Scribd
Upload
80 views1 page

Q.P. Code: 262941

This document is an exam for a Pharm.D degree program. It contains two sections. Section I has two long-form questions about (a) the components and working principle of a mass spectrometer and deuterium exchange reactions and nuclear Overhauser effect, and (b) the principle and instrumentation of gas chromatography and detectors used in UV-visible spectrophotometers. Section II contains 7 short-form questions about topics like total consumption burners, HPTLC analysis, distinguishing isomers using IR spectroscopy, electrophoresis, X-rays, potentiometric titrations, and thermogravimetric analysis. The exam tests students' knowledge of modern pharmaceutical analytical techniques.

Uploaded by

S Regurathi Pandian
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
80 views1 page

Q.P. Code: 262941

This document is an exam for a Pharm.D degree program. It contains two sections. Section I has two long-form questions about (a) the components and working principle of a mass spectrometer and deuterium exchange reactions and nuclear Overhauser effect, and (b) the principle and instrumentation of gas chromatography and detectors used in UV-visible spectrophotometers. Section II contains 7 short-form questions about topics like total consumption burners, HPTLC analysis, distinguishing isomers using IR spectroscopy, electrophoresis, X-rays, potentiometric titrations, and thermogravimetric analysis. The exam tests students' knowledge of modern pharmaceutical analytical techniques.

Uploaded by

S Regurathi Pandian
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
You are on page 1/ 1

THE TAMIL NADU DR. M.G.R.

MEDICAL UNIVERSITY

[LP 941] NOVEMBER 2019 Sub. Code: 2941

M.PHARM. DEGREE EXAMINATION


(PCI New regulations 2016)
SEMESTER-I
BRANCH II – PHARMACEUTICAL CHEMISTRY  MPC
PAPER I – MODERN PHARMACEUTICAL ANALYTICAL
TECHNIQUES

Q.P. Code : 262941

Time : Three hours Maximum : 75 Marks

I. Elaborate on: (2 x 20 = 40)

1. a) With the help of a neat sketch explain the various components and working
principle of Mass Spectrometer.
b) Give a detail note on deuterium exchange reactions and Nuclear Overhauser
Effect.

2. a) Explain the principle and instrumentation of Gas Chromatography.


b) Describe the various detectors used in UV-Visible spectrophotometer.

II. Write notes on: (7 x 5 = 35)

1. Give the construction, principle and operation of Total consumption burner and
Hollow Cathode Lamp.
2. Explain the steps involved in the analysis of drugs using HPTLC.
3. How can you distinguish between two isomers of molecular formula, C3H6O using
IR Spectroscopy?
4. Define electrophoresis, classify with examples and add a note on gel
electrophoresis.
5. Briefly explain on origin and production of X- rays.
6. Explain the principle and application of potentiometric titrations.
7. Give an account on TG curve and its applications.

*******

You might also like