Designation: C 845 – 96

Standard Specification for

Expansive Hydraulic Cement1
This standard is issued under the fixed designation C 845; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.

1. Scope paste that increases significantly in volume during the early

1.1 This specification covers hydraulic cements that expand hardening period occurring after setting. This volume increase
during the early hardening period after setting. is due principally to the reaction of the calcium aluminates and
calcium sulfates.
2. Referenced Documents 3.1.5 shrinkage-compensating concrete—a concrete made
2.1 ASTM Standards: with an expansive cement in which the expansion, if restrained,
C 33 Specification for Concrete Aggregates2 induces compressive stresses that approximately offset tensile
C 109/C 109M Test Method for Compressive Strength of stresses induced by drying shrinkage.
Hydraulic Cement Mortars (Using 2-in. or 50-mm Cube
4. Classification
Specimens)3
C 114 Test Methods for Chemical Analysis of Hydraulic 4.1 The cement covered by this specification is suitable for
Cement3 use in shrinkage-compensating concrete and shall be desig-
C 183 Practice for Sampling and the Amount of Testing of nated as Type E-1.
Hydraulic Cement3 NOTE 1—Three kinds of expansive cement are identified in Section 3
C 185 Test Method for Air Content of Hydraulic Cement by the letters K, M, and S. The appropriate letter should be used as a suffix
Mortar3 to the type designation when one of these kinds is desired. Expansive
C 188 Test Method for Density of Hydraulic Cement3 cement may also be prepared in other ways.
C 465 Specification for Processing Additions for Use in the 5. Ordering Information
Manufacture of Hydraulic Cements3
C 688 Specification for Functional Additions for Use in 5.1 When it is desired that an optional requirement apply or
Hydraulic Cements3 that the cement be of a particular kind, a specific request to this
C 806 Test Method for Restrained Expansion of Expansive effect should be made by the purchaser.
Cement Mortar3 6. Chemical Composition
C 807 Test Method for Time of Setting of Hydraulic Ce-
ment Mortar by Modified Vicat Needle3 6.1 Expansive cement shall conform to the requirements as
to chemical composition prescribed in Table 1.
3. Terminology 6.2 The purchaser has the option of specifying that the
3.1 Definitions: alkalies (Na2O + 0.658K2O) shall not exceed 0.60 % (See
3.1.1 expansive cement (K)—an expansive cement contain- Table 2).
ing anhydrous calcium aluminosulfate (4CaO·3Al2O3·SO3), NOTE 2—This limit should be specified when the cement is to be used
calcium sulfate, and uncombined calcium oxide. in concrete with aggregates that may be reactive. Reference should be
3.1.2 expansive cement (M)—an expansive cement contain- made to Specification C 33 for suitable criteria of deleterious reactivity.
ing calcium aluminate cement and calcium sulfate.
7. Physical Properties
3.1.3 expansive cement (S)—an expansive cement contain-
ing tricalcium aluminate (C3A) and calcium sulfate. 7.1 Expansive cement shall conform to the physical require-
3.1.4 expansive hydraulic cement—a cement composed es- ments prescribed in Table 3.
sentially of hydraulic calcium silicates, calcium aluminates and
8. Additions
calcium sulfates, which, upon being mixed with water, forms a
8.1 The cement covered by this specification shall contain
no additions except as follows:
1 8.1.1 Water, or a functional addition, or both, that has been
This specification is under the jurisdiction of ASTM Committee C-1 on Cement
and is the direct responsibility of Subcommittee C01.13 on Special Cements. shown to meet the requirements of Specification C 688, may be
Current edition approved Jan. 10, 1996. Published March 1996. Originally added in amounts such that the limits shown in Table 1 for loss
published as C 845–76 T. Last previous edition C 845–90. on ignition shall not be exceeded.
2
Annual Book of ASTM Standards, Vol 04.02.
3
Annual Book of ASTM Standards, Vol 04.01.

Copyright © ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United States.

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 C 845
TABLE 1 Standard Chemical Requirements adequate to ensure compliance with the provisions of this
Composition, % specification.
Magnesium oxide (MgO), max 6.0
Insoluble residue, max 1.0
11. Rejection
Loss on ignition, max 4.0 11.1 The cement may be rejected if it fails to meet any of the
requirements of this specification.
11.2 Cement remaining in bulk storage at the mill prior to
TABLE 2 Optional Chemical Requirements
shipment for a period greater than 6 months or cement in bags
Alkalies (Na2O + 0.658 3 K2O) max, % 0.60 in local storage in the hands of a vendor for more than 3
months, after completion of the tests, may be retested for
expansion and may be rejected if it fails to conform to the
TABLE 3 Physical Requirements
requirements of this specification for expansion.
Time of setting, min, minutes 75
Air content, max, vol % 12.0
11.3 Packages more than 2 % below the net weight marked
Restrained expansion of mortar: thereon, may be rejected. Also, if the average net weight of
7-day expansion: packages in any shipment, as shown by weighing 50 packages
min, % 0.04
max, % 0.10
at random, is less than that marked on the packages, the entire
28-day, percentage of 7-day shipment may be rejected.
expansion, max 115
Compressive strength, min: 12. Certification
7-day, psi(MPa) 2100(14.7)
28-day, psi(MPa) 3500(24.5) 12.1 At the request of the purchaser, the manufacturer shall
state in writing the composition of a finished cement.
12.2 The composition of any cement shall conform to that
8.1.2 At the option of the manufacturer, processing addi- shown in the statement of the manufacturer within the follow-
tions may be used in the manufacture of the cement, provided ing tolerances:
such materials in the amounts used have been shown to be not Tolerance, 6 %
harmful in accordance with Specification C 465. Silicon dioxide (SiO2) 3
Aluminum oxide (Al2O3) 2
Calcium oxide (CaO) 3
9. Test Methods
9.1 The cement shall be sampled and the properties enumer- 12.3 At the request of the purchaser, the manufacturer shall
ated in this specification shall be determined in accordance state in writing the nature, amount, and identity of any
with the following methods: processing or functional addition that may have been used.
9.1.1 Sampling—Practice C 183. Also, if requested, the manufacturer shall supply test data
9.1.2 Chemical Analysis—Test Methods C 114. showing compliance of any processing addition with the
9.1.3 Time of Setting—Test Method C 807. provisions of Specification C 465, and any functional addition
9.1.4 Air Content—Test Method C 185, using the actual with the provisions of Specification C 688.
specific gravity of the cement if it differs from 3.15 by more 12.4 Upon request of the purchaser in the contract or order,
than 0.05 in calculating the air content. a manufacturer’s certification that the material during produc-
9.1.5 Restrained Expansion of Mortar—Test Method C 806. tion was tested in accordance with this specification together
9.1.6 Compressive Strength—Test Method C 109/C109M, with a report of the test results shall be furnished at the time of
except that a water-cement ratio of 0.500 shall be used, the shipment.
specimens shall be covered with a polyethylene sheet or other 13. Packaging and Package Marking
suitable material for preventing loss or gain of moisture at the
13.1 When the cement is delivered in packages, the words“
surface of the specimens during the moist storage period in the
expansive cement,” the type, the kind (if the cement is one of
molds, and the specimens shall remain in the molds for 3 days.
the three kinds defined in Section 3), the name and brand of the
9.1.7 Density—Test Method C 188.
manufacturer, and the net weight shall be plainly marked on
10. Inspection each package. Similar information shall be provided in the
shipping documents accompanying the shipment of packaged
10.1 Every facility shall be provided the purchaser for
or bulk cement. All packages shall be in good condition at the
careful inspection and sampling of the finished cement. The
time of inspection.
finished cement may be inspected and sampled either at the
mill or at the site of the work, as may be specified by the 14. Storage
purchaser. The following periods from time of sampling shall 14.1 The cement shall be stored in a manner such as to
be allowed for completion of testing: permit easy access for proper inspection and identification of
7-day test 12 days each shipment and in a suitable weathertight building that will
28-day test 33 days
protect the cement from dampness and minimize warehouse
10.2 The manufacturer shall provide suitable facilities to set.
enable the inspector to check the intergrinding or blending
operation used to produce cement by either means. The plant 15. Keywords
facilities for intergrinding or blending and inspection shall be 15.1 calcium aluminate; calcium aluminosulfate; calcium

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 C 845
oxide; calcium silicate; calcium sulfate; cement; expansive;
hydraulic; shrinkage-compensated; tricalcium aluminate

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