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Advanced Materials Characterization Methods: Prof. Zhumabay Bakenov Dr. Aishuak Konarov

The document provides instructions for advanced materials characterization methods, including how to prepare samples for XRD analysis by placing powder samples in glass or aluminum sample holders and smoothing the surface. It also introduces the Match software for identifying materials from sample data and zero-background sample holders for small sample amounts. The document is presented by Prof. Zhumabay Bakenov and Dr. Aishuak Konarov on methods for analyzing materials sample data using X-ray diffraction.

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Hussain Ali Murtaza
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47 views9 pages

Advanced Materials Characterization Methods: Prof. Zhumabay Bakenov Dr. Aishuak Konarov

The document provides instructions for advanced materials characterization methods, including how to prepare samples for XRD analysis by placing powder samples in glass or aluminum sample holders and smoothing the surface. It also introduces the Match software for identifying materials from sample data and zero-background sample holders for small sample amounts. The document is presented by Prof. Zhumabay Bakenov and Dr. Aishuak Konarov on methods for analyzing materials sample data using X-ray diffraction.

Uploaded by

Hussain Ali Murtaza
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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Advanced Materials Characterization

Methods

Prof. Zhumabay Bakenov


Dr. Aishuak Konarov

Prof. Z. Bakenov 1
Laboratory of XRD

• You will be given some samples data


• Identify the material
• Analyze the data using software

Prof. Z. Bakenov 2
Match

https://www.crystalimpact.com/match/download.htm
XRD

Prof. Z. Bakenov 4
Prof. Z. Bakenov 5
Sample preparation
~ glass sample holder ~

1. Powder sample put in the 3. Smooth the surface of a sample with


sample holder the back of a glass plate

2. Hold a sample with a glass 4. Wipe the glass holder with


plate. cloth

6
Sample preparation
~ aluminum sample holder ~

1. Put a drug packing paper on a


glass plate. After that, powder 3. Compress a sample by a
sample put in the sample finger
holder

4. Remove a drug packing paper,


2. Hold a sample with a glass turn over the sample.
plate.

7
Zero-background sample holders

• Used for small sample amounts or in order to address transparency


effects from weakly absorbing samples
• Available for the standard sample holder and the ASC-6 sample
changer

8
Prof. Z. Bakenov 9

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