ASTM D638-02a-Standard Test Method For Tensile Properties of Plastics
ASTM D638-02a-Standard Test Method For Tensile Properties of Plastics
ASTM D638-02a-Standard Test Method For Tensile Properties of Plastics
INTERNATIONAL
1. Scope * 1.6 This standard does not purport to address all of the
1.1 This test method covers the determination of the tensile
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
properties of unreinforced and reinforced plastics in the form
priate safety and health practices and determine the applica-
of standard dumbbell-shaped test specimens when tested under
bility of regulatory limitations prior to use.
defined conditions of pretreatment , temperature, humidity, and
testing machine speed. 2. Referenced Documents
1.2 This test method can be used for testing materials of any
1 ASTM Standards:
thickness up to 14 mm (0. 55 in. ). However , for testing
D 229 Test Methods for Rigid Sheet and Plate Materials
specimens in the form of thn sheeting, including film less than
Used for Electrical Insulation
1.0 mm (0. 04 in. ) in thickness, Test Methods D 882 is the
D 412 Test Methods for Vulcanized Rubber and Thermo-
preferred test method. Materials with a thickness greater than
plastic Elastomers- Tension
14 mm (0. 55 in. ) must be reduced by machining.
D 618 Practice for Conditioning Plastics for Testing
1.3 This test method includes the option of determning
D 651 Test Method for Tensile Strength of Molded Electri-
Poisson s ratio at room temperature.
cal Insulating Materials
NOTE I-This test method and ISO 527- 1 are tech;.cally equivalent. D 882 Test Methods for Tensile Properties of Thin Plastic
NOTE 2-This test method is not intended to cover precise physical Sheeting
procedures. It is recognized that the constant rate of crosshead movement D 883 Terminology Relating to Plastics
type of test leaves much to be desired from a theoretical standpoint, that
wide differences may exist between rate of crosshead movement and rate
D 1822 Test Method for Tensile- Impact Energy to Break
of strain between gage marks on the specimen, and that the testing speeds Plastics and Electrical Insulating Materials
specified disguise important effects characteristic of materials in the D 3039/D 3039M Test Method for Tensile Properties of
plastic state. Furter, it is realized that varations in the thicknesses of test Polymer Matrix Composite Materials
specimens, which are permtted by these procedures , produce varations in D 4000 Classification System for Specifying Plastic Mate-
the surface-volume ratios of such specimens, and that these varations may rials 7
influence the test results. Hence, where directly comparable results are D 4066 Classification System for Nylon Injection and Ex-
desired , all samples should be of equal thckness. Special additional tests
trusion Materials 7
should be used where more precise physical data are needed.
NOTE 3- This test method may be used for testing phenolic molded D 5947 Test Methods for Physical Dimensions of Solid
resin or lamnated materials. However, where these materials are used as Plastic Specimens
electrcal insulation , such materials should be tested in accordance with E 4 Practices for Force Verification of Testing Machines
Test Methods D 229 and Test Method D 651. E 83 Practice for Verification and Classification of Exten-
NOTE 4-For tensile properties of resin-matrx composites reinforced someter
with oriented continuous or discontinuous high modulus 20- GPa
0 X 10 psi) fibers , tests shall be made in accordance with Test
E 132 Test Method for Poisson s Ratio at Room Tempera-
Method D 3039/D 3039M.
ture
E 691 Practice for Conducting an Interlaboratory Study to
1.4 Test data obtained by this test method are relevant and
appropriate for use in engineering design.
5 The values stated in SI units are to be regarded as the Annual Book of ASTM Standards Vol 10. 01.
standard. The values given in parentheses are for information Annual Book of ASTM Standards Vol 09. 01.
only. 4 Annual Book of ASTM Standards Vol 08. 01.
5 Discontinued; see 1994 Annual Book of ASTM Standards Vol 10. 01.
the specimen that wil be in the grips, and interposing thin continuously records shall be used. An extensometer classified
pieces of abrasive cloth, abrasive paper, or plastic , or rubber- by Practice E 83 as fulfilling the requirements of a B-
coated fabric, commonly called hospital sheeting, between the classification within the range of use for modulus measure-
ments meets this requirement.
specimen and the grp surface. No. 80 double-sided abrasive
2 Low- Extension Measurements-For elongation-at-
paper has been found effective in many cases. An open-mesh
fabric, in which the theads are coated with abrasive , has also yield and low-extension measurements (nominally 20 % or
grps. /
less), the same above extensometer, attenuated to 20 % exten-
been effective. Reducing the cross-sectional area of the speci-
sion , may be used. In any case , the extensometer system must
men may also be effective. The use of special types of grips is
sometimes necessar to eliminate slippage and breakage in the
meet at least Class C (Practice E 83) requirements , which
include a fixed strain error of 0. 001 strain or :! 1.0 % of the
indicated strain , whichever is greater.
1.4 Drive Mechanism- drve mechanism for imparing 3 High- Extension Measurements-For making mea-
to the movable member a uniform, controlled velocity with surements at elongations greater than 20 % , measuring tech-
respect to the stationar member, with this velocity to be niques with error no greater than:! 10 % of the measured value
regulated as specified in Section 8. are acceptable.
1.5 Load Indicator- suitable load- indicating
mecha- 2.4 Poisson s Ratio- extensometer or axial and
Bi-axial
nism capable of showing the total tensile load cared by the transverse extensometers capable of recording axial strain and
test specimen when held by the grips. Ths mechansm shall be transverse strain simultaneously. The extensometers shall be
essentially free of inertia lag at the specified rate of testing and capable of measuring the change in strains with an accuracy of
shall indicate the load with an accuracy of:! 1 % of the 1 % of the relevant value or better.
indicated value , or better. The accuracy of the testing machine NOTE 8- Strain gages can be used as an alternative method to measure
shall be verified in accordance with Practices E 4. axial and transverse strain; however , proper techniques for mounting
strain gages are crucial to obtaining accurate data. Consult strain gage
NOTE 7-Experience has shown that many testing machines now in use
suppliers for instruction and training in these special techniques.
are incapable of maintaing accuracy for as long as the periods between
inspection recommended in Practices E 4. Hence, it is recommended that 3 Micrometers- Suitable micrometers for measuring the
each machie be studied individually and verified as often as may be width and thickness of the test specimen to an incremental
found necessar. It frequently wil be necessar to perform this function discrimination of at least 0. 025 mm (0. 001 in. ) should be used.
daily.
All width and thickness measurements of rigid and semirigid
1.6 The fixed member, movable member, drive mecha- plastics may be measured with a hand micrometer with ratchet.
nism, and grps shall be constrcted of such materials and in A suitable instrument for measuring the thickness of nonrgid
such proportions that the total elastic longitudinal strain of the test specimens shall have: (1) a contact measuring pressure of
system constituted by these pars does not exceed 1 % of the 25 :! 2. 5 kPa (3. 6 :! 0. 36 psi), (2) a movable circular contact
total longitudinal strain between the ,two gage marks on the test foot 6. 35 :! 0. 025 mm (0. 250 :! 0. 001 in. ) in diameter , and (3)
specimen at any time during the test and at any load up to the a lower fixed anvil large enough to extend beyond the contact
rated capacity of the machine. foot in all directions and being parallel to the contact foot
7 Crosshead Extension Indicator- suitable extension within 0. 005 mm (0. 0002 in. ) over the entire foot area. Flatness
indicating mechanism capable of showing the amount of of the foot and anvil shall conform to Test Method D 5947.
change in the separation of the grips, that is, crosshead 1 An optional instrument equipped with a circular con-
tact foot 15. 88 :! 0. 08 mm (0. 625 :! 0. 003 in. ) in diameter is
movement. This mechansm shal be essentially free of inertial
lag at the specified rate of testing and shall indicate the recommended for thickness measuring of process samples or
crosshead movement with an accuracy of :! 10 % of the larger specimens at least 15. 88 mm in minimum width.
indicated value.
(extensometer)-A suitable instr-
2 Extension Indicator
6. Test Specimens
ment shall be used for determning the distance between two 1 Sheet, Plate, and Molded Plastics:
designated points within the gage length of the test specimen as 1 Rigid and Semirigid Plastics-The test specimen shall
the specimen is stretched. For referee purposes , the extensom- conform to the dimensions shown in Fig. 1. The Type 1
eter must be set at the full gage length of the specimen , as specimen is the preferred specimen and shall be used where
shown in Fig. 1. It is desirable, but not essential, that this suffcient material having a thickness of 7 mm (0. 28 in. ) or less
instrment automatically record ths distance , or any change in is available. The Type II specimen may be used when a
, as a function of the load on the test specimen or of the material does not break in the narow section with the preferred
elapsed time from the star of the test , or both. If only the latter Type I specimen. The Type V specimen shall be used where
is obtained, load- time data must also be taken. This instrment only limited material having a thickness of 4 mm (0.16 in. ) or
shall be essentially free of inerta at the specified speed of less is available for evaluation , or where a large number of
o D638-
Lon
us-
urn
ied
.at-
en-
ust
ich
the
TYPE IV
ea-
ch- Specimen Dimensions for Thickness, T, mm (in.
lue 7 (0.28) or under Over 7 to 14 (0. 28 to 0. 55), incl 4 (0.16) or under
Dimensions (see drawings) Tolerances
Type I Type II Type III Type IV Type
W-Width of narrow section 13 (0. 50) 6 (0.25) 19 (0. 75) 6 (0.25) 18 (0. 125) :!0. (:!0. 02)B,
L-Length of narrow section 57 (2. 25) 57 (2. 25) 57 (2. 25) 33 (1. 30) 53 (0. 375) :!0. (:!0. 02)c
Wo-Width overall , min 19 (0. 75) 19 (0. 75) 29 (1. 13) 19 (0. 75) + 6.4 ( + 0. 25)
Wo-Width overall, min 53 (0. 375) + 3. 18 (+ 0. 125)
, of Lo-Length overall, min 165 (6. 183 (7. 246 (9. 115 (4. 63. 5 (2. no max (no max)
G-age length' 50 (2. 00) 50 (2. 00) 50 (2. 00) 62 (0. 300) :!0. 25 (:!0. 010)c
G-age length 25 (1. 00) :!0. 13 (:!0. 005)
mre D-Distance between grips 115 (4. 135 (5. 115 (4. 65 (2. 25. 4 (1. :!5 (:!0.
ting R-Radius of filet 76 (3. 00) 76 (3. 00) 76 (3. 00) 14 (0. 56) 12. 7 (0. :!1 (:!0. 04)c
radius (Type IV) 25 (1. 00) :!1 (:!0.04)
age RO-uter
A Thickness, shall be 3. 2:! 0.4 mm (0. 13 :! 0. 02 in. ) for all types of molded specimens , and for other Types I and II specimens where possible. If specimens are
the machined from sheets or plates , thickness, may be the thickness of the sheet or plate provided this does not exceed the range stated for the intended specimen type.
ltal For sheets of nominal thickness greater than 14 mm (0. 55 in. ) the specimens shall be machined to 14 :! 0. 4 mm (0. 55 :! 0. 02 in. ) in thickness, for use with the Type III
specimen. For sheets of nominal thickness between 14 and 51 mm (0. 55 and 2 in. ) approximately equal amounts shall be machined from each surface. For thicker sheets
oed.
both surfaces of the specimen shall be machined , and the location of the specimen with reference to the original thickness of the sheet shall be noted. Tolerances on
gid thickness less than 14 mm (0. 55 in. ) shall be those standard for the grade of material tested.
het. For the Type IV specimen , the intemal width of the narrow section of the die shall be 6. 00 :! 0. 05 mm (0. 250:! 0. 002 in. ). The dimensions are essentially those of Die
C in Test Methods D 412.
gid The Type V specimen shall be machined or die cut to the dimensions shown , or molded in a mold whose cavity has these dimensions. The dimensions shall be:
W= 18 :! 0. 03 mm (0. 125 :! 0. 001 in.
tact = 9. 53 :! 0. 08 mm (0. 375 :! 0. 003 in.
G = 7. 62 :! 0. 02 mm (0. 300 :! 0. 001 in. ), and
(3) R= 12. 7 :! 0.08 mm (0. 500 :! 0. 003 in.
tact The other tolerances are those in the table.
Supporting data on the introduction of the L specimen of Test Method D 1822 as the Type V specimen are available from ASTM Headquarters. Request RR:D20- 1 038.
oot The width at the center shall be +0. 00 mm, - 10 mm ( +0. 000 in. 004 in. ) compared with width Wat other parts of the reduced section. Any reduction in
less at the center shall be gradual, equally on each side so that no abrupt changes in dimension result.
For molded specimens, a draft of not over 0. 13 mm (0. 005 in. ) may be allowed for either Type I or II specimens 3. 2 mm (0. 13 in. ) in thickness, and this should betaken
into account when calculating width of the specimen. Thus a typical section of a molded Type I specimen , having the maximum allowable draft , could be as follows:
on- G Overall widths greater than the minimum indicated may be desirable for some materials in order to avoid breaking in the grips.
r IS Overall lengths greater than the minimum indicated may be desirable either to avoid breaking in the grips or to satisfy special test requirements.
; or Test marks or initial extensometer span.
13 mm)
or 0. 005 in. max
(0.
hall
eI -n..... (12.50 in.
Lere 70 mm)
less FIG. 1 Tension Test Specimens for Sheet, Plate, and Molded Plastics
n a
Ted
Lere
specimens are to be exposed in a limited space (thermal and should be used when diect comparsons are requied between
) or environmental stabilty tests , etc. ). The Type IV specimen materials in different rigidity cases (that is, nonrgid and
D638- 02a
semigid). The Type II specimen must be used for all
materials with a thickness of greater than 7 mm (0. 28 in. ) but
not more than 14 mm (0. 55 in. 89 mm, min.
1.2 Nonrigid Plastics-The test specimen shall conform (3. 50 in.
to the dimensions shown in Fig. 1. The Type IV specimen shall
be used for testing nonrgid plastics with a thickness of 4 mm
(0. 16 in. ) or less. The Type II specimen must be used for all 51 mm, min.
materials with a thckness greater than 7 mm (0. 28 in. ) but not (2. 00 in,
more than 14 mm (0. 55 in.
1.3 Reinforced Composites-The test specimen for rein-
forced composites , including highly ortotropic laminates S.
material to be tested.
NOTE 9-Test results have shown that for some materials such as glass 51 mm, min.
cloth , SMC , and BMC laminates , other specimen types should be (2. 00 in.
considered to ensure breakage within the gage length of the specimen , as
mandated by 7.
NOTE 100When preparng specimens from certain composite lami-
nates such as woven roving, or glass cloth, care must be exercised in
cutting the specimens parallel to the reinforcement. The reinforcement 89 mm , min.
wil be significantly weakened by cuttng on a bias, resulting in lower (3. 50 in.
laminate properties, unless testing of specimens in a direction other than
parallel with the reinforcement constitutes a varable being studied.
NOTE II- Specimens prepared by injection molding may have different
tensile propertes than specimens prepared by machining or die-cutting DIMENSIONS OF ROD SPECIMENS
because of the orientation induced. Ths effect may be more pronounced
Standard Length
in specimens with narow sections. Total Calculated
specimen at the center of its length so that the wall section after 2 (Ve) 19. 6 (0.773) 356 (14. 02) 381 (15)
24. 0 (0.946) 361 (14. 20) 381 (15)
machining shall be 60 % of the original nominal wall thick- 7 ('116)
4 (V.) 27. 7 (1.091) 364 (14. 34) 381 (15)
ness. This groove shall consist of a straight section 57. 2 mm 5 (3f) 33. 9 (1.333) 370 (14. 58) 381 (15)
(2. 25 in. ) in length with a radius of 76 mm (3 in. ) at each end 12. 7 ('1) 39. 0 (1.536) 376 (14. 79) 400 (15. 75)
15. 9 (S/) 43. 5 (1.714) 380 (14. 96) 400 (15. 75)
joining it to the outside diameter. Steel or brass plugs having 19. 0(%) 47. 6 (1.873) 384 (15. 12) 400 (15. 75)
diameters such that they wil fit snugly inside the tube and 22. 2 (7e) 51. 5 (2.019) 388 (15. 27) 400 (15. 75)
having a length equal to the full jaw length plus 25 mm (1 in. 25.4 (1) 54. 7 (2.154) 391 (15.40) 419 (16.
60. 9 (2.398) 398 (15. 65) 419 (16.
shall be placed in the ends of the specimens to prevent 31. 8 (1V.)
38. 1 (1 V2) 66.4 (2. 615) 403 (15. 87) 419 (16.
crushing. They can be located conveniently in the tube by 42. 5 (1%) 71.4 (2. 812) 408 (16. 06) 419 (16.
separating and supporting them on a theaded metal rod. 50. 8 (2) 76. 0 (2.993) 412 (16. 24) 432 (17)
tories
0.456
Axial Strain, Ea
642
897
rhree
-0 Transverse Strain, Et
16.
Applied Load, P
d and FIG. 4 Plot of Strains Versus Load for Determination of Poisson s Ratio
lue of
ints of 11.3. 1 Percent Elongation-Percent elongation is the the specimen.
change in gage length relative to the original specimen gage 11. Poisson Ratio-The axal strain , Ea' indicated by the
ired in
length , expressed as a percent. Percent elongation is calculated axial extensometer, and the transverse strai , E , indicated by
using the apparatus described in 5. the transverse extensometers, are plotted against the applied
:n. the percent
11.3. 1.1 Percent Elongation at Yield-Calculate load as shown in Fig. 4. A straight line is drawn though
(if one elongation at yield by reading the extension (change in gage each set of points , and the slopes dP and of these
Jture. lengt) at the yield point. Divide that extension by the original lines are determned. Poisson s ratio is then calculated as
1.,
described in 5. 1.7.
with 11.3. 1 Nominal strain at break-Calculate the nominal J1 (de ) I (de (2)
of the strai at break by reading the extension (change in grip
11. 1 The errors that may be introduced by drawing a
)f the separation) at the point of rupture. Divide that extension by the
straight line though the points can be reduced by applying the
aterial original grp separation and multiply by 100.
method of least squares.
11.4 Modulus of Elasticity-Calculate the modulus of elas-
ticity by extending the intial linear porton of the load- . 11.7 For each series of tests, calculate the arthmetic mean
th by
of all values obtained and report it as the " average value" for
;e) by extension curve and dividing the difference in stress corre-
the paricular property in question.
len in sponding to any segment of section on this straight lie by the
11. 8 Calculate the standard deviation (estimated) as follows
ascals correspondig difference in strain. All elastic modulus values
shall be computed using the average initial cross-sectional area and report it to two significant figures:
thee
:ength of the test specimens in the calculations. The result shall be 2 -
nX2) I (n - 1) (3)
yield expressed in pascals (pounds- force per square inch) and
cable, reported to thee significant figures.
, the 11.5 Secant Modulus-At a designated strai, ths shall be
where:
calculated by dividing the corresponding stress (nominal) by estimated standard deviation
break
the designated strain. Elastic modulus values are preferable and = value of single observation
. D638- 02a
= number of observations , and 12. 1.9 Tensile strength at yield or break , average value
X = arthetic mean of the set of observations. standard deviation
, and
11.9 See Anex Al for information on toe compensation. 12. 1. 0 Tensile stress at yield or break , if applicable
average value , and standard deviation
TABLE 5 Tensile Strength at Break, 10 psi , for Eight 12. 1.11 Percent elongation at yield , or break , or nominal
Laboratories, Five Materials strain at break , or all three , as applicable , average value , and
standard deviation
Mean
Polypropylene 2. 97 1. 54 1. 65 4.37 4. 12. 1.12 Modulus of elasticity, average value , and standard
Acrylic 9.
Cellulose acetate butyrate 4. 82 0. 058 0. 180 0. 164 0. 509
09 0. 452 0. 751 1. 27 2.
Glass-reinforced polyester 20. 8 0. 233 0.437 0. 659 1.
deviation
12. 1.3 Date of test , and
12. 1.4 Revision date of Test Method D 638.
Glass-reinforced nylon 23. 6 0. 277 0. 698 0. 784 1.
A Tensile strength and elongation at break values obtained for unreinforced
13. Precision and Bias 12
propylene plastics generally are highly variable due to inconsistencies in necking
or "drawing " of the center section of the test bar. Since tensile strength and 13.1 Precision-Tables 6 are based on a round-robin test
elongation at yield are more reproducible and relate in most cases to the practical
conducted in 1984 , involving five materials tested by eight
usefulness of a molded part, they are generally recommended for specification
purposes. laboratories using the Type I specimen , all of nominal 0. 125- in.
thickness. Each test result was based on five individual
determnations. Each laboratory obtained two test results for
TABLE 6 Elongation at Break, %, for Eight Laboratories, Five
each material.
Materials
Mean
TABLE 8 Tensile Yield Elongation, for Eight Laboratories, Eight
68 0. 20 2. 33 0. 570 6.
Glass-reinforced polyester 3.
Materials
Glass-reinforced nylon 3. 87 0. 10 2. 13 0. 283 6.
Acrylic 13. 21 2.
1. 05 3. 65 5. 80 10.
87 6. 62 5. 29
Cellulose acetate butyrate 14. Material
Test
Speed
Values Expressed in Percent Units
18.
Polypropylene 293. 0 50. 9 119. 0 144. 0 337. in.lmin Average
A Tensile strength and elongation at break values obtained for LOPE
unreinforced 17.
propylene plastics generally are highly variable due to inconsistencies in necking LOPE 14. 1.02
or " drawing" of the center section of the test bar. Since tensile strength and LLOPE 15.
elongation at yield are more reproducible and relate in most cases to the practical LLOPE 16.
usefulness of a molded part , they are generally recommended for specification LLOPE 11.
purposes. LLOPE 15. 1.27
HOPE 1.40
HOPE 1.23
TABLE 7 Tensile Yield Strength, for Ten Laboratories, Eight
Materials
Test Values Expressed in psi Units TABLE 9 Tensile Break Strength, for Nine Laboratories, Six
Material Speed. Materials
in.lmin Average
Test Values Expressed in psi Units
LOPE 1544 52. 64. 146. Material Speed
179.
LOPE 1894 53. 61.2 148. in.lmin Average
171.
LLOPE 1879 74. 99. 207. 279. LOPE 1592
LLOPE 1791 49. 52. 74. 146.4 209.
75. 137. 212. LOPE
LLOPE 2900 1750 66. 102. 186. 288.
55. 87. 155. 246. LLOPE
LLOPE 1730 63. 4379 127. 219. 355. 613.
96. 178. 268. LLOPE
HOPE 4101 196.
2840 78. 143. 220. 401.
371. 549. 1041.3 LLOPE
HOPE 3523 175. 1679 34. 47. 95. 131.
478. 492. 1338. LLOPE 2660 119. 166. 333. 465.
12. Report 13. 1.1 Tables 7- 10 are based on a round-robin test con-
12. 1 Report the following inormation: ducted by the poly olefin subcommttee in 1988 , involving eight
12. 1 Complete identification of the material tested, includ- polyethylene materials tested in ten laboratories. For each
ing type , source , manufactuer s code numbers , form , principal material , all samples were molded at one source , but the
dimensions , previous history, etc., individual specimens were prepared at the laboratories that
12. 1.2 Method of preparg test specimens tested them. Each test result was the average of five individual
12. 1.3 Type of test specimen and dimensions determnations. Each laboratory obtained three test results for
12. 1.4 Conditioning procedure used each material. Data from some laboratories could not be used
12. 5 Atmospheric conditions in test room for varous reasons , and this is noted in each table.
12. 1.6 Number of specimens tested, 13. 1.2 In Tables 2- , for the materials indicated , and for
12. 1.7 Speed of testing, test results that derived from testing five specimens:
12. 1.8 Classification of extensometers used. A description
of measurng technque and calculations employed instead of a 12 Supporting data are available from
minimum Class- C extensometer system ASTM Headquarers. Request RR:D20-
1125 for the 1984 round robin and RR:D20- 1170 for the 1988 round robin.
). ).
o D638- 02a
and TABLE 10 Tensile Break Elongation , for Nine Laboratories, Six ent equipment on different days , those test results should be
Materials judged not equivalent if they difer by more than the value
icable Test Values Expressed in Percent Units for that material and condition. (This applies between different
Material Speed
in.!min Average laboratories or between different equipment within the same
ominal
567 166.
laboratory.
lOPE 31. 59. 88.
, and LDPE 569 61. 89. 172. 249. 13. 1.2. 5 Any judgment in accordance with 13. 1.2.3 and
LLDPE 890 25. 113. 71. 318. 13. 1.2.4 wil have an approximate 95 % (0. 95) probability of
andard LLDPE 64.4 11.7 18. 32.
803 25. 104.4 71. 292.
being correct.
LLDPE
LLDPE 782 41. 96. 116. 270. 13. 1.2. 6 Other formulations may give somewhat different
results.
13. 1.2. 7 For furter information on the methodology used in
13. 1.2. 1 Sr is the within- laboratory standard deviation of
ths section , see Practice E 691.
the average; = 2. 83 r. (See 13. 1.2.3 for application of
13. 1.2. 8 The precision of ths test method is very dependent
,in test 13. 1.2. 2 SR is the between- laboratory standard deviation of
upon the uniformty of specimen preparation , standard prac-
. eight the average; = 2. 83 SR' (See 13. 1.2.4 for application of
comparng two test results for tices for which are covered in other documents.
25- in. 13. 1.2. 3 Repeatability-In
13. Bias-There are no recognized standards on which to
vidual the same material , obtained by the same operator using the
base an estimate of bias for this test method.
Its for same equipment on the same day, those test results should be
judged not equivalent if they differ by more than the value
for that material and condition.
14. Keywords
13. 1.2.4 Reproducibility-In comparng two test results for 14. 1 modulus of elasticity; percent elongation; plastics;
Eight
the same material , obtained by different operators using differ- tensile propertes; tensile strength
ANNEXES
. (Mandatory Inormation)
ALl In a typical stress-strain cure (Fig. ALl) there is a material. It is an arifact caused by a takeup of slack and
toe region AC, that does not represent a property of the alignment or seating of the specimen. In order to obtain correct
values of such parameters as modulus, strain , and offset yield
Six
point this arifact must be compensated for to give the
corrected zero point on the strain or extension axis.
A1.2 In the case of a material exhbiting a region of
Hookean (linear) behavior (Fig. ALl), a continuation of the
09.
linear (CD) region of the curve is constrcted through the
88.
13. zero-stress axis. Ths intersection (B) is the corrected zero-
01. strain point from which all extensions or strains must be
31.
65.
measured , including the yield offset (BE), if applicable. The
elastic modulus can be determed by dividig the stress at any
point along the line CD (or its extension) by the strain at the
same point (measured from Point defined as zero-strain).
con-
eight A1.3 In the case of a material that does not exhibit any
each linear region (Fig. A1. 2), the same kind of toe correction of the
t the zero-strain point can be made by constrcting a tangent to the
. that maximum slope at the inflection point (H' This is extended to
idual intersect the strai axis at Point the corrected zero-strain
ts for point. Using Point B' as zero strain , the stress at any point (C'
used on the cure can be divided by the strain at that point to obtain
a secant modulus (slope of Line B' C' For those materials
Strain
d for with no linear region , any attempt to use the tangent though
NOTE I-Some char recorders plot the mior image of this graph. the inflection point as a basis for determnation of an offset
FIG. A1. 1 Material with Hookean Region yield point may result in unacceptable error.
:D20-
D638- 02a
Strain
NOTE I-Some char recorders plot the mior image of ths graph.
FIG. A1. 2 Material with No Hookean Region
A2. elastic limit-the greatest stress whic.h a material is in plastics is debatable , the propriety of applying the term " modulus of
capable of sustaining without any permanent strain remaining elasticity " to describe the stiffness or rigidity of a plastic has been
upon complete release of the stress. It is expressed in force per seriously questioned. The exact stress-strain characteristics of plastic
materials are very dependent on such factors as rate of stressing,
unit area , usually pounds- force per square inch (megapascals). temperature , previous specimen history, etc. However, such a value is
NOTE A2. Measured values of proportonal lit and elastic limit useful if its arbitrar nature and dependence on time, temperature, and
var greatly with the sensitivity and accuracy of the testing equipment, other factors are realized.
cO D638- 02a
square inch) per minute. The initial rate of stressing can be
calculated from the initial slope of the tensile stress (nominal)
----1--- versus time diagram.
specimen. of the test specimen , that is , the change in length per unit of
original length. It is expressed as a dimensionless ratio.
A2. percent reduction of area (nominal)-the difference
A2. 16. nominal strain at break-the strain at the moment
measured at the point
between the original cross-sectional area
of rupture relative to the original grp separation.
of rupture after breakng and afer all retraction has ceased
expressed as a percent of the original area.
,Ius of
A2. 17 tensile strength (nominal the maximum tensile
been A2.10 percent reduction of area (true)-the difference
stress (nominal) sustained by the specimen during a tension
test. When the maximum stress occurs at the yield point
plastic between the original cross-sectional area of the test specimen
:ssing, (A2. 21), it shall be designated tensile strength at yield. When
and the minimum cross-sectional area withn the gage bound-
,lue is
ares prevailing at the moment of ruptue , expressed as a
the maximum stress occurs at break , it shall be designated
, and
percentage of the original area.
tensile strength at break.
A2. 11 A2. 18 tensile stress (nomina I)-the tensile load per unit
:ction proportional limit-the greatest stress which a
material is capable of sustaining without any deviation from area of minimum original cross section , within the gage
proportonalty of stress to strain (Hooke s law). It is expressed boundares , cared by the test specimen at any given moment.
,trai in force per unit area, usually megapascals (pounds-force per It is expressed in force per unit area , usually megapascals
)f the square inch). (pounds- force per square inch).
It is
NOTE A2. 8- The expression of tensile properties in terms of the
mds- A2.12 rate of loading-the change in tensile load cared minimum original cross section is almost universally used in practice. In
by the specimen per unit time. It is expressed in force per unit the case of materials exhbiting high extensibility or necking, or both
time , usually newtons (pounds-force) per minute. The initial (A2. 15), nominal stress calculations may not be meanngful beyond the
;tress-
yield
rate of loading can be calculated from the intial slope of the yield point (A2. 21) due to the extensive reduction in cross-sectional area
"2. 1): load versus time diagram. that ensues. Under some circumstances it may be desirable to express the
:I!
tensile properties per unit of minimum prevailing cross section. These
properties are called tre tensile propertes (that is, tre tensile stress, etc.
A2.13 rate of straining-the change in tensile strai per
.strai unit time. It is expressed either as strain per unit time , usually ill
A2. 19 tensile stress-strain curve-a diagram in which
metres per metre (inches per inch) per minute, or percent
values of tensile stress are plotted as ordinates against corre-
ion of elongation per unit time , usually percent elongation per minute.
sponding values of tensile strain as abscissas.
The initial rate of straining can be calculated from the initial
The
slope of the tensile strain versus time diagram.
I gage A2. 20 true strain (see Fig. A2. 2) is defined by the follow-
yield NOTE A2. 5- ing equation for E
The initial rate of strainig is synonymous with the rate of
Isi), crosshead movement divided by the initial distance between crossheads
only in a machine with constant rate of crosshead movement and when the
imen specimen has a uniform original cross section
, does not " neck down, " and
does not slip in the jaws.
where:
dL = increment of elongation when the distance between
the gage marks is
A2.22 yield strength-the stress at which a material exhib- A a E' TENSILE STRENGTH AT BREAI
its a specified limiting deviation from the proportonalty ELONGATION AT BREAK
stress to strain. Unless otherwise specified , ths stress wil be B. TENSILE STRENGTH AT YIELD
ELONGATION AT YIELD
the stress at the yield point and when expressed in relation to C. TENSILE STRESS AT BREAK
the tensile strength shall be designated either tensile strength at ELONGATION AT BREAK
yield or tensile stress at yield as required in A2. 17 (Fig. A2. 3). D D TENSILE STRESS AT YIELD
ELONGATION AT YIELD
(See offset yield strength.