Classic Line: Planetary Mills
Classic Line: Planetary Mills
Classic Line: Planetary Mills
IDEAL FOR
GEOLOGY AND MINERALOGY
CERAMICS
CHEMISTRY
BIOLOGY
PHARMACEUTICALS
METALLURGY
MATERIAL TECHNOLOGY
SAMPLE PREPARATION
FOR ANALYSIS
classic line
fritsch classic line
A D VA N TA G E S T O Y O U O F T H E F R I T S C H
C L A S S I C L I N E AT A G L A N C E :
• Fast grinding to below 1 µm
• Up to 800 rpm
• Grinding bowls and balls in 8 different materials to suit all needs and
world wide patent for the first Laboratory Planetary Mill. In 1996 FRITSCH also
Since then FRITSCH Planetary Mills have become the standard in industry and
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pulverisette 6
W O R L D W I D E S TA N D A R D
Worldwide, FRITSCH Planetary Mills of the classic line are Planetary Ball Mills – high-performance all-rounders in routine
the laboratory standard for the widest range of applications. laboratory work
The name PULVERISETTE is synonymous with fast, loss- In Planetary Ball Mills, the comminution of the material to be
free fine grinding of samples, operator friendly, consistent ground takes place primarily through the high-energy impact of
reproducibility and long, reliable service life even under grinding balls. To achieve this, the grinding bowl, containing the
continuous, heavy duty usage. material to be ground and grinding balls, rotates around its own
axis on a main disk whilst rotating rapidly in the opposite direction.
All classic line Planetary Mills are characterised by At a certain speed, with this configuration, the centrifugal force
particularly easy, ergonomic operation, offer fast and easy causes the ground sample material and grinding balls to separate
cleaning and guarantee safe clamping of the bowls. from the inner wall of the grinding bowl. The grinding balls then
cross the bowl at high speed and further grind the sample
Depending on the fineness required, the grinding can be material by impact against the opposite bowl wall. In addition
performed dry, in suspension or in inert gas. In addition impact between the balls themselves on
to comminution, you can also use the Planetary Mills of the sample material adds to the size
the FRITSCH classic line for mixing and homogenising reduction process.
k
di s
ng
Select with confidence the right option for your special needs can be found at www.fritsch.de
ve m
Rotation of the
from the unique FRITSCH classic line -range of Planetary Ball
Mo
grinding bowl
Mills!
Working principle of Planetary Ball Mills
3
fritsch classic line
THE PROGRAMME
4
Free FRITSCH-sample grinding!
Send us your samples - we will advise you which mill is the right one for you.
Or take a look in the practical grinding report database by logging on
www.fritsch.de select menu item Sample Preparation / Solutions.
High performance
Ideal for the smallest quantities Unique a variable transmission ratio
in minimum space
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fritsch classic line
P U L V E R I S E T T E 5 classic line
T H E F R I T S C H P L A N E TA R Y M I L L
• Fast comminution of laboratory samples with up to 400 rpm
• 4 or 2 working stations
FA S T A N D F I N E
6
TECHNICAL DATA
Electrical details
100-120/200-240 V/1~, 50-60 Hz, 1300/1600 watt
Motor shaft power in accordance with
VDE 0530, EN 60034
1.5 kW
Weight with 4 working stations 2 working stations
Net 120 kg 100 kg
Gross 155 kg 135 kg
Dimensions w x d x h
Bench top instrument: 58 x 67 x 57 cm
Packing w x d x h
Pallet case: 100 x 72 x 83 cm
Emissions value of workplace according to IEC 61672-1
Up to approx. 83 dB(A)
(depending on the material to be ground, grinding bowls/balls, selected
rotational speed)
Order no. for 4 working stations 2 working stations
05.5000.00 05.6000.00
Fast and reliable: The practical Safe- Saves time: Simultaneous grinding of up to 8
Lock-System samples
APPLICATION EXAMPLES
Geology and mineralogy Rock, gravel, sand, minerals
Ceramics Porcelain, sintered ceramics, clay, fireclay
GTM
Chemistry Pesticides, fertilisers, salts,
inorganic and organic materials
compatible
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fritsch classic line
P U L V E R I S E T T E 6 classic line
T H E F R I T S C H P L A N E TA R Y M O N O M I L L
• Special grinding force due to a rotational speed of up to 650 rpm
• Low space requirements and ergonomic design
• Particularly easy-to-use
• Timer programming precise to ± one second
• Suitable for grinding hard to soft materials, dry or in suspension
• Perfect mixing and homogenising of emulsions
• Simultaneous processing of up to 2 samples
• Useful capacity up to 225 ml
• Bowl sizes 80 ml, 250 ml and 500 ml volume
HIGH PERFORMANCE IN
M I N I M U M S PA C E
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TECHNICAL DATA
Electrical details
100-120/200-240 V/1~, 50-60 Hz, 1100 watt
Motor shaft power in accordance with VDE 0530,
EN 60034
0.75 kW
Weight
Net 63 kg
Gross 83 kg
Dimensions w x d x h
Bench top instrument: 37 x 53 x 50 cm
Packaging w x d x h
Wooden case: 68 x 54 x 72 cm
Emissions value of workplace according to IEC 61672-1
Up to approx. 85 dB(A)
(depending on the material to be ground, grinding bowls/balls, selected
rotational speed)
Order no.
06.2000.00
APPLICATION EXAMPLES
Geology and mineralogy Rock, gravel, sand, minerals
Ceramics Porcelain, sintered ceramics, clay, fireclay
GTM
Chemistry Pesticides, fertilisers, salts,
inorganic and organic materials
compatible
INF
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1
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fritsch classic line
P U L V E R I S E T T E 7 classic line
T H E F R I T S C H P L A N E TA R Y M I C R O M I L L
• Rotational speed up to 800 rpm
• Fast fine grinding of small quantities
• Small footprint
• Programmable microprocessor control
• Up to 99 repetitions of the grinding cycle
• Suitable for grinding hard to soft materials, including in suspension
• Simultaneous processing of up to 2 samples
• Useful capacity up to 2 x 20 ml
•Grinding bowl sizes of 12 and 45 ml volume
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TECHNICAL DATA
Electrical details
100-120/200-240 V/1~, 50-60 Hz, 880 watt
Motor shaft power in accordance with VDE 0530,
EN 60034
0.37 kW
Weight
Net 35 kg
Gross 55 kg
Dimensions w x d x h
Bench top instrument: 37 x 53 x 50 cm
Packaging w x d x h
Wooden case: 68 x 54 x 72 cm
Emissions value of workplace according to IEC 61672-1
Up to approx. 82 dB(A)
(depending on the material to be ground, grinding bowls/balls, selected
rotational speed)
Order no.
07.4000.00
Unbeatably fast: Rotational speed up Impressive: Fast and fine grinding of smallest
to 800 rpm quantities
APPLICATION EXAMPLES
Geology and mineralogy Rock, gravel, sand, minerals
Ceramics Porcelain, sintered ceramics, clay, fireclay
Chemistry Pesticides, fertilisers, salts,
inorganic and organic materials
Biology Plants, leaves, freeze-dried samples
Pharmaceuticals Ophthalmological agents, gels, creams, extracts,
drugs, pastes, dragées, tablets
Metallurgy Ores, sinters
Material technology Pigments, precious materials, new materials,
alloys, mechanical alloying and activating
Analysis preparation Spectroscopy, X-ray fluorescence,
X-ray structure analysis, chromatography
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fritsch classic line
P U L V E R I S E T T E 4 classic line
T H E F R I T S C H VA R I O - P L A N E TA R Y M I L L
• Flexible configurable grinding conditions: impact and/or friction
U N I Q U E : W I T H VA R I A B L E
T R A N S M I S S I O N R AT I O
In contrast to conventional Planetary Mills, the rotational How the variable PULVERISETTE 4 classic line functions
speed of the grinding bowls and supporting disk can be
configured separately in the PULVERISETTE 4 classic line. You can directly influence the movement and paths of the grinding
Advantage to you: A single mill for mechanical activating balls by varying the transmission ratio between the grinding bowls
and alloying providing optimum grinding conditions suited and supporting disk: Depending on the setting, you can obtain high
to the respective material to be ground and the size of impact energy or high friction, according to your needs, or have
the grinding bowls and balls! For results that cannot be your PULVERISETTE 4 classic line operate as a Centrifugal Mill.
achieved with other Ball Mills. You are free to choose all intermediate levels and combinations
between friction-based and impact-based comminution. This
makes the mill uniquely versatile.
The mill is controlled by integral software, in which up to
9 programmes can be saved and then loaded quickly and
easily via the mill display.
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TECHNICAL DATA
Electrical details
400 V/3~, 50-60 Hz, 6000 watt
Motor shaft power in accordance with VDE 0530,
EN 60034
2.2 kW supporting disk
2.5 kW planetary disk
Weight
Net 320 kg
Gross 380 kg
Dimensions w x d x h
Floor instrument: 60 x 80 x 110 cm
Packaging w x d x h
Wooden case: 85 x 85 x 140 cm
Emissions value of workplace according to IEC 61672-1
Up to approx. 81 dB(A)
(depending on the material to be ground, grinding bowls/balls, selected
rotational speed)
Order no.
04.1030.00
APPLICATION EXAMPLES
Material technology Pigments, precious materials, new materials,
alloys, mechanical alloying and activating
Geology and mineralogy Rock, gravel, sand, minerals
Ceramics Porcelain, sintered ceramics, clay, fireclay
Chemistry Insecticides, fertilisers, salts,
inorganic and organic materials
Biology Plants, leaves, freeze-dried samples
Pharmaceuticals Ophthalmological agents, gels, creams, extracts,
drugs, pastes, dragées, tablets
GTM
compatible
Metallurgy
Analysis preparation
Ores, Sinters
Spectroscopy, X-ray fluorescence,
INF
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I O N PA G E
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fritsch classic line
GTM
compatible GTM - Gas Pressure and Temperature
Measuring System
• Adaptation of the measurement rate to the signal dynamic for maximum possible
battery life
This Gas Pressure and Temperature Measuring Through the continuous direct measurement of gas pressure
and temperature, it is possible to monitor thermal effects
System developed in cooperation with the as well as physical and chemical reactions or pressure
variations within the grinding bowl. To achieve this, the
Fraunhofer Institute for Applied Material Research grinding bowl is simply used with a radio transmitter located
in the lid, without any modification to the mill itself. The
(IFAM) in Dresden, is for use with the Planetary monitored data is passed by a receiver to a computer
running a special WINDOWSTM programme and allows for
Mills PULVERISETTE 4, PULVERISETTE 5 and graphical presentation of the measurement values and
collating them in an ExcelTM table.
PULVERISETTE 6 of the FRITSCH classic line
systems.
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TECHNICAL DATA
• System requirements: Standard WINDOWSTM-PC
• UHF radio transmitter, 10 mW, no approval or fees necessary
• Up to two transmitter components can be operated simultaneously in the mill
• Measurement rate for single and dual transmission operation of up to
approx. 200 measurement value/s
• Pressure measurement range 0 to 800 kPa (8 bar)
• Temperature measurement range of the transmitter component 10 to 70 °C
• Resolution of pressure signal: < 0.024 kPa
• Resolution of temperature signal: 0.025 K
• Permissible transient (-2 s) heat of reaction 30 kJ
• Receiver component also functions as charging station for the batteries of the transmitter component
• Range of pressure up to 15 m
• RS232 connection to PC
• 250 ml or 500 ml bowls made of stainless steel
Y O U R A D VA N TA G E S W I T H G T M
The GTM-System can be used wherever batch quantities are Extremely rapid phase formations can for the first time be
ground in a totally enclosed container. Special grinding bowls obser ved IN SITU as an adiabatic process without heat
made of stainless steel in capacities 250 ml and 500 ml are exchange from the system.
available.
Adjustment of the grinding parameters rotational speed, balls/
The GTM-System provides valuable information sample material ratio and grinding time can be performed first
- Investigations in the area of mechanical alloying for the time without expensive, time-consuming and abortive trials.
production of new amorphous and nano-crystalline materials
- Monitoring and optimisation of grinding processes in industrial Due to precise measurement of reaction times, for example,
applications new materials can be prepared through specific addition of
reaction partners, or produced with special mechano-chemical
Through measurement of the grinding bowl temperature, it is properties.
possible to make an integral statement on temperature as a
process variable that takes account of the effects of all friction,
impact and transformation processes. The continuous and highly
sensitive measurement of the gas pressure in the grinding bowl
allows the detection of very rapid reactions. The measured gas
pressure describes, amongst other things, the interactions of
the gas with the surfaces created during grinding (adsorption
and desorption of gases).
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fritsch classic line
To avoid the risk of contaminating the samples with abrasion from the grinding elements, we offer grinding bowls and grinding
balls in 8 different materials for the FRITSCH classic line. In normal cases, grinding bowls and balls of the same material
are used. To shorten the grinding time, balls with a higher density and correspondingly higher impact energy can be used,
e.g. tungsten carbide balls in a steel bowl or zirconium oxide balls in a silicon nitride bowl.
G assing lid
Through the use of a special lid on the grinding bowl, you can
also grind your samples in inert atmospheres. Two valves
allow for easy and safe filling of the bowls with inert gas while
they are firmly clamped in the mill. A special Additional Lock-
System is required for gas-tight removal and transportation
(see below).
ADDITIONAL LOCK-SYSTEM
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T E C H N I C A L D ATA
* At www.fritsch.de, you can find the corresponding element analyses with detailed information about the materials.
I. Grinding balls > 5 mm: Recommended number of balls per grinding bowl
II. Grinding balls > 3 mm: Recommended ball mass per grinding bowl in grams
The quantity of grinding balls may be reduced by up to 15%; but, increased abrasion will occur. The specified number/mass of balls per bowl is the minimum quantity; depending
on the material properties, it may need to be increased.
In normal cases, grinding bowls and balls of the same material are used. To shorten the grinding time, larger or heaver balls with higher density can be used, e.g.: Tungsten
carbide balls in a steel bowl or zirconium oxide balls in a silicon nitride bowl.
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fritsch classic line
O R D E R I N G D ATA
Order No. Article Order No. Article
PLANETARY MILLS classic line GRINDING BOWL WITH LID AND SEAL RING classic line
PLANETARY MILL pulverisette 5 Grinding bowl 500 ml volume
Instrument without grinding bowls and balls, incl. Safe-Lock for pulverisette 4, pulverisette 5 and pulverisette 6
clamping system 50.1050.00 Agate
• with 4 grinding bowl fasteners 50.1060.00 Sintered corundum (99.7% Al2O3)
05.5000.00 For 100-120/200-240 V/1~, 50-60 Hz, 1300/1600 watt* 50.1310.00 Silicon nitride, with steel casing
• with 2 grinding bowl fasteners 50.1110.00 Zirconium oxide
05.6000.00 For 100-120/200-240 V/1~, 50-60 Hz, 1300/1600 watt* 50.1100.00 Stainless steel
50.1090.00 Tempered steel
50.1010.20 Replacement seal ring PTFE 110/101 mm diameter for silicon nitride
grinding bowls
50.1230.20 Replacement seal ring PTFE 116/100 mm diameter for all other grin-
ding bowls
assing lid with 2 valves and seal ring for grinding bowls 500 ml
G
50.8000.00 Agate
50.9150.00 Silicon nitride
50.9100.00 Zirconium oxide
50.8200.00 Stainless steel
If further grinding bowls and transmitters are required, please ask! 50.8400.00 Tempered steel
50.1230.16 Replacement seal ring Viton for gassing lid
Gassing lid with 2 valves and seal ring for grinding bowls 250 ml
50.8100.00 Agate
50.8900.00 Silicon nitride
50.8950.00 Zirconium oxide
50.8300.00 Stainless steel
50.8500.00 Tempered steel
50.8600.00 Hardmetal tungsten carbide
50.2010.16 Replacement seal ring Viton for gassing lid for agate and silicon nitride
grinding bowls
50.2230.16 Replacement seal ring Viton for gassing lid for all other grinding bowls
Gassing lid with 2 valves and seal ring for grinding bowls 80 ml
50.8810.00 Agate
50.8840.00 Zirconium oxide
50.8800.00 Stainless steel
50.8700.00 Tempered steel
50.8880.00 Hardmetal tungsten carbide
50.4230.16 Replacement seal ring Viton for gassing lid
90.1400.00 Additional lock-system for all grinding bowls 500 ml, 250 ml, 80 ml
volume (for the transport of the closed grinding bowl with gassing lid)
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Test our
Order No. Article
GRINDING BALLS (PER PIECE)
Grinding balls 40 mm diameter
55.0400.06 Sintered corundum (99.7% Al2O3)
55.0400.31 Silicon nitride
instruments
in practice!
55.0400.27 Zirconium oxide
55.0400.10 Stainless steel
55.0400.09 Tempered steel
55.0400.08 Hardmetal tungsten carbide
+49 67 84 70 0
www.fritsch.de
Technical specifications are subject to change without notice. 19
Jaw Crushers and Disk Mills · classic line
IDEAL FOR
PRE-, FINE- AND ULTRA-FINE-GRINDING
OF HARD AND BRITTLE MATERIALS IN
THE AREAS
- GLASS AND CERAMICS INDUSTRY
- MINING AND METALLURGY
- GEOLOGY AND MINERALOGY classic line
- CHEMICAL INDUSTRY
- SOIL RESEARCH
JAW crUshErs
DisK Mills
fritsch Jaw
Backenbrecher
Crushers and
· Scheibenmühlen
Disk Mills · Scheibenschwingmühlen
FRITSCH . O N E ST E P A H E A D .
and innovation - for fast industrial applications as well as for
2
fA s t c O M M i N U t i O N O f h A r D A N D
B r i t t l E M At E r i A l s
3
fritsch Jaw Crushers
P U LV E R I S E T T E 1
classic line
t h E c O M PA c t P r E - c r U s h E r
• Very fast, uniform comminution
4
The funnel of the FRITSCH Jaw Crusher
PULVERISETTE 1 classic line is particularly
accessible, quickly and easily filled even with
larger sample quantities and easy to clean.
Its design enables the crushed material to
be automatically conveyed into the crushing
chamber – blockages are practically impos-
sible.
A practical plexiglas cover for optical inspec-
tion of optimum material flow.
Especially safe and dust-free: The enclosed grinding chamber prevents users
from reaching inside and ensures a safe and dust-free operation of all moving
parts. An integrated connection makes it very simple to combine the instru-
ment with a dust exhaust system for automatic removal of the fine dust arising
View of the grinding chamber with the during grinding. The dust exhaust system is also very useful when cleaning
housing removed the grinding parts.
5
fritsch Jaw Crushers
P U LV E R I S E T T E 1
classic line
OUr sUggEstiON
Double the service life of your crushing jaws – they can be easily
turned around on the FRITSCH Jaw Crusher PULVERISETTE 1 classic line.
select the right material combination! rohs (restriction of the use of certain hazardous substances)
For the comminution of RoHS samples – such as for the XRF
The crushing jaws and lateral support walls of the FRITSCH analysis – crushing jaws and support walls made of chromium-
Jaw Crusher PULVERISETTE 1 classic line are available in free steel are particularly well suited.
6 different materials in order to avoid undesired contami-
nation due to material abrasion. The standard version is iron-free pre-crushing
equipped with fixed and movable crushing jaws as well as For completely iron-free pre-crushing of medium-hard brittle
lateral support walls made of tempered steel. samples, for example in the ceramics industry, we can
Normally, crushing jaws and support walls of the same mate- equip your FRITSCH Jaw Crusher PULVERISETTE 1 classic
rial are used. Since the lateral support walls are subject to line with crushing jaws made of zirconium oxide, lateral
low stresses, however, the standard lateral support walls support walls in zirconium oxide or aluminium, and with a
made of tempered steel can often be retained. special PVC funnel. So you will have absolute protection
against iron contamination, such as for dental ceramics.
*
At www.fritsch.de, you can find the corresponding element analyses with
detailed information about the materials.
1)
Crushing jaws of zirconium oxide are only suitable for crushing ceramic
materials, minerals, etc. and never for hard-tough samples, such as metals.
6
tEchNicAl DAtA
Electrical details
irON-frEE griNDiNg Model I, 400 V/3~, 50-60 Hz, 1450 watt
Model I, 230 V/1~, 50-60 Hz, 1570 watt
For iron-free grinding, use the practical Model I, 115 V/1~, 50-60 Hz, 1900 watt
Model II, 400 V/3~, 50-60 Hz, 2780 watt
PVC funnel. Motor shaft power in accordance with VDE 0530, EN 60034
Model I, 1.1 kW
Model II, 2.2 kW
Weight
Model I, net 177 kg, gross 202 kg
Model II, net 205 kg, gross 230 kg
Dimensions w x d x h
Model I and model II, bench top instrument 40 x 80 x 80 cm
Packaging w x d x h
Model I and model II, wooden case 90 x 75 x 90 cm
Emissions value of workplace
according to DiN EN isO 3746:2005
Approx. 85 dB(A)
(depending on the material to be crushed)
Order no. 400 V/3~ 230 V/1~ 115 V/1~
Model I 01.5030.00 01.5020.00 01.5010.00
Model II 01.7030.00
Powerful: Coarse basalt rock crushed by the PULVERISETTE 1 classic line (model I)
at gap position 2 to the final fineness shown in the collecting vessel on the right.
APPlicAtiON EXAMPlEs
Mining and metallurgy Niobium-titanium, ferrovanadium, chrome vanadium,
tungsten carbide, ores, coal, slag, coke
chemistry Wide variety of various raw materials
geology and mineralogy Granite, basalt, barite, silicates and other rocks
glass industry Frits, glass, raw materials
ceramics industry Dental ceramics, steatite, fire-clay, sintered ceramics,
electrotechnical porcelain
rocks and soils Bauxite, clinker, quartz, concrete
final fineness 1 – 15 mm
feeding Batchwise/continuous
grinding parts Fixed and movable crushing jaws
Eccentric oscillations 308 movements/min
conformity CE mark
guarantee 2 years
7
fritsch Disk Mill
P U LV E R I S E T T E 13
classic line
• Simple operation
8
Especially accurate: The precision sliding
table of the FRITSCH Disk Mill PULVERI-
SETTE 13 classic line for precise gap
setting with an accuracy of 0.1 mm – for
rapid, precise operation and exactly repro-
ducible grinding results.
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fritsch Disk Mill
P U LV E R I S E T T E 13
classic line
OUr sUggEstiON
Lengthen the service life of the grinding disks in your
FRITSCH Disk Mill by simply changing the rotational direction
of the maintenance-free three-phase geared motor.
select the appropriate grinding disks high final fineness in minimum time
For every FRITSCH Disk Mill PULVERISETTE 13 classic line, With the FRITSCH PULVERISETTE 13 classic line, you can
you need at least one fixed and one movable grinding disk, achieve high final finenesses in a very short grinding time.
which are available in various materials. We have listed some examples here – always in refer-
Normally, two grinding disks of the same material are ence to 1 kg feed quantity and 20 mm particle size and
selected, which must always be harder than the sample arranged by material types from hard to medium-hard.
to be ground.
Material to grinding time gap setting fineness throughput
be ground (min) (mm) (µm) kg/h
MAtEriAl DAtA fOr fiXED AND MOVABlE griNDiNg DisKs 90 % < x 50 % < x
Material Main component Abrasion Use for material to Basalt 2.1 1.0 600 28
of the material* resistance be ground 3.5 0.1 220 60 17
Hardened cast steel Cr – Fe Good Hard, brittle samples Clinker 2.0 0.5 900 450 30
Manganese steel Mn – Fe Good Very hard, brittle 10.0 0.1 220 60 6
samples Slate 1.4 1.0 1500 45
Hardmetal tungsten WC Very good Very hard, abrasive 2.2 0.1 300 90 27
carbide samples Hard coal 3.5 1.0 800 17
Zirconium oxide1)
ZrO2 Good Medium-hard, brittle 13.5 0.1 250 100 4
samples, iron-free Limestone 2.0 1.0 1000 420 30
grinding 6.3 0.1 210 100 10
Thomas meal (potash) 1.3 1.0 1000 350 45
*
At www.fritsch.de, you can find the corresponding element analyses with 2.3 0.5 350 150 36
detailed information about the materials. Pumice stone 3.5 0.5 600 250 17
1)
Grinding disks of zirconium oxide are only suitable for grinding ceramic 5.0 0.1 150 30 12
materials, minerals, etc. and never for hard-tough samples, such as metals. Glass 2.5 3.0 4000 2240 25
3.3 2.0 2500 1600 18
3.8 1.0 1400 800 16
10
tEchNicAl DAtA
irON-frEE griNDiNg Electrical details
400 V/3~, 50-60 Hz, 1830 watt
For completely iron-free grinding of hard-brittle and medium-hard solid samples, Motor shaft power in accordance with VDE 0530, EN 60034
1.5 kW
for example for dental ceramics, we can equip your FRITSCH Disk Mill Weight
Net 140 kg
PULVERISETTE 13 classic line with a thorough polymer interior coating – Gross 170 kg
Dimensions w x d x h
together with grinding disks made of zirconium oxide – an absolutely Bench top instrument 44 x 87 x 40 cm
Packaging w x d x h
reliable protection against iron contamination. Wooden case 100 x 52 x 70 cm
Emissions value of workplace
according to DiN EN isO 3746:2005
Approx. 89 dB(A)
(depending on the material to be ground)
Order no.
13.1030.00
Filling of the funnel with pre-crushed glass Grinding result with a gap width of 1 mm
bottles
APPlicAtiON EXAMPlEs
Mining and metallurgy Ores, coal, coke, slags
ceramics industry Steatite, sintered ceramics, electrotechnical porcelain,
fire-proof clay, dental ceramics
rocks and soils Bauxite, slags, quartz, clinker, gypsum, chalk
glass industry Frits, different glass types, raw materials
soil research Dried soil samples, sewage sludge, hydrological sedi-
ments, drilling cores
P U LV E R I S E T T E 1 / 13
classic line
P O W E r f U l c O M B i N At i O N – P r E - A N D
for fast, continuous pre- and fine-grinding particularly of Pre- and fine-grinding, with
large quantities of coarse material, the combination of the quartzite stones as example
Select the appropriate grinding parts and the de- 2 Intermediate results of the
PUlVErisEttE 1
sired configuration from the options available for the
Final fineness down to 1 mm
PULVERISETTE 1 and 13 classic line on pages 6–7
and 10–11.
12
irON-frEE PrE- AND fiNE-griNDiNg
The FRITSCH-Combination is also available for completely iron-free
pre- and fine-grinding. Details can be found on page 6.
APPlicAtiON EXAMPlEs
Mining and metallurgy Ores, coal, coke, slags, niobium-titanium, ferrovanadium,
chrome vanadium, tungsten carbide
geology and mineralogy Granite, basalt, barite, silicates and other rocks
glass industry Frits, glass, raw materials
ceramics industry Steatite, fire-clay, sintered ceramics, electrotechnical
porcelain, dental ceramics
rocks and soils Bauxite, clinker, quartz, concrete, slags, gypsum, chalk
13
fritsch Vibrating Cup Mill
P U LV E R I S E T T E 9
classic line
s t r O N g E r , fA s t E r , B E t t E r
• More power with new drive concept
14
Especially ergonomic: The PULVERI-
SETTE 9 grinding sets, which have been
considerably reduced in weight, are placed
at an optimised working height on a
practical guide rail and then easily moved
to the final position.
Especially well-arranged: The Especially intelligent: A special Especially safe: Tensioned in seconds
self-explanator y, multilingual detector automatically detects with one hand and one grip, the com-
menu navigation on the LCD when you use an agate grinding pletely new rapid and anti-twist tension-
display for setting the grinding set for grinding and reduces the ing for the grinding set.
time precisely to the second, rotational speed independently.
the pause periods and the
rotational speed as well as the
programming and storage of
grinding cycles.
15
fritsch Vibrating Cup Mill
P U LV E R I S E T T E 9
classic line
O U R S U GG E STI O N
Grinding sets with high density, e.g. tempered steel
or tungsten carbide, reduce the grinding time.
Select the appropriate grinding set Optimises your grinding process: the FRITSCH-motor with
torque-optimised frequency converter
Grinding sets in 5 different materials and 3 different sizes
from 50 ml to 250 ml volume are available for the FRITSCH In the Vibrating Cup Mill, the grinding is per formed by
PULVERISETTE 9 – for each application the suitable one! horizontal circular oscillations of the grinding set on a vibrating
plate. The grinding set consisting of ring and puck comminute
the grinding sample with extremely high pressure, impact
Material data for the grinding sets
forces and friction. In this form of grinding, the transmission
Material Main component Density Abrasion Use for material to
of the material* g/cm3 resistance be ground of forces onto the grinding sample is much more important
Tempered steel Fe – Cr 7.9 Good Brittle,
hard samples than the pure motor power. For this reason, FRITSCH as the
Chromium-free steel Fe – Cr 7.8 Fairly good Brittle, first provider worldwide, developed for the PULVERISETTE 9
hard samples
Hardmetal tungsten WC 14.3 Very good Very hard, a special motor and now equipped it with an especially
carbide abrasive samples
Agate SiO2 2.65 Good Soft to medium- interference-resistant, torque-optimised frequency converter
hard, brittle, which fulfils all the relevant safety standards worldwide. It
fibrous samples
Zirconium oxide¹) ZrO2 5.9 Good Medium-hard, ensures that the motor output is precisely matched to the
brittle,
fibrous samples, grinding material and grinding set - which optimises the energy
iron-free grinding consumption.
*
t www.fritsch.de, you can find the corresponding element analyses with detailed
A
information about the materials.
1)
Grinding sets of zirconium oxide are only suitable for grinding ceramic materials,
minerals, etc. and never for hard-tough samples, such as metal.
16
tEchNicAl DAtA
Electrical Details
230-240 V/1~, 50-60 Hz, 1200 watt
100-120 V/1~, 50-60 Hz, 1200 watt
Motor shaft power in accordance with VDE 0530, EN 60034
1.1 kW
Weight
Net 267 kg
Gross 330 kg
Dimensions w x d x h
Floor instrument 77 x 76 x 116 cm
Packaging w x d x h
Pallet box 82 x 88 x 147 cm
Emissions value of workplace
according to DiN EN isO 3746:2005
Approx. 74 dB(A)
(depending on the material to be ground and grinding set)
Order no. 230-240 V/1~ 100-120 V/1~
09.5000.00 09.5001.00
Pressure elements automatically lift the grinding set, the anti-rotation lock tensions
them absolutely safe and the safety switch checks the firm position.
APPlicAtiON EXAMPlEs
Mining For processing coal, ores or minerals for physical or chemical
analysis
Metallurgy For grinding blast furnace slag or cast iron samples to
determine additives
ceramics industry For grinding rock samples to produce raw powder to determine
CaCO3- and MgO-content or clinkers to study the constancy of
the mineralogical structure
Agriculture and For preparing samples for chemical analysis of soils, sludges
How to go mobile with the Vibrating Cup Mill: On
environment or vegetable samples
request, we can supply the PULVERISETTE 9 on heavy
duty wheels with arresting brake. infrared and X-ray For preparing samples in a short grinding time without
fluorescence analysis contamination due to undesired abrasion.
PUlVErisEttE 1, model ii
the manually-operated hydraulic fritsch Pellet Instrument incl. fixed and movable crushing jaw and lateral support
walls made of tempered steel
Press is ideal for fast and easy preparation of both: 01.7030.00 For 400 V/3~, 50-60 Hz, 2780 watt
The PULVERISETTE 1 with voltage of „/3~“ can only be operated on a
solid and highly permeable pellets of solid samples three-phase supply network.
Other voltages on request.
for X-ray fluorescence analysis or infrared spectros-
Crushing jaws for model II
copy. 43.3010.09* Fixed crushing jaw made of tempered steel
43.3020.09* Movable crushing jaw made of tempered steel
43.3030.10 Fixed crushing jaw made of stainless steel
43.3040.10 Movable crushing jaw made of stainless steel
The pressure force is variable up to max. 250 kN and 43.3011.09 Fixed crushing jaw made of chromium-free steel
43.3021.09 Movable crushing jaw made of chromium-free steel
is automatically relieved in case of overstress. The 43.3130.23 Fixed crushing jaw made of manganese steel
43.3140.23 Movable crushing jaw made of manganese steel
pressing tool for pellets with 40 mm diameter is in- 43.3050.08 Fixed crushing jaw made of hardmetal tungsten carbide
43.3060.08 Movable crushing jaw made of hardmetal tungsten carbide
cluded in delivery, a 32 mm diameter pressing tool 43.3100.27 Fixed crushing jaw made of zirconium oxide 1)
43.3110.27 Movable crushing jaw made of zirconium oxide 1)
is optional.
Fixed and movable crushing jaws made of steel with grooved surface
on request.
It's as easy as this: Fill in the sample, close the mag- Lateral support walls for model II
43.3070.09* 1 pair made of tempered steel
netically-held door and build-up the desired pressure 43.3080.10 1 pair made of stainless steel
43.3071.09 1 pair made of chromium-free steel
using the hand lever - that's it. 43.3090.08 1 pair made of hardmetal tungsten carbide
43.3150.13 1 pair made of aluminium
43.3160.27 1 pair made of zirconium oxide 1)
If your pellets require binding agents for stabilisation, Accessories for iron-free pre-crushing for model II
01.7410.00 Funnel PVC incl. clamping strips
please contact us and we will be happy to assist. (Please note: fixed and movable crushing jaws made of zirconium oxide
and lateral support walls made of zirconium oxide or aluminium are
additionally necessary!)
* Included in the basic price of the instrument; when ordering a deviating specification from the
standard accessories, please specify the exact article number of the replacement part.
18
Order no. Article Order no. Article
AccEssOriEs fOr JAW crUshEr PUlVErisEttE 1, MODEl i + ii cOMBiNAtiON Of JAW crUshEr AND DisK Mill
PUlVErisEttE 1/13 classic line
Dust exhaust system
43.9050.00 Dust exhaust system, dust category "M"
according to DIN EN 60335-2-69
for 230 V/1~, 50-60 Hz, 1000 watt
43.9055.00 Paper filter bag for exhaust system (pack = 5 pieces) 2)
43.9052.00 Plastic bag for exhaust system (pack = 5 pieces) 2)
43.9051.00 Filter set polyester for exhaust system 2)
For continuous operation JAW crUshEr PUlVErisEttE 1 AND DisK Mill PUlVErisEttE 13
43.5100.00 Mounting rack for combined use of the Jaw Crusher PULVERISETTE 1 iN thE DEsirED cONfigUrAtiON
with the Disk Mill PULVERISETTE 13 To order a Combination for fast pre- and fine-grinding in a single step,
Select the desired configuration from the options offered for the order both instruments individually in the desired configuration plus the
PULVERISETTE 13 on pages 10-11. associated mounting rack that combines the instrument into a single
high-performance grinding instrument.
Select the desired configuration from the options offered for the
DisK Mill classic line PULVERISETTE 1 and 13 on pages 6-7 and 10-11.
43.5100.00 Mounting rack for combined use of the Jaw Crusher PULVERISETTE 1
PUlVErisEttE 13 with the Disk Mill PULVERISETTE 13
F R I T S C H PA R T I C L E S I Z I N G
For over 25 years, FRITSCH is also the right choice in the area of high-tech
particle technology: for particle size determination in the convergent laser
beam or by means of dynamic light scattering (DLS) as well as for analysis
of particle shape and size with dynamic image analysis. For exact, reliable
and reproducible results down to the lower nanometer range. Of course, in
the typical FRITSCH quality for easy, fast and reliable particle size analysis.
www.fritsch-sizing.com
2
CONTENTS
S E R V I C E A N D C O N S U L T A T I O N ......................... 4 – 5
FRITSCH helps you quickly and easily to find exactly the right laboratory
instrument for your application – including a free sample grinding. Benefit
from our decades of experience.
M I L L I N G ........................................................................... 6 – 23
FRITSCH-high per formance mills are the laborator y standard around
the world – as Planetary Mills, Ball Mills, Cutting Mills, Rotor Mills,
Beater Mills, Jaw Crushers, Disk Mills and Mortar Grinders for specific
applications.
S I E V I N G ......................................................................... 24 – 25
FRITSCH Sieve Shakers offer ease of use and guarantee precise,
reproducible sieve analysis.
D I V I D I N G ....................................................................... 26 – 27
FRITSCH instruments are second to none for dividing, feeding and ease
of cleaning adding to the performance of your mills, sieve shakers and
particle sizers. They are your guarantee for accurate reproducible sample
preparation.
www.fritsch.de
3
FRITSCH Service and Consultation
Yet another essential side of FRITSCH: Detailed consultation and comprehensive service –
practically anywhere in the world. To help you find exactly the right laboratory instruments
for your specific applications without long drawn out costly investigations – it’s our aim to
provide reliable solutions to questions about laboratory technology in our field of expertise.
TEST US – WE
F R E E S A M P L E G R I N D I N G A N D A N A LY S I S
Finding the right mill can be so easy: Simply send us a sample of your choice – we will perform a
free grinding or particle size analysis and send you a detailed grinding/size analysis report.
O N - S I T E T E S T I N T H E M O B I L E L A B O R AT O R Y
Test the FRITSCH instruments with your own samples – practically and simply in our fully
equipped laboratory bus. Simply schedule a date and we will drive by.
4
A R E P R E PA R E D !
T E C H N I C A L A P P L I C AT I O N C O N S U LT AT I O N
We will advise you on all technical application questions: via phone or personally. Or meet with
us at major national and international fairs and exhibitions.
WORLD-WIDE SERVICE
Wherever you are: FRITSCH is always nearby. With a global network of international
representative offices employing highly trained staff offering: application consultation, advice
on installation, maintenance and repair.
5
FRITSCH Milling
T H E RIGHT M IL L
F O R FIRST-RATE A N A LYSIS
E N S U R E T H E Q U A L I T Y O F Y O U R A N A LY S I S B Y C H O O S I N G
THE RIGHT MILL
The quality of every product or material analysis depends on For this reason, FRITSCH offers a wide selection of high-
the quality of the sample preparation. It is therefore extremely per formance mills in various product groups for ever y
important to consider all the individual milling parameters in application and every specific need: Planetary Mills premium
order to make an informed choice: material properties, feed line and classic line, Ball Mills, Cutting and Rotor Mills, Jaw
size and volume of the sample, grinding time and desired final Crushers, Disk Mills and Mortar Grinders.
particle size, any abrasion of the grinding parts – all these
factors are significant. And of course the costs.
T H E R I G H T M I L L F O R E V E R Y M AT E R I A L
For a simple orientation, you can find the recommended mills for the most common material categories in this brochure.
More detailed information offers the practical grinding report database at www.fritsch.de/solutions. There you will find
comparison grindings with detailed information.
O R S I M P LY G I V E U S A C A L L – O U R E X P E R T S W I L L B E H A P P Y T O A S S I S T Y O U .
6
M AT E R I A L TA B L E
Abrasives Ball Mills, Planetary Mills, P-9 Lime Ball Mills, Planetary Mills, P-2
Alloys Ball Mills, Planetary Mills, P-1 Materials research Planetary Mills, P-4, P-5
Analysis Ball Mills, Planetary Mills, P-14 Mechanical alloying/ Planetary Mills, P-4
Animal fodder Cutting Mills, P-0, P-23 activation
Biology Ball Mills, Planetary Mills, Cutting Mills Metallurgy Planetary Mills, P-1, P-9
Bones P-19, P-25, P-0 Minerals Ball Mills, Planetary Mills, P-1, P-13, P-9
Building materials Ball Mills, Planetary Mills, P-1, P-13, P-9 Mining Ball Mills, Planetary Mills, P-1, P-13, P-9
Catalysts Ball Mills, Planetary Mills, P-1 Ores Ball Mills, Planetary Mills, P-1, P-13, P-9
Cement clinker Ball Mills, Planetary Mills, P-1, P-13, P-9 Pharmaceuticals P-14, P-2
Ceramics Ball Mills, Planetary Mills, P-1, P-13, P-9 Pigments Ball Mills, Planetary Mills, P-2
Coal Ball Mills, Planetary Mills, P-16, P-1, P-13 Plants Cutting Mills, P-2, P-14
Coating powder Ball Mills, Planetary Mills, P-14 Plastics Cutting Mills, P-14
Compound materials Cutting Mills, P-25/P-19 Combination, P-14 Refractory Ball Mills, Planetary Mills, P-1, P-13, P-9
Drugs Ball Mills, Planetary Mills, Cutting Mills materials
Electronic scrap Cutting Mills, P-0, P-14 Rocks Ball Mills, Planetary Mills, P-1, P-13, P-2, P-9
Environment Cutting Mills, P-0, P-23 RoHS Cutting Mills, P-0, P-9, P-14
Feed (pellets) Cutting Mills, P-2, P-14 Rubber Cutting Mills, P-14
Fertilisers Ball Mills, Planetary Mills, P-14, P-2 Sediments Ball Mills, Planetary Mills, P-2, P-9
Fibres Ball Mills, Planetary Mills, P-1, P-13, P-9 Slags Planetary Mills, P-1, P-9
Foils Cutting Mills Soil research Ball Mills, Planetary Mills, P-1, P-13
Food Ball Mills, Planetary Mills, Cutting Mills, P-2 Spectroscopy Ball Mills, Planetary Mills, P-14
Glass Ball Mills, Planetary Mills, P-1, P-13, P-9 Spices Cutting Mills, P-14
Grains Cutting Mills, P-14 Tablets Ball Mills, Planetary Mills, P-2
Household waste Cutting Mills, P-25/P-19 Combination Textiles Cutting Mills
Leather Cutting Mills Wood Cutting Mills, P-14
M AT E R I A L T Y P E S – D E F I N I T I O N
Every FRITSCH mill is suitable for specific material types as shown in the product tables on the following pages. We
have also summarised the material types for the most common materials, as an additional service for you.
Glass, cement, calcite, coal, ash, sewage sludge, catalysts, soil, polluted land Medium-hard
samples, tablets, fertilisers, pellets
Grain, gypsum, salts, talc, animal feed, graphite, leaves, grass, pigments, Soft
spices, dragées, mica
Alloys, ceramics, salts, tablets, silicon carbide, silicon nitride, coke, coal, Brittle
embrittled, e.g. with liquid nitrogen: plastics, duroplast, rubber, perspex
7
FRITSCH premium line and classic line
The FRITSCH
premium principle
Making the best even better: With the FRITSCH premium principle we go one step
further – because even proven and well-tried laboratory mills can always be improved, especially
in detail. Therefore we listened intensively to our customers and continuously collected sugges-
tions for improvement from their daily practical work. This has resulted in the creation of new
instrument concepts that raise our own standards: the FRITSCH premium line is growing.
Due to increased performance all models of the FRITSCH premium line are more powerful than comparable
instruments. And more practice-orientated equipment elements make working with them even easier, more
comfortable, faster and safer. For premium results and absolute reliability. FRITSCH premium line – the
new high-tech standard for the modern laboratory.
Page 10 – 11 Page 20
8
FRITSCH classic line – international standard
Page 22 e e
Fi na l te st ph as Fi na l te st ph as
avai la bl e 20 14 avai la bl e 20 14
9
FRITSCH Milling
A Q U A N T U M L E A P I N T O T H E N A N O C L A S S – E X T R E M E LY H I G H - S P E E D M I L L I N G
W I T H S U N K E N B O W L S R O TAT I N G AT U P T O 1 1 0 0 R P M .
10
REVOLUTIONARY SELFLOCK-TECHNOL-
O G Y : P R O V I D E S A N E X T R E M E LY FA S T
BOWL CHANGE IN JUST TWO MOTIONS.
11
FRITSCH Milling
Planetary Mill
IDEAL FOR PULVERISETTE 5 classic line
GEOLOGY AND MINERALOGY
MATERIALS TECHNOLOGY Fast and fine
MECHANICAL ALLOYING/
ACTIVATION
SAMPLE PREPARATION
FOR ANALYSIS
CERAMICS
CHEMISTRY
4 working stationss 2 working stations
ons
BIOLOGY
PHARMACEUTICALS
METALLURGY
12
Free FRITSCH sample grinding!
Send us your sample – we will advise you which mill is the right one for
you. Or take a look in the practical grinding report database by logging
on www.fritsch.de/solutions.
Hard, medium-hard, soft, brittle, tough, moist Hard, medium-hard, brittle, moist Hard, medium-hard, soft, brittle, tough, moist
1 2 2
80, 250, 500 ml 12, 45 ml 12, 45, 80, 250, 500 ml
0.1 – 40 mm 0.1 – 15 mm 0.1 – 40 mm
10 mm 5 mm 10 mm
10 ml 0.5 ml 0.5 ml
225 ml 40 ml 450 ml
< 1 µm < 1 µm < 1 µm
4 min 3 min 4 min
Dry/wet Dry/wet Dry/wet
Yes Only possible in glove box Yes
Yes No Yes
100 – 650 rpm 100 – 800 rpm 0 – 400 rpm
63 kg 35 kg 320 kg
Bench top instrument: 37 x 53 x 50 cm Bench top instrument: 37 x 53 x 50 cm Floor instrument: 60 x 80 x 110 cm
13
FRITSCH Milling
To avoid the risk of contaminating the samples with abrasion To shorten the grinding time, grinding bowls and balls with
from grinding elements, we offer grinding bowls and grinding a higher density and correspondingly higher impact energy
balls in 8 different materials for the FRITSCH classic line can be used.
and premium line. In normal cases, grinding bowls and balls
of the same material are used.
ed.
T HE R I GH T M AT ER IA L
FOR EVERY
AP PLI C ATI O N
GASSING LID
Through the use of a special lid on the grinding bowl, you can
also grind your samples in inert atmospheres. Two valves
allow for easy and safe filling of the bowls with inert gas
while they are firmly clamped in the mill. A special additional
Lock-System is required for gas-tight removal and transport.
14
FRITSCH Ball Mills
FRITSCH Ball Mills are the most effective laboratory mills materials are available. FRITSCH ball mills are also the ideal
for rapid batchwise comminution of medium-hard to very lab assistants for mixing and homogenising.
hard samples down to the finest particle sizes. The grinding
can take place dry or wet. Grinding sets of many different
15
FRITSCH Milling
Cutting Mills are ideal for comminution of soft to medium- Various knife geometries and replaceable blades ensure
hard, fibrous or tough materials as well as plastics and for maximum flexibility and durability. Cutting tools of various
preparation of heterogeneous mixtures. The samples are steel types as well as of hardmetal tungsten carbide can be
comminuted by cutting and shearing forces, and the selected used for controlling the abrasion problems.
sieve insert determines the final fineness.
Cutting Mill
IDEAL FOR PULVERISETTE 15
PLASTICS AND TEXTILES
AGRICULTURE AND FORESTRY Effective and inexpensive
ENVIRONMENT
RoHS
ANALYTIC
CONSTRUCTION MATERIALS
CHEMISTRY
FOODSTUFFS
16
Unmatched ease of cleaning!
FRITSCH cutting mills allow the entire
grinding chamber to be opened without tools
in seconds with just two simple motions
for complete cleaning of all grinding parts.
Unbeatably fast, simple and efficient!
Easy cleaning due to simply Powerful pre-crushing Pre-crushing and fine comminution
exchangeable cutting tools even for larger samples in a single step
17
FRITSCH Milling
Due to their high grinding energy, Beater Mills are the best To avoid undesired abrasion, the FRITSCH Variable Speed
choice for soft to medium-hard and brittle samples – including Rotor Mill PULVERISETTE 14 classic line can be equipped
plastics. The material is comminuted through impact and with rotors made of stainless steel, titanium or with titanium
friction forces. The final fineness of the samples depends on nitride or tungsten carbide coatings.
the selected sieve insert.
18
Mor tar Grinder
The FRITSCH Mortar Grinder is an all-purpose mill suitable contamination, grinding sets are offered in seven different
for a wide range of materials: hard-brittle to soft-wet and materials.
the popular choice in the chemical/pharmaceutical area. Its
gentle grinding through pressure and friction makes it the
ideal mill for grinding tablets in galenics. To avoid the risk of
Mortar Grinder
IDEAL F0R PULVERISETTE 2
PHARMACY
FOODSTUFFS
Gentle grinding
without thermal effects
CHEMISTRY
GLASS AND CERAMICS INDUSTRY
AGRICULTURE AND FORESTRY
MINING AND METALLURGY
GEOLOGY AND MINERALOGY
19
FRITSCH Milling
The most powerful FRITSCH Jaw Crusher ever: up to 3 kW The combination of the PULVERISETTE 1 premium line e with
drive power ensure an exceptionally high throughput during the Disk Mill PULVERISETTE 13 premium line (p 22) – with
pre-crushing. The crushing jaws are completely retractable/ integrated sample divider – is ideal for automatic and con-
removable for easy cleaning. Integrated dust exhaust channels tinuous comminution of large quantities down to analytical
provide optimal working conditions. fineness – including coarse materials.
20
FRITSCH Jaw Crushers classic line
The Jaw Crusher PULVERISETTE 13 classic line e is the The combination with the FRITSCH Disk Mill PULVERI-
classic “workhorse” for the pre-crushing of brittle materials. SETTE 13 classic line e (see page 23) is ideal for automatic
FRITSCH offers grinding parts for these instruments made and continuous comminution of large quantities down to
of various steel types, tungsten carbide and zirconium oxide. analytical fineness – including coarse materials.
21
FRITSCH Milling
The FRITSCH Disk Mill PULVERISETTE 13 premium line tal gap display and presentation of all parameters on a
is the premium model for efficient fine grinding of hard- well-designed display.
brittle to medium-hard solids: Even more power ful and
safer due to automatic locking of the collecting vessel
and grinding chamber, even easier to operate due to digi-
Disk Mill
PULVERISETTE 13
IDEAL FOR
premium line
MINING AND METALLURGY
CERAMICS INDUSTRY
Comminution down to 100 μm –
absolutely reproducible with digital display
ROCKS AND SOILS
GLASS INDUSTRY
SOIL RESEARCH
22
FRITSCH Disk Mills classic line
The FRITSCH Disk Mill PULVERISETTE 13 classic line is Based on a new drive concept, the completely modified
most suited for size reduction within the medium particle FRITSCH Vibrating Cup Mill PULVERISETTE 9 offers an
size range. Comminution takes place through pressure and extra-fast grinding with up to 1500 rpm: extremely quiet and
shearing force. simple to operate, due to lighter grinding sets, convenient
one-hand lever tensioning and multilingual menu navigation.
Disk Mill
Vibrating Cup Mill
PULVERISETTE 13
IDEAL F0R PULVERISETTE 9
classic line
AGRICULTURE AND ENVIRONMENT
ORE AND GEOLOGY LABORATORIES
Ideal for comminution Fastest comminution
down to 100 μm thanks to powerful drive
SPECTROSCOPY PREPARATION
INFRARED AND X-RAY
FLUORESCENCE ANALYSIS
MINING AND METALLURGY
CERAMICS INDUSTRY
ROCKS AND SOILS
GLASS INDUSTRY
SOIL RESEARCH
Pellet P
Press
For fast an
and easy preparation of both: solid and highly permeable pellets for X-ray fluorescence
analysis or infrared spectroscopy – manual, hydraulic, easy.
• Variable p
pressure force of up to 250 kN
• Simple operation
o via hand lever
• Solid and compact with impact-resistant cladding
• Easy cleaning
clea
23
FRITSCH Sieving
With their innovative and practical features, the new These instruments offer maximum comfort and precision
generation of FRITSCH Sieve Shakers satisfy all requirements with automatic amplitude control, programme selection,
for accurate and reproducible sieving analysis and even control and evaluation software as well as high-quality sieve
exceed requirements in many areas. stack tensioning system.
Measuring range: 20 μm – 63 mm
Dry sieving Max. sample quantity (approx.): 2 kg
Sieving time (approx.): 3 – 20 min
Measuring range: 20 μm – 10 mm
Wet sieving Max. sample quantity (approx.): 20 – 100 g
Sieving time (approx.): 3 – 10 min
Max. number of sieves per sieve stack 10 (50 mm height) or 16 (25 mm height)
Max. height of sieve stack 550 mm
Automatic sieve analysis with evaluation software AUTOSIEVE Yes
Testing instrument calibration according to ISO 9001 Yes
Interfaces Yes
Intermittent mode Yes
Memory for 9 sieve programmes Yes
Weight 21 kg
Dimensions w x d x h Bench top instrument: 37 x 40 x 20 cm
24
The top model ANALYSETTE 3 PRO can be integrated into FRITSCH Sieve Shakers are available for sieves up to
any quality management system according to DIN EN ISO 450 mm in diameter for dry, wet and micro-precision sieving.
9001 as a testing instrument thanks to state-of-the-ar t The automatic sieving analysis is performed by the control
electronics and maximum reliability. and evaluation software AUTOSIEVE.
The best deal in size separation Ideal for large sample quantities
Sieving Sieving
Measuring range: 20 μm – 10 mm
Max. sample quantity (approx.): 20 – 100 g –
Sieving time (approx.): 3 – 10 min
– –
3 kg 42 kg
0.5 – 3 mm 0.1 – 2 mm
Manual Automatic
200 mm, 250 mm, 300 mm, 315 mm, 350 mm, 400 mm, 450 mm
100 mm, 200 mm or 8“
and 8“, 12“, 16“, 18“
10 (50 mm height) or 16 (25 mm height) 12 (65 mm height)
550 mm 845 mm
Yes Yes
No Yes
No Yes
No Yes
No Yes
230 V/1~, 50-60 Hz, 200 watt
100-240 V/1~, 50-60 Hz, 50 watt
115 V/1~, 50-60 Hz, 200 watt
21 kg 135 kg
Bench top instrument: 37 x 40 x 20 cm Floor instrument: 58 x 59 x 130 cm
25
FRITSCH Dividing Feeding Cleaning
The instruments of the FRITSCH LABORETTE line will make a representative sample. Its unique combination of three
your work more efficient and guarantee reproducible and dividing methods achieves previously unheard of dividing
representative sample preparation – the foundation for precision. Variable division ratios and the design in several
every precise analysis! The FRITSCH Rotary Cone Sample variants guarantee adaptation to a wide range of applications
Divider creates the optimal basis for reliable analysis of with a dividing accuracy of up to 99.9%.
26
The FRITSCH LABORETTE 24 is the ideal instrument for Both models of the FRITSCH LABORETTE 17 gently clean
efficient feeding of mills, sample dividers, mixers, sieve sensitive parts such as test sieves, micro-precision sieves,
shakers, balances and other laboratory instruments. filters, glassware and laboratory instruments and also help
in accelerating chemical reactions as well as dispersing
suspensions.
IDEAL FOR
- SIEVING
- MEASURING THE QUANTITATIVE
PARTICLE SIZE DISTRIBUTION OF
SOLIDS AND SUSPENSIONS
- SEPARATING
- FRACTIONING
SIEVE SHAKERS
FRITSCH Sieve Shakers
well-conceived instruments for every application, with FRITSCH concepts that make the work
simpler and faster – easy to operate, reliable and long-lasting. For dry, wet and micro-precision siev-
ing, with extensive accessories and the modified analysis software AUTOSIEVE. Typically FRITSCH!
2
ANALYSETTE 3 SPARTAN ANALYSETTE 3 PRO ANALYSETTE 18
Simple sieving for Precise sieving Effective sieving
all tasks with amplitude control of large quantities
Sieve diameter from 100 mm to 450 mm, mesh widths from 5 µm – 125 mm
3
FRITSCH Vibratory Sieve Shaker
A N A LY S E T T E 3 PRO
Precise sieving with
automatic amplitude control
The high performance Vibratory Sieve Shaker ANALYSETTE 3 PRO offers everything you need for fast
determination of quantitative particle size distribution in the laboratory. As a shaking sieve system
with an electromagnetic drive oscillates the sieve stack into regulated vertical oscillations, and is the
ideal solution for sieving sample quantities up to 2 kg and a measurement range from 5 µm to 63 mm.
The ANALYSETTE 3 PRO is perfectly suited for fast quality control of incoming and outgoing products,
offers user-friendly operation and is low-noise, robust and long-lasting.
1 2 3
FRITSCH Advantage The specially developed FRITSCH wet FRITSCH Advantage The unique, warp-free FRITSCH
sieving lid with 2 rotation nozzles for an uniform spraying of EASYTWIST sieve stack tensioner for tensioning the
the material to be sieved from above and by an additional sieve stack with high-quality, steel-reinforced plastic
interposed sieving ring above the sieve with the largest bands. Your benefit: Faster, simpler setup in just a
amount of finely sieved material. few steps, unobstructed work without annoying rods,
Your benefit: Improved sieving effect for faster results – and lower space requirements and more safety. Particularly
the most efficient wet sieving that has ever existed. beneficial: The tensioning system is already included in
the instru
instrument price.
4
S TA N D A R D S - C O M P L I A N T F O R I N T E G R AT I O N
INTO ISO 9001 QUALITY MANAGEMENT
5
FRITSCH Vibratory Sieve Shaker
A N A L Y S E T T E 3 SPARTAN
Simple sieving for all tasks
The little sister of the ANALYSETTE 3 PRO for all typical sieving tasks in the laboratory with optical
adjustment of the amplitude on the running instrument. Complete with the practical FRITSCH
sieve stack tensioning system EASYTWIST and the possibility of automatic evaluation of the sieve
analysis using the extensive FRITSCH evaluation software AUTOSIEVE.
ANALYSETTE 3 SPARTAN
6
TECHNICAL DATA
ANALYSETTE 3 PRO ANALYSETTE 3 SPARTAN
Method of analysis Sieving Sieving
Dry sieving
Measuring range 20 µm – 63 mm* 20 µm – 63 mm*
Max. sample quantity (approx.) for sieves < 63 mm: up to 2 kg* for sieves < 63 mm: up to 2 kg*
for sieves < 100 µm: up to 100 g* for sieves < 100 µm: up to 100 g*
Sieving time (approx.) 3 – 20 min* 3 – 20 min*
Wet sieving
Measuring range 20 µm – 10 mm 20 µm – 10 mm
Max. sample quantity (approx.) 20 – 100 g* 20 – 100 g*
Sieving time (approx.) 3 – 10 min* 3 – 10 min*
Micro-precision sieving
Measuring range 5 µm – 100 µm
Max. sample quantity (approx.) 0.05 – 0.5 g*
Sieving time (approx.) 30 – 60 min*
Max. weight of sieve stack 3 kg 3 kg
Amplitude 0.1 – 3 mm 0.5 – 3 mm
Amplitude control automatic manual
Sieve diameters 100 mm, 200 mm or 8“ 100 mm, 200 mm or 8“
Max. number of sieves per sieve stack 10 (50 mm height) 10 (50 mm height)
or 16 (25 mm height) or 16 (25 mm height)
Max. height of sieve stack 550 mm 550 mm
Automatic sieve analysis with
evaluation software AUTOSIEVE Yes Yes
Testing instrument calibration according
to ISO 9001 Yes No
Interface Yes No
Intermittent mode Yes No
Memory for 9 parameter combinations Yes No
Convertible to
Vibratory Micro Mill PULVERISETTE 0 Yes Yes
Electrical details 100-240 V/1~, 50-60 Hz, 50 watt 100-240 V/1~, 50-60 Hz, 50 watt
Weight
Net/gross 21 kg / 26 kg 21 kg / 26 kg
Dimensions w x d x h
Bench top instrument 37 x 40 x 20 cm 37 x 40 x 20 cm
Packing details w x d x h
Cardboard box 50 x 43 x 30 cm 50 x 43 x 30 cm
Emissions value of workplace according
to DIN EN ISO 3746:2005 (depending on
approx. 63 dB(A)
the material to be sieved and instrument configuration) approx. 63 dB(A)
Order no. 03.7020.00 03.8020.00
*Depending on the material to be sieved and the sieves used
7
FRITSCH Accessories
A C C E S S O R I E S A N A LY S E T T E 3
Sieves FRITSCH Micro-Precision Sieves Sieve clamping lid, sieve pans and
For dr y and wet sieving with mesh Available only from FRITSCH: With the interposed sieve pans for dry sieving
widths from 20 µm to 63 mm. All are micro-precision sieves, the ANALY- For observation of the sieving process,
especially light, robust and manu- SETTE 3 PRO is suitable for wet-sieving sieve clamping lids made of plexiglas
factured in high quality (no soldered of fine materials from 5 µm to 100 µm are available for FRITSCH test sieves
seam!). Highly alloyed stainless steel and for dry sieving of the smallest sam- of 100 mm or 200 mm/8“ diameter.
protects against corrosion and simpli- ple quantities from 0.05 – 0.5 g. The You also receive a clamping lid made
fies cleaning. Groove-free mesh tran- micro-precision sieves of pure nickel of polyamide (without window) to
sitions prevent contamination of the foil with a sieve diameter of 100 mm sieve materials for which metallic
sieving material. Available in accor- feature a large open sieving surface. contamination must be avoided. Of
dance with ISO 3310 -1 or ASTM E-11- Blockages are reliably prevented by the course, we also offer corresponding
1995 in the diameters 200 mm (height etched-in holes that widen toward the sieve pans and sieves made of plastic.
50 mm or 25 mm), 100 mm (height bottom. The matching clamping set, Sieve pans and interposed sieve pans
40 mm) or 8“ (height 2“). Every sieve is sieve clamping lid, sieve pan, sieve for multiple sieving operations in a
laser-engraved, optically measured and spacer and fast locking clamp along single process are available in stainless
delivered with a compliance certificate. with the large sieve sur face permit steel for all sieve sizes.
efficient sieving.
8
C E R T I F I C AT E S
For certification of the ANALYSETTE 3 PRO as an inspection instrument, a 3.1 EN 10204 inspection certificate
as well as a form for IQ/OQ documentation are available. A 3.1 EN 10204 inspection certificate is also
offered for FRITSCH test sieves in accordance with ISO 3310-1.
Of course, we would also be happy to recertify your Vibratory Sieve Shaker ANALYSETTE 3 PRO and FRITSCH
test sieves according to ISO 3310-1 at our headquarters in Idar-Oberstein or directly at your location.
IQ/OQ documentation is also available for the ANALYSETTE 3 SPARTAN.
Sieve clamping lid, interposed sieve Universal sieve tensioning system Sieving aids
rings and sieve pans for wet sieving TorqueMaster For dry sieving of materials with a high
Only available from FRITSCH: During For precise results: The electrically share of fine particles, 10 mm agate
wet sieving with test sieves (200 mm/ tensioned and easy-to-operate FRITSCH balls or 20 mm rubber balls should be
8“), the practical clamping lid with TorqueMaster applies constant and used as sieving aids for medium and
2 rotation nozzles ensures an uniform reproducible tensioning forces to the large sieves and 5 mm agate balls
spraying of the sieving material and an sieve stack through precisely controlled for fine sieves. Your advantage: They
optimal sieving effect. Special inter- fastening of the sieve clamping lid. prevent clogging of the sieve mesh.
posed sieving rings with three nozzles Essential when using the ANALYSETTE
are available for simultaneous spraying 3 PRO as inspection instrument
of the top and bottom sieves. A sieve according to ISO 9001.
clamping lid of plexiglas with 1 nozzle
is also offered for wet sieving with
100 mm test sieves. The corresponding
sieve pans with outlet are available for
all sieve sizes.
9
FRITSCH Heavy Duty Analytical Sieve Shaker
A N A LY S E T T E 18
Effective sieving of large quantities
The ANALYSETTE 18 is the robust, Heavy Duty Analytical Sieve Shaker from FRITSCH. It can
effortlessly sieve up to 15 kg of material between 20 µm and 125 mm. The three-dimensional
sieving motion ensures particularly fast sieving results without manual re-sieving, and also optimal
reproducibility.
ww
FRITSCH Ad
Advantage Universal suppor t
plate for sieves
sieve with diameters of 200, 250,
300, 315, 350
350, 400 and 450 mm as well as
8, 12, 16 or 18
18“. Sieves with mesh width from
20 µm to 125 mm in accordance with ISO
3310-1 and ASTM
A E-11-1995 are available.
10
TECHNICAL DATA
ANALYSETTE 18 ANALYSETTE 18
Method of analysis Sieving Electrical details 230 V/1~, 50-60 Hz, 200 watt
Dry sieving 115 V/1~, 50-60 Hz, 200 watt
Measuring range 20 µm – 125 mm* Weight
Max. sample quantity (approx.) 15 kg* Net/gross 135 kg / 157 kg
Sieving time (approx.) 5 – 60 min* Dimensions w x d x h
Max. weight of sieve stack 42 kg Floor instrument 58 x 59 x 130 cm
Amplitude 0.1 – 2 mm Packing details w x d x h
Amplitude control Automatic Wooden case 84 x 79 x 55 cm
Sieve diameters 200 mm, 250 mm, 300 mm, 315 mm, 350 mm, Emissions value of workplace
400 mm, 450 mm and 8“, 12“, 16“, 18“ according to DIN EN ISO 3746:2005
Max. number of sieves per sieve stack 12 (65 mm height) (depending on the material to be sieved
Max. height of sieve stack 845 mm and instrument configuration) approx. 73 dB(A)
Automatic sieve analysis Order no. 230 V/1~, 50 – 60 Hz 115 V/1~, 50 – 60 Hz
with evaluation software AUTOSIEVE Yes 18.3020.00 18.3010.00
Testing instrument calibration according
to ISO 9001 Yes
Interface Yes
Intermittent mode Yes
Memory for 10 parameter combinations Yes
* Depending on the material to be sieved and the sieves used
closed opened
11
FRITSCH ANALYSETTE 3
O R D E R I N G D ATA
Order no. Article Order no. Article
VIBRATORY SIEVE SHAKER SPECIAL ACCESSORIES
ANALYSETTE 3 PRO + SPARTAN ANALYSETTE 3 PRO + SPARTAN
Instrument without clamping lid, test sieves and sieve pan Accessories for gentle cleaning of test sieves and micro-precision sieves
03.7020.00 Model PRO, for 100-240 V/1~, 50-60 Hz For gentle cleaning of the test sieves and micro-precision sieves, we recommend
03.8020.00 Model SPARTAN, for 100-240 V/1~, 50-60 Hz the FRITSCH Ultrasonic Cleaners LABORETTE 17.
More information can be found at www.fritsch.de.
Accessories for dry sieving
31.2020.00 Clamping lid plexiglas for test sieves 200 mm/8“ dia. Recertification of the Vibratory Sieve Shaker ANALYSETTE 3 PRO and
31.2050.00 Clamping lid polyamide (without window) for all test sieves FRITSCH test sieves according to ISO 3310-1 on request.
up to 200 mm/8“ dia.
31.2100.00 Sieve tensioning system TorqueMaster (consisting of clamping lid plexiglas Computer, colour ink jet printer and laser printer on request.
for test sieves 200 mm/8“ dia. and electrical tool 100-240 V/1~, 50-60 Hz)
31.2010.00 Clamping lid plexiglas for test sieves 100 mm dia.
31.1300.03 Interposed sieve pan made of stainless steel 200 mm dia., 50 mm height
31.1320.03 Interposed sieve pan made of stainless steel 8“ dia., 2“ height
31.1000.03 Sieve pan made of stainless steel 200 mm dia., 50 mm height
31.1020.03 Sieve pan made of stainless steel 8“ dia., 2“ height
31.1040.03 Sieve pan made of stainless steel 100 mm dia., 40 mm height
Certification
96.0010.00 Inspection certificate 3.1 EN 10204 for FRITSCH Sieve Shaker
ANALYSETTE 3 PRO
96.0200.00 IQ/OQ documentation (questionnaire format - for filling out by customer)
for FRITSCH Sieve Shaker ANALYSETTE 3 PRO
96.0100.00 IQ/OQ documentation (questionnaire format - for filling out by customer)
for FRITSCH Sieve Shaker ANALYSETTE 3 SPARTAN
31.0900.00 Inspection certificate 3.1 EN 10204 for FRITSCH test sieves
according to ISO 3310-1
Sieving aids
55.0050.05 Agate ball 5 mm dia. (15 pcs. per sieve)
55.0100.05 Agate ball 10 mm dia. (10 pcs. per sieve)
31.0180.15 Rubber ball 20 mm dia. (5 pcs. per sieve)
Sieve covers
31.1200.03 Sieve cover made of stainless steel for test sieves 200 mm dia.
31.1220.03 Sieve cover made of stainless steel for test sieves 8“ dia.
31.1240.03 Sieve cover made of stainless steel for test sieves 100 mm dia.
Sieve pans made of stainless steel with and without outlet are also
available in 200 mm dia., 25 mm height and 8“ dia., 1“ height.
12
O R D E R I N G D ATA
Order no. Article
Ordering example for test sieves in other diameters
TEST SIEVES 200 mm dia., 50 mm height,
200 mm dia., 25 mm height,
ANALYSETTE 3 PRO + SPARTAN 8“ dia., 2“ height,
Frame and mesh wire made of stainless steel 100 mm dia., 40 mm height
with compliance certificate
100 mm/200 mm/8“ dia. Deviation ISO 3310-1 ASTM
from standard mesh width E-11-1995
sieve size mm/µm mesh
If you would like a test sieve in other diameters, please take note of the ordering
examples to the right.
13
FRITSCH ANALYSETTE 18
Instrument without test sieves and sieve pan, incl. tensioning and
sieve cover
18.3020.00 for 230 V/1~, 50-60 Hz
Order no. Mesh width ASTM • E-11-1995
18.3010.00 for 115 V/1~, 50-60 Hz
ISO 3310-1 mm/µm mesh
Accessories for test sieves 400 mm dia.
34.0040.02 125• mm
37.1000.01 Sieve pan made of stainless steel 400 mm dia.
34.0050.02 100 mm
37.1100.01 Interposed sieve pan made of stainless steel 400 mm dia.
34.0060.02 90• mm
37.0010.16 Replacement seal ring NBR for test sieves 400 mm dia.
34.0000.02 63• mm
34.0080.02 45• mm
Accessories for automatic evaluation of sieve analysis
34.0100.02 31.5• mm
03.2900.00 Software AUTOSIEVE for Windows
34.0200.02 25 mm 1“ = 25 mm
for control and automatic evaluation of sieve analysis
34.0300.02 22.4• mm 7/8“ = 22.4 mm
34.0400.02 20 mm
Sieving aids
34.0600.02 18 mm ~ 3/4“ = 19 mm
37.0200.16 1 vulkollan cube (minimum 20 cubes per sieve)
34.0800.02 16• mm 5/8“ = 16 mm
Laboratory analysis balance, computer, colour ink jet printer and laser 34.0900.02 14 mm ~ 0.53“ = 13.2 mm
printer on request. 34.1000.02 12.5 mm ~ 1/2“ = 12.5 mm
34.1100.02 11.2• mm 7/16“ = 11.2 mm
34.1200.02 10 mm ~ 3/8“ = 9.5 mm
34.1300.02 9 mm
34.1400.02 8• mm 5/16“ = 8 mm
34.1500.02 7.1 mm ~ 0.265“ = 6.7 mm
34.1600.02 6.3 mm 1/4“ = 6.3 mm
34.1700.02 5.6• mm ~ no. 31/2 = 5.6 mm
34.1800.02 5 mm ~ no. 4 = 4.75 mm
34.2000.02 4• mm no. 5 = 4 mm
34.2100.02 3.55 mm no. 6 = 3.35 mm
34.2200.02 3.15 mm
34.2300.02 2.8• mm no. 7 = 2.8 mm
34.2400.02 2.5 mm ~ no. 8 = 2.36 mm
34.2600.02 2• mm no. 10 = 2 mm
34.2700.02 1.8 mm
34.2800.02 1.6 mm ~ no. 12 = 1.7 mm
34.2900.02 1.4• mm no. 14 = 1.4 mm
34.3000.02 1.25 mm ~ no. 16 = 1.18 mm
34.3100.02 1.12 mm
34.3200.02 1• mm no. 18 = 1 mm
34.3300.02 900 µm
34.3400.02 800 µm ~ no. 20 = 0.85 mm
34.3500.02 710• µm no. 25 = 0.71 mm
34.3600.02 630 µm ~ no. 30 = 0.6 mm
34.3700.02 560 µm
34.3800.02 500• µm no. 35 = 0.5 mm
34.3900.02 450 µm
34.4000.02 400 µm ~ no. 40 = 0.425 mm
34.4100.02 355• µm no. 45 = 0.355 mm
34.4200.02 315 µm ~ no. 50 = 0.3 mm
34.4300.02 280 µm
34.4400.02 250• µm no. 60 = 0.25 mm
34.4500.02 224 µm
34.4600.02 200 µm ~ no. 70 = 0.212 mm
34.4700.02 180• µm no. 80 = 0.18 mm
34.4800.02 160 µm ~ no. 100 = 0.15 mm
34.4900.02 140 µm
34.5000.02 125• µm no. 120 = 0.125 mm
34.5100.02 112 µm
34.5200.02 100 µm ~ no. 140 = 0.106 mm
34.5400.02 90• µm no. 170 = 0.09 mm
34.5600.02 80 µm
34.5800.02 71 µm ~ no. 200 = 0.075 mm
34.6000.02 63• µm no. 230 = 0.063 mm
When ordering test sieves, please quote if the sieves should be delivered according to
ISO 3310-1 or ASTM.
Test sieves and sieving accessories in other diameters and mesh widths on request.
All above mentioned mesh widths are also available as test sieves with 200 mm/8“ dia.