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Soal TRK 1

1. The document appears to be notes from a chemical engineering class, containing solutions to homework problems involving reactor design and kinetics. 2. Problem 11.3 involves a pulse input experiment in a vessel that produced inconsistent results, either due to experimental error or the actual experiment being done incorrectly. 3. Problem 13.3 involves calculating the vessel dispersion number and fraction of baffled reactor volume from experimental residence time distribution data collected in a tubular reactor. 4. Problem 13.11 involves calculating the true rate constant for a first-order homogeneous reaction accounting for deviations from ideal plug flow in a packed bed reactor, and estimating the error incurred by assuming plug flow.

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Gilang Adi Setyawan
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335 views5 pages

Soal TRK 1

1. The document appears to be notes from a chemical engineering class, containing solutions to homework problems involving reactor design and kinetics. 2. Problem 11.3 involves a pulse input experiment in a vessel that produced inconsistent results, either due to experimental error or the actual experiment being done incorrectly. 3. Problem 13.3 involves calculating the vessel dispersion number and fraction of baffled reactor volume from experimental residence time distribution data collected in a tubular reactor. 4. Problem 13.11 involves calculating the true rate constant for a first-order homogeneous reaction accounting for deviations from ideal plug flow in a packed bed reactor, and estimating the error incurred by assuming plug flow.

Uploaded by

Gilang Adi Setyawan
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as DOCX, PDF, TXT or read online on Scribd
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1. Nidia Intan L. OS 8.

12316 201 011


2. TUGAS TRK LANJUT
Irwan Hidayatulloh 2316 201 012
3. Meiliefiana 2316 201 013
Kelompok 3
11.3 A pulse input to a vessel gives the results shown in Fig. P11.3.
(a) Are the results consistent?
(Check the material balance with the experimental tracer curve.)
(b) If the results are consistent, determine the amount of tracer introduced M, and
the E curve.

SOLUTION :
a) Check for consistency : from the experiment
V
t́= t́=luas segitiga
v
60 cm3 1
t́= =15 min t́= × ( 18× 1+21× 2 )
4 cm 3 /s 3
t́=20 min
The tracer comes out too late. Thus the experiment was done incorrectly or
inconsisntent.

11.11 A liquid macrofluid reacts according to AR as it flowsthrough a vessel. Find the
conversion of A for this flow patterns and kinetics as shown.

SOLUTION :

CA0 = 0.1mol/L

-rA = k

k= 0.03 mol/Lmin

Because k= 0.03 mol/Lmin shows zero order reaction

CA CA
=∫ E dt
CA 0 CA 0

CA kt
=1−
CA 0 CA 0

kt
0=1−
CA 0
kt
0=1−
CA 0

0,03
0=1− t
0,1

t=3,33 min

CA 0
For t < or t <3,33 min
k

CAF=0

XAF =1

13.3 RTD studies were carried out by Jagadesh and Satyanarayana in tubular reactor
(L= 1,21 m ID = 35 mm). A squirt of NaCL solution (5N)was rapidly injected at
the reactor entrance, and mixing cup measurements were taken at the exit. From
the following results calculate the vessel dipersion numbes, also the fraction factor
of reactor volume taken up by the baffles.

SOLUTION :

ml
v=1300
mnt

t (sec) t (av) C Tc t2c


0 20 10 0 0 0
20 25 22.5 60 1350 30375
25 30 27.5 210 5775 158813
30 35 32.5 170 5525 179563
35 40 37.5 75 2812,5 105469
63218,
40 45 42.5 35 1487,5 8
22562,
45 50 47.5 10 475 5
13781,
50 55 52.5 5 262,5 3
55 70 62.5 0 0 0
17687,
Total 335 565 5 573781

ṫ=
∑ tc = 17687,5 =31,31 sec
∑ c 565
2 ∑ t2 c 2
σ = −t = 35,52 sec
∑c

Vessel dispersion number

D σ2
= =0,6437
uL 2 t˙2

Reactor volume

V =L2 π r 2

V =(1,21 ×10¿¿ 2)2 ( 3,14 ) ¿ ¿

V =1164 cm3

ml cm 3
v=1300 =21,667
mnt sec

V 1164
ṫ= = =53,72 sec
v 21,667

Volume baffle = 486 cm3

13.11. Kinetika dari homogeneous liquid reaction dipelajari dalam sebuah reaktor alir,
dan untuk mendekati aliran plug, reaktor dengan panjang 48-cm di pack dengan 5-
mm pelet tidak berporos. Jika konversi adalah 99% untuk waktu tinggal rata-rata
dari 1 detik, hitung rate konstan untuk reaksi orde pertama

(A) dengan asumsi bahwa cairan lewat di aliran plug melalui reaktor
(B) akuntansi untuk penyimpangan aliran yang sebenarnya dari aliran plug
(C) berapakah error dalam perhitungan k jika penyimpangan dari aliran plug tidak
dianggap?
Data: Bed voidage ε = 0,4

Partikel Reynolds nomor Rep, = 200

Jawab

a. Menghitung k dengan asumsi aliran plug flow


Untuk k reaksi orde 1st maka
Ca0
Kτ = ln
Ca
1 Ca0
Kτplug = ln
τ Ca
1
= (4.6) = 4.6 sec-1
1 sec

b. Menghitung accounting for deviation dari plug flow bedasarkan model dispersi
Dari gambar 13.17 untuk Rep, = 200 dan ε = 0,4 di dapatkan
Dε D
=1 maka = 2.5
udp udp

Dengan menggunakan persamaan 22

L k true D
= = 1 + kτ
L p k measure uL

D dp
= 1 + kτ
udp L

5 mm
= 1 + (4.6) (2.5) ( ¿
480 mm

= 1.1198

Maka k true = (4.6 sec-1)( 1.1198) = 5.15 sec-1

( 4.6 ) −(5.15)
c. Error = x 100%
(5.15)
= 10.68 % .................nilainya kecil sehingga bisa di abaikan

14.6 Suatu aliran suspended fine solids (v = 1 m3 / min) melewati dua reaktor mix flow
yang di pasang seri, masing-masing berisi 1 m 3 lumpur. Segera setelah partikel
masuk ke reaktor, konversi menjadi produk dimulai dan akan selesai setelah dua
menit di dalam reaktor. Ketika partikel meninggalkan reaktor, reaksi berhenti.
Berapa fraksi dari partikel tersebut yang terkonversi sempurna menjadi produk
dalam sistem ini?
Jawab

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