DATA SET #1

RUN # 1 RUN # 2
Agitator & baffle Agitator only

Time/s Λ1 /S Time/s Λ1 /S
0 0.0073 0 0.00691
60 0.007 60 0.00662
120 0.0065 120 0.00643
180 0.0064 180 0.00631
240 0.0063 240 0.00623
300 0.0063 300 0.00617
360 0.0062 360 0.00613
420 0.0062 420 0.0061
480 0.0062 480 0.00609
540 0.0061 540 0.00607
600 0.0061 600 0.00606
660 0.0061 660 0.00605
720 0.0061 720 0.00604
780 0.0061 780 0.00604
840 0.0061 840 0.00603
900 0.0061 900 0.00604

Measured Parameters Measured Parameters

[NaOH] 0.100 M [NaOH] 0.100 M

Ethyl acetate 0.100 M Ethyl acetate 0.100 M

NaOH flow rate 40 cm3/min NaOH flow rate 40 cm3/min
Ethyl acetate flow Ethyl acetate
rate 40 cm3/min flow rate 40 cm3/min
Reactor Volume 1 dm3 Reactor Volume 1 dm3
Temperature 26 °C Temperature 26 °C
 RUN # 3
Agitator only

Time/s Λ1 /S
0 0.00613
60 0.00667
120 0.00775
180 0.00752
240 0.0076
300 0.00838
360 0.00869
420 0.00857
480 0.00874
540 0.00963
600 0.00952
660 0.00958

Measured Parameters
[NaOH] 0.100 M

Ethyl acetate 0.100 M

NaOH flow rate 40 cm3/min
Ethyl acetate
flow rate 40 cm3/min
Reactor Volume 1 dm3
Temperature 26 °C
 Data Set #2
RUN # 1 RUN # 2
Agitator & Baffle Agitator only

Conductiv Conductiv
0
Temp/ C Time/sec ity/S *10-3 0
Temp/ C Time/sec ity/S *10-3
(Λo) (Λo)

0 18.84 32.4 0 16.67

34.4 60 8.67 32.3 60 8.66
34.7 120 8.45 32.2 120 8.38
34.6 180 8.22 32.1 180 8.18
34.5 240 8.07 32 240 8.05
34.4 300 7.96 31.9 300 7.96
34.2 360 7.89 31.8 360 7.89
34.1 420 7.84 31.8 420 7.85
34 480 7.81 31.7 480 7.82
34 540 7.8 31.7 540 7.79
33.8 600 7.81 31.6 600 7.78
33.7 660 7.81 31.5 660 7.77
33.7 720 7.81 31.5 720 7.77
31.4 780 7.76
31.3 840 7.76
31.2 900 7.77
31.2 960 7.77
31.1 1020 7.77

Measured Parameters Measured Parameters

[NaOH] 0.100 M [NaOH] 0.100 M
Ethyl aceta0.100 M Ethyl aceta0.100 M
NaOH flow40 cm3/min NaOH flow40 cm3/min

Ethyl Ethyl
acetate acetate
flow rate 40 cm3/min flow rate 40 cm3/min
Reactor V 1 dm3 Reactor V 1 dm3
 RUN # 3
No Agitator, no baffle

Conductiv
0
Temp/ C Time/sec ity/S *10-3
(Λo)

30.4 0 16.63
30.4 60 17
30.3 120 17.08
30.3 180 17.1
30.3 240 17.48
30.3 300 17.44
30.2 360 17.56
30.2 420 17.8
30.1 480 17.66
30.1 540 17.77
30 600 18.37

Measured Parameters
[NaOH] 0.100 M
Ethyl aceta0.100 M
NaOH flow40 cm3/min

Ethyl
acetate
flow rate 40 cm3/min
Reactor V 1 dm3
0.61 0.967742 -0.01424 -0.21467
0.64 2.117149 0.325751 -0.19382
0.75 2.811621 0.448957 -0.124939
0.84 3.926702 0.594028 -0.075721
0.91 3.952569 0.596879 -0.040959
Chart Title
0
-0.1 0 0.1 0.2 0.3 0.4

-0.05

Pressure Drop vs Boil-up Rate

-0.1

0.685
log dP cm/ H2O

-0.15
0.585
-0.2
0.485

0.385
-0.25
0.285

0.185

0.085

-0.015
-0.18 -0.13 -0.08 -0.03
log Boil-up rate ltr/hr
 Chart Title
0.2 0.3 0.4 0.5 0.6 0.7

0.685

0.585

0.485

0.385

0.285

0.185

0.085

-0.015
-0.03
100 19.7
75 19.15
50 19.05
25 15.6
0 0

Ethanol/Water Calibration Curve

25

19.05 19.15
20
15.6
Refractive Index

15

10

0
0
0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75

Mol% Ethanol
 Calibration Curve

19.05 19.15 19.7

5 50 55 60 65 70 75 80 85 90 95 100 105

Mol% Ethanol
 Data Set #3
RUN # 1 RUN # 2
Agitator & Baffle Agitator, no baffle

Conductiv Conductiv
Temp/0C Time/sec ity/mS Temp/0C Time/sec ity/mS
(Λo) (Λo)

30.5 0 13.79 30,3 0 13.66

30.5 10 7.09 30.3 10 6.80
30.5 20 6.82 30.3 20 6.79
30.4 30 6.73 30.3 30 6.71
30.4 40 6.63 30.2 40 6.62
30.3 50 6.56 30.2 50 6.56
30.3 60 6.50 30.2 60 6.50
30.3 70 6.42 30.1 70 6.44
30.2 100 6.21 30.1 100 6.26
30.1 120 6.11 30.0 120 6.17
30.1 150 5.95 30.0 150 6.02
30.0 180 5.82 30.0 180 5.91
30.0 210 5.67 30.0 210 5.79
30.0 240 5.60 30.0 240 5.70
30.0 270 5.52 30.0 270 5.61
30.0 300 5.44 30.0 300 5.53
30.0 330 5.35 30.0 330 5.46
30.0 360 5.30 30.0 360 5.39

30.0 390 5.24 30.0 390 5.34

30.0 420 5.20 30.0 420 5.28

30.0 450 5.14 30.0 450 5.23
30.0 480 5.10 30.0 480 5.18
30.0 510 5.06 30.0 510 5.14
30.0 540 5.02 30.0 540 5.11
30.0 570 4.99 30.0 570 5.06
30.0 600 4.96 30.0 600 5.02
30.0 630 4.93 30.0 630 5.00
30.0 660 4.91 30.0 660 4.96
30.0 690 4.88 30.0 690 4.93
30.0 720 4.85 30.0 720 4.90
30.0 750 4.83 30.0 750 4.88
30.0 780 4.82 30.0 780 4.86
30.0 810 4.80 30.0 810 4.83
30.0 840 4.78 30.1 840 4.81
30.0 870 4.76 30.1 870 4.79
30.0 900 4.75 30.1 900 4.77
30.0 930 4.71 30.1 930 4.76
30.0 960 4.70 30.1 960 4.73
30.0 990 4.69 30.1 990 4.72
30.0 1020 4.67 30.1 1020 4.70
30.0 1050 4.66 30.1 1050 4.68
30.0 1080 4.64 30.1 1080 4.65
30.0 1110 4.63 30.1 1110 4.65
30.0 1140 4.62
30.0 1170 4.61
30.0 1200 4.59
30.0 1230 4.59
30.0 1260 4.58
 RUN # 3
No agitator, no baffle

Conductiv
Temp/0C Time/sec ity/mS
(Λo)

30,3 0 14.82
30.3 30 14.75
30.3 60 14.76
30.3 90 14.63
30.3 120 14.52
30.3 150 14.65
30.4 180 14.40
30.4 210 14.30
30.4 240 14.47
30.4 270 14.51
30.4 300 14.37

Measured Parameters
[NaOH] 0.100 M
Ethyl acetate 0.100 M
NaOH flow rate 40 cm3/min

Ethyl acetate flow

rate 40 cm3/min
Reactor Volume 1 dm3

These conditions were maintained

for all three runs.