Rr411812 X Ray Metallography
Rr411812 X Ray Metallography
Rr411812 X Ray Metallography
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IV B.Tech I Semester Supplimentary Examinations, February 2008
X-RAY METALLOGRAPHY
(Metallurgy & Material Technology)
Time: 3 hours Max Marks: 80
Answer any FIVE Questions
All Questions carry equal marks
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1. Discuss the history of X-radiations. Describe the methods for X-ray production.
[16]
2. (a) Draw the following planes and directions in a tetragonal unit cell (001), (011),
(113), [110], [201], [101]. Show cell axes.
(b) Rubidium is a BCC crystal. The angle of diffraction for (321) set of planes is at
270 for the first order reflection. The wavelength of X-rays used is 0.0711nm.
Calculate the interplanar distance of the planes. What is the atomic radius of
Rubidium atom? [8+8]
5. Giving the principle, Describing the design and with a neat sketch explain the
working of focusing Cameras. [16]
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Code No: RR411812 Set No. 2
IV B.Tech I Semester Supplimentary Examinations, February 2008
X-RAY METALLOGRAPHY
(Metallurgy & Material Technology)
Time: 3 hours Max Marks: 80
Answer any FIVE Questions
All Questions carry equal marks
⋆⋆⋆⋆⋆
1. (a) What is the frequency (per second) and energy per quantum (in joules) of
x-ray beams of wavelength 0.71A0 (Mo Kα ) and 1.54A0 (Cu Kα )? [7]
(b) Calculate the velocity and kinetic energy with which the electrons strike the
target of an X-ray tube operating at a voltage ‘V’. Determine the short-
wavelength limit of the continuous spectrum emitted and the maximum energy
per quantum of radiation? [9]
2. (a) Explain the phenomenon ‘scattering by a unit cell’ with neat sketch. [9]
(b) Structure factor is independent of the shape and size of the unit cell. Explain.
[7]
3. (a) Describe Laue method of X-ray diffraction. [9]
(b) What does the each intense point in X-ray diffraction represent in Laue pat-
tern? Explain. [7]
4. (a) How does Debye-Scherrer diffraction pattern look? [4]
(b) Where is Debye-Scherrer method useful? [6]
(c) Explain how a powder camera is superior to a Diffractometer with examples.
[6]
5. Compare the following:
(a) Powder method and Laue method
(b) Debye-Scherrer Camera and Guinier Camera. [8+8]
6. (a) Cu Kα radiation is incident on a Xenon filled proportional counter. Calculate
the ratio of average pulse size in the escape peak to that in the normal peak.
(b) Write a note on energy-intensive Diffractometry. [8+8]
7. What is the basic principle involved in crystal structure determination? Explain
various steps involved in determination of unknown structures. [16]
8. Write notes on the following:
(a) Focussing Cameras
(b) Techniques used in stress measurements. [8+8]
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Code No: RR411812 Set No. 3
IV B.Tech I Semester Supplimentary Examinations, February 2008
X-RAY METALLOGRAPHY
(Metallurgy & Material Technology)
Time: 3 hours Max Marks: 80
Answer any FIVE Questions
All Questions carry equal marks
⋆⋆⋆⋆⋆
2. (a) In a drawing of a hexagonal prism, indicate the following planes and directions:
(1210), (1012), (1011), [110], [111], [021]. Show cell axes.
(b) What is Stereographic Projection? Show the lattice reorientation caused by
turning on stereographic projection. [8+8]
6. What is the principle involved in transmission Laue method? With a neat sketch
explain the transmission Laue method? [16]
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Code No: RR411812 Set No. 4
IV B.Tech I Semester Supplimentary Examinations, February 2008
X-RAY METALLOGRAPHY
(Metallurgy & Material Technology)
Time: 3 hours Max Marks: 80
Answer any FIVE Questions
All Questions carry equal marks
⋆⋆⋆⋆⋆
2. (a) For BCC Iron, compute (i) the interplanar spacing (ii) the diffracting angle for
the (220) set of planes. The lattice parameter of Iron is 0.2889 nm. Assume
that a monochromatic radiation having a wavelength of 0.1541 nm is used and
the order of reflection is done.
(b) (i) Calculate the interplanar spacing for (110) and (221) sets of planes in
Aluminum (ii) When a monochromatic X-ray beam of X-rays of wavelength
0.1542 nm is used, the first order reflection from (113) set of planes occurs at
θ . What is the value of θ ? [8+8]
5. (a) The transmission Laue Pattern is made up of Copper Crystal with a specimen
to film distance of 4 Cm. The (111) planes of the Crystal make an angle 4o
with the incident beam. What minimum tube voltage is required to produce
(111) reflection?
(b) Why is a diffractometer used for the measurement of the intensity of X-rays.
Explain the general features of this diffractometre. [8+8]
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Code No: RR411812 Set No. 4
7. A Transmission pinhole photograph is made of a sheet of Aluminum 0.5 mm thick
with Cu Kα radiation. Consider only the (111) reflection which occurs at 2θ = 38.40
. Imagine the sheet to be divided into four layers, the thickness of each being equal
to one fourth of the total thickness. Calculate the fraction of the total diffracted
energy for each layer. [16]
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