(Reaffirmed!2014) !

Free Standard provided by BIS via BSB Edge Private Limited to Schneider -
Chennai([email protected]) 165.225.104.124 [for non-commercial use only]

( Reaffirmed 2005 )
(Reaffirmed!2014)!
(Reaffirmed 2019)
is I 1648 .. IriS
Indian Standard
SPECIFICATION FOR
SILICONE COMPOUNDS FOR
APPLICATION ON HIGH
PORCELAIN INSULATORS
F.lectrical Insulators and Accessories Sectional Committee, ETDC 3
Chairman Representing
Smu L. C. JAIN Central \Vater & Power Commission ( Power Wing ),
New Delhi
Members
ADDITIONAL CRIEF ENGINEER, Directorate General of Posts & TeJleg~~..pllJ
P~&TEL£GRAPHS,JABALPUR ment of Communications ).
DIRECTOR OF Tu.EGR.U'HlI L ( Almnatt )
DiVDtONAL ENGINEER,
GlIAPHlI (C) (Alt6rnat6)
SHIll V. R. ANANTHANARAYANAN Potteries Limited, Calcutta
CHANDAN PANlWIli ( lilt6rnat6
SHRI S. S. AROKIAIIWAMY Tamil Nadu Electricity Board, Madras
SHIU P. S. THIRUKAVUXXARAillI (Alternat6)
DR A. S.BHADURI National Teat House, Calcutta
SHRI S. K.
MUXHERJEE ( Allmr$)
SHIll B. C. DAW All India Pottery Manufacturers'
Calcutta
SHRI B. C. BANERJU ( AllmJat6 )
Smu A. N. Du Damodar Valley Corporation. Calcutta
Smu A. C. BosE ( Alt6rnat6 )
DIliIBO'IOR OF REmAIotCB Maharuhtra State Electricity Board,
(TRACTION AND Research, )'>mgm & Standards
,lMlrALLoAT..J .. ) Ministry of Railways, Lucknow
DEptmi' DIRBcToB. STANDAIWI ( )
DllU!(lTOR ( TRANPofWlON ) Water & Power Commiuion ( Power Wing ),
Delhi
DEPUTY DluOTOR (TaANSMtUIOH
R. K. DATTA POI'i~~",in Co Pvt Ltd, Calcutlta.
D. T. GlJIISAlIANI DiI:'ectDralte General of Supplies & DiJli>OULis (Impec-
Wing)
SRIll G. R. BHATIA ( ..4Jlmklu )
SIDl S. C.Josm DiI:ec~orate General ofTeclmical De\relopm1ent, New
(I Copyri,i., 1975
INDIAN STANDARDS INSTITUrION
This publication is protected the Indian Copyright Act ( XIV of 1957) IJld
reproduction in whole or in except with writton pormissiol1 of tho
publisher mail be doomed to an iDflt'iDilllDlat of copyri(Jht under tbo uid Act..
U I 7148 .. 197.5
( ~iftom pa,. 1 )
Mmlml
SIUU N. D. KAPOOR Development Centre,
SmuT.
SIUUH.M. Electricity
M.
SaRI Electrical;
Smu
SmuK. P~=~~=:,u Se&hasayee IndWluies Ltd, South Areot District
Smu, (AltmulU)
IbtG.M. Indian Electrical ManuCac:turerll' Auociatioa.
Bombay
Smu K. N. JAYA1ItAII (AltmulU)
SIUU P. S. RAMAN New Government Electric Factory, BanpJore
Smu E. P. WIL1'UJ:D (AltmulU)
Smu A. SAUBAYooRTHY MY80re POl'eelaiWi Ltd, Bangalore
Smu K. N. JAYAllAK (A1Urmau )
SHRI P. S. SATMAN State Boaro, Pam.la
Smu K. L. BHATIA (Allmlau)
A. P. SOTHAPATHY Rum! Electrification Ltd, New Delhi
A. K. MUJlHoJo ( Allmlal,)
S. SsnroLUlON W. S. Imulatod of India Ltd, Madras
V. SRINIVASAN (Allmlau )
High Tenaion Insulator Factory, Raneb.i
Director General, lSI (&-offirio MmWlr )
s.ull4T.Y
Smu R. C.JAIN
Deputy Director ( Elec tech), lSI
Panel Silicone Compounds for Electrical Insulators, ETDC 3 : P5

DR B. CaOWDmJJI.Y Research, ~ Standllitds OrganizatJ.on, M.i.nifI..
tryofRBilwa~,LUdW~
DKpUTY DxuCTOa ( Cmuaf!A1.) (.dltmratI)
S:mu P. C. MANKO!)! Gujarat Electricity Board, Baroda
SHIUJ. S. kyo (AltmulU)
SHill A. L. MOHANA RAo Andhra Praacm State Electricity Board, Hyderabad
S:mu M. VENXA']1!;IIWARLU (Allmiau )
Smt! S. R. MUltmtRJEE Mctroarc Private Limited. Calcutta
DR KALYAN KUMAR BAmRJEE (AltmuIU
SBRl N. RANOAKAlAN Madras
SHIU K. C. SEAL
SmtrJ. S. SHAH Mom Lubricants, Bombay
SHIRr N. C. MAvANl (A1Urmau)
SHIRr K. SlTHARAMA. R.<\o Indian Oil Corporation Ltd, Bombay
SHill A. MAJUMDAR (Altnnau)
K. SUBRAYANYAK Maharaahtra State Electricity Board, Bombay
L. VBNKATAIUBBU scmasayee Industria Ltd, South Arcot DUtrict
2
IS I 1648 .. 1915
Indian Standard
SPECIFICATION FOR
SILICONE COMPOUNDS FOR
APPLICATION ON HIGH VOLTAGE
PORCELAIN INSULATORS
o. FOREWORD
Indian Standard was adopted. by the Indian Standards Institution
1975, after the draft finalized. by the Electrical Insulators and
AcoeulOn,!:S Sectional Committee had been the Electrotechni·
Di..riaic~n Council. '
0.2 This specification deals with silicone compounds suitable for application
either hand or by brush or by sprayer on the surface of high voltage
poJ~eLain or glass msulators to prevent by their action the
Halilho'ver of insulators due to pollution of the inslulator surltace
coal dusts, cement dusts, and chemical
0.3 There are various types of silicone compounds, all of which a:re not
suitable as anelecmcal insulating material for the of prevention
of Ba.shover due to pollution. Silicone oil is also suitable for this
It shall, however, be ensured that the application of the silicone
COIllPOiunlD shall not lower the electrical characterlStics of the insula ton:.
0.4 .The hydrocarbon based compounds are also emlplo~yed for the purpose
of prevention of pollution on insulators.
0.5 For the purpose of deciding whether a particular of this
standard is complied with, the final value observed or ca!lcuJiatcr:i, Clmr~::ss·
result of a test. shall be rounded. off in accordance : 2-
The number of significant retained in the rounded off value
should be the same as that of the value in this standard.
1. SCC:)PE
1.1 This standard covers the composition, classification and reC;lui.!:en:lents
of lilic,one compounds suitable for application the surface
poJ'Cdain insulators to prevent by their and en(:ap:suL1ltiIltg
flashover of insulators due to atl1nos:ph(~ric pollutilon.
J
IS I '1648 .. 1m
2. TERMINOLOGY
2.0 For the purpose of this standard, the following definitions shall
2.1 Softening Point - The at which a substance attains a
of softness under specified conditions of test.
2.2 Arc Resistance - The numerical value of the time in seconds from
the start of the test until failure the formation of a continuous
line between the electrodes shaH be recorded as the measure of the arc
tance of the cOlnpou:nd.
3. COMPOSmON
3.1 Silicone or are of an
siloxane oil with a rea,SOl!lat>ly curve
thickners such as gra,phite. or molybdenum
sul.phlde. The pr()perti4es these thi~::kn,ers nature of the
COlrIlp.ouind and consequently the possible uses. All thickners are
not suitable the of of atmospheric pollution. The
materials should be smooth in texture and free from
and dirts.
4. CLASSIFICATION
4.1 Silicone for application on high insula ton are
divided into the following two types:
A :..- In or compound form ready to be applied on the
cleaned insulator hand or brush.
B - In to be "PJ,,"'""y, on the cleaned insulator
by suitable methods dippin;g.
5. REQ,UlB.EMENTS
5.1 Silicone compounds for application on voltage insulaton shall
comply with all the requirements covered in and' 53 for type A and
type B respe<:tively
5.2 A Silicone ComlJOuiDd
5.2.1 General- It shall be translu<;ent, vaselindike with
resistance to heat and oxidation and small change in
COlrJ.,Slliterlcy over a wide temperature range. It shall inert and
ph'ysi()lo~tic~Llly inert ( nontoxic), and shall not attack and their
associa.ted fittings. The nontoxicity shall be by a recogmsed.

testing institution. It shall have the following other characteristics:
a) Physical charactnidics
1) Colour In its patural fonn. the colour should be trarulluccnt
white, light grey or cream.
NOTE - A or pigment of any colour except may be
if required by user, r,rovided the finished meetli the
requirements speclficatibn.
2) Odour - The silicone compound shall be odourless.
3) Specific Gravity - Thl': gravity shall be approximately
1-0 when measured at
4) Service - There shall be almost no change in the
viscosity of compound in the temperahU'e range of
50"C to plus 200"0.
5) Unworked Penetration The silicone compound shall have
the penetration characteristics as follows:
Unworked penetration =
Minimum 200
Maximum 260
Worked penetration Maximum 300
6) Bleed or Oil Separation - The silicone compound shall not
have the bleed or oil separation more than 10 percent.
7) Volatility or Weight Loss on Heating - This loss of "lU'''VS,tC
compound shall not exceed 3 percent.
8) Solvent - The silicone shall be insoluble.
When the compound is immersed in the following solvents,
the allowable loss in weight for the compound in each solvent
shall not exceed as below:
Solvent Maximum Pnunt lim
by Weight
Distilled water 0-4
lllOpropyl alcohol ( 91 percent) 10'0
alcohol 7'0
Ethylene glycol 0'5
Glycerine 0-5
9) Solidifying Point - The silicone compound have the soU·
4'1,'"""", point not exceeding -60°C.
IS I '1641 .. 19'75
10) :)oltelrUD:g' Point - The COlmp!ound shall remain unsoftened at
of 200"C tested in accordance with
IS:
11) Acid Value - The acid value- of the silicone compound shall
be 0'3.
b) Electrical characteristics
I) Electric Strength - The silicone compound shall have the
minimum electric of 10 kV /rom.
2) Volume Resistivity - The silicone compound shall have the
fonowing values of the volume resistivity:
at 27"C - about 1016 ohm. cm, and
at 150"C-about 1'3 X l()lllohm.cm.
3) Surface KesistivIIlV - The silicone compound shall have the
minimum surface of IOU ohm.cm.
4) The silicone compound shall have the dielectric loss ( taD:R'etlt
at room temperature (dry) at different as
Frequency Value of the 3
50 Hz about 0'000 1
0-1 MHz about 0-000 9
1 MHz about 0'001
5) The silicone shall have the dielectric constant
to 3 at room )
6} Arc Resistance The arc resistance of the silicone compound
shall be 80 seconds or more.
c) IUsistance to chemicals Fully resistant to water vapour,
melhanol, elharol, . mineral vegetable
oils, 25 percent 10 percent sul.phuri:c hydro-
chloric acid ( 1 : 15). 10 percent nitric coo!km:g salt solution.
resistant to acetone, 40 percent cold caustic-
soda, SO ......·rp.d cold caustic potash.
Not resistant to concentrated SW]PhllriC acid and nitric acid,
toluol, xylol, white spirit, ethyl carbon tetrachloride,
butanol.
B IDieoDe Com'DCMUld
5.3.1 The characteristics· of the ..,I1 ....n." .. compoWld in the solution shall
be as in 5.2.
:».3.2 Solvent component should not be more than 80 per'cellt. The
manufacturers sha.ll declare the percentage contents of silicone coIIlpc:nmd
in the solution.
5.3.3 The solvent sha.ll not have deleterious effect on the insulator
fittings. galvanised components, spray guns and spray hot-sticks.
5.3.4 It should be kept in mind that it the of the solution
is high, it cannot be sprayed with hand spray
guns.
6. TEST ME'rBC)DS
6.1 Method for the Determ.iaatioa of PeaetradoD - The penetration
of the worked and unwol'ked, shall be determined in accord-
ance with [P: 60 ]-1971 ....
6.2 Method for die DetermJ...doD otVoladlity 01' He.uDgW.!kJIt.t
Lo•• aad Bleed. or on Separadoa
6.2.1 Apparatus - The following sha.ll be re<:Jluir'ed:
a) Wire gauge filter cone, 40 mm diameter and 40 mm slant height;
made from nickel gauge of No. 60 mesh in accordance with
b) 100 mm higb and
convection ).
P,oettiu" the cone from a rod supported on the rim of
which shall a lid. Maintain the temperatnre of the
± 5°0 for 24 hours.
NOTE - The rod will need to be tared with the beaker. The cone lhaU be hard
Ioldered or mlded at the joint in order to withstand the high temperature.
Weigh the entire aasembly and ca.lculate the per'cetltaJte ~i18.pl()rIiLtion
as follows:
~~~~t X 100 percent
Lift the cone from the it against the inside edge
of the tip of the cone. Weigh
pro4ucIII: P: 60 Conmtency of lubrieaq
IS, '1648 .. It7S

the beaker containing the separated fluid and calculate the percentage of
the oil separation as follows:
0 I'1 separa t'IOn -- Gain in weight of beaker

Weight of sample X
100
percent
6.3 Method fGr the DetermiDatiGn Gf InsGlubility - About 3 g of the

compound, accurately weighed, shall be smeared around the inside of a
weighed glass beaker of 250 ml capacity. Approximately 100 ml of the solu-
tic~ are enough to immerse the compound and shall be poured into the con-
tainer. The container shall be tightly capped with metal foil and left to stand
for a period of 7 days at a temperature between 22"C and 28"C. At intervals
of aprroximately 24 hours, the solution shall be stirred by moderate manuaJ
rotation of the container. At the end of the 7-day period, the solution
shall be poured off, and the container and compound rinsed carefully with
successive washes of distilled water until all solvent has been removed.
The container and compound shall be dried for 20 hours in an oven at
70"C followed by desiccation for 4 hours over calcium chloride. A blank
shall be run to determine the loss due to evaporation which occurs during
the treatment. A final weight less than the original weight of the container
-and compound shall indicate removal of soluble constituents.
6.4 Method fGr the DetenninatiGn Gf Solidifying PGmt - Maintain
the material at a temperature of -60°0 for a period of 24 hours. At the
end of this period examine the material for any signs of solidification or
cracking. At -60°C the material shall not solidify or crack. A slight
increase in stiffness of the compound may be disregarded.
6.S Test Method fGr Softening PGint - The method described in

IS: 1205-1958* shall be used. The temperature of the compound shall
be 200°C for the determination of the softening point.
6.6 Method for the Determination of the Add Value - The test
procedure shall be same as given in IS: 1448 [P: 2 ]-1967t.
6.7 MethGd fGr the Determinadcm Gf Electric Strength- Place the
compound in a porcelain container fitted with 12'7 mm diameter steel or
brass electrodes set 1'25 mm apart, similar to that described in IS: 7084-
1973t. Subject the container and its contents to a slow reduction in air
pressure ( taking 10 minutes to reduce to 10 ) to cause minimum
movement of compound. Continue the pressure reduction to less than
1'0 mm of mercury and maintain at this pressure for one hour or until all
traces of air bubbles have been removed. Slowly restore to atmosph'Cl"ic
(IDetermination of softening point.
fMethods of test for petroleum and its products: P; 2 Acidity (jirstrevisicn ).
tSpeCificatiOD for bitumen baied filling compoundJ for dectric:aJ purposa.
1I.'.... lI75
-preuw."e and then maintain th.e coIltainer and its contents at a temperature
of27·C for 3 hours. Then carry out the·electrir: strength test
at2rC.
For test voltage source o~ber details. reference may be made
to 84.5 to "2.9 of IS :7084-1973·,
voltage applied to the electrode is gradually
zero to 12-5 kV nm in 10 to seconds and maintain at this value
fOr one minute.
Test two samples of the material. If one sample fails to withstand
the specified proof voltage for one minute, test a third If thia
sample fails, the whole'lot may be rejected.
6.8 Method fOll' the Determbm.dOD of VoiUD.U!t Reld,sdvity- Test two
llpedm.ens of material at room temperature and two specimens at 150"C.
Use a guarded electrode system corresponding to shown in
1 in a suitable cell that shall allow precise and measurable
set:tar!iLti(J.n of the unguarded with respect to the guarded within
mmtWd3mm.
UNGUARO!D
ELECTRODE
FlO. 1 TYPIOAL AlulA.NOElolBNT FOR DETERMINATION 0.,
VOLmm~
For tests at room temperature maintain the electrodes, test cell, and
ma·tenal to be tested, at 27"C for not less than 24 hours. Spread a layer of the
ma'teri:alover the lower ) electrode to a depth somewhat thicker
than the desired test taking care to avoid trapping air bubbles.
Bring the unguarded towards the upper electrode until the
material is in contact with the guarded electrode and guard ring and
adjust the electrode gap to the desired figure. allowing the material to
spread over the whole electrode and again taking care to prevent
trapping of air.
*Speci.f.ic:atiOD for bitwDcD baaed liIIiDa' compounds for deurieal purpc!IIIC'.I.

,
U I 7648 .. 1975
Measure the eIc,etriica.l resistance between unguarded and guarded

electrodes after for one minute at a potential of 500 ± 50
volts dc.
Volume resmti.vitv- Rohm.cm
where
A. = area in cmll of the guarded electrode,
S "'" thickness in cm of the and
R = measured resistance in ohms.
at elevated spread the layer of material over
ele¢tr.odc::s at room and then maintain electrodes.
test cell, material at 150 ± not less than 4 hours before finally
adjusting the distance between the unguarded and guarded electrodes.
Measure resistance at 150 ± 2°0 and calculate the resistivity as described
above.
The volume resisti.vity shall be recorded as the arithmetic mean of'
&he volume of the tested, at each temperature.
6.9 Method Detenniuaticm 01 Surface Relldstivity The
pr(lC~:iUI'e for test at shall be the same as described in 6.8, but the
C!:1CiCUlIC test circuit be as described in IS: 3396-1965"'..
6.10 Method lor the 01 Dielec:trie Loss Tlll.lllt!!at aad
Diiele,etll'ie Coastaat specimens of the material shall be tested in
accordance with IS: 4486-1967t for 1hese requirements.
6.11 Are Resntlll.llee Test Method - The arc resistance shall be deter-
mined in air at 27°C using a 3'0 m.m of the compound lipread on a
layer of thermal glass, such as quarts or The electrodes, the electrode
holders, the supply to the electrodes circuit arrangement shall be
in IS: 2
0-1 mm. horizontal
The arc electrodes shall be cleaned with a soft clean
dal:npen~:a with alcohol, then dried with a soft, clean dry cloth before
"'Methods volume and surface resistivities. of electrical insulating ma'teriab.

tRecommended methods for the determination of the permittivity
dissipation factor of electrical insulating materials at power. audio &nd
including metre wavelengths.
tMethod for determination of the comparative index of lOUd inNlati.ng
materia.lt.
10
•.,..
.
'1.PA.CKlNG
'1.1 Silicone shall be packed in air-tight, clean and
containers.
8. MA.RKING
8.1 Each container shall carry the toUowing information:
a) Name or trade-mark of the numufac:tul:'er,
b) Type,
c) Year of manufacture, and
Quantity.
8.1.1 The containers may also be marked with the lSI Certification
Mark.
I marked producm are a1!1O continu-

as a furtba- safeguard. Details of
lSI Certification Mark may be granted
obtain~~ firom the Indian Standards Iutitutiou.
9. SAMPLING
9.1 The: recommended llallrlpling scheme is given in Appendix A.
PPENDIX A
(Clause 9.1)
SAMPLING POR THE SILICONE COMPOUNDS
A-I. GENERAL REQ.UlREMENTS OP SAMPLING

A..l.l precautions shaD be taken to avoid contamination while
transferring samples to and glass
containers.
A-l.2 Each container aftet shall be sealed &ir-tight and
marked wi ch as sample number,
the date of sanlpling, of manufacture of material, and other
11
is : 76f8 • 1975
A·2. SCALE OF SAMPLING
A-2.1 Lot - In a single consignment, all the containers of the same type,
size, and drawn fi'om the same batch of manufacture shall constitute a lot.
If a consignment is dcclan:d or known to consist of different batches of
manufacture or of dilfercnt sizes of containers or of different types of
material then the containers belonging to the same batch under the Silme
size and type shall be grouped together and each such group shall
cv;~stitute a separate lot.
A-2.1.1 Samples shall be tested for each lot for ascertammg the
conformity of the material to the requirements of the specification.
A-2.2 The number of containers (n) to be selected from a lot shall depend
on the size of the lot (N) and shall be as given in Table 1.
TABLE 1 NUMBER OF CONTAINERS TO BE SELECTED FOR SAMPLING
LOT SIZE NUMBER OP CONTAINERS

TO BE SELECTED
N n
(I) (2)
Up to 20 3
21 to 40 4
41 " 80 5
81 " 120 6
121 " 200 8
201 and above 10
NOTE - In the case of very small lots where the selection of three containers may be
uneconomical, thc number of containers to be selected and the criterion for judging the
conformity of the lot to the specification shall be as agreed to between the purchaser
and the supplier.
A-2.3 The containers shall be selected at random and in order to ensure the
randomness of selection, a random number table shall be used. In case
such a table is not avaifable, the following procedure may be adopted:
Starting from one container; count them in one order as
1,2,3, ..................... , up to r and so on, where r is the integral
part of N/n ( N being the lot size and n the number of containers to
be selected). Every rth container thus counted shall be withdrawn
to give samples for test.
12
IS I 7648 .. 1'75
A~3. PREPARATION OF TEST SAMPLES AND RE1FElWrcm
SAMPLE
A-l.t To ensure that the taken from each container
tive of the contents, the contents shall be mixed th,w","alhl" shaking
or by or both.
A~3.2 After the contents are thoroughly a representative
portion of the material shall be taken with the of a suitable sampling
instrument from each of the containers selected. total quantity of
the material drawn from each container shall be sufficient to conduct tests
for all as in this standard.
A-l.3 The material taken from each container shall be divided into three
equal parts, each an individual One set of the individual
representing n containers shall be marked for the
purcllasier, another for the supplier and the third to be used as a reference
A-S." All the samples shall be transferred to separate containers. These

containers shall then be air- tiflht and labelled with full identification
n~lrtl('lIl>lrl: as in
A-3.5 The reference consisting of a set of n individual samples
representing n containers shall bear the seals of both the purchaser
and the supplier. shall be kept at a to between the
purchaser and the and shan be used in case of any dispute
between the two.
A~. NUMBER OF TESTS

A-f.l Tests for requirements as given in 5.2.1 (a) and 5.2.1 (b) shall
be on each of the individual sanlpl;es taken for this purpose.
A-S. CRITERIA FOR CONFORMITY

A-S.I A lot shall be as conforming spe:cifi,cation if the
s3xnples tested meet all the re{luirerneJrlts given in and
(b).
13
243
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Free Standard provided by BIS via BSB Edge Private Limited to Schneider -

Chennai([email protected]) 165.225.104.124 [for non-commercial use only]

Panel Silicone Compounds for Electrical Insulators, ETDC 3 : P5

associa.ted fittings. The nontoxicity shall be by a recogmsed.

b) 100 mm higb and

IS, '1648 .. It7S

0 I'1 separa t'IOn -- Gain in weight of beaker

6.3 Method fGr the DetermiDatiGn Gf InsGlubility - About 3 g of the

6.S Test Method fGr Softening PGint - The method described in

*Speci.f.ic:atiOD for bitwDcD baaed liIIiDa' compounds for deurieal purpc!IIIC'.I.

Measure the eIc,etriica.l resistance between unguarded and guarded

Volume resmti.vitv- Rohm.cm

"'Methods volume and surface resistivities. of electrical insulating ma'teriab.

I marked producm are a1!1O continu-

A-I. GENERAL REQ.UlREMENTS OP SAMPLING

TABLE 1 NUMBER OF CONTAINERS TO BE SELECTED FOR SAMPLING

LOT SIZE NUMBER OP CONTAINERS

A-S." All the samples shall be transferred to separate containers. These

A~. NUMBER OF TESTS

A-S. CRITERIA FOR CONFORMITY

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