Unit III Final Notes
Unit III Final Notes
Introduction
Several non-destructive testing methods are available for evaluation of material’s quality
and component’s integrity. Each of these methods is based on a particular physical
principle. Generally the following non-destructive testing methods are widely used.
1. Visual Examination (i) with naked eye (ii) with optical aids
5. Ultrasonic testing
6. Radiography
Modern methods: Besides above, some more modern methods are also getting increasing use
for on-line monitoring of plant components: preferably in power plants, petrochemical plants,
chemical and fertilizer plants etc. These methods are
Visual Inspection
It is the simplest, cheapest and most widely used amongst all the non-destructive testing
methods. A simple visual test can reveal gross surface defects easily and quickly,
however for detection of finer defects, devices/equipments having high degree of
precision and illumination are required.
The illumination of test piece is provided by light. An adequate lighting of about 80-100
lux is essential for visual inspection by naked eye.
Equipment used for visual inspection: A visual inspection may be accomplished by naked eye
or with the help of an optical aid. These optical aids are equipped with lighting system and
magnifying devices. Following devices/instruments/ equipments are generally involved in visual
checks.
Optical microscopes
Borescope
Endoscope
Flexicope
Telescope
Holography
Closed circuit television
Microprocessors and computers
Image processing and pattern recognition techniques
The optical microscope having magnifications 10 x to 2000 x are generally used for inspection.
The borescope is used to inspect the inside portion of a hollow chamber, narrow tube, or a bore.
It is a precision built-in system consisting complex arrangement of prisms, lenses, and light
source.
The endoscope is similar to a borescope but incorporates a superior optical system and high-
intensity light source. It also has the facility of viewing at various angles.
Flexicope is a flexible fiber-optic borescope that can view the defects around corners and
`through passages’ having multi-directional changes. Its field of vision is of about 100°.
Telescope is used to examine those surfaces which are inaccessible or whose vision is concealed.
For that purpose, the help is taken of a ‘periscope’ or a ‘closed circuit TV’.
The microprocessors and computers assist in a very reliable, quick and easy visual inspection.
The techniques of image processing and pattern recognition are used when a large number of
components are assessed for automatic acceptance or rejection.
Fields of application: Visual inspection method is mainly suitable for checking in the following
applications.
Leakage in components
Misalignment of parts
Cracks and fractures
Corrosion and erosion
Minute discontinuities
Defects in welds
1. Cleaning of the surface by removing scales, grease, oil, paints, dust, dirt, and other chemicals
etc. followed by drying.
3. Removal of excess penetrant from the entire surface except from the cracks/defects/cavities.
This is essential to get contrast (bright and dark) visibility between defective and non-defective
portions of the surface.
4. Thin coating of developer over the surface to draw the penetrant out of crack so as to
increase its visibility. The developer also covers the surface with a color that increases the visual
contrast to the penetrant.
5. Scanning under ultraviolet or visible light to recognize the defect. It may be done with UV
or laser incident light and evaluation of defect may be accomplished with human eye or
automated optical scanners.
Testing materials: Following materials are generally used to conduct the above test.
Penetrating liquid: Petroleum-based or water-based carrier fluid + fluorescent red color dye for
visible light or yellow-green color dye for UV light.
Advantages :
This test can be applied to almost any type of metals, nonmetals, magnetic or non
magnetic type.
Cost of test is very less as it does not require any instrument or electronic display units.
This technique is more suitable for detecting the flaws in highly magnetic materials
(ferromagnetic materials) e.g. Fe, Ni, Co and their alloys which can be easily magnetized.
This method is capable of detecting flaws/discontinuities that are open to surface and/or
just below the surface.
The inspection method is based on the principle that “a flaw distorts the magnetic field
that has been impressed upon the sample to be tested”. Wherever a flaw interrupts the
flow of magnetic lines of force, some of these lines exit and re-enter the sample at certain
points.
These points form the opposite magnetic poles and attract the magnetic particles
sprinkled over the sample surface. The quantity of magnetic particles thus accumulated,
indicates the approximate shape and size of the flaw.
The magnetic particles are applied in the form of powder or as liquid suspension. The
liquid suspension form is known as ‘magnetic ink’ and is more common in use.
The color of magnetic particles is chosen to be in contrast with the color of the sample
surface for easy distinguishing and detection.
For maximum sensitivity, the magnetic flux is oriented at 90° to the direction of
discontinuity; but the flux is induced in different directions when the probable flaw
orientations are not known.
Magnetization may be done using a direct current source or an alternating current source, or by
half-wave rectification. For this purpose portable type, stationary type, heavy duty type, DC and
AC type equipments are available.
The simplest way of magnetizing a sample (test piece) is to use a permanent magnet. The
direction of flux flow lines are shown therein.
The intensity of flux can be varied by selecting either (i) a strong or weak magnet, or (ii) by
introducing a gap in the flux path with the help of a non- magnetic material.
1. The sample is cleaned of the grease, paint, scales etc. from its surface.
4. The distribution of powder (dense or loose, oriented or distorted) is viewed under proper
illumination of daylight or black-light source. The level of illumination is generally kept up to
500 lux at the sample surface.
5. All the relevant indications are marked after draining the magnetic ink. For maintaining a
permanent record, the sample area under inspection is photographed. Alternatively, it may be
covered with a transparent adhesive film which when taken off, presents the indication of the
sample area based on magnetic particles adhered to it.
6. The ferromagnetic sample is demagnetized by either heating above its curie temperature or by
applying the coercive force in opposite direction to the originally induced magnetic field.
ADVANTAGES:
According to Faraday’s law, “when a magnetic field cuts a conductor or vice versa, an electric
current will flow through the conductor if, a closed path is provided over which the current can
circulate”.
And the Oersted’s theory states that “a magnetic flux will exist around a current carrying coil in
proportion to the number of turns in the coil and the current”.
Production of eddy current: Based on the above principles, an alternating current of 1 kHz to 2
MHz frequency is allowed to flow in a coil (also called probe) as shown in Figure. It produces an
alternating magnetic field around it.
This coil induces an eddy current due to electromagnetic induction, in the metallic material to be
inspected, when brought in close proximity of the metallic surface. The eddy current is generally
parallel to the coil winding but its flow gets disturbed in presence of any
flaw/defect/discontinuity in material.
Then it generates an alternating magnetic field in opposite direction which can be detected in the
form of voltage across another coil, or by a change in impedance value of the original coil
Requirement of depth of penetration and frequency: The depth of penetration and frequency
of eddy current is a very important factor for accuracy of the test. If the eddy current does not
penetrate through the material’s thickness, it is likely to overlook the internal defects.
The depth of penetration d and the frequency f are related to each other by
d = 500/( σµrf)1/2
Applications: The eddy current method is employed for evaluating the following parameters.
To measure the conductivity of a metal that may vary with material characteristics.
To determine the hardness and strength of materials, since the change in these properties
also changes the conductivity value.
To determine the dimensions of thin components and sheets, and thickness of the
coatings. Because difference in conductivity exists between coated and non-coated parts.
In detecting the discontinuities such as inclusions, cracks etc.
For online testing of wires, bars, tubes etc., and their automated analysis with the help of
microprocessors.
Advantages :
• Low cost.
• No final cleanup required.
• ECI is very sensitive to small cracks and defects.
• Equipment are portable.
• Minimum part preparation required.
• Applicable to both ferrous and non ferrous metals
Disadvantages:
• Trained operators are generally required.
• Surface finish and roughness may interfere.
• Depth of penetration is limited.
• Only applicable to conductive materials.
Interpretation may be difficult
Ultrasonic Testing
Ultrasonic testing utilizes the high frequency ultrasonic waves for testing of surfaces and internal
defects/flaws in metals and non- metals. These waves are generated by Piezoelectric
transducers in the frequency range of 1 to 10 MHz.
Velocity of these waves depends on the nature of transmitting medium. It is 300 m/s in air at sea
level but is lower in solid medium. Therefore in common test materials, the acoustic wavelengths
λ (velocity = frequency x wavelength) are of the order of 1 to 10 mm. During the test, a highly
directional sound beam is transmitted to the workpiece, that propagates through the material but
is dissipated or reflected by flaws/defects.
These flaws are recorded by a set of instruments and display systems using ‘pulse-echo
technique’.
The ultrasonic testing provides information regarding the size, depth and location of flaws/defect
in materials.
Flaw detection set-up: A typical flaw detection system consists of the following main
units.
Ultrasonic transducer (or crystal probe)
Pulse transmitter
Receiver amplifier
Cathode ray oscilloscope along with time base generator and a timer (or clock)
Cables
In this method, the ultrasonic waves are produced by piezoelectric effect within the ultrasonic
transducer. The piezoelectric action is reversible interaction between elastic strain and electric
field.
If the piezoelectric crystal is slightly compressed, it produces an electric signal. Similarly, when
this crystal is excited with an alternating current of ultrasonic frequency, the ultrasonic waves are
produced. Thus the ultrasonic transducer acts as receiver as well as transmitter.
Crystal probe: The transducer (piezoelectric crystal) may be made of Quartz, Lithium sulfate
(LiSO4), Lead niobate (PbNbO3), Barium titanate (BaTiOO ), Lead zirconate titanate (PZT).
Amongst these the quartz is most commonly used material due to its excellent piezoelectric
properties, mechanical and dielectric strength, and thermal stability. It can operate at high
temperatures up to about 500°C. This crystal is mounted suitably in a probe before use. The
probe protects the transducer from mechanical damage and also the operator from electric shock.
Testing procedure: While inspecting a work-piece, the transducer is placed on the workpiece
surface as shown in Figure (a). The electric pulse is fed from the transmitter to the probe through
a cable.
1. The piezoelectric transducer in the probe is shock-excited by short but high voltage pulse so
that it vibrates at its own resonant frequency for a few oscillations.
3. The ultrasonic echo pulse is picked-up by the same probe which reconverts it into electric
signal.
4. Voltage of this electric signal is much smaller than the transmitted pulse, therefore, it needs to
be amplified.
5. The amplification of echo signal is accomplished in receiver- amplifier. It also filters the
signal to some extent. After amplification, the signals are rectified and fed to deflection plates of
cathode ray tube (CRT).
6. Any flaw/defect in the workpiece, reflects the waves. And this reflection is displayed on the
oscilloscope screen as shown in Figure (b).
7. Since the deflection plates (and hence the screen) are calibrated along x and y axes, therefore
depth of flaws and their location in the workpiece can be readily seen on screen.
Applications: The pulse-echo technique, described above is the most versatile method among
various methods of ultrasonic inspections. It is widely used in the following applications.
Radiography
In this test, the X-rays and gamma-rays are used to detect deep seated internal defects. The short
wavelengths of X-rays permit it to penetrate through the opaque materials. The depth of
penetration depends on the intensity of X-rays used. For industrial radiography, the hard X-rays
are used.
These are produced by X-ray generators available in different ranges of voltage and current.
Modern X-ray generators are available in specifications up to 450 kV and 15 mA. They are also
equipped with dual focal and ultra-small focal spots. Radiograph: During testing, the X-ray
source is applied on one side of the component to be inspected and a photosensitive film is
placed on the other side.
When X-ray beam is passed through the component, the film is exposed and displays the flaws
as light and dark images. Voids appear as dark image while the non-defective areas appear as
non-dark (light) image. The exposed film is called radiograph.
High Energy X-ray Source: Radiographic examination of much thicker components can be
accomplished by using a high-energy X- ray source. The energy value of such sources may be as
high as 1 MeV or more. X-ray machines like Van De Graff type electrostatic generator,
synchrotron, betatron etc. are used for this purpose. These machines can examine the steel pieces
of up to 300 mm thickness.
Gamma ray radiography: Gamma rays are the electromagnetic radiations that are emitted
from an unstable nucleus. They emit one or a few discrete wavelengths instead of a broad band
of wavelengths as emitted by X-ray machines (sources).
Therefore, the radiography by gamma- rays is independent of external power, and with simple
apparatus and compact radiation source. This facilitates the inspection of even those assemblies
in which the access to their interior is difficult.
Co-60, Ir-192, Cs-137, Th-170 radio-isotopes are generally used as gamma radiography source.
Amongst these the cobalt-60 is most common due to intense radiation obtained from its tiny
source.
Advantages :
Disadvantages :
THERMOGRAPHIC INSPECTION:
Infrared thermography is a technique for producing a visible image of invisible infra red
radiations emitted by objects due to their thermal conditions
When compared with other classical nondestructive testing techniques such as ultrasonic
testing or radiographic testing, thermographic inspection is safe, nonintrusive and
noncontact, allowing the detection of relatively shallow subsurface defects (a few
millimeters in depth) under large surfaces and in a fast manner)
(1) Passive, in which the features of interest are naturally at a higher or lower temperature
than the background, for example: the surveillance of people on a scene;
(2) Active, in which an energy source is required to produce a thermal contrast between
the feature of interest and the background, for example: an aircraft part with internal
flaws.
1. lock-in (or modulated) thermography and pulsed thermography, which are optical
techniques applied externally;
2. vibrothermography,[14] which uses ultrasonic waves (amplitude modulated or pulses)
to excite internal features.
In vibrothermography, an external mechanical energy source induces a
temperature difference between the defective and non-defective areas of the object.
In this case, the temperature difference is the main factor that causes the emission
of a broad electromagnetic spectrum of infrared radiation, which is not visible to the
human eye.
The locations of the defects can then be detected by infrared cameras through the
process of mapping temperature distribution on the surface of the object
Test equipment
Thermographic camera :
Types of thermography
Use sensors that work by the change of resistance, voltage or current when heated by
infrared radiation
Principle :
Procedure :
Advantages
DISADVANTAGES
Applications:
• Acoustic Emission is unlike most other nondestructive testing (NDT) techniques in two
regards.
• The first difference pertains to the origin of the signal. Instead of supplying energy to the
object under examination, AET simply listens for the energy released by the object.
• the second difference is that AET deals with dynamic processes, or changes, in a
material. This is particularly meaningful because only active features (e.g. crack growth)
are highlighted. The ability to discern between developing and stagnant defects is
significant
KAISER EFFECT:
1. Material emits minute pulses of elastic energy when placed under stress.
2. Once a given load was applied and the acoustic emission from that noise had ceased, no
further emission would occur until the previous stress level was exceeded, even if the
load was removed and later reapplied
3. The acoustic emission (AE) testing method where the material being inspected generates
signals that warn of impending failure.
4. Solid materials emit sonic or ultrasonic acoustic emissions when they are mechanically or
thermally stressed to the point where deformation or fracturing occurs.
5. During plastic deformation, dislocations move through the material’s crystal lattice
structure producing low-amplitude AE signals, which can be measured only over short
distances under laboratory conditions.
PRINCIPLE : The class of phenomena whereby transient elastic waves are generated by
the rapid release of energy from localized sources within a material,, or the transient
elastic waves so generated.
• Acoustic emission may be defined as a transient elastic waves generated by the rapid
release of energy within a material.
• Data acquisition device performs filtration, signals’ parameters evaluation, data analysis
and charting.
• AE Sensors : Purpose of AE sensors is to detect stress waves motion that cause a local
dynamic material displacement and convert this displacement to an electrical signal.
• AE sensors are typically piezoelectric sensors with elements maid of special ceramic
elements like lead zirconate titanate (PZT). Mechanical strain of a piezo element
generates an electric signals.
• Sensors may have internally installed preamplifier (integral sensors). Other types of
sensors include capacitive transducers, laser interferometers.
• Magnets usually used to hold sensors on metal pressure vessels. Grease and oil then used
as a couplant.
Procedure :
Acoustic emission testing works by mounting small sensors onto a component under test.
The sensors convert the stress waves into electrical signals, which are relayed to an
acquisition PC for processing.
The waves are captured when the component is submitted to an external stimulus, such as
high pressures, loads or temperatures.
As the damage grows in the component, there is a greater release of energy.
The rates in which the acoustic emission is detected, the activity, and the intensity of the
acoustic emission, the loudness, are monitored and used for assessing structural integrity
and for health monitoring of components.
Detection AE
Processing of AE Signals
Displaying AEsignals
Locating AE signals
d Bottom of Form
Acoustic emission can be applied to a range of applications and materials. These include:
Structures
Machines
Processes
Advantages :
High sensitivity.
Early and rapid detection of defects, flaws, cracks etc.
Real time monitoring
Cost Reduction
Defective area location: only critical defects provide sustainable Acoustic Emission
sources.
Minimization of plant downtime for inspection, no need for scanning the whole structural
surface.
Minor disturbance of insulation.
Disadvantages:
• It can be used only for surface of concrete.
• Not applicable to know the voids inside.
• The size of defects cannot be quantified and hence conventional NDT methods, eg
ultrasonics, must be used.
• Overpressurisation of the vessel is required and hence some disruption to normal
operation is necessary, but this is much less than is normally required for conventional
inspection