Stirred Tank Reactors
Stirred Tank Reactors
MATRICULATION NUMBER:
LEVEL: 400LEVEL
DEPARTMENT: CHEMICAL ENGINEERING
GROUP: A4
SERIAL NUMBER: 034
COURSE CODE: CHE401
TITLE OF EXPERIMENT: SHELL AND TUBE HEAT EXCHANGER
EXPERIMENT NUMBER: 02
AIM OF EXPERIMENT:
I. To demonstrate indirect heating or cooling by transfer of heat
II. To perform an energy balance across a shell and tube heat exchanger and
calculate the overall efficiency at different fluid flow rate
III. To demonstrate the difference between parallel flow and countercurrent
flow and the effect on heat transferred and temperature efficiencies
IV. To determine the overall heat transfer coefficient for a tubular heat
exchanger using the Logarithmic Mean Temperature Difference to perform
calculations
V. To investigate the effect of changes in hot and cold fluid flow rate on the
temperature efficiencies and overall heat transfer coefficient
DATE OF EXPERIMENT: 08/02/2021
DATE OF SUBMISSION: 12/02/2021
INSTRUCTOR’S NAME: ENGR. EKENE EGHAREVBA ETINOSA
Care must be taken when handling the shell and tube heat exchanger. Corrosion
and pipe lagging must be looked out for. Also avoid touching hot surfaces of the
equipment.It was concluded that if flow rates are alternated, we could see the
effect of flow rate on the transfer of heat. In the first instance; when the flow
rates were set far apart at 3 and 1L/min, we saw a very low heat transfer which
quickly rose when the flow rates difference was reduce by a measly 0.5
difference.
The convective heat transfer, simply known as convection is the transfer of heat
from one place to another by the movement of fluids. It is the most dominant
form of heat transfer in liquids and in gases.
A heat exchanger is a device used to transfer heat between two or more fluids.
The fluids can be single or two phase and, depending on the exchanger type, may
be separated or in direct contact. Devices involving energy sources such as
nuclear fuel pins or fired heaters are not normally regarded as heat exchangers
although many of the principles involved in their design are the same.
There are three primary classifications of heat exchangers according to
their flow configuration;
1. Parallel – flow
2. Cross – flow
3. Counter – current
Shell and tube heat exchanger is a device that consists of a shell and a bundle of
tubes mounted inside it. One fluid runs through the tubes, and another fluid flows
Double pipe heat exchangers are the simplest exchangers used in industries. On
one hand, these heat exchangers are cheap for both design and maintenance,
making them a good choice for small industries. On the other hand, their low
efficiency coupled with the high space occupied in large scales, has led modern
industries to use more efficient heat exchangers like shell and tube or plate.
However, since double pipe heat exchangers are simple, they are used to teach
heat exchanger design basics to students as the fundamental rules for all heat
exchangers are the same.
Another type of heat exchanger is the plate heat exchanger. These exchangers are
composed of many thin, slightly separated plates that have very large surface
areas and small fluid flow passages for heat transfer. Advances
in gasket and brazing technology have made the plate-type heat exchanger
increasingly practical. In HVAC applications, large heat exchangers of this type are
called plate-and-frame; when used in open loops, these heat exchangers are
normally of the gasket type to allow periodic disassembly, cleaning, and
inspection. There are many types of permanently bonded plate heat exchangers,
such as dip-brazed, vacuum-brazed, and welded plate varieties, and they are
often specified for closed-loop applications such as refrigeration. Plate heat
exchangers also differ in the types of plates that are used, and in the
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configurations of those plates. Some plates may be stamped with "chevron",
dimpled, or other patterns, where others may have machined fins and/or
grooves. When compared to shell and tube exchangers, the stacked-plate
arrangement typically has lower volume and cost. Another difference between
the two is that plate exchangers typically serve low to medium pressure fluids,
compared to medium and high pressures of shell and tube. A third and important
difference is that plate exchangers employ more countercurrent flow rather than
cross current flow, which allows lower approach temperature differences, high
temperature changes, and increased efficiencies.
A third type of heat exchanger is a plate and shell heat exchanger, which
combines plate heat exchanger with shell and tube heat exchanger technologies.
The heart of the heat exchanger contains a fully welded circular plate pack made
by pressing and cutting round plates and welding them together. Nozzles carry
flow in and out of the plate pack (the 'Plate side' flow path). The fully welded
plate pack is assembled into an outer shell that creates a second flow path (the
'Shell side'). Plate and shell technology offers high heat transfer, high pressure,
high operating temperature, uling and close approach temperature. In particular,
it does completely without gaskets, which provides security against leakage at
high pressures and temperatures.
A fourth type of heat exchanger uses an intermediate fluid or solid store to hold
heat, which is then moved to the other side of the heat exchanger to be released.
Plate and fin heat exchangers are usually made of aluminum alloys, which provide
high heat transfer efficiency. The material enables the system to operate at a
lower temperature difference and reduce the weight of the equipment. Plate and
fin heat exchangers are mostly used for low temperature services such as natural
gas, helium and oxygen liquefaction plants, air separation plants and transport
industries such as motor and aircraft engines.
Shell and tube heat exchangers, which is our main focus; consist of a series of
tubes which contain fluid that must be either heated or cooled. A second fluid
runs over the tubes that are being heated or cooled so that it can either provide
the heat or absorb the heat required. A set of tubes is called the tube bundle and
can be made up of several types of tubes: plain, longitudinally finned, etc. Shell
and tube heat exchangers are typically used for high-pressure applications (with
pressures greater than 30 bar and temperatures greater than 260 °C).[4] This is
because the shell and tube heat exchangers are robust due to their shape.
Several thermal design features must be considered when designing the tubes in
the shell and tube heat exchangers: There can be many variations on the shell and
tube design. Typically, the ends of each tube are connected
to plenums (sometimes called water boxes) through holes in tube sheets. The
tubes may be straight or bent in the shape of a U, called U-tubes.
Tube diameter: Using a small tube diameter makes the heat exchanger
both economical and compact. However, it is more likely for the heat
exchanger to
foul up faster and the small size makes mechanical cleaning of the fouling
difficult. To prevail over the fouling and cleaning problems, larger tube
diameters can be used. Thus to determine the tube diameter, the available
space, cost and fouling nature of the fluids must be considered.
Tube length: heat exchangers are usually cheaper when they have a smaller
shell diameter and a long tube length. Thus, typically there is an aim to make
the heat exchanger as long as physically possible whilst not exceeding
production capabilities. However, there are many limitations for this, including
space available at the installation site and the need to ensure tubes are
available in lengths that are twice the required length (so they can be
withdrawn and replaced). Also, long, thin tubes are difficult to take out and
replace.
Tube pitch: when designing the tubes, it is practical to ensure that the tube
pitch (i.e., the centre-centre distance of adjoining tubes) is not less than 1.25
times the tubes' outside diameter. A larger tube pitch leads to a larger overall
shell diameter, which leads to a more expensive heat exchanger.
Tube corrugation: this type of tubes, mainly used for the inner tubes,
increases the turbulence of the fluids and the effect is very important in the
heat transfer giving a better performance.
Fixed tube liquid-cooled heat exchangers especially suitable for marine and harsh
applications can be assembled with brass shells, copper tubes, brass baffles, and
forged brass integral end hubs.
In a parallel flow heat exchanger, the two fluid streams (hot and cold) flow
through the heat exchanger in the same direction. The two fluid streams enter at
one end of the heat exchanger and leave at the other end. it is clear that the
temperature difference between the fluid streams decreases from the inlet to the
outlet of the heat exchanger. Parallel flow heat exchangers are rarely employed
due to their requirement of large surface area for heat transfer.
In a counter flow heat exchanger, the two fluid streams flow in relatively
opposite directions. The fluid streams enter at opposite ends. Counter flow heat
exchangers provide the maximum heat transfer rate for a given surface area.
Hence, they are the most widely used heat exchangers.
Log mean temperature difference (LMTD) = (θ1 − θ2)/ln (θ1 − θ2)… (6)
QH = mH x CpH x (t1-t2)
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Hot water flow rate (Cw )
QC = mC x CpC x (T2-T1)
Where:
The use of the LMTD arises straightforwardly from the analysis of a heat
exchanger with constant flow rate and fluid thermal properties.
( t 1 −T 2 )−( t 2−T 1 )
LMTD=
( t 1 −T 2 )
ln
( t 2 −T 1 )
Q
U=
A×LMTD
Where:
ρv ( d s −d o )
ℜ=
μ
At which
ds = Shell diameter, m
Viscosity, taken at average fluid temperature in the shell, Pa.s
As = Exchange area, m2
The Shell and Tube Heat Exchangers are one of the most popular types of
exchanger due to the flexibility the designer has to allow for a wide range of
pressures and temperatures.
A shell and tube exchanger consists of a number of tubes mounted inside a
cylindrical shell. Two fluids can exchange heat, one fluid flows over the outside of
the tubes while the second fluid flows through the tubes. The fluids can be single
or two phase and can flow in a parallel or a cross/counter flow arrangement.
The shell and tube exchanger consists of four major parts:
Front Header; this is where the fluid enters the tube-side of the exchanger.
It is sometimes referred to as the Stationary Header.
General Procedure
A quick inspection was performed to make sure that the equipment was in
perfect condition.
All valves were initially closed except V1 and V2.
Hot tank was filled through a water supply hose connected to valve V 2; with
valve closed as it got filled.
The cold water tank was then filled up by opening valve V 1. The valve was
left opened for continuous water supply.
A drain hose was connected to the cold water drain point.
The equipment was now ready to be run
Experiment 1
The main power was switched on. The heater for the hot water tank was
also switched on and the temperature controller set to 71oC.
The water temperature in the hot water tank was allowed to reach the set
point.
The flow rate of the hot and cold fluids were set at 3L/min and 1L/min
respectively
Valves V3 and V4 were adjusted and opened to obtain the desired flowrates
for hot water and cold water streams, respectively.
The system was allowed to reach steady state for a few minutes and values
for T1, T2, T3 and T4 were recorded.
Experiment 2
The system was then allowed to cool for some minutes to get it to the
required room temperature for optimum result
The flow rate was set at a constant value of 2L/min and 1L/min for the hot
and cold respectively
The temperature was then adjusted to a set temperature of 50 oC
When the required temperature has been reached and normalized the
readings are then taken
This is done repeatedly with a temperature increase of 10 oC until 80 oC is
achieved
The values of T1, T2, T3, T4 are taken for all temperatures.
Table 1: Values recorded for experiment with varying flow rates at set
temperature 71oC
1. 1 1.6667 x 10-5
2. 1.5 2.50005 x 10-5
3. 2 3.3334 x 10-5
4. 3 5.0001 x 10-5
Table 2: Conversion of flow rate
S/ Temperat Cold Hot Hot fluid Hot fluid Cold fluid Cold fluid
N ure in fluid fluid inlet outlet inlet outlet
controller flow flow Temperat Temperat Temperat Temperat
display T rate rate ure T1 (oC) ure T2 (oC) ure T3 (oC) ure T4 (oC)
(oC) Fc Hc
(L/mi (L/mi
n) n)
1 50 1.0 2.0 50.4 44.0 27.2 31.9
Density of fluid
S/N T (°C) ρ
(Kg/m3)
1. 50 988.037
2. 60 983.200
5. 70 977.771
6. 80 971.799
Table 4: Density of fluid (water) at different temperature (From Perry’s
Handbook).
To ensure unit uniformity of the hot and cold flow rates, we have to convert
L/min to m3/s to ease our calculation when trying to compute the mass flow rates.
This experiment was conducted by using the HT30X Heat Exchanger Service Unit
apparatus which is used as cooling devices
The experiment; Shell and Tube Heat Exchanger was conducted with the aim of;
The experiment was conducted using the Armfield Shell and tube heat exchanger
at flow rates of 1L/min, 1.5L/min, 3L/min and 2L/min for the hot and cold fluid.
The experiment was also conducted using varying temperatures and operating
conditions.
The Logarithmic Mean Temperature Difference value for the first set of runs
showed an increase of 1.1531oC for the Logarithmic Mean Temperature. The
difference, which seems to indicated a neigh negligible temperature increase.
While the second set of runs show a steady increase of the Logarithmic Mean
Temperature Difference.
In the use of a shell and tube heat exchanger, several precaution must be put in
place. They include;
The use of a heat exchanger help to tell a lot about heat transfer in fluids. The
Armfield Heat Exchanger was used for this experiment can be seen to be another
contributing factor to the results gotten from this experiment. Factors such as the
irregular flow rates and the slow leaking of water from the various hoses that we
could not properly clamp.
It was observed that even with a high heat transfer capacity of water, it did not
perform very well at low flow rates as well as temperature. This can be seen in
reverse with the experiment where the temperature was raised.
Operating conditions that affect the rate of heat transfer could be the flow rate,
temperature and pressure of the fluid.
The temperature can also be taken into consideration as we saw that the
temperature of the cold fluid rose to high levels when we set the temperature of
the hot fluid to a temperature of 80 degrees. This would explain why steam is
preferably used in plants and industries to achieve higher transfers like in oil and
fat industries.
In conclusion; when alternating flow rate we could see the effect of flow rate on
the transfer of heat. In the first instance when the flow rates were set far apart at
3 and 1L/min. we saw a very low heat transfer which quickly rose when the flow
rates difference was reduce by a measly 0.5 difference.
TECHNICAL DATA:
Inner tube inside diameter (di) = 0.00515 (m)
Inner tube outside diameter (do) = 0.00635 (m)
Heat transmission Length (L) = 1.008 (total) (m)
Hot fluid volume flow rate qvhot (m3/s)
Hot fluid inlet temperature T1 (°C)
Hot fluid outlet temperature T2 (°C)
Cold fluid volume flow rate qvcold (m3/s)
Cold fluid inlet temperature T3 (°C)
Cold fluid outlet temperature T4 (°C)
Hot fluid Hc (°C)
Cold fluid Fc (°C)
From Perry’s Handbook, the standard values of Specific heat capacity of water
(Hot and cold fluid);
Cp(c) = 4183.00J/Kg.K
Cp(h) = 4175.00J/Kg.K
CALCULATIONS:
A. Calculations for mass flow rate:
Recall that;
Mass flow rate = Qv x ρ
Where;
Qv = Volumetric flow rates
Ρ = Density of fluid
For experiment 1:
Using the formula above;
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At Qv = 5.0001 x 10-5(m3/s) and ρ (67.0°C) = 979.459 (Kg/m3)
ṁh = (5.0001 x 10-5) x (979.459) = 0.049 Kg/s
For experiment 2:
Using the same formula above;
At ρ (50.0°C) = 988.037 (Kg/m3) and Qv (hot) = 3.3334 x 10-5(m3/s)
ṁh = (3.3334 x 10-5) x (988.037) = 0.0329 Kg/s
U = q/A˳θm
Where:
U = Overall heat transfer coefficient
A˳ = Area with respect to outer base diameter (A˳= 4πd˳L)
(A˳ = 4π x 0.00635 x 1.008 = 0.0804m2)
θm = Logarithmic mean temperature difference
q = Total heat transfer
For experiment 1:
Using the formula above;
For experiment 2:
Using the same formula above
At Qh = 879.09W, A˳= 0.0804 m2, θm = 17.6363°C
U = (879.09)/(0.0804 x 17.6363)= 619.97W/m 2.oC
At Qh = 1218.77W, A˳= 0.0804 m2, θm = 25.6383°C
U = (1218.77)/(0.0804 x 25.6383)= 591.26W/m 2.oC
At Qh = 1279.39W, A˳= 0.0804 m2, θm = 33.2500°C
U = (1279.39)/(0.0804 x 33.2500)= 478.58W/m 2.oC
At Qh = 1474.44W, A˳= 0.0804 m2, θm = 40.5970°C
U = (1474.44)/(0.0804 x 40.5970)= 451.73W/m 2.oC
Where;
Temperature of hot fluid inlet (th1) = T1
Temperature of cold fluid outlet (tc2) = T4
Temperature of cold fluid inlet (tc1) = T3
For experiment 1:
Using the formula above;
At T1 = 67.0°C, T3 = 27.1°C, T4 = 28.8°C
ηh = (28.8 – 27.1)/ (67.0 – 27.1) x 100 = 4.2607%
At T1 = 69.9°C, T3 = 27.2°C, T4 = 29.4°C
ηh = (29.4 – 27.2)/(69.9 – 27.2) x 100 = 5.1522%