Lab Guide To Reporting and Measurement
Lab Guide To Reporting and Measurement
GUIDE TO
REPORTING AND MEASUREMENT
(version: 2018)
Please keep this guide safe and in good condition as you will use it
throughout your 1st and 2nd semester laboratory activities.
Name: ____________________________
Guide to Reporting and Measurement: January 2018
CONTENTS
FOREWORD .............................................................................................................................................................3
B1 Overview .................................................................................................................................................... 15
B2 TYPE A evaluation of uncertainty ............................................................................................................... 17
B3 TYPE B evaluation of uncertainty ............................................................................................................... 19
B4 Combination of uncertainty in one measurement .................................................................................... 22
SECTION C – CALCULATIONS WITH UNCERTAINTIES ........................................................................................... 26
2
FOREWORD
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Guide to Reporting and Measurement: January 2018
You can take these safety skills to whichever scientific field you may venture. Here are three basic rules of the
laboratory:
You must wear enclosed and sturdy shoes, and bare feet and/or open shoes (e.g. flip-flops) are not
allowed in the laboratory. This rule minimises the risk of you injuring your feet, such as due to broken
glass or equipment dropped from the benches.
No eating is allowed in the laboratory and drinking is only allowed from closed containers. It is safer
to take a short break from the laboratory if you feel the need for refreshment. Occasionally hazardous
substances such as radioactive sources are used in the laboratory, therefore this rule minimises the
risk of you injuring yourself due to an exposure to a hazardous substance. It also minimises damage to
equipment, such as the damage of electrical equipment due to water contact, and maintains the
laboratory as a clean space to work in.
Behave professionally in the laboratory and be considerate and respectful of students in nearby
groups. More workplace accidents happen when people fool around than when they carry out their
normal work.
A useful reference to read more about laboratory practice is Etiquette in the Laboratory (1976), American
Journal of Physics, 7 (44). See http://scitation.aip.org/content/aapt/journal/ajp/44/7/10.1119/1.10320
Laboratory staff
During practical sessions, the laboratory space is managed by the following people:
The academic in charge;
The chief scientific officer and scientific officer;
The lab manager, and
The demonstrators.
You can ask any of the people above for help during the course of a practical, for issues such as conducting an
experiment, administration of the laboratory course, concerns about safety and faulty or damaged
equipment. If you are absent from a practical or tutorial or want to query a tutorial or practical mark
entered on WebApp or Vula, get in touch with the lab manager; Mr. Mark Christians.
Pre-practical preparation
Before you attend each practical session, read through the material on the practical that you are about to
perform and take a look at the relevant instructional videos in the link given below. You will use the practical
time the most efficiently if you come prepared and ready to ask questions.
http://www.phy.uct.ac.za/phy/courses/PHYLAB1.
Practical groups
It is intended this course is undertaken in cooperative learning environment. We believe that working in
groups of 3 is best for these activities. Compare your responses to those of your work partners. Help each
other to figure out what is going on. Resolve any difficulties that you might have and call a demonstrator if
you need to.
You can choose your own group at the beginning of the semester. We use these groups to allocate and
schedule the marking of laboratory reports, so please submit a registration form for your group to the lab
manager in the first session of the semester. This will remain your group, and your laboratory day, for the
rest of the semester. However, if you want to change your group at any time and for any reason, please talk
to the lab manager who can assist you in arranging a different group and change in registration, as well as
making sure your marked lab reports are returned to the correct session.
4
Some guidance on how to work in groups is given in the following pages:
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Guide to Reporting and Measurement: January 2018
What if I am put in
a group with people
that I don’t get on I have found that even when I think
with too well? that I don’t get on with someone,
after a while when we have
focused on what we have to do,
things actually turn out fine. I have
rarely met anyone that I can
absolutely not work with.
But anyway, the groups don’t stay
together permanently, so you
won’t be with the same people
forever!
What can I do
so that our group works
well together?
When you are stuck on a question, there are a number of questions that you
should ask yourselves before you call a demonstrator:
Do we understand the question?
Have we consulted the Guide to Reporting and Measurement?
Would it be useful to draw a diagram?
What question are we going to ask the demonstrator?
... this is very important ... it’s no use saying to the demonstrator,
“We’re stuck” ... or ... “We don’t know what to do.”
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SECTION A – PERFORMING AN EXPERIMENT
A1 Planning an experiment
There are a number of stages to an experiment, each requiring you to think about different things.
Stage 1. Identify the problem that needs solving, or the question that needs answering. What is the
aim of the experiment? Think about what results you need in order to make a valid
conclusion.
Stage 2. Plan your experiment carefully (see notes below).
Stage 3. Do the experiment and complete the analysis of the data.
Stage 4. Formulate your conclusions to the experiment based your results.
Stage 5. Communicate your experiment in the form of a report.
Never rush into taking readings without careful planning. Of course, it is a good thing to familiarise yourself
with the apparatus before starting, but before doing serious measurements sit down and plan carefully
exactly what you are going to do. In most cases you will be working with one or two other students in the
laboratory. It is important that you discuss things with them. Listen to each other’s opinions and talk to a
demonstrator, if necessary.
Some important considerations are:
What are the main steps that I need to carry out? A flow chart is often useful.
What apparatus do I need and how does it work?
Are there any precautions that I need to take?
How much time do I have for the experiment?
What variables are involved and what exactly must I measure?
How many measurements do I need to make?
What tables must I draw up? Detailed tables should be drawn up before taking readings as the tables
will serve as a guide.
What are the main steps in the analysis? Again, a flow chart is often useful.
Which graphs (if any) will I need to plot?
What influences will affect the measurements? Make a list beforehand and add to it as you proceed.
After the experiment, reflect on how well your plan worked, noting both successful aspects and failures of the
plan. Keep in mind the structure of your report that you will have to write. Remember that if, while writing
the report, you suddenly remember that you did not record something important while doing the experiment,
it will be too late!
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Tables and figures must be referred to in the text, e.g. “The apparatus was arranged as shown in Figure 1”;
“The data gathered were recorded as shown in Table 1 below” or “The data in Table 1 were used to plot the
graphs in Figure 1, 2 and 3.” These brief statements help to link the different parts of the report.
Then examine and extract important aspects of the data and use these to explain various relationships or
determine your measurement results. For example, what is the shape of your graph and what does it suggest
in terms of the relationship between the variables? If it is a straight line, what is the value of the slope?
Remember to quote your results with the appropriate significant figures and the corresponding uncertainties.
How does an expected value compare with your own and what reasons can you give for this? You may give
tentative explanations for your data but be careful not to mix facts with opinions.
Conclusion and recommendations:
This is normally a section in which you say what the investigation has shown and to what extent the problem
or claim stated in the introduction has been resolved. Remember that any conclusions must be supported by
evidence from your data. Always quote any final results, together with their uncertainties in your conclusion.
Avoid making vague statements such as “This was a successful experiment.” You may also need to discuss
sources of uncertainty and any improvements that could be made to the apparatus (and measurements).
Again, avoid meaningless phrases such as “it was caused by human error.”
Writing a report allows you to reflect critically on the whole experiment and check your understanding of the
purpose of the investigation as well as produce an accurate record of it. Note that an physics practical is not a
set of procedures designed to reproduce some “correct” answer. It is a problem that has been posed that
requires an experimental solution which may include making measurements, implementing different
procedures and techniques and then the formulation of a suitable report.
Whether you graduate and leave with a B.Sc. to work in industry or whether you stay on at
university to become a post-graduate student, you will find that report writing will remain as
one of the most important activities in your career.
Scientific style
Very often, in reports of this kind, writers prefer to use the passive construction or impersonal style to report
procedures followed in conducting experiments, by writing, for example:
“Five measurements were taken,” instead of “I / We took five measurements.”
Both styles are acceptable. As you do most of your practicals in groups, you are likely to visualise what you did
as a group and report it as a group activity in which case the personal pronoun “we” is appropriate. However,
once you have chosen a style of writing, then you must use it throughout your report and not switch back and
forth between the two.
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A3 Drawing tables and graphs
Tables are a way of organising your data in a structured way while you are working in the laboratory as well as
a way of presenting your data in a clear way when you write your report. A graph is an extremely useful way
to both present readings of two variables that vary as a function of each other, as well as to analyse the data
in order to extract further information. This section describes what we call the “general rules” for preparing
tables and graphs.
Data Calculations
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Interpretation of graphs
One of the aims in investigating physical phenomena is to establish the relationship between the variables
that are being measured. For example, if we are investigating an object that is experiencing uniform
acceleration, 𝑎, then we will find the function describing the relationship between velocity, 𝑣, and time, 𝑡, to
be a straight line of the form,
𝑦 = 𝑚𝑥 + 𝑐;
an example of which is shown in graph (a) of Figure 2. In this case,
𝑣 = 𝑢 + 𝑎𝑡 ,
where 𝑢 is the initial velocity.
On the other hand, the relationship between the position, r, and the time, t, will be of the form,
𝑦 = 𝑎𝑥 2 + 𝑏𝑥 + 𝑐,
i.e. a parabola as shown in graph (b) of Figure 2. In this example we will find,
1
𝑟(𝑡) = 𝑟0 + 𝑢𝑡 + ,
2𝑎𝑡 2
12
where 𝑟0 is the initial position. Some other functions that you will encounter are the hyperbola, which is
shown in graph (c) of Figure 2 and of the form,
𝑥𝑦 = 𝑐,
and the exponential function which is shown in graph (d) of Figure 2 and of the form,
𝑦 = 𝑎𝑒 𝑏𝑥 .
Note that we say that “𝑦 is proportional to 𝑥” if a graph of 𝑦 versus 𝑥 yields a straight line through the origin.
i.e. 𝑦 = 𝑚𝑥 + 𝑐 with 𝑐 = 0. Sometimes “directly proportional to” is used which means the same thing.
However, if 𝑐 0, then we cannot say that “𝑦 is proportional to 𝑥”, but can only say that “𝑦 is linearly related
to 𝑥”.
y (a) y (b)
𝑦 = 𝑚𝑥 + 𝑐 𝑦 = 𝑎𝑥 2 + 𝑏𝑥 + 𝑐
x x
y y
(c) (d)
Hyperbola Exponential
𝑥𝑦 = 𝑐 𝑦 = 𝑎𝑒 𝑏𝑥
x x
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Guide to Reporting and Measurement: January 2018
A4 Significant figures
What are significant figures?
The number of figures that convey meaningful information in recorded data are known as the “number of
significant figures”.
Significant figures in a number are:
All non-zero digits (e.g., 54 has two significant digits while 456.78 has five significant digits).
All zeros appearing anywhere between two non-zero digits (e.g., 302.05 has five significant digits).
All trailing zeros, where the number has a decimal point (e.g., 36.65000 has seven significant digits).
Leading zeros are not significant (e.g., 0.0003 has only one significant figure).
Do not confuse significant figures with decimal places. The number of decimal places refers to the number of
figures after the decimal point, e.g., 46.320 mm has five significant figures, but three decimal places; while
0.0040 mm has two significant figures, but four decimal places.
Recording significant figures in readings and calculations
When taking readings, the number of significant figures recorded is determined by the precision of the
instrument. For example, if the scale on a particular instrument makes it possible to read a mass to 1/10th of a
gram, then it is incorrect to record the reading of some mass to 1/100th of a gram, i.e., in such a case the
recording of a mass of say 12.4 g would be correct, but recording that same mass as 12.40 g using the same
instrument would be incorrect.
Similarly, when using a typical wooden laboratory metre rule to measure distance, you can only take readings
to the nearest millimetre. For example, you may record the reading of a distance as say 127 mm, but to
record a reading of 127.0 mm will be unreasonable because that degree of precision (to 0.1 mm) cannot be
achieved when using a typical laboratory meter rule. (Consider the problem of parallax.)
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SECTION B – MEASUREMENT UNCERTAINTY
B1 Overview
The purpose of undertaking a measurement in science is to provide knowledge about some physical quantity.
The physical quantity that we may wish to investigate is called the measurand, e.g., the measurement may be
the air pressure in a soccer ball, the temperature of the air in a room, or the voltage across a resistor.
It is important to realise that the value of a measurand can never be determined with absolute certainty. The
best that can be achieved through a process of measurement is to improve our knowledge about some
specified measurand. We cannot think of a measurand as having some “true” or “exact” value that can
actually be found; we have to think of the knowledge that we have of any measurand always as being limited
and incomplete.
The following framework for measurement uncertainty is based on a probabilistic approach and the relevant
standards are expressed in ISO/IEC 17025. These standards are clarified in the associated Guide to the
Expression of Uncertainty in Measurement (GUM) as well as in the ISO International Vocabulary of Basic and
General Terms in Metrology (VIM). They are also documented in the NIST Technical Note 1297 of 1994.
Note that the term “error” is often used quite loosely in conversation in laboratory work but it is important to
realise that the word “error” is not synonymous with “uncertainty”. The term “uncertainty” is clearly defined,
while use of “error” may be misleading, so the use of the word “error” in the context of laboratory work is
discouraged.
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Guide to Reporting and Measurement: January 2018
There are two ways to evaluate the standard uncertainty, a TYPE A evaluation and a TYPE B evaluation; and
the method you will use depends on the nature of the measurement.
If a number of readings are available, in which there is scatter, then a statistical, TYPE A, evaluation of
the uncertainty should be used.
All other evaluations of uncertainty are TYPE B evaluations. TYPE B evaluations may be applied to
many sources of uncertainty, e.g., the rating of the instrument, the reading of a scale, the correction
factors that may need to be applied to the measurement, etc.
The TYPE A and TYPE B evaluation methods are discussed in detail in the sections that follow.
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B2 TYPE A evaluation of uncertainty
In a TYPE A evaluation of the uncertainty, a statistical method is used to infer the value of the uncertainty
associated with a measurement by quantifying the “scatter”, or the “spread” in the values of a set of data.
There are two commonly used cases:
2) The data are a set of readings of the form: (𝑥1 , 𝑦1 ), (𝑥2 , 𝑦2 ) … . (𝑥𝑛 , 𝑦𝑛 )
In this case the function that is used to analyse the data is
‘linearised’ (details to be covered in E2 Linearising
equations) and the data pairs, (𝑥𝑖 , 𝑦𝑖 ) i = 1, 2, …n are
plotted as a straight line in the form 𝑦 = 𝑚𝑥 + 𝑐.
A technique known as a ‘least squares fit’ is used to fit a
line to the data and then the best approximation and the
standard uncertainty may be derived from the gradient
𝑚 ± 𝑢(𝑚) and the intercept 𝑐 ± 𝑢(𝑐)of the fitted line.
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Guide to Reporting and Measurement: January 2018
The following equations are used to calculate the parameters used to determine the uncertainty associated
with the measurement:
𝑛
1
Mean of the data: 𝑥̅ = ∑ 𝑥𝑖 … (B2-1)
𝑛
𝑖=1
𝑛
1
Standard deviation: 𝜎=√ ∑(𝑥𝑖 − 𝑥̅ )2 … (B2-2)
(𝑛 − 1)
𝑖=1
𝜎
Standard uncertainty: 𝑢(𝑥) = … (B2-3)
√𝑛
Note:
1) *The assumption that the distribution of the values of the readings is normal validates the statement
that “the experimental standard deviation of the mean is the standard uncertainty 𝑢(𝑥)” for the
majority of cases. However, it is important to realise that a different approach may be required where
the distribution of values is not ‘normal’.
2) Because a Gaussian distribution was assumed, the probability that the measurand lies within one
standard uncertainty of the best approximation, is 68%.
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B3 TYPE B evaluation of uncertainty
A TYPE B evaluation of uncertainty is any evaluation of an uncertainty that is not a TYPE A evaluation. So, for
example, if the uncertainty as a result of the rating of the instrument has to be evaluated, or if only one
reading is available, then a non-statistical TYPE B evaluation of uncertainty is performed.
The methods of TYPE B evaluation of uncertainty will be presented by way of examples.
Just by looking at the position of the needle on the gauge we can see that the best approximation of the
measurand is: p = 34 kPa. (There is only one reading.)
Now we want to evaluate the uncertainty associated with the manufacturer’s rating of the instrument,
𝑢(𝑝𝑟𝑎𝑡𝑖𝑛𝑔 ). The reason for selecting this source is because the bourdon gauge is a simple instrument and so
the uncertainty due to the rating of the instrument far outweighs the contribution of all the other applicable
sources of uncertainty. Typically, for a bourdon tube gauge, the uncertainty in the rating of an instrument of
the type shown here is ±2.5% of the full scale deflection (FSD) of the instrument; and in this case, FSD is 160
kPa. The standard uncertainty (due to the rating) associated with this instrument will be:
2.5
𝑢(𝑝𝑟𝑎𝑡𝑖𝑛𝑔 ) = 160 kPa × = 4.0 kPa … (B3-1)
100
And so the result of the measurement of the pressure shown on this instrument will be quoted as:
𝑝 ± 𝑢(𝑝) = (34.0 ± 4.0) kPa.
In every measurement, the instrument manufacturer’s specification needs to be checked to determine the
instrument rating. Caution: check whether the manufacturer’s rating has been given to one or more standard
deviations; as this has to be taken into account when you combine the uncertainties, see D1 Quoting a result.
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The reason for dividing by √2 in equation B3-2 is because this is the factor applicable to the assumptions
regarding a rectangular pdf.
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Example 3: Uncertainty associated with reading an analogue display
In this example, the measurand is a temperature T but now the instrument chosen to take readings of the
temperature has an analogue display. The reading you see on the thermometer is shown in Figure 7.
The best approximation of the measurand is 𝑇1 = 75 °C (there is only one reading).
In this example the only source of uncertainty that we will take into account is the uncertainty associated with
the reading of the dial of the instrument, 𝑢(𝑇read ). This uncertainty arises because the instrument really tells
us is that the temperature is between 70 °C and 80 °C, and is most probably 75 °C.
The reason for dividing by √6 in equation B3-3 is because this is the factor applicable to the assumptions
made regarding a triangular pdf.
Note that the total area under the pdf is equal to 1, meaning that there is a 100% probability of the
measurand being in the ± a interval. Moreover, the grey shaded area under the triangular pdf has an area of
0.65, so there is a 65% probability that the measurand is in the ± u interval. Therefore, because a triangular
distribution was assumed, the coverage probability that the measurand lies within one standard uncertainty,
i.e., within ± 𝑢(𝑇) of the best approximation T, is 65%.
𝑢(𝑘) = √[𝑢(𝑘1 )]2 + [𝑢(𝑘2 )]2 + [𝑢(𝑘3 )]2 + [𝑢(𝑘4 )]2 + ⋯ … (B4-1)
It does not matter whether the uncertainty associated with the individual sources has been determined by
means of a TYPE A or a TYPE B evaluation, they can all be combined using equation B4-1. Before you combine
uncertainties, make sure that they have all been adjusted to relate to the one (or the same) standard
uncertainty.
The displayed reading is the best approximation of the measurand, in this case 1.55 V.
Consider that in this measurement there are two sources of uncertainty to be evaluated:
1) the uncertainty associated with the rating of the instrument, 𝑢(𝑉rating ) and
2) the uncertainty associated with reading the display, 𝑢(𝑉read ).
The typical rating for a moving coil instrument of this kind is 2% of the full scale deflection (FSD).
2
So in this case the standard uncertainty, 𝑢(𝑉rating ) = 3.0 V × = 0.060 V.
100
To evaluate the uncertainty in the reading, consider that the lower and upper bounds of the value of the
measurand are 1.5 V and 1.6 V and that the evaluation of this uncertainty may be modelled on a triangular
pdf, so
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The standard uncertainties are combined:
2
𝑢(𝑉) = √[𝑢(𝑉rating )] + [𝑢(𝑉read )]2 = √(0.060 V)2 + (0.021 V)2 = 0.064 V
Finally, the battery voltage can be quoted as V = (1.550 ± 0.064) V, to one standard uncertainty. Given that the
standard uncertainty was obtained by using a triangular probability density function, the coverage probability
(level of confidence) in this result is 65%.
The oscilloscopes in PHYLAB1 have the following ratings, to one standard uncertainty:
±5% on the x axis (for time-base between 0.1 μs and 50 ms per division),
±3% on the y axis (for voltage between 5 mV and 5 V per division).
After careful consideration, you decide that the peak-to-peak voltage spans 5.8 divisions and so the best
estimate of V is 5.8 V (5.8 Divisions × 1.0 Volt/Division).
Now there are three sources of uncertainty to be evaluated:
1) the uncertainty associated with the instrument rating,
2) the uncertainty associated with the reading at the top peak on the display, and
3) the uncertainty associated with the reading at the bottom peak on the display.
The oscilloscopes in PHYLAB1 have a rating of ±3% on the y axis to one standard uncertainty (for voltage
between 5 mV and 5 V per division). Therefore the standard uncertainty associated with the rating is,
3
𝑢(𝑉rating ) = 5.8 V × = 0.17 V.
100
To evaluate the uncertainty associated with the reading of the display, consider that the lower and upper
bounds of every reading will be 0.1 of a division on either side of the best approximation anywhere on the
display and that the evaluation of this uncertainty may be modelled on a triangular pdf. We need to multiply
the uncertainty in divisions by the sensitivity scale of the oscilloscope settings to achieve an uncertainty in
volts:
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Guide to Reporting and Measurement: January 2018
Finally, these three standard uncertainties are combined to give the combined standard uncertainty
associated with the measurement of V. Note the uncertainty in reading the top and bottom peaks on the
display are equivalent:
2 2 2
𝑢(𝑉) = √[𝑢(𝑉rating )] + [𝑢(𝑉read,top )] + [𝑢(𝑉read,bottom )] = √(0.17 V)2 + 2(0.041 V)2 = 0.18 V.
After careful consideration, you decide that the period spans 7.6 divisions, and so the best approximation of T
is 3.8 ms (i.e. 7.6 Divisions × 0.5 ms/Division).
Again there are three sources of uncertainty to be evaluated:
1) the uncertainty associated with the instrument rating,
2) the uncertainty associated with the reading on the left of the display, and
3) the uncertainty associated with the reading at the right of the display.
The oscilloscopes in PHYLAB1 have a rating of ±5% on the x axis to one standard uncertainty (for time-base
between 0.1 μs and 50 ms per division). Therefore, the standard uncertainty associated with the rating is,
5
𝑢(𝑇rating ) = 3.8 ms × = 0.19 ms.
100
To evaluate the uncertainty associated with the reading of the display, consider that the lower and upper
bounds of every reading will be 0.1 of a division on either side of the best approximation anywhere on the
display and that the evaluation of this uncertainty may be modelled on a triangular pdf. We need to multiply
the uncertainty in divisions by the sensitivity scale of the oscilloscope settings to achieve an uncertainty in
volts:
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(𝑇upper − 𝑇lower ) (0.1 − (−0.1)) DIV ms
𝑢(𝑇𝑟𝑒𝑎𝑑 ) = = × 0.5 = 0.021 ms.
2√6 2√6 DIV
As with the measurement of the voltage, these standard uncertainties are combined to give the combined
standard uncertainty associated with the measurement of T:
2 2 2
𝑢(𝑇) = √[𝑢(𝑇rating )] + [𝑢(𝑇read,left )] + [𝑢(𝑇read,right )] = √(0.19 ms)2 + 2(0.021 ms)2 = 0.19 ms.
Note that as 𝑢(𝑇rating ) is considerably larger than 𝑢(𝑇read ) by an order of magnitude larger, it dominates the
combined uncertainty, 𝑢(𝑇).
The result of this measurement can be quoted as:
Period T = (3.80 ± 0.19) ms, to one standard uncertainty.
And given that the standard uncertainty was obtained by using a triangular probability density function, the
coverage probability (level of confidence) in this result is 65%.
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Guide to Reporting and Measurement: January 2018
2 2 2
𝑢(𝑅) 𝑢(𝐴) 𝑢(𝐵)
[ ] = [𝑎 ] + [𝑏 ]
Product of variables 𝑅 𝐴 𝐵
𝑅 = 𝑐 𝐴𝑎 𝐵𝑏 or
Coefficients a, b & c are constants (numbers 2 2
with zero uncertainty) 𝑢(𝐴) 𝑢(𝐵)
𝑢(𝑅) = 𝑅√[𝑎 ] + [𝑏 ]
𝐴 𝐵
Correlated variables
(consider co-variance if the instrument used more than
once in the same experiment)
𝑢(𝑅) = √𝑎 𝑢(𝐴)
𝑅=𝑎𝐴
Coefficient a is a constant (numbers
with zero uncertainty).
Note: these equations are three results from a general function for the propagation of uncertainties. To find out more, consult the full
version of this guide at the UCT Physics website, “Measurement Manual”.
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C2 Examples of uncertainty calculations
In identifying sources of uncertainty, consider that the problem of parallax is a significant contributor to the
uncertainty associated with both measurements, while there is also an uncertainty as to where the centre of
mass of the ball might actually be.
The best approximation for the position of 𝑥ring is 0.0 cm, because the metre stick was lined up that way (we
did not have to start at zero but in this case we did and we read in centimetres as the unit of the instrument).
Using a triangular pdf, the standard uncertainty, 𝑢(𝑥ring ) can be evaluated as:
The position of the centre of the ring relative to the metre stick may be quoted as 𝑥ring = (0.000 ± 0.041) cm,
to one standard uncertainty.
The best approximation of the position of the ball, 𝑥ball is 66.4 cm. Using a triangular pdf, the standard
uncertainty, 𝑢(𝑥ball ) can be evaluated as:
The position of the centre of the ball relative to the metre stick may be quoted as 𝑥ball = (66.400 ± 0.082) cm,
to one standard uncertainty.
To find the effective length L of the pendulum we need to subtract the position of one from the position of
the other. The best approximation of L is the difference between the two best approximations of the
measurements so:
𝐿 = (𝑥ball − 𝑥ring ) = (66.4 cm − 0.00 cm) = 66.4 cm.
Therefore the best approximation of L is 66.4 cm.
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Guide to Reporting and Measurement: January 2018
We combine the two standard uncertainties, 𝑢(𝑥ball ) and 𝑢(𝑥ring ), using the first equation in Table C1-1. The
appropriate formula for the calculation of the combined standard uncertainty is:
2
𝑢(𝐿) = √[𝑢(𝑥ball )]2 + [𝑢(𝑥ring )] = √(0.082 cm)2 + (0.041 cm)2 = 0.092 cm
Finally, the effective length of the pendulum is L = (66.400 ± 0.092) cm, to one standard uncertainty. Given
that the standard uncertainty was obtained by using a triangular probability density function, the coverage
probability (level of confidence) in this result is 65%.
[𝑢(𝑥)]2 = [1 𝑢(𝑑1 )]2 + [1 𝑢(𝑑2 )]2 = [0.25 m]2 + [0.25 m]2 , so 𝑢(𝑥) = 0.3535 m.
Using the second method, where 𝑥 = 2𝑑. By means of the tape measure you determine 𝑑 =
(56.00 ± 0.25 m). Which means that the ‘best approximation’ of the total distance 𝑥 = 2𝑑 = 2(56.00) =
112.00 m.
Now, with reference to Table C1-1, (correlated variables) you calculate 𝑢(𝑥):
The result of either calculation will be quoted as: 𝑥 ± 𝑢(𝑥) = 112.00 ± 0.35 m.
𝑥 112.0 m
𝑣= = = 343.3 m s −1 .
𝑡 0.326 s
28
Now, with reference to Table C1-1, (measurements are being multiplied) you calculate 𝑢(𝑥):
2 2 2
𝑢(𝑣) 𝑢(𝑥) 𝑢(𝑡)
[ ] = [1 ] + [−1 ]
𝑣 𝑥 𝑡
2
𝑢(𝑣) 0.36 m 2 0.018 s 2
[ ] = [1 ] + [−1 ]
343.3 m s −1 112.0 m 0.326 s
The result of the calculation will be quoted as: 𝑓 ± 𝑢(𝑓) = (384.6 ± 8.2) Hz.
Note in all these examples, the uncertainty is quoted to two (2) significant figures, and the best approximation
has the same number of decimal places as the uncertainty. See the next section, D1, for more information on
quoting.
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Guide to Reporting and Measurement: January 2018
D1 Quoting a result
The outcome of a measurement and/or an experiment is the best approximation of the measurand as well as
the standard uncertainty, for example, the result of a measurement of gravitational acceleration 𝑔 may be:
𝑔 = (9.790 ± 0.052) ms −2 .
Note that:
The result of a measurement is not a single value (not a point), it is an interval of values.
The greater the uncertainty, the ‘wider’ the interval that quantifies the result of the uncertainty in the
measurement.
Because there is always some uncertainty in measurement, the width of the interval is never zero!
(has three decimal places here) and (two sig. figures and three decimal places here).
It may be convenient on occasion to express a standard uncertainty 𝑢(𝑥) as a fraction of the best approximation
of the measurand 𝑥. Thus, we may sometimes refer to
𝑢(𝑥)
the fractional uncertainty given by , or
𝑥
𝑢(𝑥)
the percentage uncertainty given by × 100 %.
𝑥
For example, if the quoted result of a measurement is (3.60 0.32) units, then the fractional uncertainty is 0.32
/ 3.60 = 0.09 and the percentage uncertainty is 9%.
This form of quoting the uncertainty is commonly used by manufacturers of electronic components where the
uncertainty in the quoted value is called the “tolerance” and it is quoted as a percentage of the nominal value
of the component.
For example, if the value of a resistor is given as 220 Ω with a tolerance of 5%, it means that the resistance of
the resistor is (220 ± 11) Ω.
30
Quoting experimental results as in many textbooks
There are other ways of quoting the results of experiments and a common method used in textbooks is, for
example, the quoting of the Universal Gas Constant R to be:
R = 8.31451(72) J K−1 mol−1.
The seven and two in brackets indicate that the last two digits ‘51’ have an uncertainty of ‘72’ associated with
them; in other words, the book value is:
R = (8.31451 0.00072) J K−1 mol−1.
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Guide to Reporting and Measurement: January 2018
Figure 13: Probability density functions (pdfs) of a measurement corresponding to coverage factors
of 1 (a) and 2 (b).
The result in Figure 13(a) may be described as “𝑚 = (83.50 0.12) g, where the number following the symbol
is the numerical value of the standard uncertainty 𝑢 = 0.12 g and defines an interval estimated to have a
coverage probability of 58 percent”.
The result in in Figure 13(b) may be described as “𝑚 = (83.50 0.19) g, where the number following the
symbol is the numerical value of an expanded uncertainty 𝑈 = 𝑘 𝑢 with 𝑈 determined from a standard
uncertainty 𝑢 = 0.12 g and a coverage factor 𝑘 = 1.65, and defines an interval estimated to have a coverage
probability of 95 percent”.
We are 58 % confident that the value of the mass lies between 83.38 g and 83.62 g.
We are 95 % confident that the value of the mass lies between 83.31 g and 83.69 g.
We are 100 % confident that the value of the mass lies between 83.30 g and 83.70 g.
Note that by introducing an expanded uncertainty and coverage factor 𝑘 > 1, we are not affecting the result
of the measurement. We are only changing the way that we present the result.
Note in PHYLAB1 courses, it is rarely required to quote uncertainties to a greater coverage probability than
𝑘 = 1. We include this section here so you are aware of it for future study.
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D2 Comparing results
To say that two results are “close” or “nearly the same” is meaningless in the context of laboratory work.
The results of any two experiments can only be meaningfully compared if the intervals associated with each of
the results are known.
More specifically:
If the intervals that represent the results of two measurements overlap, then we say these two results
“agree within experimental uncertainty.”
If the intervals that represent the results of two measurements do not overlap, then we say these
results “do not agree within experimental uncertainty.”
For example, say three students measure the period 𝑇 of a pendulum and they each quote the result as
follows:
𝑇1 = (5.73 ± 0.41) s
𝑇2 = (5.62 ± 0.10) s
𝑇3 = (6.28 ± 0.25) s
The three measurements may be presented in the form of intervals on a number line:
5.2 5.3 5.4 5.5 5.6 5.7 5.8 5.9 6.0 6.1 6.2 6.3 6.4 6.5 T (s)
| | | | | | | | | | | | | |
𝑇1 X
𝑇2 X
𝑇3 X
Note that the intervals associated with 𝑇1 and 𝑇2 overlap, and therefore “these two results agree
within experimental uncertainty”.
The intervals associated with 𝑇1 and 𝑇3 also overlap so “these two results agree within experimental
uncertainty”.
However, the interval associated with 𝑇3 does not overlap with the interval associated with 𝑇2 and
therefore “these two results do not agree within experimental uncertainty.”
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Guide to Reporting and Measurement: January 2018
The final result in this case may then be recorded as: “the best approximation of the voltage 𝑉 is 1.520 volts
with a combined standard uncertainty of 0.023 volts.”
34
Example 2: A set of dispersed digital readings
Now let us presume that we are trying to measure the acceleration due to gravity 𝑔 by observing the period
𝑇 of a pendulum of length 𝑙. We determine that 𝑙 = 0.2619 0.0058 m (where 𝑢(𝑙) results from a Type B
evaluation of uncertainty with an analogue metre stick).
We then use a digital stopwatch to measure the period of the pendulum. You cause the pendulum to oscillate
and then record the time for 20 complete swings. You repeat this procedure 10 times and observe the data:
Table D3-2: Data recorded using a digital stopwatch.
Time for 20 swings, 𝑇20 (s) Period, 𝑇 = 𝑇20 /20 (s)
19.56 21.31 0.978 1.066
20.49 20.82 1.025 1.041
20.76 19.78 1.038 0.989
20.63 20.39 1.032 1.020
21.56 20.02 1.078 1.001
Since we observe a dispersion (scatter) in the readings, the best estimate of the period 𝑇 is given by the
arithmetic mean 𝑇̅, which is 1.027 s, and the standard uncertainty associated with the scatter is given by the
experimental standard deviation of the mean, which is 0.010 s. Then 𝑢(𝑇̅) = 0.010 s. This is a Type A
evaluation of uncertainty. Another source of scatter you might consider is the uncertainty in the gradient of a
linear graph (“the scatter in the (𝑥, 𝑦) data, 𝑢(𝑚)”).
Let us say that the manufacturers of the stopwatch report that it is accurate to 0.5%. Then the uncertainty
associated with the internal calibration or rating, 𝑢(𝑇rating ), will be:
𝑙 4𝜋 2 𝑙
𝑇 = 2𝜋√ → 𝑔= .
𝑔 𝑇2
This is our model equation for this measurement. The best approximation for 𝑔 is given by,
4𝜋 2 (0.2619 m)
𝑔= = 9.8028 ms −2 .
(1.027 s)2
The uncertainty budget for this measurement is shown below.
Table D3-3: Uncertainty budget for the measurement of gravitational acceleration, 𝒈.
Uncertainty component Standard uncertainty Type of evaluation
Scatter in the 𝑇 data, 𝑢(𝑇̅) 0.010 s Type A
Rating of the stopwatch, 𝑢(𝑇rating ) 0.0051 s Type B
Reading of 𝑙 from the analogue metre 0.0058 m Type B
stick, 𝑢(𝑙)
The combined uncertainty for 𝑇 is 𝑢(𝑇) = √(0.010 s)2 + (0.0051 s)2 = 0.011 s.
𝑢(𝑙) 2 𝑢(𝑇) 2
The standard uncertainty for 𝑔 is given by 𝑢(𝑔) = 𝑔√( ) +( )
𝑙 𝑇
0.0058 m 2 0.011 s 2
𝑢(𝑔) = (9.8028 ms −2 )√( ) + (2 ) = 0.302 ms −2 .
0.262 m 1.027 s
The final result may then be recorded as: “the best estimate of the acceleration due to gravity 𝑔 is 9.80 m s-2
with a standard uncertainty of 0.30 m s-2.”
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Guide to Reporting and Measurement: January 2018
Use a least squares fit to fit a straight line to the data, the equation of
which is 𝑦 = 𝑚𝑥 + 𝑐. See E3 Method of least squares.
Extract the information you are after from the coefficients m and c of
the fitted function.
Calculation
Calculate the value of the measurand you are after and do the
necessary uncertainty calculations to determine the uncertainty in the
final result. See C1 Calculation of uncertaint.
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E2 Linearising equations
When presented with a relationship between experimental variables that is not linear, the method of
‘linearising’ can be used extract information from recorded data.
Effectively, you rearrange the non-linear equation to take the form of a linear equation; 𝑦 = 𝑚𝑥 + 𝑐. After
plotting values on a graph for 𝑦 against 𝑥, you can use the gradient, 𝑚, and 𝑦-intercept, 𝑐 to calculate useful
values.
Example:
Consider an experiment to investigate the relationship between the position 𝑠 of an object over time 𝑡 while
that object is subject to a uniform (constant) acceleration 𝑎. This experiment is underpinned by the following
kinematic equation:
1 2
𝑠= 𝑎𝑡 + 𝑢𝑡 + 𝑠0 , … E2-1
2
where 𝑢 is the initial velocity and 𝑠0 is the initial position of the object.
If a set of data, (𝑡𝑖 , 𝑠𝑖 ), i = 1, 2, 3, …, n, were collected, then it would be difficult to determine the coefficients
𝑎, 𝑢 and 𝑠0 by plotting a graph of the equation E2-1 because the relationship between the position 𝑠 and the
time 𝑡 is a parabola of the form 𝑦 = 𝑎𝑥 2 + 𝑏𝑥 + 𝑐.
Equation E2-1 can be ‘linearised’ by considering the position relative to the initial position 𝑠0 and by dividing
throughout by 𝑡 ( given that 𝑡 ≠ 0 ):
𝑠 − 𝑠0 1 … E2-2
= 𝑎𝑡 + 𝑢.
𝑡 2
𝑠−𝑠0
In the rearranged equation, there is a linear relationship between and 𝑡, of the form, 𝑦 = 𝑚𝑥 + 𝑐:
𝑡
𝑠 − 𝑠0 1
= 𝑎 𝑡+𝑢
𝑡 2
𝑦 = 𝑚 𝑥+𝑐
𝑠𝑖 −𝑠0
Therefore plotting a graph with calculated values of (𝑡𝑖 , ) as the values (𝑥𝑖 , 𝑦𝑖 ) should yield a linear
𝑡𝑖
relationship.
You can now determine the acceleration, 𝑎, in equation E2-1 from the gradient of the graph and the initial
velocity, 𝑢, from the 𝑦-intercept.
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Guide to Reporting and Measurement: January 2018
𝑛 ∑ 𝑥𝑖 𝑦𝑖 − ∑ 𝑥𝑖 ∑ 𝑦𝑖
𝑚= … E3-1
𝑛 ∑ 𝑥𝑖 2 − (∑ 𝑥𝑖 )2
∑ 𝑥𝑖 2 ∑ 𝑦𝑖 − ∑ 𝑥𝑖 𝑦𝑖 ∑ 𝑥𝑖
𝑐= … E3-2
𝑛 ∑ 𝑥𝑖 2 − (∑ 𝑥𝑖 )2
Let 𝑑𝑖 = 𝑦𝑖 − (𝑚𝑥𝑖 + 𝑐), the distance between each data point and the line of best fit. The uncertainties
associated with m and c can be determined using:
∑ 𝑑𝑖 2 𝑛
𝑢(𝑚) = √ ( ), … E3-3
2 2
𝑛 ∑ 𝑥𝑖 − (∑ 𝑥𝑖 ) 𝑛 − 2
∑ 𝑑𝑖 2 ∑ 𝑥𝑖 2 𝑛
𝑢(𝑐) = √ ( ). … E3-4
2 2
𝑛(𝑛 ∑ 𝑥𝑖 − (∑ 𝑥𝑖 ) ) 𝑛 − 2
A computer is generally available to you in PHYLAB1 and the method of least squares can be employed using
the following programs:
Microsoft Excel (by typing in the equations) or
LinearFit (by entering the data).
If a computer is not available, use your calculator to draw up tables of data as suggested below and solve the
equations above. Some calculators will allow you to analyse data pairs.
𝑖 𝑥𝑖 𝑦𝑖 𝑥𝑖 2 𝑥𝑖 𝑦𝑖 𝑑𝑖 2
… … … … … …
… … … … … …
… … … … … …
∑ 𝑥𝑖 ∑ 𝑦𝑖 ∑ 𝑥𝑖 2 ∑ 𝑥𝑖 𝑦𝑖 ∑ 𝑑𝑖 2
38
E4 Using EXCEL (2010 version)
places can be achieved using the buttons marked . To outline the cells or add borders to your table
use the button marked . To add headings (and units) to columns, click on the cell and TYPE as you
would normally do. To produce superscripts and subscripts in the titles, select the text you want to raise or
lower, and use the right click to access the “Format Cells” menu. Then select “Superscript” or “Subscript”.
Further options can be accessed in the Excel menus or using the right-click menu.
the chart sub-type option which allows you to plot the points without lines. Under the CHART TOOLS set
of menus, you can change the Design (colour and style of data points), Layout (add titles, axes-titles, gridlines)
and the Format (chart size). Move your plot into the desired position by clicking just inside the borders and
dragging it to where you want it positioned. Other options can be accessed by selecting the chart with a right-
click of the mouse. You can change the origin and scale of the plot so that your graph covers most of the page.
To change the scale on the 𝑥-axis, click on the axis to select it. Next right-click to access the FORMAT AXIS
option and in the Axis Options sub-menu, adjust the minimum and maximum values as required. You can also
change the number of decimal places or to scientific exponent form under the Number sub-menu.
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Guide to Reporting and Measurement: January 2018
E5 Using LINEARFIT
LinearFit can be used to calculate the slope 𝑚 ± 𝑢(𝑚) and the intercept 𝑐 ± 𝑢(𝑐) of the linear line of best fit.
To start the program, click on the LinearFit shortcut on the desktop. The program will open and present the
page as shown in Figure 16. Type the 𝑥 and 𝑦 values into the appropriate columns, or alternatively import
your data in a .csv file (e.g. saved from Excel) in the format 𝑥, 𝑦, 𝑢(𝑥), 𝑢(𝑦) and LinearFit will automatically
calculate 𝑚 ± 𝑢(𝑚) and 𝑐 ± 𝑢(𝑐). When printing, don’t forget to add your student number to help you
identify your work at the printers.
40
SECTION F – EXAMPLE OF FITTING A GAUSSIAN
Consider an example in which the measurand is the time taken for you to travel from wherever you live to the
university campus. So, for the next 40 trips to the university you use the stopwatch on your cell phone to
determine your travel time in minutes, i.e. you take a set of readings.
The data are tabulated as follows:
Table F-1: Time taken to get from home to campus (in minutes).
A simple calculation shows that the average time taken is 17.39 minutes.
We wish to present this data in a histogram, so the next step is to draw up a frequency table (or distribution
table). Note that in this example a bin width of 0.5 minutes was chosen. The choice of bin width is arbitrary
and is normally chosen to suit the data.
Table F-2: Frequency table for data in Table F-1.
Having decided that the Gaussian probability density function (pdf) is a suitable probability density function
by which to model our knowledge of the measurand, we need to consider the implications. The probability
density function of a continuous random variable is a function that can be used to obtain the probability
that the random variable may take a specific value within some given interval.
When the probability density function (pdf) is normalised and portrayed graphically, the probability that
the random variable may take a specific value within a given interval is indicated by the area under the
graph subtended by that interval. So, if the given interval is all possible values, then the total area under
the pdf is “1” (unity), meaning that the probability that the specified value exists is also 1. As the interval is
made “narrower”, so the probability that the specific number is within that interval becomes less.
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Guide to Reporting and Measurement: January 2018
The important features of the Gaussian pdf are illustrated graphically in Figure 19.
The equations used to calculate the standard deviation are given in B2 TYPE A evaluation of uncertainty, and
the standard deviation can also be found graphically by drawing a horizontal line at 0.61 of the maximum
height of the Gaussian, as shown in Figure 19.
In laboratory work, the use of the standard deviation gives a measure of the consistency of the measurement
process that was used in an experiment, and makes it possible to specify the level of confidence with which
the result of the measurement is quoted. In this case, the coverage probability (level of confidence) is 68%, as
explained in Figure 19.
However, exercise caution as the standard deviation and mean are only appropriate metrics for data that can
be modelled with a Gaussian distribution. You may encounter data that is better modelled with a different
distribution (e.g. radioactive decay is modelled with a Poisson distribution).
42