Modular Compact

Rheometers MCR 72
MCR 92
 MCR 72 and MCR 92

See things change

With a rheometer, you can follow the change in your sample’s viscosity – The MCR series has opened more doors and created more
from one measuring point to the next. You instantly gain deeper insights testing possibilities than any other rheometer in the world. In
into your sample’s deformation, flow behavior and structure – so you can keeping with this tradition, MCR 72 and MCR 92 now round
change matters in your favor. off the family as your “entry tickets” to the world of rheology.
Starting out in rheometry, your two wisest choices are MCR 72 and To help you get rapidly acquainted with this exciting field and
MCR 92 from Anton Paar – real rheometer “pearls”, streamlined for your all its possibilities, MCR 72 and MCR 92 come with a wealth of
daily lab routine, easy to use in a Plug and Play fashion and available at application know-how and introductory materials you will only
an accommodating price. find at Anton Paar.
 Is a single-point measurement sufficient to describe the flow behavior of my sample?

For quality control, a single-point check might be sufficient.

What can you do with a rheometer? But in general, a single-point measurement provides limited
information about the flow behavior of materials.

To describe a sample’s flow behavior to its full extent you single point
need a rheometer. From just one measurement, rheometers
provide a flow curve in a wide speed and torque range.
This curve shows the behavior of a sample under varying
What is the difference between a viscometer and a rheometer? conditions, such as different shear rates and temperatures. dark chocolate
milk chocolate
white chocolate

Viscometers are simple devices. They are based on mechanical ball Test method Industry
bearings or torsional spring bearings that rotate a measuring system Viscosity curves of different types of chocolate compared to single-point measurements.
(e.g. a bob or a spindle) in a single direction. They are ideal for fast
Rotation General
and simple tests.

Rheometers reveal the full spectrum of a sample under the

conditions you define.

For example: Rheological measurements show you the structure of a

sample by providing insight into the viscoelastic behavior.
Rheometer principles
How can I determine the feel and long-term stability of my cream or ointment?
Rheometers are built to be more sensitive than viscometers.
They have two measurement modes: rotational and oscillatory. Long-term stability and the “feel” when a cream or
G�, G��
Accessories such as plates, bobs, cones, heating and cooling ointment is applied on the skin are important quality lg G�
chambers make it possible to study the sample’s properties under criteria in the cosmetics and pharmaceutical industries.
a wider range of conditions. Rheometers are an excellent tool for Using a rheometer you can evaluate the elastic
lg G��
research, process and product development as well as for quality portion (G�) and viscous portion (G��) of a sample in an
control. amplitude-sweep test. The relationship between these
Measuring systems
portions defines how strong the internal network of the
sample is, which affects long-term stability and the way
a cream feels on the skin when being applied.
lg γ
Test method Industry
Cream 1 has a gel-like or solid structure because the elastic portion G� is higher than the
viscous portion G��.

Rotation Oscillation General

G�, G��
lg G��

Will my paint have a nice glossy finish or will it show brush marks and drips? lg G�

Test method Industry

One important quality factor of paint is the surface These curves show
Amplitude
a paint which sags
leveling and sagging behavior once it is applied, (red), a paint which Sweep Cosmetics
Oscillation
since a smooth, glossy and homogenous surface has trouble leveling lg γ
(green) and a paint
with no droplets or splashes is generally required. which has a good Cream 2 behaves more like a liquid as in this case G�� is higher than G�.
The structural strength of the paint should not be finish (blue)

too high or too low, to be sure that the internal

structure recovers in exactly the right time period
to create a good finish. These characteristics are
often referred to as thixotropic behavior. When Is my slurry pumpable and flowable?
developing or improving paint, the material’s
time-dependent rheological behavior has to be
balanced to get the required result. The processing and transport characteristics of slurries
are strongly dependent on their rheological properties.
A rheometer can simulate this behavior in With a rheometer you can simulate flow resistance in
rotational mode using a structural regeneration pipes and see the result as flow and viscosity curves.
test (“3 Interval Time Test/3 ITT”). You can also determine the yield point in a flow curve
(controlled shear stress mode) which will help you solve 0

problems with slurries that are difficult to pump.

Test method Industry Test method Industry

These flow and viscosity curves show the rheological behavior of a slurry. The yield point τ
Controlled Shear
0

can be calculated from the flow curve (blue). The viscosity curve (red) gives information about
3 ITT Rotation Paints/Coatings Stress Test Building Materials/Mining the flow behavior of a slurry when being pumped through pipes.
Rotation
Welcome to the World of Rheology

Rheological measurements can give you so much more

information about your products – but where to start and
how to interpret the results?

To help you on your way to becoming a rheology expert,

Anton Paar gives you access to a wealth of practical
information on the www.world-of-rheology.com website.
Here you can browse through entertaining eLearning
courses, download application reports for your industry,
register for a free webinar or read through the “tips and
tricks” sections.

Introducing Joe Flow, the virtual rheology expert

Let Joe Flow, our virtual rheology expert, be your guide to the exciting world of rheology.
He will first guide you through the online course “Basics of Viscometry” to provide you with
the basic knowledge of liquids in flow. Then you can learn about the basics of rheology
and gain knowledge which will help you in your daily work.

Joe Flow’s book “Applied Rheology – With Joe Flow on Rheology Road” explains the laws
of viscosity and elasticity and provides tips for avoiding errors in your measurements. This
is a good reference for everyone starting out in rheology.

Further training
Anton Paar offers seminars and webinars to help you acquire the know-how
you need to get the most out of your rheometer. Thanks to Anton Paar’s global
network of subsidiaries and sales partners you will find almost every course in
our program offered in your area and language.

Your knowledge database

Are you interested in “time- and frequency-dependent measurements
on printing inks” or the “rheological characterization of cheese”? These
application reports and hundreds of others are available for a wide range of
applications and samples on the World of Rheology website. They form a
huge database of rheological know-how at your disposal.
The outstanding features
of MCR 72 and MCR 92

Designed for your application 25 years of experience in one motor

MCR 72 is equipped with a ball-bearing motor and The air-bearing-supported synchronous EC motor of
provides measurements in rotational and also for special MCR 92 deploys a frictionless synchronous movement
applications in oscillatory mode. MCR 92 provides of the rotor inside that enables the most sensitive and
measurements in both rotation and oscillation and has therefore most precise movements. Whether investigating
air-bearing motor technology. There is a wide range of solids or low-viscosity liquids your results are accurate
accessories available for both models so you can build across a wide viscosity range.
the setup which perfectly suits your application.

Clear view of the sample

Unmatched reproducibility
TruRay is a unique lighting concept which gives you a
Reproducible settings are essential for obtaining reliable clear view of the sample and measurement surface. This
and reproducible results. MCR 72 and 92 feature is especially important when filling the measuring gap.
a motor-driven elevation mechanism and SafeGap
(Austrian Patent AT 517074) technology, which ensure
that the setting of the measuring gap is always identical
for every measurement and exactly reproducible
Automatic tool recognition
every time. Furthermore, the slow and precise setting and configuration
minimizes any influence on the sample’s structure.
Toolmaster is the only completely contact-free automatic
tool recognition and configuration system for rheometers.
Easy fitting of measuring systems It recognizes measuring systems and temperature control
units as soon as these are connected to the rheometer
so you don't need to enter this data manually.
When changing between measuring systems,
QuickConnect gives you great ease-of-use. This quick-
fitting coupling allows one-handed connection of the
measuring systems, and ensures fast, convenient system Step-by-step software
changes without the use of a screwing mechanism.
The intuitive RheoCompass software helps you find
the templates you need, customize test and analysis
Most accurate temperature control definitions, export your data and much more. You are
guided through your first rheological measurements
with predesigned but individually adaptable templates,
Temperature has the biggest influence on rheological
including integrated videos for extra support.
measurements. To counteract this MCR 72 and MCR 92
can be used with several air-cooled Peltier temperature
units. These CoolPeltier units with an integrated fan for
counter-cooling are an accurate, fast and energy-efficient
alternative to liquid-circulator counter-cooling systems.
 Your application - Anton Paar solutions

Application Typical samples Measuring procedure Test types Specifications Units MCR 72 MCR 92

Paints & coatings Architectural paints Viscosity Viscosity curve (ROT) Bearing - Ball Air
Wall paints Yield/flow point Amplitude sweep (OSC) EC motor (brushless DC) with high-resolution optical encoder -
Automotive paints Thixotropic effect 3 Interval Time Test (ROT/OSC)
Rotation mode -
Printing inks and pastes Structural decomposition & regeneration Frequency sweep (OSC)
Sedimentation/stability Oscillation mode - (1

Direct strain controller -

Food Chocolate Viscosity Viscosity curve (ROT)
Ketchup Yield/flow point Amplitude sweep (OSC) Direct stress controller -
Mayonnaise Thixotropic effect 3 Interval Time Test (ROT/OSC) Maximum torque mNm 125 125
Dairy products Structural decomposition & regeneration Frequency sweep (OSC)
Minimum torque, rotation µNm 200 1
Sauces Sedimentation/stability
Minimum torque, oscillation µNm 200 1
Polymers Polymer solutions Viscosity Viscosity curve (ROT) Torque resolution nNm 100 100
Polymer melts Temperature behavior Amplitude sweep (OSC) Angular deflection, set value µrad 1 to ∞ 1 to ∞
Frequency sweep (OSC)
Temperature test (ROT/OSC) Angular deflection, resolution nrad 614 614
Step rate, time constant ms 100 100
Step strain, time constant ms 100 100
Petrochemicals Drilling fluids Viscosity Viscosity curve (ROT) Minimum angular velocity (2 rad/s 10 -4 10 -4
Slurries and muds Yield/flow point Amplitude sweep (OSC)
Crude oils Thixotropic effect 3 Interval Time Test (ROT/OSC) Maximum angular velocity rad/s 157 157
Lubricants and greases Structural decomposition & regeneration Temperature test (ROT/OSC) Minimum angular frequency (3 rad/s 10 -3 10 -4
Temperature behavior Frequency sweep (OSC) Maximum angular frequency rad/s 628 628
Sedimentation/stability
Minimum speed (CSS/CSR) rpm 10 -3 10 -3
Resins Resins Viscosity Viscosity curve (ROT) Maximum speed rpm 1500 1500
Adhesives Temperature behavior Temperature test (ROT/OSC) Maximum temperature range °C -40 to 400 -40 to 400
Glues
SafeGap (Austrian Patent AT 517074), normal force limiter during gap setting -
TruRay, dimmable illumination of sample area -
Pharmaceuticals Salves and ointments Viscosity Viscosity curve (ROT) Connections USB, Ethernet, RS232, analog interfaces, Pt100 port
Pastes and creams Yield/flow point Amplitude sweep (OSC) Dimensions mm 380 x 660 x 530 380 x 660 x 530
Emulsions, dispersions and Thixotropic effect 3 Interval Time Test (ROT/OSC)
Weight kg 33 33
suspensions Structural decomposition & regeneration Frequency sweep (OSC)
Sedimentation Thermal loop test (OSC) QuickConnect for measuring systems, screwless -
Long-term stability Temperature test (ROT/OSC) Toolmaster, measuring system -
Temperature behavior
Toolmaster, measuring cell -
Cosmetics Shampoos Viscosity Viscosity curve (ROT) CoolPeltier, Peltier-controlled plate system with built-in cooling option that
Shower gels Yield/flow point Amplitude sweep (OSC) °C 25 below ambient but not lower than -5 up to +200 (4
requires no additional accessories for counter-cooling
Lotions and creams Thixotropic effect 3 Interval Time Test (ROT/OSC)
Actively Peltier-controlled hood that requires no additional accessories for
Hair gels Structural decomposition & regeneration Frequency sweep (OSC) °C -5 to +200 (4
counter cooling
Toothpaste Sedimentation Temperature test (ROT/OSC)
Nail polish Temperature behavior Thermal loop test (OSC) CoolPeltier, Peltier-controlled cylinder system with built-in cooling option that
°C 15 below ambient but not lower than +5 up to +150 (4
Makeup Long-term stability requires no additional accessories for counter-cooling
Virtually gradient-free (horizontal, vertical) temperature control -

Electronic trim lock for the measuring system -

Temperature device Temperature range Materials Measuring systems Heating rate Cooling rate
Automatic gap control/setting, AGC/AGS -
P-PTD 200/AIR/18P -5 °C to +200 °C Up to Up to Rheometer software:
40 °C/min 40 °C/min
Test designer -

Report designer -
H-PTD 200/AIR/18P -5 °C to +200 °C Up to Up to
40 °C/min 40 °C/min User management -

C-PTD 150/XL/AIR/18P +5 °C to +150 °C Up to Up to Also available as EDU Edition (for educational institutions only):
7 °C/min 7 °C/min
- MCR 72 or MCR 92 plus accessories
with a special academic discount
- Free EDU Package and EDU Student Packages
including lab equipment and educational material
as well as office supplies and giveaways

Note:

1) Depending on sample properties.

Measuring systems 2) Depending on measuring point duration and sampling time, practically any value is achieved.
3) Set frequencies below 10 -4 rad/s are of no practical relevance due to the measuring point duration >1 day.
4) System temperature, sample temperature may vary. For measurements at very high or low temperatures a calibration in the sample gap is recommended.

Cone-plate Parallel-plate Concentric-cylinder Double-gap Stirrer RheoCompass (9177015), Toolmaster (3623873) and CoolPeltier (9177056) are registered trademarks of Anton Paar.

Legend: included
© 2018 Anton Paar GmbH | All rights reserved.
Specifications subject to change without notice.
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