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Gujarat Technological University

This document contains the details of an exam for an Advanced Spectral Analysis course taken by a student with the given enrollment number. The exam contains 7 questions with 3 sub-questions each, for a total of 80 marks. The questions cover topics like UV-Vis spectroscopy, IR spectroscopy, NMR spectroscopy, mass spectrometry, thermal analysis techniques like DTA and TGA, chromatography techniques like HPLC, GC, TLC and their applications in qualitative and quantitative analysis of organic compounds.

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Rishita Chauhan
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85 views1 page

Gujarat Technological University

This document contains the details of an exam for an Advanced Spectral Analysis course taken by a student with the given enrollment number. The exam contains 7 questions with 3 sub-questions each, for a total of 80 marks. The questions cover topics like UV-Vis spectroscopy, IR spectroscopy, NMR spectroscopy, mass spectrometry, thermal analysis techniques like DTA and TGA, chromatography techniques like HPLC, GC, TLC and their applications in qualitative and quantitative analysis of organic compounds.

Uploaded by

Rishita Chauhan
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as PDF, TXT or read online on Scribd
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Seat No.: _____ Enrolment No.

_____________

GUJARAT TECHNOLOGICAL UNIVERSITY


M.PHARM - SEMESTER–2 EXAMINATION – SUMMER-2019

Subject Code: MPC201T Date: 27/05/2019


Subject Name: Advanced Spectral Analysis
Time: 10:30 AM TO 01:30 PM Total Marks: 80
Instructions:
1. Attempt any five questions.
2. Make suitable assumptions wherever necessary.
3. Figures to the right indicate full marks.

Q.1 (a) Explain Woodward – Fieser rule for α, β-carbonyl compounds 06


(b) Explain and give examples of the types of transition occur in organic 05
compounds.
(c) Explain principle and application of UV-Vis. Spectroscopy 05
Q.2 (a) Write a note on ATR –IR 06
(b) Write note on Super critical fluid Chromatography 05
(c) Write principal, instrument and application of CEMS 05
Q.3 (a) Describe the factors affecting the chemical shift 06
(b) Write the principle of NOESY spectroscopy 05
(c) HECTOR NMR 05
Q.4 (a) Enumerate various types of Mass analyzer. Discuss quadrupole mass analyzer 06
with appropriate diagram.
(b) Write principal, instrument and application of LC-FTIR 05
(c) Mc Lafferty rearrangement 05
Q.5 (a) What is thermal method of analysis? Discuss principle and applications of 06
differential thermal analysis (DTA)
(b) Define and describe TGA. Discuss the thermogravimetric curve of Calcium 05
oxalate monohydrate
(c) What is enzyme immune-assay? Describe double sandwich ELISA technique 05
for antigen measurement.
Q. 6 (a) Write principal, instrument and application of Flash Chromatography 06
(b) Write principal, instrument and application of Raman Spectroscopy 05
(c) Write note on Ring rule 05
Q.7 (a) Write note on RIA of Digitalis 06
(b) Write principal, instrument and application of GCMS 05
(c) Write principal, instrument and application of HPTLC 05

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