AEROSPACE AMS5554 REV.

F
MATERIAL
Issued 1957-09
SPECIFICATION Revised 2011-07

Superseding AMS5554E
Steel, Corrosion and Heat-Resistant, Seamless Tubing
16.5Cr - 4.5Ni - 2.9Mo - 0.10N
Annealed
(Composition similar to UNS S35000)

RATIONALE

AMS5554F revises response to heat treatment (3.5.2, Table 2) and results from a Five Year Review and update of this
specification.

1. SCOPE

1.1 Form

This specification covers a corrosion and heat-resistant steel in the form of thin-wall seamless tubing.

1.2 Application

This tubing has been used typically for parts, such as fluid lines, requiring high strength and oxidation resistance up to
800 °F (427 °C), but usage is not limited to such applications.

2. APPLICABLE DOCUMENTS

The issue of the following documents in effect on the date of the purchase order forms a part of this specification to the
extent specified herein. The supplier may work to a subsequent revision of a document unless a specific document issue
is specified. When the referenced document has been cancelled and no superseding document has been specified, the
last published issue of that document shall apply.

2.1 SAE Publications

Available from SAE International, 400 Commonwealth Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside
USA and Canada) or 724-776-4970 (outside USA), www.sae.org.

AMS2243 Tolerances, Corrosion and Heat-Resistant Steel Tubing

AMS2248 Chemical Check Analysis Limits, Corrosion and Heat-Resistant Steels and Alloys, Maraging, and Other
Highly-Alloyed Steels, and Iron Alloys

AMS2371 Quality Assurance Sampling and Testing, Corrosion and Heat-Resistant Steels and Alloys, Wrought
Products and Forging Stock

__________________________________________________________________________________________________________________________________________
SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is
entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising therefrom, is the sole responsibility of the user.”
SAE reviews each technical report at least every five years at which time it may be reaffirmed, revised, or cancelled. SAE invites your written comments and suggestions.
Copyright © 2011 SAE International
All rights reserved. No part of this publication may be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical,
photocopying, recording, or otherwise, without the prior written permission of SAE.
TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada) SAE values your input. To provide feedback
Tel: +1 724-776-4970 (outside USA) on this Technical Report, please visit
Fax: 724-776-0790 http://www.sae.org/technical/standards/AMS5554F
Email: [email protected]
SAE WEB ADDRESS: http://www.sae.org
SAE AMS5554F Page 2 of 5

AMS2634 Ultrasonic Inspection, Thin Wall Metal Tubing

AMS2807 Identification, Carbon and Low-Alloy Steels, Corrosion and Heat-Resistant Steels and Alloys, Sheet,
Strip, Plate, and Aircraft Tubing

2.2 ASTM Publications

Available from ASTM International, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959,
Tel: 610-832-9585, www.astm.org.

ASTM E 8/E 8M Tension Testing of Metallic Materials

ASTM E 353 Chemical Analysis of Stainless, Heat-Resisting, Maraging, and Other Similar Chromium-Nickel-Iron
Alloys

ASTM E 426 Electromagnetic (Eddy-Current) Examination of Seamless and Welded Tubular Products, Austenitic
Stainless Steel and Similar Alloys

ASTM E 1417 Liquid Penetrant Testing

3. TECHNICAL REQUIREMENTS

3.1 Composition

Shall conform to the percentages by weight shown in Table 1, determined by wet chemical methods in accordance with
ASTM E 353, by spectrochemical methods, or by other analytical methods acceptable to purchaser.

TABLE 1 - Composition
Element min max
Carbon 0.08 0.12
Manganese 0.50 1.25
Silicon -- 0.50
Phosphorus -- 0.040
Sulfur -- 0.030
Chromium 16.00 17.00
Nickel 4.00 5.00
Molybdenum 2.50 3.25
Nitrogen 0.07 0.13

3.1.1 Check Analysis

Composition variations shall meet the applicable requirements of AMS2248.

3.2 Condition

Cold drawn, annealed, and descaled.

3.3 Fabrication

Tubing shall be produced by a seamless process. Any surface finishing operation applied to remove objectionable pits
and surface blemishes shall be performed prior to final anneal. A light polish to improve external surface appearance may
be employed after solution heat treatment and, if performed, the product shall be subsequently passivated.
SAE AMS5554F Page 3 of 5

3.4 Heat Treatment

Tubing shall be annealed by heating to 1850 to 1975 °F (1010 to 1079 °C), holding at the selected temperature within
±25 °F (±14 °C) for a time commensurate with cross-sectional wall thickness, and cooling as rapidly as possible to room
temperature.

3.5 Properties

Tubing shall conform to the following requirements:

3.5.1 As Received

3.5.1.1 Flarability

Specimens as in 4.3.1 from tubing 0.500 to 2.000 inches (12.70 to 50.80 mm), inclusive, in nominal OD shall withstand,
without formation of cracks or other visible defects, flaring at room temperature by being forced axially with steady
pressure over a hardened and polished tapered steel pin having a 74-degree included angle to produce a flare having a
permanent expanded OD not less than 1.20 times the original nominal OD.

3.5.1.1.1 Flarability requirements for tubing under 0.500 inch (12.70 mm) or over 2.000 inches (50.80 mm) in nominal
OD shall be as agreed upon by purchaser and vendor.

3.5.2 Response to Heat Treatment

Tubing shall have the following properties after being austenite conditioned by heating to 1710 °F ± 25 (932 °C ± 14),
holding at heat for not less than 45 minutes per inch (25 mm) of nominal thickness, and cooling as rapidly as possible to
room temperature; cold treated by cooling to -100 °F (-73 °C), or lower, holding at this temperature for not less than
1 hour for wall thicknesses up to 0.010 inch (0.25 mm), inclusive, and not less than 3 hours for wall thicknesses over
0.010 inch (0.25 mm), and warming in air to room temperature; and tempered by heating as specified at 850 °F ± 25
(454 °C ± 14), holding at heat for not less than 3 hours, and cooling in air.

3.5.2.1 Tensile Properties

Shall be as shown in Table 2, determined in accordance with ASTM E 8/E 8M.

TABLE 2 - Minimum Tensile Properties (SCT 850 Condition)

Property Value
Tensile Strength 185 ksi (1276 M Pa)
Yield Strength at 0.2% Offset 150 ksi (1034 MPa)
Elongation in 2 inches (50.8 mm) 8%

3.6 Quality

Tubing, as received by purchaser, shall be uniform in quality and condition and shall have a finish conforming to the best
practice for high quality aircraft tubing. It shall be smooth and free from heavy scale or oxide, burrs, seams, tears,
grooves, laminations, slivers, pits, and other imperfections detrimental to usage of the tubing. Surface imperfections, such
as handling marks, straightening marks, light mandrel and die marks, shallow pits, and scale pattern, will not be
considered injurious if the imperfections are removable within the tolerances specified for wall thickness, but removal of
such imperfections is not required.

3.6.1 When specified by purchaser, tubing shall be subjected to fluorescent penetrant inspection in accordance with
ASTM E 1417, to ultrasonic inspection in accordance with AMS2634, to electromagnetic (Eddy-Current)
examination in accordance with ASTM E 426, or to any combination thereof. Standards for acceptance shall be
as established by purchaser.
SAE AMS5554F Page 4 of 5

3.7 Tolerances

Shall conform to all applicable requirements of AMS2243.

4. QUALITY ASSURANCE PROVISIONS

4.1 Responsibility for Inspection

The vendor of tubing shall supply all samples for vendor's tests and shall be responsible for the performance of all
required tests. Purchaser reserves the right to sample and to perform any confirmatory testing deemed necessary to
ensure that the tubing conforms to specified requirements.

4.2 Classification of Tests

4.2.1 Acceptance Tests

Composition (3.1), nondestructive inspection when specified (3.6.1), and tolerances (3.8) are acceptance tests and shall
be performed on each heat or lot as applicable.

4.2.2 Periodic Tests

Flarability (3.5.1.1) and tensile properties (3.5.2.1) are periodic tests and shall be performed at a frequency selected by
the vendor unless frequency of testing is specified by purchaser.

4.3 Sampling and Testing

Shall be in accordance with AMS2371 and the following:

4.3.1 Specimens for flarability test (3.5.1.1) shall be full tubes or sections cut from a tube. The end of the specimen to
be flared shall be cut square, with the cut end smooth and free from burrs, but not rounded.

4.4 Reports

The vendor of the product shall furnish with each shipment a report showing the results of tests for composition of each
heat and for nondestructive inspection, when specified, and tolerances of each lot, and stating that the product conforms
to the other technical requirements. This report shall include the purchase order number, heat and lot numbers,
AMS5554F, size, and quantity.

4.5 Resampling and Retesting

Shall be in accordance with AMS2371.

5. PREPARATION FOR DELIVERY

5.1 Sizes

Except when exact lengths or multiples of exact lengths are ordered, straight tubing will be acceptable in mill lengths of
6 to 20 feet (1.8 to 6.1 m) but not more than 10% of any shipment shall be supplied in lengths shorter than 10 feet (3 m).

5.2 Identification

Shall be in accordance with AMS2807.

SAE AMS5554F Page 5 of 5

5.3 Packaging

Tubing shall be prepared for shipment in accordance with commercial practice and in compliance with applicable rules
and regulations pertaining to the handling, packaging, and transportation of the tubing to ensure carrier acceptance and
safe delivery.

6. ACKNOWLEDGMENT

A vendor shall mention this specification number and its revision letter in all quotations and when acknowledging
purchase orders.

7. REJECTIONS

Tubing not conforming to this specification, or to modifications authorized by purchaser, will be subject to rejection.

8. NOTES

8.1 A change bar (l) located in the left margin is for the convenience of the user in locating areas where technical
revisions, not editorial changes, have been made to the previous issue of this document. An (R) symbol to the left
of the document title indicates a complete revision of the document, including technical revisions. Change bars and
(R) are not used in original publications, nor in documents that contain editorial changes only.

8.2 Terms used in AMS are clarified in ARP1917.

8.3 Dimensions and properties in inch/pound units and the Fahrenheit temperatures are primary; dimensions and
properties in SI units and the Celsius temperatures are shown as the approximate equivalents of the primary units
and are presented only for information.

8.4 Purchase documents should specify not less than the following:

AMS5554F
Size of tubing desired
Quantity of tubing desired
Methods for nondestructive testing and standards for acceptance, if required (See 3.6.1).

PREPARED BY AMS COMMITTEE "F"