unless you are installing a remote interface, this is the last task for installing a Polycold Cryochiller.
Electric Shock
The compressor electrical box contains hazardous voltages. Fail-
ure to have a qualified electrician do all electrical work could result
in serious injury or death.
• Do not reach inside the unit with power applied.
• Have a qualified electrician perform all electrical work.
Extreme Temperatures
The compressor's heads and discharge line may be hot when
operating. Contact with the hot surface may result in minor or mod-
erate injury.
• Do not reach inside the compressor compartment when the unit
is operating.
• Do not touch the compressor's heads or discharge lines.
1. With the Polycold Cryochiller in Standby, make sure the minimum water flow rate is
adequate for the temperature of the water. See Cooling Water on page 3-6.
2. Select LOCAL.
3. Listen to the compressor. It should run continuously without cycling or turning off.
4. If the back side of the system is not accessible, disregard this step.
If the back side of the system is accessible, remove the unit's lower rear panel and locate the oil
sight glass on the body of the compressor. Oil level should be 1/8 to 1/2 full on a compressor that
has been running for at least 60 minutes. Preferred level is 1/8 full. See Figure 4-43.
Record the compressor oil level after the compressor has run for at least 60 minutes.
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Polycold Cryochiller Installation
Installation and Operation Manual Evaluate the Polycold Cryochiller / Place Into Service
Oil Level
Sight Glass
7. Evacuate the vacuum chamber where the cryosurface is installed to at least 0.01 torr (1.33 Pa).
NOTE: If a dual circuit system, select Cool for both refrigerant circuits.
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Installation Polycold Cryochiller
Evaluate the Polycold Cryochiller / Place Into Service Installation and Operation Manual
9. Check the outlet temperature of the cooling water. The drain line (OUT) should be 16 to 41°C (60
to 105°F) If not, adjust the water flow to attain a temperature in this range.
10. If there is any ice or water on the refrigerant line, turn off the unit and remove the ice or water. Apply
additional insulation at the points where ice was formed or another complete layer of insulation if
the lines were icy. Re-evaluate the cryopump starting at Step 1 of this section.
MAXIMUM 20 °C 20 °C
COIL IN -COIL OUT __________°C
DIFFERENCE
NOTE: If a dual circuit system, select Defrost for both refrigerant circuits.
13. Record the time it takes for the cryosurface to defrost. Actual Defrost Time:________ minutes
When Defrost completes, the unit automatically switches to Standby. Default temperature is 20 C.
14. Open the vacuum chamber. The cryosurface should be dry and at room temperature or warmer.
15. Recheck the balance pressure, see Table 3-10, and cooling water temperature, see Table 3-6, to
verify that the Polycold Cryochiller is operating within specifications. Check that TC8, and TC10 if
a dual circuit, are at or near 20C.
16. Record all measurements taken in this task in a maintenance log for future use as a baseline.
17. Go to Installation Checklist Table 4-1. Initial and date this task. Go to the next task on the checklist.
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Polycold Cryochiller Installation
Installation and Operation Manual Install Seismic Restraints
Item Description
Electrical Category Type 2 - Equipment is energized. Energized circuits are covered or insulated
The Cryochiller is provided with four (4) seismic anchor points for mounting seismic restraints. Two (2)
anchor points are located on the left and on the right side of the frame. See Table 4-6 for dimensions.
Seismic bracket design and construction is the responsibility of the facility where the Cryochiller is
installed.
Item Description
Mounting Hole Size (2) 9/16 inch (14.28mm) thru holes on the left side and on the
right side of the bottom frame
Fasteners on System Up to 1/2 inch (M12) hardware including backing flat washers
against the inside Cryochiller frame.
1. Confirm that the Cryochiller is in its final position and adequate access for operation
and service is provided.
2. Secure the seismic brackets to the Cryochiller using 1/2 inch (12mm) hardware. Use flat washers
for backing against the inside frame. Use lock washers as appropriate.
3. Secure the seismic brackets to the floor using appropriate hardware as required by the bracket
design and facility or local regulations.
5. Go to the Installation Checklist Table 4-1. Initial and date this task.
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Installation Polycold Cryochiller
Install Seismic Restraints Installation and Operation Manual
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Polycold Cryochiller
Installation and Operation Manual
5 Interfacing
Interfacing refers to the methods for communication with or control of the Polycold Cryochiller.
The Polycold Cryochiller interfaces with many different communication and control protocols. Actual
available interfaces is dependent on the model. The available interface options are as follows:
• RS-232 (standard)
• Gauge Relay (standard)
• Human Machine Interface (HMI) (standard)
• Ethernet - Host and Service
• Profibus
• DeviceNet
• 24V DI/DO Remote
All interfaces either connect to external terminals on the Remote Interface Panel or pass through the
panel and connect on the panel on the top of the Low Voltage Box. The connections that are available
on each unit depend on the communications options ordered with that unit.
Remote Interface
Panel
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Interfacing Polycold Cryochiller
RS-232 Interface Installation and Operation Manual
RS-232 Interface
Cable Standard RS-232 Null Modem cable with 9-pin D male connector
RS-232
Connection
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Polycold Cryochiller Interfacing
Installation and Operation Manual Gauge Relay (J4)
The Gauge Relay connection provides external control to place each refrigerant circuit into Cool Mode.
Item Description
Cable Terminal Pins (4) crimp-style male pins for 16 to 18AWG wire size.
Circuit 2 Control Pins 3 and 4 (Only on units with full Circuit 2 control)
When the refrigerant circuit is in Standby mode and the Gauge Relay is enabled and the appropriate
Gauge Relay contact pair is provided a 24V AC/DC (-25%/+17%) 10MA input voltage across a Gauge
Relay pin pair, the selected refrigerant circuit goes into the current default Cool mode.
Example: A Granville-Phillips (G-P) Mini-Convectron® Gauge is used to control circuit 1. This gauge
has a pair of Process Setpoint Relay contacts that close when the gauge detects the setpoint pressure.
• One side of the relay contacts on the
gauge is connected to a 24V power
source. Gauge
Relay
• The other side of the relay contacts on Connection
the gauge is connected to either pin 1
or pin 2 of the Polycold Cryochiller
Gauge Relay input.
• Common for the 24V power source is
connected to the remaining pin 2 or pin
1 of the Polycold Cryochiller Gauge
Relay input.
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Interfacing Polycold Cryochiller
Human Machine Interface - HMI Installation and Operation Manual
The HMI consists of a 4-line display and a keypad for navigation and selection.
Navigation Keys
Cool/Standby/Heat Keys
Each Mode has a green LED which is illuminated when the mode is active.
Remote Key
OK LED
• If OK LED is lit, indicates compressor contactor is closed. (compressor on)
• If OK LED is not lit, indicates compressor contactor is not closed.
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Polycold Cryochiller Interfacing
Installation and Operation Manual HMI Display
Fault LEDs
Fault LED (amber and red) indicates a warning or fault has occurred.
Red fault LED is reserved for High Pressure Faults
Some Faults cause the compressor contactor to open (Compressor OFF)
Reset Button
HMI Display
Use Navigation keys to move to each display menu and make selections.
• HMI display is 4 rows with 20 characters per row.
• Use Arrow keys to scroll cursor up and down through current screen selections
• Use Enter key to select highlighted item.
• Pressing an Arrow key to move the cursor past the end of a nested display returns you to the
next higher display.
• If highlighted item has an right arrow (>), then Enter will bring you to a nested sub-menu.
• If highlighted item does not have a right arrow (>), then Enter toggles the selection or allows
data entry using the up and down arrows.
HMI Display
• Press the up and down arrow key to advance to additional items on the same menu.
• Asterisk at the end of a menu item (*) indicates the current setting.
• Up and down arrows in the display indicate more display selections are available. Use the up
and down arrows to advance up and down in the display.
• Right arrow (>) at the end of a menu line indicates this entry has additional nested pages. Use
the Enter key to display the nested menu.
• After a period of inactivity, the display selection returns to the previous display until it reaches
the Home Screen Display. The period of inactivity is configurable.
• Selecting a nested display opens the nested display at the selection that was last displayed.
• Numeric values in the display may be either a reported value or a set point value.
• Reported display values cannot be changed.
• Set point display values may be changed by using the Enter key to open the value for setting
and then using the up and down arrows to change the value of each digit and using the Enter
key to move to next digit and then use the Enter at the last digit to store the value.
• Display illustrations in this chapter show the full list of screen options for each nested display.
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Interfacing Polycold Cryochiller
HMI Display Installation and Operation Manual
Home Screen is the default HMI display that is displayed at initial power up and after a configurable
internal 30 seconds (default) of HMI keyboard inactivity at each of the nested menus.
The 4-line display shows the mode for each circuit plus user programmable information as shown in the
tables below.
LN2, LN3 and LN4 values are programmed from the appropriate HOME SCREEN LN(number) MEAS
selection in the MONITOR CONFIG display under CONFIGURATION display. Selecting the blank
selection for the LN value leaves that line blank.
1 user selected value from LN2 list Static display of selected LN2 value
1 user selected value from LN3 list Static display of selected LN3 value
Up to 8 user selected values from Static display if only 1 LN4 value is selected.
LN4 list
Scrolling display of all selected LN4 values if 2 or more
values are selected.
Table 5-2: Default HMI Home Menu for Dual Circuit Units
1 user selected value from LN3 list Static display of selected LN3 value
Up to 8 user selected values from Static display if only 1LN4 value is selected.
LN4 list
Scrolling display of all selected LN4 values if 2 or more
values are selected.
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Polycold Cryochiller Interfacing
Installation and Operation Manual HMI Display
CKT 1 MODE
C1 MODE
C2 MODE
COOL
MONITORED TEMP XXX.X
STANDBY*
USER MONITORED XXX.X
DEFROST
COMPRESSOR ON*
COMPRESSOR OFF
Go to
SYSTEM STATUS
System Status
SHOW ALL> on page 5-8
CRYO COOLER>
CKT1 STATUS>
CKT2 STATUS>
STACK STATE SCREEN>
FAULT STATE
NO FAULT
CONFIGURATION Go to
Configuration
CONTROL CONFIG>
MONITOR CONFIG>
Page 1 on page
SET COMM PARAMS> 5-9
SET PRESSURE UNITS>
DATE XX-XX-XXXX
TIME XX:XX:XX
SERVICE MENU Go to
S/N XXXXXXXXX
Basic Service
M/N XXXXXXXXX on page 5-13
SW VER XX.XX.XX.XX
DSP VER XX.XX.XX.XX
CPRS HRS XX
LAST RCHG
AUTHORIZATION CODE
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Interfacing Polycold Cryochiller
HMI Display Installation and Operation Manual
System Status
From
HMI Top Menu
On Page 5-8
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Polycold Cryochiller Interfacing
Installation and Operation Manual HMI Display
Configuration Page 1
From
HMI Top
Menu on
page 5-7
See Also
Configuration
Page 2 on page
5-10
CONTROL CONFIG
LOCAL / REMOTE
CONTROL PARAMETERS>
SET CKT1 COOL MODE>
SET CKT1 DEFR MODE>
SET CKT2 COOL MODE>
SET CKT2 DEFR MODE>
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Interfacing Polycold Cryochiller
HMI Display Installation and Operation Manual
Configuration Page 2
From
HMI Top Menu
on page 5-7
See Also
Configuration
Go to
Set Comm
Parameters on
page 5-12
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Polycold Cryochiller Interfacing
Installation and Operation Manual HMI Display
Control Parameters
From
Configuration
Page 1 on
page 5-9
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Interfacing Polycold Cryochiller
HMI Display Installation and Operation Manual
From
Configuration
Page 2 on
page 5-10
MANUAL> COMP SIGNAL LOGIC > COMM SPEED> COMM SPEED XXX
INFO> RMT SIGNAL LOGIC > MAC ID> ADDRESS>
OP MODE LOGIC >
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Polycold Cryochiller Interfacing
Installation and Operation Manual HMI Display
Basic Service
From
HMI Top Menu
on page 5-7
SERVICE MENU
S/N XXXXX
M/N XXXXXXXXXX
SW VER XX.XX.XX.XX
DSP VER XX.XX.XX.XX
CPRS HRS XX
LAST RCHG NONE
AUTHORIZATION CODE>
AUTHORIZATION CODE
0.*.*.*.*.*
Go to
Service
Manual
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214072 Revision B 5-13
Interfacing Polycold Cryochiller
Ethernet Installation and Operation Manual
Ethernet
Host and Service Ethernet communication is an available option on some packages. Ethernet connec-
tion requires specific protocols for setting IP and Mask addresses. Set the Cryochiller Ethernet settings
using the HMI - Configuration - Set Comm Params - Ethernet menus. Set PC settings as stated below.
The Cryochiller is a non DHCP connection. The host or service PC will not automatically set the IP
address. If the IP address is changed, a new connection using the new IP address must be made.
Ethernet
Host Ethernet
Connection Service
Connection
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Installation and Operation Manual Profibus
Profibus
Profibus communication is an available option. Refer to Profibus Interface User Manual, p/n 200989.
Profibus is a communication protocol designed for controlling process equipment. It uses its own hard-
ware and software command set to retrieve system data and to control some functions such as Mode
selection and turning the compressor on and off.
Speed 9.6k, 19.2K, 45.45K, 93.75, 187.5K, 500K, 1.5M, 3M, 6M, 12M
Set by: ProfiBus master controller
Read by:
Host command PROFIBUS_PARAMS,SPEED
HMI “Set Comm Params”
Profibus
Pass-Through
Profibus
Connection
in Center of
LV Top Panel
Figure 5-6: Profibus Pass-Through and Low Voltage Box Top Panel Connection
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Interfacing Polycold Cryochiller
DeviceNet Installation and Operation Manual
DeviceNet
DeviceNet communication is an available option. Refer to DeviceNet Interface User Manual, p/n
213645.
DeviceNet is a communication protocol designed to interconnect control devices for data exchange. It
uses its own hardware and software command set to retrieve system data and has the ability to control
some functions such as Mode selection and turning the compressor on and off.
DeviceNet
Connection
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Polycold Cryochiller Interfacing
Installation and Operation Manual 24V DI/DO Remote Interface
The optional 24V DI/DO interface connection allows for direct wiring for inputs to and outputs from the
Polycold Cryochiller similar to earlier PFC models.
The 24V DI/DO may be Isolated or Non-Isolated. Both isolated and non-isolated can control Single Cir-
cuit or Dual Circuit systems. See System Operational State Commands on page 7-16.
24V DI/DO Remote pins are either incoming commands or outgoing data.
• Incoming command lines carry control signals from the remote user to the Polycold Cryochiller.
• Incoming command lines are referred to as “Operate”.
• Outgoing data information lines send data from the Polycold Cryochiller to the remote user.
• Output data lines are either active or inactive.
• MaxCool Cryochiller Remote provides 2 set point relays instead of optional on the PFC.
• MaxCool Cryochiller Remote provides 1.2A maximum to power external devices.
• MaxCool Cryochiller Remote Interface does not support outgoing analog temperature signals.
• The Indicate Remote signal on the PFC goes away when in Remote mode when the compres-
sor is off. On the MaxCool Cryochiller, this signal stays on.
• This behavior is configurable in v1.4.0.3 and above by command
LEGACY_REMOTE,COMP_SIGNAL_LOGIC or from HMI -> Top Menu -> Configuration ->
Set Comm Params -> Legacy Remote -> Comp Signal Logic.
• Default behavior in v1.4.0.3 is PFC backward compatible when v1.4.0.3 is installed. Users
will see a change from the previous MaxCool behavior. In v1.4.0.3, jumping Pins 1/2 is not
necessary as this function is controlled by software.
• Remote compressor on/off is supported by the MaxCool using pins 1 and 2.
• Connect a switch or relay contact set to pins 1 and 2 to remotely control the compressor.
• Connect a jumper between pins 1 and 2 to bypass the remote compressor control.
• Customers who used J11 with a PFC unit must add a jumper between pins 1 and 2 on their
side of the 37 pin connector. See also Remote EMO Connector Wiring on page 12-7.
• This behavior is configurable in v1.4.0.3 and above by command
LEGACY_REMOTE,COMP_SIGNAL_LOGIC or from HMI -> Top Menu -> Configuration ->
Set Comm Params -> Legacy Remote -> Comp Signal Logic.
• Default behavior in v1.4.0.3 is PFC backward compatible when v1.4.0.3 is installed. Users
will see a change from the previous MaxCool behavior. In v1.4.0.3, jumping Pins 1/2 is not
necessary as this function is controlled by software.
• When both COOL and DEFROST Legacy Remote signals are High, early PFC behavior was to
put unit in Cool Mode. Original MaxCool behavior put unit in Standby Mode.
• This behavior is configurable in V1.4.0.3 and above by command
LEGACY_REMOTE,OP_MODE_LOGIC or from HMI -> Top Menu -> Configuration -> Set
Comm Params -> Legacy Remote -> Op Mode Logic.
• Default behavior in v1.4.0.3 is PFC backward compatible when v1.4.0.3 is installed. Users
will see a change from the previous MaxCool behavior.
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Interfacing Polycold Cryochiller
24V DI/DO Remote Interface Installation and Operation Manual
Connector 37 pin (Amp CPC-23) Male pins 37 pin (Amp CPC-23) Female pins
Use kit 840104-00 Use kit 840105-00
Output 24VAC (10MA) output from Polycold Internal relay contacts in the Polycold
Connections Cryochiller when active. Cryochiller close when active.
1.2 A maximum total output. Contact rating is 10A
Customer must supply external relay Customer must supply 24 V AC/DC
or indicator to detect the output. power which is returned by the output
relay contacts when output is active.
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Polycold Cryochiller Interfacing
Installation and Operation Manual 24V DI/DO Remote Interface
24V DI/DO
Remote
Connector
4 1 1 4
9 5 5 9
15 10 10 15
22 16 16 22
28 23 23 28
33 29 29 33
37 34 34 37
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Interfacing Polycold Cryochiller
24V DI/DO Remote Interface Installation and Operation Manual
If a Polycold Cryochiller with the new 24V DI/DO non-isolated interface is replacing a PFC unit that used
the standard PFC remote interface, please note that the Cryochiller isolated remote has some differ-
ences. Please carefully review the wiring information in this section.
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Polycold Cryochiller Interfacing
Installation and Operation Manual 24V DI/DO Remote Interface
If a Polycold Cryochiller with the new 24V DI/DO non-isolated interface is replacing a PFC unit that used
the standard PFC remote interface, please note that the Cryochiller isolated remote has some differ-
ences. Please carefully review the wiring information in this section.
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Interfacing Polycold Cryochiller
24V DI/DO Remote Interface Installation and Operation Manual
If a Polycold Cryochiller with the new 24V DI/DO isolated interface is replacing a PFC unit that used the
optional PFC isolated remote interface, please note that the Cryochiller isolated remote has some dif-
ferences. Please carefully review the wiring information in this section.
1. External power supply can be connected per customer requirements (reversible supply support)
2. Active HIGH inputs and active LOW outputs. - Wire as above.
3. Active LOW inputs and active HIGH outputs. - Wire as above but reverse polarity of external power supply
4. Active HIGH input and active HIGH outputs. - Connect GND signal at the INPUT_COMMON TERMINALS
(Pin 2, 14 and 24 of 37-Pin CPC connector) and +24V DC at the OUTPUT_COMMON TERMINALS (Pins 4, 6,
10 and 17 of 37-Pin CPC connector)
5. Active LOW inputs and active LOW outputs - Connect +24DC at the INPUT_COMMON terminals (Pins 2, 14
and 24 of 37-Pin CPC connector) and GND signal at the OUTPUT_COMMON terminals (Pin-4, 6, 10 and 17 of
37-Pin CPC connector)
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Polycold Cryochiller Interfacing
Installation and Operation Manual 24V DI/DO Remote Interface
If a Polycold Cryochiller with the new 24V DI/DO isolated interface is replacing a PFC unit that used the
optional PFC isolated remote interface, please note that the Cryochiller isolated remote has some dif-
ferences. Please carefully review the wiring information in this section.
1. External power supply can be connected per customer requirements (reversible supply support)
2. Active HIGH inputs and active LOW outputs. - Wire as above.
3. Active LOW inputs and active HIGH outputs. - Wire as above but reverse polarity of external power supply
4. Active HIGH input and active HIGH outputs. - Connect GND signal at the INPUT_COMMON TERMINALS
(Pin 2, 14 and 24 of 37-Pin CPC connector) and +24V DC at the OUTPUT_COMMON TERMINALS (Pins 4, 6,
10 and 17 of 37-Pin CPC connector)
5. Active LOW inputs and active LOW outputs - Connect +24DC at the INPUT_COMMON terminals (Pins 2, 14
and 24 of 37-Pin CPC connector) and GND signal at the OUTPUT_COMMON terminals (Pin-4, 6, 10 and 17 of
37-Pin CPC connector)
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Interfacing Polycold Cryochiller
24V DI/DO Remote Interface Installation and Operation Manual
1. Locate the remote control plug parts kit that shipped with the unit. Note that the cus-
tomer must provide a cable that is suitable for their interface requirements.
3. Remove no more than 13mm (1/2 inch) of the outer cable jacket that covers the cable wire bundle.
4. Strip 4mm (5/32 inch) of insulation from each of the wires and pre-tin each wire.
5. Solder each wire to the solder tail of a pin. Do not insert the wire into the hole on the solder tail.
6. Cut the heat shrinkable insulating tubes into 13mm (1/2-inch) lengths. Slide one of the insulation
tubes onto each soldered wire but do not shrink at this time.
7. Insert each pin into the appropriate contact socket on the back side of the connector. Push each pin
in until it clicks into place. Gently tug the wire to confirm the pin is properly inserted.
8. Slide the 13mm (1/2-inch) long insulating tubes down to the connector so that they cover the unin-
sulated wire and solder joint. Shrink the insulating tubes in place using a heat gun.
9. Thread the connector back shell onto the connector and screw it on until tightened firmly.
10. Install the cable clamp using the two screws provided and tighten it over the cable jacket so it firmly
holds the cable. The cable clamp may be reversed for large or small cables.
Connector Connector
Back Shell Cable Clamp
Wire Side
Figure 5-14: 24V DI/DO Remote Solder-tail Connector Wiring (non-isolated male pins shown)
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Polycold Cryochiller
Installation and Operation Manual
6 Operation
Introduction
The Polycold Cryochiller is ready to operate as soon as it is installed.
The Polycold Cryochiller has many different methods of operation that can be used to meet the specific
needs of your application.
This chapter discusses the standard operating methods as well as other methods used for a variety of
different application requirements and system configurations.
Review this chapter and your application to ensure that you use the appropriate features and get the
best performance from your system.
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Operation Polycold Cryochiller
System Components Installation and Operation Manual
System Components
Circuit 1
Lift Rings (optional) x 4
Refrigerant
Lines
Feed (left)
Return (right)
EMO Switch
(optional)
HMI Circuit 2
Display Refrigerant
and Lines
Keypad Feed (left)
Return (right)
Communications
Compressor Panel
ON/OFF Switch
Valve Access
Panel
Circuit Breakers
CB1 and CB2
(CB3 behind panel)
Power In
Cooling Water
In/Out
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Polycold Cryochiller Operation
Installation and Operation Manual Local Controls and Indicators
System
Display
System
Keypad
Control
Navigation Optional
Keys EMO
Switch
CKT 1
Control
Compressor
CKT 2 On / Off
Control Switch
(optional)
Communication
and Status
HMI Keypad
Down or Right
Arrow
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Operation Polycold Cryochiller
Local Controls and Indicators Installation and Operation Manual
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Polycold Cryochiller Operation
Installation and Operation Manual Single Circuit Modes of Operation
Standby
When the unit is in Standby, the Cool and Defrost solenoid valves are closed. The unit circulates (and
cools) the refrigerant in the “stack” in the top of the refrigeration unit. The refrigerant is not pumped to
the cryosurface. The refrigerant is coldest when the unit is operating in this mode because it has the
least heat load.
All solenoids and valves are closed when in Standby mode with the exception of the following:
• Freezeout Prevention valve logic based on the FRZ_PREVENT_SETPT Host command value
controlled around the Coldest Liquid Temperature (TC4) thermocouple reading. Default is
-148C.
• Logic associated with compressor startup where the Buffer valve may be opened
• Logic for the Cylinder Unloader solenoid for power management
If the Cylinder Unloader solenoid is enabled, it is activated if the unit is in Standby for more than the time
designated by the command POWER_MGMT_STANDBY_DELAY. Default value is 20 minutes.
E_MGMT_ENABLE is enabled by default if the system is equipped with Cylinder Unloader.
Compressor will continue to run when in Standby Mode.
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Operation Polycold Cryochiller
Single Circuit Modes of Operation Installation and Operation Manual
After power up, when the compressor is turned on, the system always defaults to Standby mode.
On system Alarm/Fault which shuts down the compressor, once the compressor is turned back on, the
system defaults to Standby mode.
Standby mode can be selected using HMI or the command line interface.
If the unit is in a Standby mode, another mode (Cool or Defrost mode) can be selected.
Cool
When the unit is put into Cool, the Cool solenoid valve opens and the Defrost solenoid valve closes.
Cold refrigerant is pumped into the feed line then to the cryosurface and cools the cryosurface and
returns through the return line to the refrigeration unit. Inside the refrigeration unit, the refrigerant
releases the heat it absorbed from the cryosurface and then it is pumped through the system to repeat
the process.
Cool Cool valve is open continuously until the unit is switched to Standby or Defrost. The cryo-
(Standard) surface gets as cold as possible as fast as possible for the applied heat load.
Defrost
When the unit is put into Defrost, the Cool solenoid valve closes and the Defrost solenoid valve opens.
Hot refrigerant is pumped from the unit into the feed line then to the cryosurface where it warms the
cryosurface and returns through the return line. The unit automatically switches to Standby when the
return temperature or coil out temperature has reached the programmable set point temperature.
Some optional configurations of the Polycold Cryochiller include multiple Defrost Modes
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Polycold Cryochiller Operation
Installation and Operation Manual Dual Circuit Modes of Operation
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Operation Polycold Cryochiller
Compressor Safety Chain Installation and Operation Manual
Compressor ON/OFF switch Switch on HMI panel controls compressor contactor. Must be manually
(SW1) turned on for contactor to close and compressor to run.
Circuit breaker CB1 (CB1) CB1 controls input power for entire compressor unit
Must be manually turned on or manually reset.
Circuit breaker CB2 (CB2) CB2 controls power to the low voltage transformers
Must be manually turned on or manually reset.
Circuit breaker CB3 (CB3) CB3 controls low voltage power to the control PC Board.
If off, the main control PC Board looses power and contactor opens
and all electrical valves close
Must be manually turned on or manually reset.
Emergency Off Button (EMO) EMO provides emergency control for compressor contactor.
(if equipped on unit) If the EMO button is pressed in, compressor contactor opens.
EMO button must be manually disengaged to enable contactor
Optional Remote Emergency Remote EMO provides remote emergency control for compressor con-
Off Button (EMO) tactor.
(if equipped on unit) If the Remote EMO connection is open, compressor contactor opens.
Remote EMO connection must be closed to enable contactor
Compressor Over Temp Over Temp switch is a thermal cut out switch located inside the com-
Switch pressor motor and wired in series with the compressor power.
Opens when compressor motor temperature is above the rated value.
Closes when compressor motor temperature is below rated value.
Pressure switch (PS1) Pressure switch is mounted in compressor discharge line. Wired in
series with EMO and SW1. Trigger pressure is preset.
Switch opens if discharge pressure is above the rated value.
Switch closes when pressure is below rated value.
Software “Thermal Overload” Software monitors system performance comparing suction and dis-
Fault charge pressures. Generates “Thermal Overload” fault when condi-
tions are met. Fault condition opens the compressor contactor.
Fault resets after a 30 minute wait period.
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Polycold Cryochiller Operation
Installation and Operation Manual Polycold Cryochiller Startup
System Boot/Power-Up
1. Before compressor power up, read the pressure gauge and compare the reading to the
recorded system static pressure. If the pressure reading is off by greater than 10%,
record the value and contact service for advice.
Compressor Startup
Use one of the following methods to start the compressor after system boot up completes.
• If the compressor switch is in the OFF position when system boot up com-
pletes, switch the compressor switch to ON
• If the compressor switch is in the ON position when system boot up completes,
toggle the compressor switch to OFF and then to ON.
• If the compressor does not startup, refer to Compressor Safety Chain on page
6-7 and Compressor Motor Troubleshooting on page 10-4.
2. Use the Remote button to set the system to Local mode (Remote LED not Lit)
4. After the compressor starts, the Standby LED is on until the operating mode is changed.
NOTE: Several conditions prevent compressor starting. See Compressor Motor Troubleshooting
on page 10-4
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Operation Polycold Cryochiller
Operating the Polycold Cryochiller with a Cryocoil Installation and Operation Manual
1. Follow the System Boot/Power-Up and Compressor Startup procedures in the previ-
ous section.
If the unit is off for more than 12 hours, it may take up to 30 minutes after going into Standby
to attain complete precooling.
4. Once the unit has cooled to the desired temperature, the circuit may be switched to Cool mode any
time after the vacuum chamber has achieved vacuum. Most users switch to Cool at crossover
when opening the high vacuum valve. The cryocoil will start capturing water vapor within 60 sec-
onds.
NOTE: Experiment to determine the shortest pumpdown time for each application.
The sooner the unit is switched to Cool, the faster the vacuum chamber's pumpdown time
will be. However, switching too soon may cause the cryocoil to capture too much water
vapor causing the cryocoil's apparent surface temperature to rise and limit the ultimate
attainable base pressure.
NOTE: You can use a relay contact from a vacuum gauge on your system to control when to switch
into cool. See Gauge Relay (J4) on page 5-3.
1. Switch the unit to Defrost using the unit's control panel or remote control.
NOTE: Start Defrost so that the cryocoil is warm before the vacuum chamber reaches atmospheric
pressure. A typical Defrost takes 4 minutes or less. The exact time depends upon the
length of the refrigerant line and the size of the cryocoil.
2. By default, the unit terminates Defrost when the return temperature of the refrigerant reaches 20°C.
This assures that no additional moisture condenses on the cryocoil from the atmosphere.
The thermocouple and the end point temperature are user configurable if a shortened Defrost cycle
is desired.
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Polycold Cryochiller Operation
Installation and Operation Manual Operating the Polycold Cryochiller with a Cryobaffle
Defrost Hazard
If large amounts of water are collected during the vacuum cycle,
liquid or ice may drop from the cryocoil during Defrost.
You may need to provide a drip pan or similar device to prevent liq-
uid water from accumulating in an undesirable location
NOTICE
Dual Polycold Cryochiller Defrosting
When defrosting one circuit while the other circuit is in Cool, the temperature of
the circuit in cool may increase.
Review the required temperatures for the affected process to make sure the
warming does not affect the process. If the temperature change is not accept-
able, wait until the completion of the cool process before performing Defrost.
Both circuits may be defrosted at the same time.
1. Switch the unit to Standby using the unit's control panel or remote control.
3. When in Standby, the refrigeration unit cools the refrigerant so the unit is ready to go into Cool
mode.
NOTE: If the unit is off for more than 12 hours, it may take up to 30 minutes after going into Standby
to attain complete precooling.
4. Evacuate the vacuum chamber where the cryobaffle is installed to at least 0.01 torr (1.33 Pa).
5. From Standby, select Cool and allow the cryobaffle to cool down.
6. Turn on the high vacuum pump. It is not necessary to wait until the cryobaffle has cooled down.
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Operation Polycold Cryochiller
Operating the Polycold Cryochiller with a Cryobaffle Installation and Operation Manual
NOTE: If the cryobaffle captures too much water, the cryobaffle's apparent surface temperature
will rise and limit the ultimate attainable base pressure. Regular defrosting is recom-
mended to "regenerate" the cryobaffle. Complete defrosting can take 8 hours or more
depending upon the amount of moisture captured, the mass of the cold surface, and the
vacuum level.
NOTICE
Do not select Defrost if the cryobaffle is not isolated from the oil diffusion or tur-
bomolecular pump. The Defrost cycle may release the captured moisture too
quickly and damage the equipment.
3. When the cryobaffle is free of moisture, return the system to Cool mode as described at the begin-
ning of this procedure.
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Polycold Cryochiller
Installation and Operation Manual
7 Host Commands
This chapter lists the common commands used by RS-232 or Ethernet for an operator to control and
configure the Polycold Cryochiller from a host or service computer. Refer to the Interface chapter in the
Polycold Cryochiller Installation and Operation manual for interconnect information.
The Host Commands are not used by Profibus or DeviceNet which each have their own communication
protocols.
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Host Commands Polycold Cryochiller
Command Format Installation and Operation Manual
Command Format
Command Format
Commands are either GET or SET commands based on comma separated parameters following the
command name. Use GET to check the status of something and SET to change a setting.
Get Example:
Get software version “$SW_VER,?P(CR)”.
Set Example:
Set cooling termination set point “DEFR_SETPT,1,19D(CR)”.
Response Format
The first character of the response from the Polycold system to the external device provides information
about the specific command received along with information about whether the command succeeded.
Letter Meaning
‘C’ Proper command, which cannot be acted upon currently for some reason which, may
be temporary or correctable. Typically because you have not entered the correct
security level.
‘F’ Invalid command or invalid data argument for the given command. Set commands
have min and max values associated with each command. If a set command uses a
value outside the min/max range, ‘F’ is the response.
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Polycold Cryochiller Host Commands
Installation and Operation Manual Command Format
Command Terms
The following will be used to represent the format of command and reply parameters.
[n] = a numeric value (0 thru 9)
[nnnn] or [nnn.n] = a multi-numeric value which may contain a decimal place
(Example: 1234 or 567.8)
[nnnnnnnn] = 32 bit number / bitfield
[c] = a character value such as an alphabetic character
[cccc] = a multi-character value which may contain alphabetic character and/or numeric values.
[A] = the reply code. The first character of the response from the Polycold system to the external
device provides information about the specific command received along with information about
whether the command succeeded. Refer to Response Code Table 7-1.
Bitfields are hexadecimal data that contain parameter data that is interpreted using the decimal value.
Follow the steps below to find the decimal values in the hexadecimal bitfield value.
• Convert the hexadecimal value to binary.
• Determine the value of each set bit by counting the binary bits starting from the least significant
bit as zero.
• Record the decimal value of all of the bits that are set.
• Look up the decimal values of each set bit in the parameter listing for the command.
4. Find the decimal value of each set binary bit by counting from the LSB with the LSB being 0.
• The table shows that hex 00002000 is decimal value 13.
5. Look up the decimal value in the parameter list. This example shows that alarm bit 13 is set.
Hex Bit Hex Digit 4 Hex Digit 3 Hex Digit 2 Hex Digit 1
Hex Value 2 0 0 0
Binary Value 0 0 1 0 0 0 0 0 0 0 0 0 0 0 0 0
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Host Commands Polycold Cryochiller
Command Format Installation and Operation Manual
Hex Bit Hex Digit 4 Hex Digit 3 Hex Digit 2 Hex Digit 1
Decimal Value 15 14 13 12 11 10 9 8 7 6 5 4 3 2 1 0
Hex Bit Hex Digit 8 Hex Digit 7 Hex Digit 6 Hex Digit 5
Hex Value 0 0 0 5
Binary Value 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
Decimal Value 31 30 29 28 27 26 25 24 23 22 21 20 19 18 17 16
Checksum Calculation
Each command must end in a valid checksum. For heavy usage, it s recommended that the checksum
be calculated using a program/script/macro.
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Polycold Cryochiller Host Commands
Installation and Operation Manual Command Format
A macro may be created in Microsoft Excel using Visual Basic to calculate a checksum of a command.
1. Open Excel.
Click the Microsoft Office button on the upper left corner.
Click on the “Excel Options” button.
Click on the check box to enable “Show Developer tab in the Ribbon”.
Click OK.
3. In the Developer Tab, Code Tab, click on “Visual Basic”. The Visual Basic program opens.
If a “Module” window does not open, click “Insert” in the Visual Basic tool bar and click “Module”.
4. Copy the command strings below and paste it into the Macro window.
Sub CalculateCheckSum()
Dim CommandString, checksum, character
Dim LengthofCommandString, Counter As Integer
checksum = 0
CommandString = Application.InputBox("Enter the Command To Calculate checkSum (ex.
SW_VER,?)", "CommandString")
LengthofCommandString = Len(CommandString)
For Counter = 1 To LengthofCommandString
character = Mid(CommandString, Counter, 1)
checksum = checksum + (Asc(character) And &H7F)
Next Counter
checksum = checksum And &HFF
checksum = &H3F And (checksum Xor (Int(checksum / (2 ^ 6))))
checksum = (&H30 + checksum) And &H7F
checksumChar = Chr(checksum)
checksumstring = "CheckSum Character is: " & checksumChar
Response = MsgBox(checksumstring, 0, "CheckSum Result")
End Sub
5. Save the Excel program using a name you might remember such as “CheckSum Macro”.
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Host Commands Polycold Cryochiller
Example of Interface Usage: Installation and Operation Manual
1. Test the Macro by closing Excel and then opening the CheckSum Macro Excel file.
2. Click on Developer tab, click Macros. Select the CalculateCheckSum Macro. Click Run.
3. Enter the sample command SW_VER,? using upper case only. Press OK.
4. Excel calculates the checksum and a checksum window appears. The window should show the
checksum is P. If not, check the command that you entered and check the macro.
5. To use the macro, follow the steps above entering the command in all caps without the $.
If the interface sends a Set command and the interface does not have control, the host will respond with
“C” which means that the command is OK but cannot be executed.
$ then response code A (accepted) then response value QF0.1.0.32 then I (response checksum)
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Polycold Cryochiller Host Commands
Installation and Operation Manual Security Levels
Most Set values for parameter Host commands are stored to non-volatile flash memory when the SET
is executed.
However, some configuration Set command values are not stored and must be set again after a power
cycle or CPU reset.
Set commands have min and max values associated with each command. If a set command uses a
value outside the min/max range, F is the response.
Set values take affect immediately and do not require a system restart or power cycle to take effect.
Security Levels
Polycold Cryochiller command functions are security protected and require that the security level be set
to a specific level in order to perform the Get or Set command functions.
• Security Level 1 - Limited Operator Access -Password: 02030A (where all 0s are zeros)
Limited user access. Allows for locking operators out of access to commands.
• Security Level 2 - Default Operator Access - Password: 02030B (where all 0s are zeros)
Normal unit access. Normal operations are available such as Cool, Defrost, Rapid BP Check.
• Security Level 3 - Some Configuration / Maintenance (manager access) Contact Brooks Poly-
cold for password Access to service menu for Zero Line Loss function to allow disconnect and
installation.
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Host Commands Polycold Cryochiller
Command Listing Format Installation and Operation Manual
User wants to set DEFR_SETPT value. This command has a Get security level of 1 and a Set level of
3. System security level is 2 by default.
• User can use a Get command for DEFR_SETPT since get is level 1.
• User cannot use Set command since the set level is 3.
• User must change the security level to 3 or above to use Set command for DEFR_SETPT.
• If a command is not accepted for security reasons, the response is “C”.
Return Value: Lists information the system returns for this command [A][nn.nn.nn.nn]
Security Level: Security required to Get the value Security required to Set the value
Command Description
SENSOR_SNAPSHOT Returns value of all current system thermocouple and state of all
system commanded valves
Return value:
1e70ff7f,0,23.5,23.5,23.5,171.8,171.8,171.8,121.1,0.0,171.8,171.8,
171.8,171.8,171.8,171.8,171.8,171.8,0.0,0.0,0.0,0.0,23.9,25.2,
0.0,0.0,0.0,0.0,0.0,180.6,92.0,0.0,0.0,0.0,0.0,0
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Polycold Cryochiller Host Commands
Installation and Operation Manual System Configuration Commands
Command Description
COMP_MOTOR_STATE Get / Set the current state of the Compressor Motor ON/OFF
Purpose: Returns identifier strings for the current software version and build number.
Parameter(s): ?
Return Value: [A][nn.nn.nn.nn] (major.minor.patch.build)
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Host Commands Polycold Cryochiller
System Configuration Commands Installation and Operation Manual
Parameter(s): ?
Example: “VENDOR_ID,?”
Interface RS-232, Ethernet
IP_ADDR IP Address
Parameter(s): ? or [nnn.nnn.nnn.nnn]
[nnn.nnn.nnn.nnn] is the IP address
Parameter(s): ? or [nnn.nnn.nnn.nnn]
[nnn.nnn.nnn.nnn] is the Gateway address
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Polycold Cryochiller Host Commands
Installation and Operation Manual System Configuration Commands
Parameter(s): ? or [nnn.nnn.nnn.nnn]
[nnn.nnn.nnn.nnn] is the Network Mask address
Example: “DEVICENET_PARAMS,?”
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Host Commands Polycold Cryochiller
System Configuration Commands Installation and Operation Manual
Parameter(s): ? or [nnnn]
[nnnn] is HMI timeout in seconds
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Polycold Cryochiller Host Commands
Installation and Operation Manual System Configuration Commands
Purpose: Get/Set the Legacy Remote compressor input signal logic. Default setting is
equivalent to jumper “J11” being placed on PFC system control board. The
compressor will not be controlled by Legacy Remote compressor on/off input
signal.
Parameter(s): ? or [n]
[n]
0 = Compressor controlled by Legacy Remote compressor input signal
Equivalent to “J11” jumper being removed from PFC system control board
1 = Compressor not controlled by Legacy Remote compressor input signal.
Equivalent to “J11” jumper being placed on PFC system control board
Units: N/A
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Host Commands Polycold Cryochiller
System Configuration Commands Installation and Operation Manual
Purpose: Get/Set the Legacy Remote, remote output signal logic. Default setting is to
remain compatible with remote signal functionality on PFC. The remote output
signal will be Low when the Compressor is off regardless of unit being in Local
or Remote control.
Parameter(s): ? or [n]
[n]
0 = Remote output signal will be:
Low when compressor is Off in Local Control
High when compressor is Off in Remote Control
Original MaxCool remote signal logic
1 = Remote output signal will be:
Low when compressor is Off in Local Control
Low when compressor is Off in Remote Control
Original PFC remote signal logic
Units: N/A
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Polycold Cryochiller Host Commands
Installation and Operation Manual System Configuration Commands
Purpose: Get/Set the Legacy Remote, operating mode logic when cool and defrost sig-
nals are both High. Default setting is to remain compatible with operating
mode functionality on PFC. When the Cool and Defrost input signals are both
High, the unit will switch to Cool operating mode.
Parameter(s): ? or [n]
[n]
0 = When both Cool and Defrost input signals are High, system will switch to
Standby Mode
Original MaxCool mode signal logic
1 = When both Cool and Defrost input signals are High, system will switch to
Cool Mode
Original PFC mode signal logic
Units: N/A
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Host Commands Polycold Cryochiller
System Operational State Commands Installation and Operation Manual
Purpose: Get/set the default system control mode on startup. This command does
not actually change the mode.
Parameter(s): ? or [mode]
[mode] is
0 = local mode
1 = remote Ethernet
2 = remote RS232
3 = remote RS485 (Not supported)
4 = remote 24V DI/DO Remote
5 = remote DeviceNet
6 = remote Profibus
Return Value: [A] or [A][n]
Parameter(s): ? or [mode]
[mode] is
0 = local mode
1 = remote Ethernet
2 = remote RS232
3 = remote RS485
4 = remote 24V DI/DO Remote
5 = remote DeviceNet
6 = remote Profibus
8 = Default Control Mode (SYSTEM_CONTROL_MODE_DEF)
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Polycold Cryochiller Host Commands
Installation and Operation Manual System Operational State Commands
Parameter(s): ?
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Host Commands Polycold Cryochiller
System Operational State Commands Installation and Operation Manual
Example: “FAULT_STATUS,?”
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Polycold Cryochiller Host Commands
Installation and Operation Manual System Operational State Commands
Return Value: [A] or [A], [alarm status bits] or [A], [circuit 1 alarm status bits], [circuit 2
alarm status bits]
The alarm name and status.
“alarm name” is the name used to refer to the alarm
“alarm status bits” is a bit field with the following values:
bit 0: 0 = warning, 1 = alarm
bit 1-4: alarm or warning level as an integer.
bit 5: alarm clear state (0 = not cleared, 1 = cleared)
bit 6: alarm acknowledge state (0 = not acknowledged, 1 = acknowl-
edged)
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Host Commands Polycold Cryochiller
System Operational State Commands Installation and Operation Manual
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Installation and Operation Manual System Operational State Commands
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Host Commands Polycold Cryochiller
System Operational State Commands Installation and Operation Manual
Purpose: Get/Set the target temperature used to define the normal capacity for non-tem-
perature controlled cooling modes to engage power management mode.
Parameter(s): ? or [nnnn]
[nnnn] is target temperature
Return Value: [A] or [A][nnnn]
Parameter(s): ? or [nnnn]
[nnnn] is delay in seconds
Return Value: [A] or [A][nnnn]
Units: Seconds
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Polycold Cryochiller Host Commands
Installation and Operation Manual System Sensor Readings
Monitor Data:
Parameter(s): ? or [n]
[n] is
1 = enabled
0 = disabled
Default Value: 1
Min: 0 Max: 1
Units: N/A
Parameter(s): ?
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Host Commands Polycold Cryochiller
System Sensor Readings Installation and Operation Manual
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Polycold Cryochiller Host Commands
Installation and Operation Manual System Sensor Readings
Purpose: Get the open/closed state of a system valve. A value of 1 indicates the
valve is open. A value of 0 indicates the valve is closed.
Parameter(s): [n],?
[n] is Valve identifier:
0 = Buffer
1 = Not Used
2 = Not Used
3 = Cylinder Unloader
4 = Freeze Out Prevention
Example: “SYSTEM_VALVE_STATE,0,?”
Note:
Purpose: Get the unit coldest liquid temperature sensor value. (TC4)
Parameter(s): ?
Return Value: [A][nnnn]
Example: “CLDST_LQD_TEMP,?”
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Host Commands Polycold Cryochiller
System Sensor Readings Installation and Operation Manual
Example: “COLD_JUNCT_TEMP,?”
Parameter(s): ?
Example: “BUFFER_LINE_TEMP,?”
Purpose: Get the Rapid Balance Pressure Check control temperature sensor
value. (TC6)
Parameter(s): ?
Example: “WARM_CTL_TEMP,?”
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Polycold Cryochiller Host Commands
Installation and Operation Manual System Actions Commands
Parameter(s): N/A
Return Value: [A]
Example: “RESET_ALARMS”
Parameter(s): ? or [n],[cccccc],[userID]
[n] is security level 1-3
[cccccc] is password
[userID] is userID string
Default Value: 2
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Host Commands Polycold Cryochiller
Compressor Configuration Commands Installation and Operation Manual
Purpose: Get / Set identifier string representing the serial number of the specified
Compressor Module.
Parameter(s): [n],? or [cccccccc]
[n] is
0 = Refrigerant compressor
1 = Nitrogen compressor
[cccccccc] is serial number string (32 character max)
Example: “COMP_SERIAL_NUM,0,?”
Purpose: Get / Set the total number of hours that the specified compressor motor
has run in its lifetime.
Example: “COMP_MOTOR_HOURS,0,?”
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Polycold Cryochiller Host Commands
Installation and Operation Manual Compressor Operational State Commands
Parameter(s): [n],?
[n] is
0 = Refrigerant compressor
1 = Not Used
Units: PSI
Example: “UNIT_BALANCE_PRESS,0,?”
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Host Commands Polycold Cryochiller
Compressor Sensor Readings Installation and Operation Manual
Parameter(s): [n],?
[n] is
0 = Refrigerant compressor
1 = Not Used
Return Value: [A][nnn.n]
Example: “COMP_DISCHRG_TEMP,0,?”
Interface RS-232, Ethernet
Purpose: Read the compressor liquid line temperature sensor value. (TC2)
Parameter(s): [n],?
[n] is
0 = Refrigerant compressor
1 = Not Used
Example: “COMP_LINE_TEMP,0,?”
Parameter(s): [n],?
[n] is
0 = Refrigerant compressor
1 = Not Used
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Polycold Cryochiller Host Commands
Installation and Operation Manual Circuit Configuration Commands
Example: “COMP_SUCT_PRESS,0,?”
Parameter(s): [n],?
[n] is
0 = Refrigerant compressor
1 = Not Used
Example: “COMP_DSCHRG_PRESS,0,?”
Purpose: Get/set the temperature set point at which to transition from Standby to Cool
mode.
Monitor Data: Coldest liquid temperature
Parameter(s): [n],?
or [n],[nnn.n]
[n] is circuit number (1or 2) or * for all circuits
[nnnn] is the set point
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Host Commands Polycold Cryochiller
Circuit Configuration Commands Installation and Operation Manual
Example: “CLDST_LQD_SETPT,1,?” Get the coldest liquid temp. set point for circuit 1
Purpose: Get/set the External Relay 1 or Relay 2 parameters These relays are internal to
the unit and contact outputs are accessible from the 24V DI/DO interface. All
MaxCool Cryochiller models equipped with a 24V DI/DO 37-pin interface include
this feature as standard.
Defines the sensor, setpoint, and parameters for sensor monitored by each relay.
Parameters:
- Relay [1..2] = Setpoint Relay 1 or Relay 2
- Setpoint Type: Sensor to monitor
None = 0,
1 = Circuit1_FeedTemp,
2 = Circuit1_ReturnTemp,
3 = Circuit1_CoilInTemp,
4 = Circuit1_CoilOutTemp,
5 = Circuit1_ProcessCtrlTemp,
6 = Circuit1_Avg_FeedReturn,
7 = Circuit1_Avg_CoilInOut,
8 = Circuit2_FeedTemp,
9 = Circuit2_ReturnTemp,
10 = Circuit2_CoilInTemp,
11 = Circuit2_CoilOutTemp,
12 = Circuit2_ProcessCtrlTemp,
13 = Circuit2_Avg_FeedReturn,
14 = Circuit2_Avg_CoilInOut,
15 = Compressor_DischargeTemp,
16 = Customer_Option1,
17 = Customer_Option2,
18 = Customer_Option3,
19 = Customer_Option4,
20 = Discharge_Pressure,
21 = Suction_Pressure
22 = Coldest_LiquidTemp ,
23 = RefrigerantLiquid_LineTemp,
24 = Not Used,
25 = Stack_WarmerTemp,
26 = Buffer_LineTemp,
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Polycold Cryochiller Host Commands
Installation and Operation Manual Circuit Configuration Commands
Parameter(s) - Relay Logic: Relay will close when either above or below Setpoint value
0: = Close_Above
1: = Close_Below
- Setpoint: Setpoint of selected sensor to initiate relay logic
- Deadband: deadband value from setpoint to open relay
Units:
Example: “SETPOINT_RELAY,1,?” Get the external vacuum device set point for Relay 1
“SETPOINT_RELAY,2,3,1,-30,5” Set the external relay set point for Relay 2,
monitor sensor Circuit1_CoilInTemp, close relay below -30c, open relay at -25c
(-30 setpoint plus the 5 degree deadband)
Purpose: Get/set the enable/disable state for using the gauge relay input to
change the mode of the circuit.
Parameter(s): [n],?
or [n],[n]
[n] is circuit number (1 or 2) or * for all circuits
[n] is the enable state of the external vacuum contact
0 = Disabled
1 = Enabled
Default Value: 0
Min: 0 Max: 1
Units:
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Host Commands Polycold Cryochiller
Circuit Configuration Commands Installation and Operation Manual
Parameter(s): [n],?
or [n],[nnn.n]
[n] is circuit number (1 or 2) or * for all circuits
[nnn.n] is the setpoint
Example: “DEFR_SETPT,1,?” Get the defrost compete set point for circuit 1.
Purpose: Get/set the enable state of the external thermocouple on the circuit. If
enabled, the external Thermocouple is used to monitor the temperature,
else the internal Return temperature Thermocouple is used.
Parameter(s): [n],?
or [n],[state]
[n] is circuit number (1or 2)
[state] is enable state
1 = Enabled
0 = Not Enabled
Default Value: 0
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Polycold Cryochiller Host Commands
Installation and Operation Manual Circuit Configuration Commands
Purpose: Get/set the alarm setpoint for the External Thermocouple if enabled.
Alarm is raised if difference between External TC temperature and
Return temperature of circuit is greater than setpoint
Parameter(s): [nnn.n] or ?
[nnn.n] is temperature difference
Default Value: 20
Units: Deg C
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Host Commands Polycold Cryochiller
Circuit Operational State Commands Installation and Operation Manual
Parameter(s): [n],?
or [n],[mode]
[n] is the circuit number (1or 2)
[mode] is
0 = COOL
1 = Not Used
2 = Not Used
3 = Not Used
4 = Not Used
5 = Not Used
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Polycold Cryochiller Host Commands
Installation and Operation Manual Circuit Sensor Readings Commands
Parameter(s): [n], ?
or [n],[mode]
[n] is the circuit number (1 or 2)
[mode] is
-1= INACTIVE (Note: Cannot “Set” this mode)
0 = STANDBY
1 = cool (default) – use the default cool mode
2 = defrost (default) – use the default defrost mode
3 = COOL
4 = Not Used
5 = Not Used
6 = Not Used
7 = Not Used
8 = Not Used
9 = DEFROST
10 = Not Used
11 = Not Used
12 = Not Used
13 = Not Used
14 = Not Used
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Host Commands Polycold Cryochiller
Circuit Sensor Readings Commands Installation and Operation Manual
Parameter(s): [n],[valve],?
[n] is circuit number (1 or 2)
[valve] is Valve identifier:
0 = Cool
1 = Not Used
2 = Defrost
3 = Not Used
4 = Not Used
5 = Not Used
Parameter(s): [n],?
[n] is circuit number (1 or 2)
Purpose: Read the circuit outlet temperature sensor value. TC10 / TC11
Parameter(s): [n],?
[n] is circuit number (1 or 2)
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Polycold Cryochiller Host Commands
Installation and Operation Manual Circuit Sensor Readings Commands
Parameter(s): [n],?
[n] is circuit number (1 or 2)
Return Value: [A][nnn.n]
Example: “CIRC_FEED_TEMP,1,?”
Purpose: Read the circuit return temperature sensor value. TC3 / TC5
Parameter(s): [n],?
[n] is circuit number (1 or 2)
Example: “CIRC_RTN_TEMP,1,?”
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Host Commands Polycold Cryochiller
Circuit Sensor Readings Commands Installation and Operation Manual
Purpose: Read the circuit process control temperature sensor value. TC7 /TC8
Parameter(s): [n],?
[n] is circuit number (1 or 2)
Example: “CIRC_PROC_CTL_TEMP,1,?”
Interface RS-232, Ethernet
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Polycold Cryochiller
Installation and Operation Manual
8 Configuration
For clarity, the letter P is used in place of the actual command checksum. See Checksum Calculation
on page 7-4 to determine the actual checksum for a specific command.
For simplicity, only a single sample of command parameters may be shown instead of listing the full set
of command options.
For full list of options for each command, go to the command description in Chapter 7: Host Commands.
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Configuration Polycold Cryochiller
Power Management - Cylinder Unloading Installation and Operation Manual
When in Standby mode, if cylinder unloading is enabled, the Cylinder Unloader goes active after a
delay period defined by the command POWER_MGMT_STANDBY_DELAY.
• E_MGMT_ENABLE,1P
Enables cylinder unloading - ? = get the status, 0 = disable, 1 = enable
• POWER_MGMT_STANDBY_DELAY,300P
Sets Cylinder Unloader to activate after the system has been in Standby mode for 300 sec-
onds and power management is enabled.
When in the Cool modes of either Standard Cool or Ramp Controlled Cool, a target temperature is used
to define the temperature at which Cylinder Unloading stays active and an additional delta temperature
that must be reached for the Cylinder Unloading to go active.
The typical temperature warming experienced with the cylinder unloader activated varies based on
application conditions. You need to verify and adjust the settings based on the performance of your
application.
• E_MGMT_ENABLE,1P
Enables cylinder unloading - ? = get the status, 0 = disable, 1 = enable
• CAPACITY_TARGET_TEMP, -120P
Sets maximum temperature of -120 for Cylinder Unloading to remain active Will only stay
active once per cycle.
• EXCESS_CAP_TEMP_DELTA,8P
Sets an 8º C delta T value that the temperature must be below
CAPACITY_TARGET_TEMP for Cylinder Unloader to begin.
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Polycold Cryochiller Configuration
Installation and Operation Manual Mode Selection
Mode Selection
All models have only one Standby mode.
Standby
Use this command to define which thermocouple to use for circuit control functions. By default, the con-
trol thermocouple for all circuit functions (i.e. defrost complete, temperature control, etc) is the Return
thermocouple for that circuit. This command allows you to select either the Coil Out, average of Coil In
and Coil Out, or customer process thermocouple.
• EXT_TC_ENABLE,1,1P enables the External Thermocouple for circuit 1.
• EXT_TC_ENABLE,1,0P enables the Internal Thermocouple for circuit 1
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Configuration Polycold Cryochiller
External Vacuum Control Installation and Operation Manual
When the circuit is in standby and the external vacuum control is enabled, a 24V signal (AC or DC)
applied to the designated contacts on the 4-pin Gauge Relay port will be detected and cause the unit
to switch to cool.
See Gauge Relay (J4) on page 5-3 for more information on the use of this feature.
• EXT_VAC_CONTACT,1,?P gets the enable/disable status of the circuit 1 Gauge Relay
control.
• EXT_VAC_CONTACT,1,1P enables the Gauge Relay input to be used for circuit 1.
A user can configure the behavior of these two relays via software. This allows the user to select the
sensor to be associated with each relay, the set point, deadband and relay logic.
See 24V DI/DO Remote Interface on page 5-17 for more information on the use of this feature.
• SETPOINT_RELAY,1,?P gets the external vacuum device setpoint for Relay 1.
• SETPOINT_RELAY,2,3,1,-30,5P sets the Relay 2 external setpoint to monitor sensor
Circuit1_CoilInTemp and close relay below -30 C with 5º C of dead band which means the
relay opens at -25º C.
• SYSTEM_CONTROL_MODE_DEF sets the default system control mode that the system
is set to on startup and that the unit goes to when the Remote key is pressed to set the unit
to remote mode.
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Polycold Cryochiller
Installation and Operation Manual
9 Preventive Maintenance
Preventive Maintenance
The best way to ensure maximum productivity for your system is through Polycold’s Preventive Main-
tenance servicing option.
Polycold recommends that the user inspect the system at daily, weekly, monthly and quarterly intervals.
Polycold recommends that every 12 months a preventive maintenance service visit is performed by
Polycold authorized service personnel.
In addition, the Polycold Engineer will record any equipment deterioration and recommend replacement
parts or repair before these items cause system failure. Preventive maintenance will result in savings
due to an increase of effective system service life.
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214072 Revision B 9-1
Preventive Maintenance Polycold Cryochiller
Preventive Maintenance Schedules Installation and Operation Manual
Interval Action
Daily Ensure the unit is functioning as expected
Weekly Ensure the unit is functioning as expected
Check Temperatures (during process)
Check Pressures (during process)
Monthly Perform Weekly Maintenance
Check Time to Cool Down
Check for air flow from E-box fans
Quarterly Perform Monthly Maintenance
Check system balance pressure
Verify LCD display is not missing characters
Verify HMI keypad / Remote Control functions properly
Verify Insulation is intact
Verify Oil Level in Compressor is appropriate
Power cycle the system. leaving it off for minimum of 10 seconds.
Replace Fan Filter (as appropriate)
Annual Perform Quarterly Maintenance
Replace fan filter (mandatory) and check fan operation
Replace valve and valve components as necessary
Review event files for errors and backup system data (future capability)
Check Cool Down Cycle Time, Pressure, and Temperature
Check Defrost Cycle Time, Pressure, and Temperature
Verify Water Flow and Temperatures
Confirm that customer-provided water filters are replaced as required
Inspect Frame, Compressor, and Components for wear
Reinsulate (as appropriate)
Perform Compressor Pump Down Test
Perform Leak Check on fittings within the Cryochiller and feedthroughs
Clean electronic control box and replace mother board battery as required
(nominally every 3-5 years)
Inspect all harness connections
Top off charge as required
Evacuate and recharge as necessary
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Polycold Cryochiller
Installation and Operation Manual
10 Troubleshooting
Troubleshooting Techniques
Successful troubleshooting involves gathering enough information and asking enough questions to
define the problem using a single statement of how the system is supposed to operate and how the sys-
tem is operating improperly.
You may be able to define and solve the problem by creating a simple statement that describes the
problem.
• Observe and list the symptoms of the problem
• Determine what is happening that is different from what should happen
• Determine the items that have the problem and those that do not
• Determine when the problem first occurred and how often it occurs
• Determine the state of the system when the problem occurred or occurs
• Reduce the list of symptoms to the primary symptom.
• List the possible causes of the symptom
• Reduce the list of causes based on what is happening and what is supposed to happen.
When contacting authorized service, have as much of the following information available as is possible.
• Record the model number, part number, and serial number from the equipment.
• Provide installed location
• Provide name, address, E-mail address, and phone number of person to contact.
• List error codes or symptoms.
• List work done on unit before problem occurred, function unit was performing when the problem
occurred, actions taken after problem occurred.
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Troubleshooting Polycold Cryochiller
Troubleshooting Tables Installation and Operation Manual
Troubleshooting Tables
Troubleshooting issues are listed in two groups:
• HMI and Observed Errors
• Remote Monitor Troubleshooting using bit mask values
Problem column shows the messages in BOLD UPPER CASE and the status of the Fault LED.
• If the system recognizes a fault, the HMI screen may display a fault message and a recom-
mended action and the Fault LED may be lit.
• If the system does not recognize a fault, the display may not provide any fault information and
the Fault LED may not be lit and the user must determine the problem.
Fault Reporting
If a Fault occurs, the HMI display automatically goes to the Fault State screen and displays the fault and
two lines of the available 3 lines of fault data using the format below:
• Line 1 - Fault State (menu selection header)
• Line 2 - Name of Fault
• Line 3 - Fault description line 1
• Line 4 - Fault description line 2, if applicable
• (scroll) - Fault description line 3, if applicable
To view current Fault information, go to the Fault State display, if required. The Fault State display
shows the current fault and descriptions as stated above.
To view additional faults, if applicable, use the down arrow to display the next fault.
To view all information for the displayed fault, press the Enter key to select the current fault and then
use the arrow keys to scroll through all three lines of information for the current fault. Note that the arrow
keys stay on the selected fault. Press the Enter key again to exit the current fault display.
To exit a selected fault, press the Enter key. The display goes back to the Fault State display and then
the arrow keys may be used to scroll through each of the active faults, if applicable.
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Polycold Cryochiller Troubleshooting
Installation and Operation Manual HMI and Observed Errors
Power Troubleshooting
Troubleshooting power requires that CB1 and CB2 are turned on.
POWER FAILURE Control voltage is outside of Check the transformer tap set-
acceptable limits. tings and ensure they are cor-
NO RECOMMENDATION rect for your supply voltage
(No HMI message) Faulty component in the power Contact authorized service
or control circuit.
No LED indicators
(No HMI message) Power consumption too close to Refer to Appendix C: CB2
CB1 maximum rated value. Excepted Wiring on page 12-5
No LED indicators
Have a qualified electrician
CB1 occasionally trips rewire CB2 to Excepted Wiring
(No HMI message) No input power Check power source fuses, cir-
cuit breakers, and wiring
No LED indicators
System does not boot up. Contact authorized service to
CB1 stays ON repair as needed
(No HMI message) Motor on/off switch fault Contact authorized service to
check the switch and replace if
Fault LED not lit required.
System boots up
Compressor will not turn on
Communication Troubleshooting
System does not communi- System electronics is “confused” Power cycle the system.
cate on RS232, Ethernet, Pro-
fibus, or DeviceNet Contact authorized Service
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Troubleshooting Polycold Cryochiller
HMI and Observed Errors Installation and Operation Manual
Troubleshooting the compressor motor requires that the Polycold Cryochiller is fully booted up.
Compressor will not start Compressor switch must be on Set compressor switch to ON.
for compressor to run.
No LEDs lit
Compressor will not start Compressor contactor circuit Turn compressor switch OFF
needs to be reset after power up. and then ON
No LEDs lit
Remote EMO connector or J11 Connect remote EMO cable or
Compressor switch is on. bypass is disconnected install J11 EMO Jumper
Compressor will not start Compressor contactor circuit Press Reset switch
needs resetting
Fault LED flashing
A Fault that opens the compres- Determine what fault is active
sor contactor is active and resolve the issue.
Compressor will not start Compressor pressure switch Wait for pressure to come down
PS1 is open indicating high dis- below the threshold level.
Fault LED flashing charge pressure
Contact authorized service if
high pressure continues
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Polycold Cryochiller Troubleshooting
Installation and Operation Manual HMI and Observed Errors
EMO SWITCH ALARM EMO switch is pressed in and Turn EMO switch clockwise to
activated disengage the switch
CHECK EMO SWITCH
Remote EMO is active - open Correct remote EMO condition
Fault LED Amber Remote EMO bypass J11 dis- Connect J11
connected
CONTACTOR CHATTERING Motor contactor is rapidly Verify power supply meets all
opening and closing requirements
CHECK POWER LINE
Verify control transformer tap
Fault LED not lit settings are correct for supply
voltage
FAN FAULT WARNING One or more electrical box cool- Check power and cable.
ing fans are not operating. Check fan operation
CHECK COOLING FAN Replace both cooling fans
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Troubleshooting Polycold Cryochiller
HMI and Observed Errors Installation and Operation Manual
DIFFERENTIAL PRESSURE PT1 > PT2 Differential 20psi Pressure Sensor Fault
PT1 = Suction Pressure Trans-
ducer Contact Authorized Service
PT2 = Discharge Pressure
Transducer
Alarm L1
HIGH SUCTION PRESSURE PT1 > 270 psi Escessive Suction Pressure
PT1 = Suction Pressure Trans-
ducer Contact Authorized Service
Alarm L1
REF PRESSURE SWITCH Refrigerant Discharge Pressure Contact authorized Service
Switch has activated.
NO RECOMMENDATION
LOW SUCTION PRESS A low suction pressure Check system balance pres-
condition has occurred. sure. See Appendix H: Rapid
REFRIGERANT LEAK Balance Pressure Check on
CHECK page 12-19
HIGH DISCHRG PRESS Discharge pressure is too high Review application to ensure it
is within the capability of the
EXCESSIVE HEAT LOAD unit.
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Polycold Cryochiller Troubleshooting
Installation and Operation Manual HMI and Observed Errors
HIGH DISCHRG TEMP Compressor discharge tempera- Check cooling water flow
REFRIGERANT LEAK ture is too high
REF LQD LINE TEMP Cooling water flow and / or Check your temperature and
temperature are outside of flow to ensure it is within
Fault LED is Amber acceptable limits. acceptable limits.
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Troubleshooting Polycold Cryochiller
HMI and Observed Errors Installation and Operation Manual
LQD LINE START TEMP Cooling water flow and / or Check your temperature and
temperature are outside of flow to ensure it is within
NO RECOMMENDATION acceptable limits during system acceptable limits.
start
Fault LED is Amber
This fault will occur during
startup if the system coolant sen-
sor fails to reach a temperature
below 42 C within 14 seconds.
NO RECOMMENDATION
CB1 has tripped Check for cause of excessive
Fault LED is Amber thermal load on the cryocoil,
C1 COOL VALVE CYCLE Cool valve requires replacement Contact authorized service
NO RECOMMENDATION
C1 DEFR VALVE CYCLE Defrost valve requires replace- Contact authorized service
ment
C2 DEFR VALVE CYCLE
NO RECOMMENDATION
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Polycold Cryochiller Troubleshooting
Installation and Operation Manual HMI and Observed Errors
Too slow to go to cool Cryosurface full and requires Defrost the cryosurface
defrosting.
Fault LED not lit Contact authorized Service
(No HMI Message) Internal battery is dead and real Reset the real time clock to cor-
time clock has reset to default rect time using remote interface
Fault LED not lit after recent power cycle
Contact authorized Service to
Date and Time rolled back have battery replaced
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Troubleshooting Polycold Cryochiller
Remote Monitor Troubleshooting Installation and Operation Manual
This section lists faults in numeric order of the bit mask value as received from the command
ACTIVE_ALARMS. See ALARM_STATUS Current Alarm Status on page 7-18.
For assistance in decoding bitmask values, see 32 Bit Numbered Bitfield on page 7-3.
Alarm L1
Bit 1 Not used N/A N/A
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Polycold Cryochiller Troubleshooting
Installation and Operation Manual Remote Monitor Troubleshooting
When FRZ_PREVENT_SETPT
> -158C, then Alarm when TC4
is lower than 6C below
FRZ_PREVENT_SETPT
When FRZ_PREVENT_SETPT
< -158C, then...
Alarm when TC4 is lower than
FRZ_PREVENT_SETPT
Warning L2
Bit 3 Not used N/A N/A
Bit 7 Pressure Transducer PT2 shows Check system load and perfor-
high discharge pressure which mance
High discharge pressure indicates excessive heat load
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Troubleshooting Polycold Cryochiller
Remote Monitor Troubleshooting Installation and Operation Manual
Alarm L1
Bit 10 Input voltage out of range of Check and correct the input
PWR_WARN_BAND voltage
Input power out of range
Voltage outside of range of
Fault LED Amber PWR_WARN_BAND for 10sec
Warning: Compressor ON Waning L2 - Comp On
Alarm: Compressor OFF (10 sec to restart compressor)
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Polycold Cryochiller Troubleshooting
Installation and Operation Manual Remote Monitor Troubleshooting
Bit 11 Refrigerant Liquid Line Tempera- Check cooling water flow and
ture (TC2) multiple conditions temperature
Refrigerant liquid line temp
TC2 is between 9C and 12C for
Fault LED Amber 1 min.
Warning L1
Warning: Compressor ON
Alarm: Compressor OFF TC2 < 9C for 15 min
Alarm L1
Refrigerant Liquid Line Temp Before Comp start Check cooling water flow and
(TC2) before and during oper- TC2 >85C temperature
ation Comp will not start
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Troubleshooting Polycold Cryochiller
Remote Monitor Troubleshooting Installation and Operation Manual
OR
Alarm L1
Bit 16 Not used N/A N/A
Alarm L1
Alarm L1
Alarm L1
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Polycold Cryochiller Troubleshooting
Installation and Operation Manual Remote Monitor Troubleshooting
Alarm L1
Alarm L1
Bit 29 One or both of the (2) E-Box Check if cooling fans are oper-
cooling fans is disconnected or ating properly
Cooling Fan has stopped
Check power for cooling fans
Fault LED not lit Warning L2
Compressor ON Repair power connection or
replace fan(s)
Bit 31 Compressor has been turned Wait one minute to clear before
ON/OFF 3 times within 1 minute compressor allowed to start
Abusive Comp On/OFF
Alarm L1
Fault LED Amber
Compressor ON
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Troubleshooting Polycold Cryochiller
Remote Monitor Troubleshooting Installation and Operation Manual
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Polycold Cryochiller
Installation and Operation Manual
The tables below list the supplied tools, recommended tools, and optional tools.
Table 11-1: Supplied Tools and Fixtures shipped with the Polycold Cryochiller
Table 11-2: Recommended Tools and Fixtures for the Polycold Cryochiller
7/16”, 9/16”, 1”, 1 1/16”, 1 5/16”, 1 11/16” wrenches for valve maintenance
1 1/16” Deep socket for valve maintenance
Table 11-3: Optional Tools and Fixtures for the Polycold Cryochiller
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Tools and Parts Polycold Cryochiller
Parts Installation and Operation Manual
Parts
Refer to the system documentation for installed components and options.
Maintenance Items
Maintenance items are dependent on the system configuration and application. Standard maintenance
items are listed in Table 11-5. Contact Brooks Automation Technical Support for additional mainte-
nance items.
171705-01 Fan Filter (one per unit, covers 2 fans) Annually or as required
Brooks Automation
11-2 214072 Revision B
Polycold Cryochiller Tools and Parts
Installation and Operation Manual Parts
Optional Parts
Brooks Automation
214072 Revision B 11-3
Tools and Parts Polycold Cryochiller
Parts Installation and Operation Manual
Brooks Automation
11-4 214072 Revision B
Polycold Cryochiller
Installation and Operation Manual
12 Appendices
Contents
Appendix A: Contact Brooks Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-1
Appendix B: Lifting Rings (Optional). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-3
Appendix C: CB2 Excepted Wiring. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-5
Appendix D: Remote EMO . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-6
Appendix E: Water Vapor Cryotrapping . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-8
Appendix F: Feedthroughs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-10
Appendix G: Zero Line Loss Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-13
Appendix H: Rapid Balance Pressure Check . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-19
Appendix I: Disconnect, Packing, and Shipping Instructions . . . . . . . . . . . . . . . . . . . . . . . . . . .12-20
Appendix J: Material Safety Data Sheets - MSDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12-21
1. Unit Information
• Serial number, Model number, Name of tool:
• Balance pressure of the unit or TC9 at ambient temperature (~ 17°C):
See Appendix H: Rapid Balance Pressure Check on page 12-19
• TC readouts 1-10 in cool mode and standby after 30 minutes:
2. Site Information
• Company Name, Site Location, Street Address, City, State Zip:
3. Contact Information:
• Primary Contact Name, Phone, and E-mail:
• Secondary Contact Name, Phone, and E-mail:
Brooks Automation
214072 Revision B 12-1
Appendices Polycold Cryochiller
Appendix A: Contact Brooks Information Installation and Operation Manual
4. Describe the malfunction observed and any error codes received during the failure.
• Time that this issue has been occurring
• Work that was done on the equipment prior to the error
• Actions taken after the error and the results of those actions
• Other information that may assist the Specialist
You can reach Polycold and Brooks Global Customer Operations Teams around the world at the times
and phone numbers below.
Table 12-1:
E-mail: [email protected]
+1-978-262-2900
E-mail: [email protected]
Germany, France, UK +49 1804 CALL GUTS (+49 1804 2255 4887)
Japan +81-45-477-5980
China +86-21-5131-7066
Taiwan +886-3-552-5225
Korea +82-31-288-2500
Singapore +65-6464-1481
For additional contact information, please go to the Brooks Automation web site at www.brooks.com.
Brooks Automation
12-2 214072 Revision B
Polycold Cryochiller Appendices
Installation and Operation Manual Appendix B: Lifting Rings (Optional)
Heavy Equipment
This unit can weigh up to 1300lbs (590kg). This unit may fall when
moved improperly which may cause serious injury or death.
To avoid this hazard, follow these precautions:
• Read the user’s manual before moving
• Use all four hoist rings with overhead lift equipment rated for use
with this load with an adequate safety factor.
• Lift with more than 45 degree angle from horizontal
Brooks Automation
214072 Revision B 12-3
Appendices Polycold Cryochiller
Appendix B: Lifting Rings (Optional) Installation and Operation Manual
When using a sling to lift the unit by the lift rings, observe the following:
• The strength the lifting device must be greater than 4 times the weight of the unit being lifted.
• Lift with 4 straps that each have a minimum strength as required by local regulations but not
less than the weight of the item being lifted.
• The length for each strap between the lift ring bolt and the lifting point must be greater than
736mm (29 inches).
• The angle between the sling strap and horizontal at each lift ring must be greater than 45°.
Strength of each
Angle of strap strap greater than full
greater than 45° weight of unit
Brooks Automation
12-4 214072 Revision B
Polycold Cryochiller Appendices
Installation and Operation Manual Appendix C: CB2 Excepted Wiring
Customers running at low voltage below 93% of nominal voltage and running the system at or near
maximum load may consider an excepted method for wiring CB2. The excepted method is to wire the
two input lines to CB2 directly from the input side L2 and L3 of CB1. This wiring change decrease the
load on CB1 and will not affect the system safety or performance. When the CB2 is wired in the
“excepted method”, wire and label “in accordance to local requirements”.
CB1
CB1
T2 and T3
L2 and L3
Output
Input
CB2
Excepted
Input
CB2 Wiring
Standard
Input
Wiring
Figure 12-2: CB2 Input Wiring: Standard CB2 Wiring (left) and Excepted CB2 Wiring (right)
Electric Shock
Contact with exposed electrical conductors may cause electric
shock and death or serious injury.
Replace all finger guards and protective covers for circuit breakers
and transformers, as provided, after electrical connections are
completed.
Brooks Automation
214072 Revision B 12-5
Appendices Polycold Cryochiller
Appendix D: Remote EMO Installation and Operation Manual
Pins 1 and 2 of J11 allow a remote device to sense the status of the Cryochiller EMO circuit.
• Open circuit between this pair of contacts indicates that the compressor contactor is off or
open.
• Closed circuit between this contact pair indicates that the compressor contactor is on and the
compressor is probably running.
Pins 3 and 4 of J11 allow a remote device to interrupt the power to the coil of the contactor which con-
trols the power to the compressor motor. Pins 3 and 4 are in series with the power to the compressor
motor contactor relay.
• When pins 3 and 4 are open, the circuit to the compressor contactor is open. The compressor
cannot operate until this pair is closed. These pins directly interrupt the wiring of the power cir-
cuit that controls the contactor.
• When pins 3 and 4 are closed, the circuit to the compressor contactor is closed. This allows the
compressor contactor to be turned on by the compressor on/off switch on the Cryochiller.
Pins 3 and 4 must be wired to a switch or a set of relay contacts or must be jumpered using the J11
EMO jumper connector.
Brooks Automation
12-6 214072 Revision B
Polycold Cryochiller Appendices
Installation and Operation Manual Appendix D: Remote EMO
Cable Connector 4-pin Cable Connector (male pins) (Amp CPC-11 - 206429-1)
Cable Terminal Pins (4) crimp-tail style male pins for 16 to 18AWG wire size.
Cable Size 16AWG wire required for pins 3 and 4
16 to 18AWG for pins 1 and 2
Cable must be less than 15M (50 feet).
EMO Status Connection Pins 1 and 2 give dry contact switch closure output signal to remote
(Output) device to monitor compressor contactor on/off.
Closed = contactor on. Open = contactor off
EMO Control Connection Pins 3 and 4 interrupt the compressor contactor circuit.
(Input) Switch set or relay contact pair or jumper wire is required for com-
pressor contactor to turn on.
Closed = contactor enabled. Open = contactor disabled
Pin 1 - Top
Pin 2 - Right
EMO Status Output
Pin 3 - Left
PIn 4 - Bottom
EMO Control Input
Brooks Automation
214072 Revision B 12-7
Appendices Polycold Cryochiller
Appendix E: Water Vapor Cryotrapping Installation and Operation Manual
For satisfactory pumping results, cryosurfaces should be operated at temperatures cold enough to pro-
vide 90% or greater trapping efficiency.
0% efficiency occurs when the cryosurface is in equilibrium with water vapor. At this efficiency, satura-
tion is reached and as many water vapor molecules escape from the cryosurface as stick to it. The
right-hand column of Table 12-1 gives the temperatures at which zero pumping occurs at the stated
pressure.
To find the best cryosurface temperature for a vacuum application, find the pressure at which the sys-
tem operates in the left column of Table 12-1 and then follow across to the column showing 90% effi-
ciency. This is the warmest temperature that the cryosurface must be for efficient water vapor pumping.
In general, the deeper the vacuum level, the colder the cryosurface must be in order to trap water vapor
at optimum efficiency. For example, for an application requiring a vacuum pressure range of 1 x 10-5
torr, the cryosurface needs to reach a temperature of -112°C or colder to achieve a water vapor trapping
efficiency of 90% or better. For an application requiring 5 x 10-7 torr, the cryosurface must be cooled to
-124°C to obtain the same efficiency.
Brooks Automation
12-8 214072 Revision B
Polycold Cryochiller Appendices
Installation and Operation Manual Appendix E: Water Vapor Cryotrapping
The average cryosurface temperature is a convenient number to use when there is a temperature gra-
dient between the coil inlet and coil outlet temperatures. The average cryosurface temperature is simply
the average of the coil inlet and coil outlet temperatures. In non-cryopumping applications, such as
those used for heat removal, it is the coil outlet temperature that is most important.
Table 12-1: Cryosurface Temperature needed for desire Water Vapor Partial Pressure
Desired Water
Vapor Partial Cryosurface Temperature Needed, °C
Pressure
torr mbar 98% 95% 90% 80% 60% 20% 0%
5.0E+00 6.7E+00 -40.8 -32.3 -25.4 -18.2 -10.5 -2.3 1.0
2.0E+00 2.7E+00 -48.7 -40.8 -34.4 -27.7 -20.6 -13.0 -9.7
1.0E+00 1.3E+00 -54.3 -46.8 -40.8 -34.4 -27.7 -20.6 -17.3
5.0E-01 6.7E-01 -59.7 -52.6 -46.8 -40.8 -34.4 -27.7 -24.5
2.0E-01 2.7E-01 -66.4 -59.7 -54.3 -48.7 -42.8 -36.5 -33.4
1.0E-01 1.3E-01 -71.2 -64.8 -59.7 -54.3 -48.7 -42.8 -39.7
5.0E-02 6.7E-02 -75.8 -69.7 -64.8 -59.7 -54.3 -48.7 -45.6
2.0E-02 2.7E-02 -81.5 -75.8 -71.2 -66.4 -61.4 -56.1 -53.1
1.0E-02 1.3E-02 -85.6 -80.1 -75.8 -71.2 -66.4 -61.4 -58.4
5.0E-03 6.7E-03 -89.6 -84.3 -80.1 -75.8 -71.2 -66.4 -63.5
2.0E-03 2.7E-03 -94.6 -89.6 -85.6 -81.5 -77.2 -72.7 -69.9
1.0E-03 1.3E-03 -98.2 -93.4 -89.6 -85.6 -81.5 -77.2 -74.4
5.0E-04 6.7E-04 -101.6 -97.0 -93.4 -89.6 -85.6 -81.5 -78.8
2.0E-04 2.7E-04 -106.0 -101.6 -98.2 -94.6 -90.8 -86.9 -84.3
1.0E-04 1.3E-04 -109.1 -104.9 -101.6 -98.2 -94.6 -90.8 -88.2
5.0E-05 6.7E-05 -112.2 -108.1 -104.9 -101.6 -98.2 -94.6 -92.0
2.0E-05 2.7E-05 -116.0 -112.2 -109.1 -106.0 -102.7 -99.3 -96.8
1.0E-05 1.3E-05 -118.8 -115.1 -112.2 -109.1 -106.0 -102.7 -100.3
5.0E-06 6.7E-06 -121.5 -117.9 -115.1 -112.2 -109.1 -106.0 -103.6
2.0E-06 2.7E-06 -125.0 -121.5 -118.8 -116.0 -113.1 -110.1 -107.8
1.0E-06 1.3E-06 -127.5 -124.1 -121.5 -118.8 -116.0 -113.1 -110.8
5.0E-07 6.7E-07 -129.9 -126.7 -124.1 -121.5 -118.8 -116.0 -113.8
2.0E-07 2.7E-07 -132.9 -129.9 -127.5 -125.0 -122.4 -119.7 -117.5
1.0E-07 1.3E-07 -135.2 -132.2 -129.9 -127.5 -125.0 -122.4 -120.2
5.0E-08 6.7E-08 -137.3 -134.5 -132.2 -129.9 -127.5 -125.0 -122.8
2.0E-08 2.7E-08 -140.1 -137.3 -135.2 -132.9 -130.6 -128.2 -126.2
1.0E-08 1.3E-08 -142.1 -139.5 -137.3 -135.2 -132.9 -130.6 -128.6
5.0E-09 6.7E-09 -144.1 -141.5 -139.5 -137.3 -135.2 -132.9 -131.0
2.0E-09 2.7E-09 -146.6 -144.1 -142.1 -140.1 -138.0 -135.9 -133.9
1.0E-09 1.3E-09 -148.4 -146.0 -144.1 -142.1 -140.1 -138.0 -136.1
Brooks Automation
214072 Revision B 12-9
Appendices Polycold Cryochiller
Appendix F: Feedthroughs Installation and Operation Manual
Appendix F: Feedthroughs
About Feedthroughs
Feedthroughs are used to provide feed and return refrigerant to and from the Polycold Cryochiller cryo-
surface through the vacuum chamber wall.
One single feedthrough typically incorporates both feed and return lines for the cryosurface.
Typical Brooks Polycold feedthroughs used with the Polycold Cryochiller have a 50mm (2.0 inch) diam-
eter barrel that fits into the vacuum chamber wall. See Figure 12-6. See Figure 12-7 for a close-up of a
feedthrough showing the diameter of the barrel of the feedthrough that fits into the hole in the vacuum
chamber wall.
P/N 409054-00 has copper tubing. P/N 409053-00 has stainless steel tubing.
Additional feedthrough models are also available from Brooks Polycold, including single-pass
feedthroughs for 25mm (1 inch) diameter holes. A total of two such single-pass feedthroughs are
required for each cryocoil.
NOTE: Brooks Automation Polycold feedthroughs are designed to be installed from the inside of
the vacuum chamber. This permits removal of the cryosurface when cleaning or servicing
the vacuum chamber.
Parameter Specification
Number 228 [57mm (2.25 inches) ID X 3 mm (0.1.25 inch) section]
Material Buna-nitrile
Surface 66mm (2.60 inches)
Surface roughness not to exceed 0.81 micron (32 micro-inch 0.000032 inch)
Must be flat, clean, and free of scratches or deposits.
Brooks Automation
12-10 214072 Revision B
Polycold Cryochiller Appendices
Installation and Operation Manual Appendix F: Feedthroughs
Figure 12-6: Polycold's Two-Inch (50 mm) Feedthrough with Port Requirements
Figure 12-7: Close-up Detail of Feedthrough Connection (Feed and Return Tubes not Shown)
Brooks Automation
214072 Revision B 12-11
Appendices Polycold Cryochiller
Appendix F: Feedthroughs Installation and Operation Manual
Brooks Automation
12-12 214072 Revision B
Polycold Cryochiller Appendices
Installation and Operation Manual Appendix G: Zero Line Loss Procedure
Item Description
Electrical Category Type 2 - Equipment is energized. Energized circuits are covered and insulated.
NOTICE
Untrained or improperly equipped personnel performing this procedure may cause
damage to the equipment.
• Only Brooks Automation, Polycold Division, trained personnel should perform
this procedure.
• Personnel performing this procedure must read and understand this proce-
dure, the Safety chapter of the Polycold Cryochiller Service Manual, and have
the proper tools and supplies ready before starting.
• Personnel performing this procedure must know the applicable regulatory and
safety codes, facility safety procedures, safety equipment, and contact infor-
mation.
Procedure
Step Action
Brooks Automation
214072 Revision B 12-13
Appendices Polycold Cryochiller
Procedure Installation and Operation Manual
Step Action
Evac Ckt 1
Valve
Common Return
Valve
Brooks Automation
12-14 214072 Revision B
Polycold Cryochiller Appendices
Installation and Operation Manual Procedure
Step Action
Pressure Gauge
1/4” Line
Hand Valve
1/4” Line
Brooks Automation
214072 Revision B 12-15
Appendices Polycold Cryochiller
Procedure Installation and Operation Manual
Step Action
Low Pressure
Gauge High Pressure
Gauge
High Pressure
Low Pressure Port
Port Vapor Charging
Port
1/4” Line 1/4” Lines
Low Pressure
Low Pressure Service Suction
Service Suction Port
Valve Stem
Brooks Automation
12-16 214072 Revision B
Polycold Cryochiller Appendices
Installation and Operation Manual Procedure
Step Action
12. Use the HMI keypad and follow the steps to select the ZERO LINE LOSS function.
• From the Main Menu, navigate to the SERVICE MENU selection. Press the Enter key to
select.
• Navigate to AUTHORIZATION CODE. Press Enter.
• Input the LEVEL 3 authorization code to access the function.
• A menu of service options appears.
• Scroll down to ZERO LINE LOSS. Press Enter.
• Scroll down to CONTINUE. Press Enter.
13. Turn on the compressor by the turning the Compressor On/Off toggle switch to On.
14. Open the Evac Ckt 1 hand valve for the refrigerant lines to be evacuated.
15. For Service Bypass Line:
• Slowly open the hand valve on the service bypass line to bleed the pressure.
• After the pressure equalizes, fully open the valve.
16. Purge the line connected to the Low Pressure Service Suction Port by loosening the fitting
(~1/4-turn) just enough to hear gas escape for approximately 2 seconds and then retighten the fit-
ting.
17. Turn the compressor suction service valve fully in to the front seated position to open the compres-
sor suction to the evacuation line.
18. Continue with the vacuum extraction until the compound pressure gauge reads 15 inches mercury
(50.8 kPag) (7.36 Psig) or lower.
Brooks Automation
214072 Revision B 12-17
Appendices Polycold Cryochiller
Procedure Installation and Operation Manual
Step Action
20. Close the Evac Ckt 1 hand valve that are opened for evacuation.
21. Turn off the compressor by turning the Compressor On/Off toggle switch to Off.
23. Confirm that the evacuation port Evac Ckt 1 hand valve is closed.
25. Disconnect all ¼” lines and “T” adapters from the compressor Low Pressure Service Suction Port
and Evac Port(s).
26. Reinstall the caps on the evacuation hand valve and the compressor low pressure service suction
port.
27. Recheck the “packing nut” on the Evacuation Valve for proper tightness to prevent possible leaks.
Brooks Automation
12-18 214072 Revision B
Polycold Cryochiller Appendices
Installation and Operation Manual Appendix H: Rapid Balance Pressure Check
The amount of time that it takes the system to reach the end of the Rapid BP Check is dependent on
the state of the system, the load of the system, and the temperature and flow rate of the cooling water.
Nominal Rapid BP Check takes approximately 15 minutes. Note that unlike other products, the Polycold
MaxCool Cryochiller does not require 48 hours to reach balance pressure.
The vacuum chamber should be in a vacuum state when operating the Rapid BP Check Mode. Oper-
ating this feature when the cryosurface is not in a vacuum environment may cause excessive heat loss
and the process may not be able to complete.
When Rapid Balance Pressure check is completed, some service functions may be performed. How-
ever, charge removal requires a waiting period of a minimum of 12.
1. Verify the vacuum chamber is in a vacuum state, typically 10-3 torr or below.
2. Use the HMI keypad to go to the SERVICE MENU and press “Enter”.
4. Enter the authorization code for Security Level 2 (Default Operator Access). Press “Enter”. See
Security Levels on page 7-7.
6. The system performs a rapid defrost and stops the Rapid BP Check procedure when the endpoint
has been reached.
7. Wait until the suction and discharge pressure transducers reach equilibrium. This typically takes
about 5 minutes.
Note that the transducers may not read the same value when at equilibrium but may have a slight
offset due to gauge accuracy.
Brooks Automation
214072 Revision B 12-19
Appendices Polycold Cryochiller
Appendix I: Disconnect, Packing, and Shipping Instructions Installation and Operation Manual
8. When the transducers are at equilibrium and hold a steady value, take a pressure reading. This is
the Balance Pressure.
NOTE: The original shipping crates or equivalent must be used when shipping the Cryochiller. If
the original crates are lost or damaged, contact Brooks Automation for replacements.
Electrical Hazard
Contact with energized equipment can cause electric shock and
result in death or serious injury.
Avoid contact with electrical circuits.
Disconnect electric energy before disassembling electric service.
NOTICE
Refrigerant removal or charging must be performed by Brooks Service personnel
or Brooks authorized service providers.
Customers must never attempt to add or remove refrigerant from the system.
Item Description
Electrical Category Type 2 - Equipment is energized. Energized circuits are cov-
ered or insulated.
840164-XX Shipping Kit
XX designates the kit version for the Polycold Cryochiller
Tools and materials: Standard tool kit and refrigerant line tools.
Moisture, Shock, and Tip indicators as required
Brooks Automation
12-20 214072 Revision B
Polycold Cryochiller Appendices
Installation and Operation Manual Appendix J: Material Safety Data Sheets - MSDS
Packing Procedure
1. Evacuate the refrigerant from the refrigerant lines and cryosurface by performing the
Zero Line Loss procedure. See Appendix G: Zero Line Loss Procedure on page 12-13
2. Carefully disconnect the cryosurface, refrigerant lines, and thermocouples and package them for
shipment.
4. Lock down the compressor to the frame by installing the double lock-down nuts on each of the (4)
compressor bolts.
5. Secure all panels firmly in place with shrink wrap or similar product.
6. Firmly secure the Polycold Cryochiller to a shipping pallet and cover with a cardboard enclosure.
Document 825103-00 provides the MSDS information for the compressor oil.
Brooks Automation
214072 Revision B 12-21
Appendices Polycold Cryochiller
Appendix J: Material Safety Data Sheets - MSDS Installation and Operation Manual
HAZARD IDENTIFICATION
Symptoms of Exposure by Route
The most significant route for overexposure is through
inhalation of high concentrations of the gas product.
Overexposure may cause central nervous system depression
and oxygen deficiency. Effects of overexposure may include
Inhalation: light-headedness, giddiness, shortness of breath, headaches,
and in extreme cases, irregular heartbeats, cardiac arrest,
and death. Symptoms of overexposure at lower
concentrations may include transient eye, nose, and throat
irritation.
Contact with rapidly released gas may cause frostbite. Other
direct dermal contact may result in skin de-fatting, dryness,
Skin Contact:
irritation, or contact dermatitis. Symptoms of frostbite may
include changes in skin color to white or grayish-yellow.
Brooks Automation
12-22 214072 Revision B
Polycold Cryochiller Appendices
Installation and Operation Manual Appendix J: Material Safety Data Sheets - MSDS
FIRST-AID MEASURES
Administer fresh air immediately. Use a bag valve mask or
Inhalation: similar device to perform artificial respiration (rescue
breathing) if needed. Get medical attention immediately.
Wash if needed. If frostbite, freezing, or cryogenic burns
occur, warm affected area in warm water. If this is not
Skin Contact: available, gently wrap affected parts in blankets. Allow
circulation to return naturally. Get medical attention
immediately.
Wash with large amounts of water or normal saline until no
evidence of chemical remains (at least 15-20 minutes). Get
Eye Contact:
medical attention immediately. Remove contact lenses if
easily possible.
Ingestion: Get medical attention immediately.
FIRE-FIGHTING MEASURES
Flashpoint: Not applicable.
Auto-ignition
Not applicable.
Temperature:
Flammable Limits (in
Not applicable.
air by volume, %)
Fire Extinguishing
Use media appropriate for surrounding materials.
Media:
Brooks Automation
214072 Revision B 12-23
Appendices Polycold Cryochiller
Appendix J: Material Safety Data Sheets - MSDS Installation and Operation Manual
Brooks Automation
12-24 214072 Revision B
Polycold Cryochiller Appendices
Installation and Operation Manual Appendix J: Material Safety Data Sheets - MSDS
Brooks Automation
214072 Revision B 12-25
Appendices Polycold Cryochiller
Appendix J: Material Safety Data Sheets - MSDS Installation and Operation Manual
TOXICOLOGICAL INFORMATION
Toxicity Data: Low order of toxicity.
Suspected Cancer
Not a suspected cancer agent.
Agent:
Irritancy of Product: Product may cause irritation through all routes of exposure.
Weak cardiac sensitization, a potentially fatal disturbance of
Sensitization to the
the heart, is caused by a heightened sensitivity to the action
Product:
of epinephrine after exposure to gas components.
Reproductive Toxicity No reproductive toxic effects on humans have been
Information: described for the components of this product.
Medical Conditions Cardiovascular, pulmonary, and central nervous system
Aggravated by medical conditions may be aggravated by inhalation of this
Exposure: gas.
Do not administer adrenaline due to the sensitizing effect of
fluorocarbons on the myocardium. Treatment of
overexposure should be directed at the control of symptoms
and the clinical condition. Exposure to fluorocarbon pyrolysis
Recommendations to
products should be considered in the diagnostic evaluation of
Physicians:
occupationally related fever of short duration and unknown
origin. Signs of exposure include tachycardia, hyperpnea,
and pharyngeal congestion; investigation may reveal
pulmonary edema and leucocytosis.
Biological Exposure
None.
Indices (BEIs):
ECOLOGICAL INFORMATION
Gas components are expected to volatilize rapidly from soil
Environmental
and water surfaces. Vapor phase gases are expected to
Stability:
degrade very slowly in the ambient atmosphere.
Effect of Material on Compounds are not expected to bioconcentrate in organisms.
Plants or Animals: Specific toxic effects are not known.
Effect of Chemical on
Bioconcentration in aquatic life is expected to be low.
Aquatic Life:
DISPOSAL CONSIDERATIONS
Preparing Wastes for
Dispose in accordance with all applicable regulations.
Disposal:
TRANSPORTATION INFORMATION
Proper Shipping Names
For Shipments of Refrigerant gases, n.o.s., 2.2, UN 1078,
Cylinders: (contains hydrofluorocarbons, inert gas).
Units contain less than 25 pounds (12 kg) of non-flammable,
For Shipments of non-toxic refrigerant gas. In accordance with Section
Refrigeration Units: 173.307 (a) (4) (i) of 49 CFR, units are not subject to the
requirements of Hazardous Materials Regulations.
Brooks Automation
12-26 214072 Revision B
Polycold Cryochiller Appendices
Installation and Operation Manual Appendix J: Material Safety Data Sheets - MSDS
REGULATORY INFORMATION
U.S. SARA Reporting
None.
Requirements:
U.S. SARA Threshold
Not applicable.
Planning Quantity:
U.S. CERCLA
Reportable Quantity Not applicable.
(RQ):
Canadian DSL/NDSL
Not applicable.
Inventory Status:
U.S. TSCA Inventory Hydrofluorocarbon gas constituents are listed on the TSCA
Status: inventory.
U.S. State Regulatory This product is subject to state worker and community Right-
Information: to-Know Acts.
California Safe
Drinking Water and
Product ingredients are not listed.
Toxic Enforcement Act
(Proposition 65):
Labeling:
CAUTION: THIS UNIT HAS INTERNAL SYSTEMS WITH
LIQUID AND GAS UNDER PRESSURE. Store and use in a
well-ventilated area where temperatures will not exceed 52o
Refrigeration Units:
C (125o F). Contact the manufacturer or a certified technician
for the repair and maintenance of internal refrigeration
systems.
Brooks Automation
214072 Revision B 12-27
Appendices Polycold Cryochiller
Appendix J: Material Safety Data Sheets - MSDS Installation and Operation Manual
OTHER INFORMATION
Only use product in accordance with its intended use.
Uses and Restrictions: Cylinders should never be refilled without permission from the
owner.
U.K. Legislation: Control of Substances Hazardous to Health as amended.
End of MSDS
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Installation and Operation Manual Appendix J: Material Safety Data Sheets - MSDS
SOLEST LT-32
MATERIAL SAFETY DATA SHEET
Material Safety Data Sheet
SOLEST LT-32
2 Hazards Identification
3 Composition/Information on Ingredients
This material contains no ingredients requiring disclosure under regulatory hazard criteria for this jurisdiction. See Section 11
Hazardous Ingredients
for additional details.
Eyes Flush with water at least 30 minutes. Get medical attention if eye irritation develops or persists.
Skin Wash with soap and water. Remove contaminated clothing. If skin irritation occurs, get medical attention. Launder
contaminated clothing before reuse.
Inhalation Remove exposed person to fresh air if adverse effects are observed.
Oral DO NOT INDUCE VOMITING. Get immediate medical attention.
Additional Information Note to physician: Treat symptomatically.
Spill Procedures Personal Protective Equipment must be worn, see Personal Protection Section for PPE recommendations. Ventilate area if
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spilled in confined space or other poorly ventilated areas. Prevent entry into sewers and waterways. Pick up free liquid for
recycle and/or disposal. Residual liquid can be absorbed on inert material.
The above data are typical values and do not constitute a specification. Vapor pressure data are calculated
unless otherwise noted.
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Installation and Operation Manual Appendix J: Material Safety Data Sheets - MSDS
SOLEST LT-32
Thermal Decomposition Smoke, carbon monoxide, carbon dioxide, aldehydes and other products of incomplete combustion.
Conditions to Avoid High temperatures.
11 Toxicological Information
-- ACUTE EXPOSURE --
Eye Irritation Not expected to cause eye irritation. Based on data from components or similar materials.
Skin Irritation May cause mild skin irritation. Does not meet Canadian D2B or EU R38 criteria. Based on data from components or similar
materials.
Respiratory Irritation No data available to indicate product or components may cause respiratory irritation under normal workplace conditions and
good industrial hygiene practices.
Dermal Toxicity The LD50 in rabbits is > 2000 mg/Kg. Based on data from components or similar materials.
Inhalation Toxicity No data available to indicate product or components may be a toxic inhalation hazard.
Oral Toxicity The LD50 in rats is > 10,000 mg/Kg. Based on data from components or similar materials.
Dermal Sensitization No data available to indicate product or components may be a skin sensitizer.
Inhalation Sensitization No data available to indicate product or components may be respiratory sensitizers.
-- CHRONIC EXPOSURE --
Chronic Toxicity No data available to indicate product or components present at greater than 1% are chronic health hazards.
Carcinogenicity No data available to indicate any components present at greater than 0.1% may present a carcinogenic hazard.
Mutagenicity No data available to indicate product or any components present at greater than 0.1% are mutagenic or genotoxic.
Reproductive Toxicity No data available to indicate either product or components present at greater than 0.1% that may cause reproductive
toxicity.
Teratogenicity No data available to indicate product or any components contained at greater than 0.1% may cause birth defects.
-- ADDITIONAL INFORMATION --
Other No other health hazards known.
12 Ecological Information
-- ENVIRONMENTAL TOXICITY --
Freshwater Fish Toxicity Not determined.
Freshwater Invertebrates Toxicity Not determined.
Algal Inhibition Not determined.
Saltwater Fish Toxicity Not determined.
Saltwater Invertebrates Toxicity Not determined.
Bacteria Toxicity Not determined.
Miscellaneous Toxicity Not determined.
-- ENVIRONMENTAL FATE --
Biodegradation Adequate data is not available to estimate the biodegradation potential of this material.
Bioaccumulation Less than 1.0% of the components display no potential to bioconcentrate.
Soil Mobility Not determined.
13 Disposal Considerations
Waste Disposal This material, if discarded, is not a hazardous waste under RCRA Regulation 40 CFR 261. Treatment, storage,
transportation, and disposal must be in accordance with applicable Federal, State/Provincial, and Local regulations.
14 Transport Information
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SOLEST LT-32
U.S. DOT Non-Bulk Not regulated.
U.S. DOT Non-Bulk NAERG Not applicable.
Canada Not regulated.
Mexico Not regulated.
Bulk Quantity 85000 KG, 187391 lbs.
Intermediate Quantity 11000 KG, 24251 lbs.
Non-Bulk Quantity 400 KG, 882 lbs.
15 Regulatory Information
-- State Regulations --
Cal. Prop. 65 This product does not intentionally contain any chemicals known by the State of California to cause cancer and/or birth
defects. Moreover, we do not routinely analyze its products for impurities which may be such chemicals.
-- Product Registrations --
U.S. Fuel Registration Not applicable.
Finnish Registration Number Not Registered
Swedish Registration Number Not Registered
Norwegian Registration Number Not Registered
Danish Registration Number Not Registered
Swiss Registration Number Not Registered
Italian Registration Number Not Registered
-- Other / International --
Miscellaneous Regulatory
Not determined.
Information
16 Other Information
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Precautionary Labels Caution.
z May cause skin irritation.
As the conditions or methods of use are beyond our control, we do not assume any responsibility and expressly disclaim any liability for any use of this product. Information
contained herein is believed to be true and accurate but all statements or suggestions are made without warranty, expressed or implied, regarding accuracy of the information, the
hazards connected with the use of the material or the results to be obtained from the use thereof. Compliance with all applicable federal, state, and local regulations remains the
responsibility of the user.
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Glossary
After Cooler: Component in the refrigeration unit that removes heat from the refrigerant vapor after
it exits the compressor
Balance pressure: The pressure in the refrigeration unit (or cryopump) when the suction and discharge
sides of the compressor are equal and the system is at room temperature. This is the
same as the charge pressure.
CE: Conformité Européene The CE Marking identifies that the product or machine is com-
plying with all of the safety requirements established by the European Union.
Charge pressure: The pressure in the refrigeration unit (or cryopump) when the suction and discharge
sides of the compressor are equal and the system is at room temperature. This is the
same as the balance pressure.
Coldest liquid: The portion of the refrigerant circuit that obtains the lowest temperature prior to evap-
oration.
Compressor: component in the refrigeration unit that raises the refrigerant pressure and causes the
refrigerant to move through the circuit
Condenser: A component in the refrigeration unit that removes heat from the refrigerant vapor after
it exits the compressor.
Cryopump: The Polycold cryogenic refrigeration system that captures water molecules in a vac-
uum chamber. It consists of a refrigeration unit, a refrigerant line, and a cryosurface
(with cryogenic feed-through).
Cryosurface: The coil or baffle in the vacuum chamber that captures water molecules by freezing
them to its surface.
Cylinder Unload: A solenoid that deactivates one of the three compressor cylinders to save power under
certain conditions.
Defrost: The rapid heating process used to remove captured water vapor from the cryocoil.
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DeviceNet: Installation and Operation Manual
DeviceNet: A system control protocol consisting of software and hardware. Uses its own command
format to gather data and command certain actions on the system.
Ethernet: A serial communication protocol for communication and configuring the XC Cryochller
from a host or service computer. Consists of a family of computer networking technol-
ogies for local area networks. Data is sent in packets with error checking so that dam-
aged data can be resent.
Feed line: The copper tube in the refrigerant line that carries refrigerant from the refrigeration unit
to the cryosurface.
Liquid line: A portion of the refrigerant circuit containing high pressure refrigerant just after it has
been cooled by the water-cooled condenser.
Polycold stack: The upper portion of the refrigeration unit that is insulated with foam.
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Installation and Operation Manual Refrigerant:
Refrigerant circuit: The path of the refrigerant that goes from the refrigeration unit, through the feed line,
through the cryosurface, through the return line, and back to the refrigeration unit.
A tank inside the refrigeration unit that maintains the gaseous refrigerant at a safe
pressure when the unit is not at operating temperature.
Refrigerant Line: feed and return lines that carry refrigerant to and from the cryocooler
Refrigeration unit: The machine containing the compressor, condenser, and stack that cools the refriger-
ant mixture to cryogenic temperatures.
Return Line: The copper tube in the refrigerant line that carries refrigerant from the cryosurface to
the refrigeration unit.
RS-232: A serial communication protocol that can command and configure the Polycold Cryo-
chiller using the system commands.
TC: Thermocouple.
Top-off charge: A refrigerant mixture that can be added to the refrigerant in the Polycold Cryochiller
Transformer Tap: Jumper or connection configuration that allows for different input voltages to be used
on the system and generate the appropriate internal voltages.
TÜV: Technical Supervision Society verifies compliance with EN and IEC standards
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UL: Installation and Operation Manual
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Index
B T
Brooks Automation Technical Support Bulletin 1-1
Contact Information i-ii TSB 1-1
C
Consumable Items 11-2
Cooling Water 3-6
Cooling Water Purity 3-7, 3-9
D
Declaration of Conformity 1-13
Dimensions 3-2
E
Electrical Hazards 2-14
H
Hazards
Electrical 2-14
Mechanical 2-12
L
Limitations 1-16
Limited Warranty 1-16
M
Mechanical Hazards 2-12
N
Notes 2-2
P
Packing Instructions 12-20
Performance Specifications 3-9
R
Recycling 2-18
S
Site Preparation 3-3
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T Installation and Operation Manual
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