3M Converting To Novec Cleaning
3M Converting To Novec Cleaning
3M Converting To Novec Cleaning
TM
Prior to converting your process to 3M Novec Engineered Fluids, 3M recommends you complete this
TM
3
Equipment Evaluation Survey and return it to your 3M representative or 3M authorized distributor.
In response, 3M will evaluate your process and provide you with recommendations on how to modify
existing equipment for effective and efficient operation with Novec fluids.
Novec ™
Dimensions of Opening
Gallons Per Hour Rating Guidelines for converting a cleaning process to
Length Width Heat:
3M Novec
™ ™
Cover: Type Elec. Volt Phase
Power Manual Steam PSIG
Hoist Type Other
Freeboard Chiller
Condensing
Temp. °F
Condensing
Refrigeration Temp. °F
Engineered
Fluids
Refrigeration Temp. °F Chilled Water Temp. °F
Chilled Water Temp. °F Other Temp. °F
Other Temp. °F
Safety Controls
Safety Controls Liquid Temp. Setting
Liquid Temp. Setting High Temp. Setting
High Temp. Setting Safety Vapor Setting North America Europe Sumitomo 3M Limited Asia Pacific and
Safety Vapor Setting Vapor Up Setting 3M Specialty Materials 3M Specialty Materials 33-1, Tamagawadai 2-chome Latin America
3M Center, Building 223-6S-04 3M Belgium N. V. Setagaya-ku, Tokyo Call (U.S.) 651 736 7123
Vapor Up Setting Other (name) Setting St. Paul, MN 55144-1000 Haven 1005, Canadastraat 11 158-8583 Japan
800 833 5045 B-2070 Zwijndrecht 813 3709 8250
Other (name) Setting (32) 3 250 7521
Process Important Notice to Purchaser: The information in this publication is based on tests that we believe are reliable. Your results may vary due
Parts Cleaned Current Solvent Usage (MO/WK) to differences in test types and conditions. You must evaluate and determine whether the product is suitable for your intended application.
Since conditions of product use are outside of our control and vary widely, the following is made in lieu of all express or implied warranties
Type Gallons (including the warranties of merchantability or fitness for a particular purpose): 3M’s only obligation and your only remedy is replacement of
product that is shown to be defective when you receive it. In no case will 3M be liable for any special, incidental, or consequential damages
Qty. Per Load based on breach of warranty or contract, negligence, strict tort, or any other theory.
Cleanliness Standards
Weight of Load
Visual
Type of Material
Ionic Testing
Cleaning Cycle Water Break 3
Immersion Other Specialty Materials
Equipment Selection 5
Parts Processing 8
Boil-Up and Agitation Rate Guidelines . . . . . . . . . . . . . . . . . . 8
Solvating Agents 9
Dimensions of Opening
Gallons Per Hour Rating Guidelines for converting a cleaning process to
Length Width Heat:
3M Novec
™ ™
Cover: Type Elec. Volt Phase
Power Manual Steam PSIG
Hoist Type Other
Freeboard Chiller
Condensing
Temp. °F
Condensing
Refrigeration Temp. °F
Engineered
Fluids
Refrigeration Temp. °F Chilled Water Temp. °F
Chilled Water Temp. °F Other Temp. °F
Other Temp. °F
Safety Controls
Safety Controls Liquid Temp. Setting
Liquid Temp. Setting High Temp. Setting
High Temp. Setting Safety Vapor Setting North America Europe Sumitomo 3M Limited Asia Pacific and
Safety Vapor Setting Vapor Up Setting 3M Specialty Materials 3M Specialty Materials 33-1, Tamagawadai 2-chome Latin America
3M Center, Building 223-6S-04 3M Belgium N. V. Setagaya-ku, Tokyo Call (U.S.) 651 736 7123
Vapor Up Setting Other (name) Setting St. Paul, MN 55144-1000 Haven 1005, Canadastraat 11 158-8583 Japan
800 833 5045 B-2070 Zwijndrecht 813 3709 8250
Other (name) Setting (32) 3 250 7521
Process Important Notice to Purchaser: The information in this publication is based on tests that we believe are reliable. Your results may vary due
Parts Cleaned Current Solvent Usage (MO/WK) to differences in test types and conditions. You must evaluate and determine whether the product is suitable for your intended application.
Since conditions of product use are outside of our control and vary widely, the following is made in lieu of all express or implied warranties
Type Gallons (including the warranties of merchantability or fitness for a particular purpose): 3M’s only obligation and your only remedy is replacement of
product that is shown to be defective when you receive it. In no case will 3M be liable for any special, incidental, or consequential damages
Qty. Per Load based on breach of warranty or contract, negligence, strict tort, or any other theory.
Cleanliness Standards
Weight of Load
Visual
Type of Material
Ionic Testing
Cleaning Cycle Water Break 3
Immersion Other Specialty Materials
3
Cleaning Process Selection
The first step in converting to 3M™ Novec™ Engineered Fluids is selecting the appropriate cleaning process. Process
selection is based upon the anticipated soils, substrates, parts geometry and throughput. The Novec fluid Cleaning Process
Selection Guidelines (Table 1) are intended to assist in process selection. Cleaning trials may also be required.
Table 1
3M™ Novec™ Engineered Fluid Cleaning and
Degreasing Process Selection Guidelines
1
Representative examples; not a complete list.
2
The Novec fluid HFE-71DE and HFE-71DA azeotropes are incompatible with many plastics.
3
Compatibility testing required.
Note: In cases where neat or azeotrope processes are not appropriate or applicable, the co-solvent process should be considered
due to its capability to clean the broad range of soils.
4
Equipment Selection
3M™ Novec™ Engineered Fluids can be used in most new installed to avoid leaks. If the equipment is currently
and existing conventional multi-sump cleaning systems. operating with HCFC-141b, the existing seals should be
The Novec fluid neat, azeotrope and blend processes can compatible with Novec fluids. Buna N and EPDM gaskets
also be used in single-sump systems. In many cases, no or are compatible with 3M™ Novec™ Engineered Fluid
minimal modifications are required in order to effectively HFE-7100, HFE-7200 and HFE-71IPA. Use only EPDM
use existing equipment. Schematics of standard vapor gaskets with 3M™ Novec™ Engineered Fluid HFE-71DE
degreasing equipment and fully modified equipment are and HFE-71DA, and with co-solvent processes.
shown in Figures 1 and 2, respectively. The Equipment
Evaluation Survey in the back of this brochure can assist When using Novec fluids in an ongoing cleaning process,
you in determining the utility of existing equipment. 3M recommends that additional equipment modifications
be considered in order to optimize the process
Prior to conducting cleaning evaluations in your plant to effectiveness and economics by increasing agitation and
verify the effectiveness of Novec fluids in existing minimizing fluid emissions.
equipment, 3M recommends that appropriate seals be
Figure 1 Figure 2
Conventional Vapor Fully-Modified Vapor
Degreasing Equipment Degreasing Equipment1
Extended
Freeboard
(100-125%)
Boil Rinse
Filtration Pump Chamber Chamber
Heating Elements and Ultrasonics
Recirculating Recirculating
Pump, Spray Heating Elements Pump, Spray
Nozzles, and/or Nozzles, and/or
Ultrasonics Ultrasonics
(Optional)
1
Fully-modified equipment can result in optimum performance
and economy when used with Novec fluid processes.
5
Optimizing Existing Equipment
3M™ Novec™ Engineered Fluid process equipment is Ultrasonics
similar to conventional vapor degreasers. For some
applications the primary modification to be considered for In most cases, submersible transducers are preferred
optimum cleaning performance is the addition of agitation because they are easy to install. Some working space will
(mechanical and/or ultrasonic). In addition, 3M urges be taken up when submersibles are used. If the
customers to implement procedures that will minimize submersibles are placed on the bottom of the boil sump,
vapor emissions. The following equipment designs and the top of the weir can be extended to make up for lost
features should be considered, if not already present: height in the boil sump. In these cases, care must be taken
to avoid reducing the height of the vapor zone. If the
• 100%–125% freeboard submersibles are placed in the bottom of the boil sump,
• a filtration system in the boil sump they must be on legs so they do not interfere with heat
• ultrasonics in the rinse sump and (if needed) boil sump transfer in the tank. Several manufacturers have developed
• chiller coil(s) above the condensing coils commercially available ultrasonic systems that are
• an auxiliary heater (if needed) effective for use in both the boil and rinse sumps.
• safety sensor adjustments
Chiller Coils
Each of these items is discussed below.
Chiller coils above the primary condensing coils will also
Freeboard (100%–125%) reduce vapor losses. The refrigeration system must be
capable of maintaining the chiller coils at a temperature of
Extending the freeboard reduces fluid vapor losses. In -20°F (-29°C). The condensing coils can be smooth
most cases, the freeboard addition is fabricated of stainless surfaced, but finned tubing is preferred for chiller coils.
steel sheet metal and bolted onto the existing freeboard. A The chiller coils must be placed directly above the
bead of silicone caulking is placed between the existing condensing coils. Depending on ambient humidity, the
freeboard and the added freeboard to ensure a tight seal. If chiller coils may require a defrost cycle to prevent
not already present, a sliding cover should be added to the formation of ice and a reduction in cooling efficiency. Two
machine. A sliding cover is preferable to a lift-off or separate lines on the chiller coils allow one to be defrosted
hinged cover since lift-off or hinged covers create a while the other maintains the cold blanket. A third set of
pumping or suction action when removed, which can dehumidifying coils located at the top of the cleaner is not
increase fluid/vapor losses. required to minimize the emissions of vapors, and should
Boil Sump Filtration not be used.
6
Safety Sensor Adjustments
The safety sensor(s) on existing equipment may Figure 3
require adjustment in order to function effectively
with 3M™ Novec™ Engineered Fluids. Figure 3 illustrates Safety Sensors
typical locations and operations of the safety sensors.
1
1 Safety Vapor Control Sensor (SVC)–Turns off heat if
vapors rise above the primary cooling coil.
4
Table 2
3M Novec Engineered Fluid Recommended Safety Sensor Settings
™ ™
Neat Cleaning System Neat Cleaning System Azeotrope Cleaning System Co-Solvent
Novec fluid HFE-7100 Novec fluid HFE-7200 Novec fluid HFE-71DE Cleaning System
Sensor & HFE-71IPA Boiling Point & HFE-71DA Boiling Point
Boiling Point 172°F (78°C) Boiling Point 144°F–194°F
140°F (60°C) 104°F (41°C) (62°C–90°C)
1. SVC 122°F (50°C) 154°F (68°C) 90°F (32°C) 122°F (50°C)
2. HTC 158°F (70°C) 190°F (88°C) 122°F (50°C) 18°F (10°C) above B.P.
3. LTC 149°F (65°C) 185°F (85°C) 113°F (45°C) 9°F (5°C) above B.P.
4. VUC 131°F (55°C) 167°F (75°C) 97°F (36°C) 131°F (55°C)
7
Part Processing
The ideal boil-up and agitation rate is based upon the anticipated soils, substrates, parts geometry and throughput. Part
Processing Boil-Up and Agitation Rate Guidelines are intended to assist in identifying optimal cleaning conditions.
Cleaning trials may also be required. For additional help in optimizing your cleaning application, call your 3M sales
representative or a 3M authorized 3M™ Novec™ Engineered Fluid distributor.
Table 3
Part Processing Boil-Up and Agitation Rate Guidelines
Agitation and Low Medium High
Boil-up1 (Agitation provided (Agitation from (Standard for
from boil and slight pump action in Ultrasonic)
spray bar action) spray bars)
LOW 1 2 3
0.5 x Boil-up rate • Open structure • Ultrasonics not • Parts with tight
metal parts (no appropriate clearances and
close tolerances) • Small amounts of small amounts of
• Parts with large carry-over2 are carry-over
heat capacity present
MEDIUM 4 5 6
1 x Boil-up rate • Open structure • Ultrasonics not • Parts with tight
parts not suited appropriate clearances and
to ultrasonics • Medium carry- medium carry-
• Medium carry- over present over
over present
• Open structure
parts with medium
heat capacity
HIGH 7 8 9
2 x Boil-up rate • Open structure • Ultrasonics not • Parts with open
plastic parts with appropriate blind holes (typical
low heat capacity • Large carry-over of electrical
connectors)
1
“Boil-up” is the rate at which material is vaporized from the boil sump (lbs./hr.), divided by the number of lbs. of material in a
completely filled rinse sump.
2
“Carry-over” is the solvent and soil carried from the cleaning sump to the rinse sump during cleaning. Examples of parts with
high, medium and low carry-over are: (high) electric motor windings, unsealed electrical connectors, and small nested parts;
(medium) electric coil windings, assembled bearings, and printed circuit boards; (low) unassembled bearings and single parts.
8
Solvating Agents for the Co-Solvent Process
The recommended solvating agents for the 3M™ Novec™ Combinations of these solvating agents are possible. The
Engineered Fluid co-solvent process are manufactured by solvating agent selected will depend on the cleaning
Petroferm, Inc. These solvating agents (e.g., SA-70, SA- application and the efficiency of the solvating agent
24) have been tested and approved for use with 3M™ chosen must be verified by the user. Your 3M
Novec™ Engineered Fluid HFE-7100. representative and your 3M authorized distributor can
offer guidance in solvating agent selection.
In addition, there are other solvating agents that can be
used in the Novec fluid co-solvent cleaning process.
Table 4
3M Novec™ Engineered Fluids Materials Compatibility
™
Testing on 3M™ Novec™ Engineered Fluid HFE-7100 and HFE-71IPA indicate good compatibility with a variety of metals,
plastics and elastomers. Novec fluid HFE-7100 is compatible with the following substrates (one hour of exposure at
boiling temperature).
Metal Plastics Elastomers
Aluminum Acrylic Butyl Rubber
Copper Polyethylene Natural Rubber
Carbon Steel Polypropylene Nitrile Rubber
302 Stainless Steel Polycarbonate EPDM
Brass Polyester
Zinc Nylon
Molybdenum Epoxy
Tantalum PMMA
Titanium PVC
Tungsten PET
Cu/Be Alloy C172 ABS
Magnesium Alloy AZ31B
3M™ Novec™ Engineered Fluid HFE-71DE and HFE-71DA are compatible with the following substrates (one hour of
exposure at boiling temperature).
9
General Operation Practices
The following operating practices are recommended to reduce vapor and dragout losses and to ensure parts are thoroughly
cleaned, rinsed and dried.
1 Eliminate drafts near the cleaning equipment. 5 Use spray only if required and then only below the
Drafts increase vapor losses by causing disturbances in cooling coils. Misdirected spraying can splash
the vapor-air interface. above the coils and increase losses.
2 A sliding cover is recommended to minimize 6 Arrange parts so that fluids drain readily. Some parts
vapor-air interface disturbances. Opening the can trap fluids, making them more difficult to rinse
cover slowly will reduce vapor losses. and increasing fluid dragout losses. Tumbling the
parts before removing them from the vapor zone will
3 Do not begin cleaning operations until the help remove excess fluid.
equipment is at operating temperature. This will
help ensure the parts are adequately heated and that 7 Do not lift parts above the vapor zone when
the rinsing agent will evaporate when the parts are transferring from the boiling sump to the rinsing sump.
raised into the freeboard area.
8 Follow machine safety, operating and maintenance
4 The parts processing rate established for your procedures.
equipment should not be exceeded. Inadequate
residence times result in liquid being removed with the 9 Perform regular checks for fluid leaks from the
part (dragout), thereby increasing fluid losses. Suitable equipment, especially piping, valves, and housings.
residence times should be established to ensure that 10 Do not place hands below the vapor line. To place
parts are completely cleaned, rinsed and dried. parts in sumps, use hooks, automated equipment or
Automation with a programmable hoist system can long-handled baskets.
ensure that the processing time is maintained at the
established rate. 11 Monitor fluid usage and locate leaks if
usage increases.
10
Equipment Evaluation Survey
TM
Prior to converting your process to 3M Novec Engineered Fluids, 3M recommends you complete this
TM
3
Equipment Evaluation Survey and return it to your 3M representative or 3M authorized distributor.
In response, 3M will evaluate your process and provide you with recommendations on how to modify
existing equipment for effective and efficient operation with Novec fluids.
Novec ™
Dimensions of Opening
Gallons Per Hour Rating Guidelines for converting a cleaning process to
Length Width Heat:
3M Novec
™ ™
Cover: Type Elec. Volt Phase
Power Manual Steam PSIG
Hoist Type Other
Freeboard Chiller
Condensing
Temp. °F
Condensing
Refrigeration Temp. °F
Engineered
Fluids
Refrigeration Temp. °F Chilled Water Temp. °F
Chilled Water Temp. °F Other Temp. °F
Other Temp. °F
Safety Controls
Safety Controls Liquid Temp. Setting
Liquid Temp. Setting High Temp. Setting
High Temp. Setting Safety Vapor Setting North America Europe Sumitomo 3M Limited Asia Pacific and
Safety Vapor Setting Vapor Up Setting 3M Specialty Materials 3M Specialty Materials 33-1, Tamagawadai 2-chome Latin America
3M Center, Building 223-6S-04 3M Belgium N. V. Setagaya-ku, Tokyo Call (U.S.) 651 736 7123
Vapor Up Setting Other (name) Setting St. Paul, MN 55144-1000 Haven 1005, Canadastraat 11 158-8583 Japan
800 833 5045 B-2070 Zwijndrecht 813 3709 8250
Other (name) Setting (32) 3 250 7521
Process Important Notice to Purchaser: The information in this publication is based on tests that we believe are reliable. Your results may vary due
Parts Cleaned Current Solvent Usage (MO/WK) to differences in test types and conditions. You must evaluate and determine whether the product is suitable for your intended application.
Since conditions of product use are outside of our control and vary widely, the following is made in lieu of all express or implied warranties
Type Gallons (including the warranties of merchantability or fitness for a particular purpose): 3M’s only obligation and your only remedy is replacement of
product that is shown to be defective when you receive it. In no case will 3M be liable for any special, incidental, or consequential damages
Qty. Per Load based on breach of warranty or contract, negligence, strict tort, or any other theory.
Cleanliness Standards
Weight of Load
Visual
Type of Material
Ionic Testing
Cleaning Cycle Water Break 3
Immersion Other Specialty Materials