MS-70 MX-50 MF-50 ML-50: 1WMPD4000477F
MS-70 MX-50 MF-50 ML-50: 1WMPD4000477F
MX-50
MF-50
ML-50
1WMPD4000477F
This manual and Marks
All safety messages are identified by the
following, “WARNING” or “CAUTION”, of
ANSI Z535.4 (American National
Standard Institute: Product Safety Signs
and Labels). The meanings are as
follows:
2. Precautions....................................................................................6
2.1. Installing the Analyzer......................................................................6
2.2. During Use........................................................................................ 7
2.3. After Use and Maintaining the Analyzer................................................8
4. Preparations ................................................................................15
5.1. Installing the Analyzer....................................................................15
5.2. Setting the Clock and Calendar.......................................................16
5.2.1. Operation ............................................................................................ 16
5.3. Proper Operation for Precision Measurement...................................17
5.3.1. Operation of the sample........................................................................ 17
5.3.2. Operation of the analyzer...................................................................... 17
5.3.3. The Glass Fiber Sheets.......................................................................... 18
1. Measurement Procedure...............................................................19
6.1. Standard Mode Operation...................................................................19
6.1.1. ACCURACY.............................................................................................19
6.1.2. Operation ............................................................................................ 19
6.2. Quick Mode Operation........................................................................22
6.2.1. ACCURACY.............................................................................................22
6.2.2. Operation ............................................................................................ 22
6.3. Program Number................................................................................ 25
6.3.1. Storing a Measurement Program to a Program Number...........................25
6.3.2. Recalling a Measurement Program with a Program Number.....................25
2. Measurement Programs...............................................................26
7.1. List of Measurement Programs...........................................................26
7.1.1. ACCURACY of the Standard Mode and Quick Mode.................................27
7.1.2. Analyzing mode of the Automatic Mode.................................................28
7.1.3. Analyzing mode of the Timer Mode........................................................28
7.1.4. Drying Program (Heating Pattern and Drying Temperature).................... 28
7.1.5. Measurement Unit ................................................................................ 29
7.2. Procedures to Store a Measurement Program......................................30
7.2.1. Standard Drying.................................................................................... 30
7.2.2. Ramp Drying......................................................................................... 33
7.2.3. Step Drying........................................................................................... 37
0. Connecting to a Printer...............................................................44
9.1. Print samples.................................................................................. 45
9.1.1. Example To Print The Whole Data At One Time......................................45
9.1.2. Example To Print Selected Items............................................................46
9.1.3. Explanation for Print Item ....................................................................48
9. Connecting to a Computer..........................................................50
10.1. RS-232C Serial Interface...................................................................51
10.2. Output Format................................................................................. 52
10.3. Command........................................................................................ 53
11. Calibration..................................................................................56
12.1. Identification Number (ID No.)..........................................................56
12.1.1. Setting the ID Number........................................................................ 56
12.2. Calibration of the Weighting Sensor..................................................57
12.2.1. Operation ......................................................................................... 57
12.3. Calibration of Drying Temperature (for MS-70 and MX-50)...............59
12.3.1. Operation ......................................................................................... 59
13. Maintenance...............................................................................63
14.1. Cleaning the Heater Unit .................................................................63
14.2. Replacement of the Halogen Lamp...................................................64
14.3. Factory Settings................................................................................ 65
14.3.1. Operation ......................................................................................... 65
14.4. Troubleshooting............................................................................... 66
14.5. Error Message.................................................................................. 67
14. Specifications..............................................................................68
15.1. Dimensions...................................................................................... 69
15.2. Accessories and Peripheral Equipment..............................................70
15. Index..........................................................................................71
A43
Blacklands Way Abingdon
Business Park Abingdon,
Oxfordshire OX14 1DY United
Kingdom Tel: +44 (0)1235
AR eu.net Internet:
http:llwww.aandd-eu.net Vat No:
NI GB 596 1273 15
NG
DCE
o A&D Instruments Ltd. hereby declare that the following weighing product conforms to the requirements of
the council directives on ...
n
Electromagnetic Compatibility (EMC) 89/336/EEC
Standards applicable :
BS EN 61326 Electrical equipment for measurement, control and laboratory use - EMC requirements
BS EN 61010 Safety requirements for electrical equipment for measurement, control and laboratory use. CE Mark First
Takeo Goto
Managing Director
Registered in England No: 2609110 - Registered Office: 24 /26 Blacklands Way Abingdon Oxon 0014 1 ER
Ground the analyzer using the ground terminal of the power cord.
Do not change the setting of the I/II switch on the rear of the analyzer. If the
incorrect setting is used, it may damage the analyzer or cause a fire.
Put correctly
Glass housing
Glass-housing
Hot Hot
Hot
Grips of
heater cover
Halogen lamp
The data memory function can store the results and output all of them at one time.
MS-70 / MX-50 MF-50 ML-50
Maximum number of storable results
100 50 30
The software, "WinCT-Moisture", a standard accessory for the MS-70 and MX-50, has a
function that can make a graph of the change of moisture content in realtime and has an
optimum temperature search program that judges heating at an appropriate temperature
setting.
The software, " WinCT", a standard accessory for the MF-50, is communication
software for transmitting data to a computer using Microsoft Windows.
The
The analyzer is equipped with a serial interface as standard. It can be connected to
a printer or computer.
The analyzer can calibrate the weighing sensor (Use special mass.) and drying
temperature (Use temperature calibrator for MS-70 and MX-50 except MF-50 and
ML-50). The analyzer can output the data required at GLP, GMP and ISO at the
end of the calibration.
The analyzer has a self check function that can detect function errors.
The analyzer displays the current change of moisture content per minute [%/ min]
in real-time. It can be used for the reference to find the analyzing mode.
There is a test sample that is used to check the moisture accuracy. (The test
sample is a part of the standard accessories except for the ML-50)
The glass fiber sheets can be used for quick and precise measurement of a liquid
sample. (The glass fiber sheets are a part of the standard accessories except for
the ML-50)
Heater cover
Grips of heater cover
Disposable
aluminum foil pan
Sample pan
Pan support
Pan handle
Halogen lamp
Power supply
voltage label
RS-232C serial
interface
Power input
Fuse, T6.3A 250V Fuse, T100mA 250V
Caution
Please confirm that the analyzer is correct for your local voltage, receptacle
type and the power cord.
Pan support
Power cord
Pan handle
Dust cover
Test sample
Sodium tartrate dihydrate, 30g
Disposable
CD-ROM aluminum foil pan
Spoon
Tweezers
Spare fuse, T100mA 250V
Spare fuse, T6.3A 250V
Accessory List
O : Standard accessory, - : Accessory by your order.
MS-70 MX-50 MF-50 ML-50
Pan support O O O O
Breeze break ring O O O O
Display cover O O O O
Power cord O O O O
Spare fuse
T100mA 250V O O O O
Spare fuse
T6.3A 250V O O O O
Instruction manual O O O O
Dust cover O O O -
Test sample O O O -
Glass fiber sheets O O O -
Spoon O O O -
Tweezers O O O -
RS-232C serial
interface cable O O - -
Sample pan 20 20 20 10
Pan handle 2 2 2 1
Disposable
aluminum foil pan 100 100 100 100
CD-ROM 1 WinCT-Moisture WinCT-Moisture WinCT -
1: Application software for Windows.
Standard mode
At gram Target quantity of sample [g]
8 Target quantity display Quick mode
Automatic mode Preset termination value [%/min.]
Drying rate At measurement Current drying rate [%/min.]
Measurement unit
% MOIST Moisture content W - D x100
/W/ is based on W W
% MOIST Moisture content (Atro) W - D x100
W/D is based on D D W: Wet sample mass
9 % MOIST D x100 D: Dried sample mass
D/W/ Dry content W
% MOIST W
/W/D Ratio x100 D
g Gram value
Heating pattern #1
Standard drying Maintains a constant Drying
drying temperature. temperature
Ramp drying Increases the drying
10
temperature gently. Drying temperature
Step drying Uses multiple steps of
the drying temperature. Drying temperature
Quick drying Quick mode 200°C
approx. 3min. Drying temperature
RESET Sets the display to zero in the unit of gram. Cancel key.
0. Align the guide hole of the breeze break ring Guide on body
to the guide on the body.
Pan support
0. Install the pan support.
Align together the D signs on the
Sign D on pan support
pan support and body.
Pan handle
Caution
Notch in the rim
For the disposable aluminum foil pan,
place it on the sample pan.
5.2.1. Operation
1. Turn on the analyzer.
The gram unit (of weighing mode) is displayed. 0.000g
2. Press and hold the SELECT key to display Cl adj .
To time Cl adj
4.3.ToPress
skip the ENTER
calendar
keysettings.
to display the calendar. ymd
Example: 15th April,Press
2002the J. or T key to proceed step 5. 02.04.15
Date adjustment
To adjust the calendar settings.
Press SELECT key. Adjust the calendar using the
following keys.
key SELECT Selects a figure.
ymd 02.04.15
J., T key Selects a value for the figure.
ENTER key.........Stores the current date and
proceeds to step 5.
RESET key...........Cancels the adjustment and
proceeds to step 5.
5. Time is displayed.
12:34:56
measurement.
Select the proper Analysis Mode to finish a measurement. Use the change of moisture
content per one minute [%/min] that is displayed during measurement as a reference
value.
The analyzer needs a pre-heating process before measurement. When measuring
samples repeatedly or continuously, the first result is always different from the others.
The pre-heating process is as follows: Put a sample pan, instead of a sample, on the
pan. Press the START key to heat it. The analyzer temperature becomes equilibrium.
Use a sample on the sample pan that has cooled to room temperature. When a sample is
put on a hot sample pan, the moisture content is diffused before measurement, and
precise results are not possible. We recommend you use multiple sample pans.
Do not pile up sample pans during a measurement.
Avoid drift and vibration of air conditioners. It may cause "measurement error" and
"unstable value". In particular, because MS-70 is sensitive instrument, it is
necessary to consider these influences.
When the difference between ambient temperature and sample temperature is
small, it may cause temperature control error.
Example: If the heating temperature is crossed to the range of 30°C and 50°C, it is
affected by an room temperature.
Check the activation of the halogen lamp with the operation indicator.
Example: If low heating temperature is set, the brightness of halogen lamp becomes dark.
Check the activation with
blinking
Sample pan
Procedure (Preparation before heating)
1 Put the glass fiber sheet on the sample pan. Glass fiber sheet
Sample pan
Glass fiber
6.1.1. ACCURACY
ACCURACY of measurement can be set either HI , MID. or LO.
The sample quantity is automatically selected by ACCURACY.
The termination value of the analyzing mode is automatically selected by
ACCURACY and minimum scale value of % display.
The analysis mode is the program to finish the measurement when a change of
moisture content per one minute becomes smaller than a preset termination value.
The settings are as follows: Specify an ACCURACY.
ACCURACY
Model
Minimum scale MID. LO
0.001 % 0.01 %/min 0.02 %/min 0.05 %/min
MS-70 0.01 % 0.02 %/min 0.05 %/min 0.10 %/min
0.1 % 0.10 %/min 0.20 %/min 0.50 %/min
0.01 % 0.02 %/min 0.05 %/min 0.10 %/min
Preset MX-50
0.1 % 0.10 %/min 0.20 %/min
Termination
value 0.05 % 0.05 %/min 0.10 %/min
MF-50 0.1 %
0.50 %/min
1%
0.1 % 0.10 %/min 0.20 %/min
ML-50
1%
Sample quantity 10 g 5g 1g
Use Precise result « Quick measurement
6.1.2. Operation
This operation explanation uses the following example of the MX-50:
Refer to "7.Selection of Measurement Method" for detail.
Input Parameters
Analysis mode....................................Standard mode
Drying temperature............................130 °C
ACCURACY LO
Sample
quantity...............................................Approximately 1 g (Automatic selection)
Analysis mode....................................0.10 %/min (Automatic selection)
Stored Parameters (Factory Settings for the MX-50)
Heating pattern..................................Standard drying ( )
Measurement unit............................... Moisture content is % MOIS
based on a wet sample T /W
Minimum scale value of % display..... 0.01 %
Minimum scale value of gram display 0.001 g
Data memory function........................Not used
Select ACCURACY
3. Press the SELECT key to select ACCURACY. ACCURACY
When ACCURACY is selected, HI , MID. or LO blinks.
Remove sample
17. Press the following key to return to gram display.
ENTER key.....Outputs (Prints) result.
SELECT key ....Returns to the weighing mode.
RESET key.....Returns to the weighing mode and
displays zero.
6.2.2. Operation
This operation explanation uses the following example of the MX-50 :
Refer to "7.Selection of Measurement Method" for detail.
Input Parameters
Analysis mode....................................Quick mode
Heating pattern...................................Quick drying ( , Automatic selection)
Drying temperature............................130 °C
ACCURACY ........................................ LO
Sample quantity.................................Approximately 1 g (Automatic selection)
Analyzing mode..................................0.20 %/min (Automatic selection)
Stored Parameters (Factory Settings for the MX-50)
Measurement unit.............................. Moisture content is % MOIS
based on a wet sample T /W
Minimum scale value of % display..... 0.01 %
Minimum scale value of gram display 0.001 g
Data memory function........................Not used
Select ACCURACY
3. Press the SELECT key to select ACCURACY.
ACCURACY
When ACCURACY is selected, HI , MID. or LO blinks.
Caution
The sample needs to be more than 0.1 g.
Spread the sample evenly.
Close
12. If the key is pressed during gram display, analysis
mode, measurement unit and minimum scale value
are displayed. If the ENTER key is pressed,
sample mass is output.
Caution
Do not press the SELECT key while Analysis time
sampling data.
Caution If the data memory function is active, the data memory number (MEM) is
displayed, in place of the program number (PROG).
end
0. Press the SELECT key to edit the parameters. PROG 2 0.000g
0.000g
2. Press the ¯ or key to select a program number Program number
PROG "2
Measurement Programs
Drying Program
Drying
Analyzing mode to Finish Heating pattern
Temperature
Measurement MX-50
MS-70, MX-50,
ML-50 MS-70 MF-50
MF-50
ML-50
Standard Measurement condition is Standard drying
automatically selected by Standard
Mode Ramp drying
ACCURACY and minimum drying
5td Step drying
value of % display.
When drying rate is less than
Quick Mode preset termination value,
Quick drying
quc measurement is completed
automatically. 30°C 50°C
When drying rate is less to to
Automatic
than preset termination 200°C 200°C
Mode
value, measurement is
U-a completed automatically. Standard drying
Standard
Timer Mode Sample is dried for a preset Ramp drying
drying
U-t time. 1min. to 480min. Step drying
Measurement is completed
Manual Mode
by the STOP key. Max.
U-m 480 min.
Drying rate: Change of moisture content per one minute [%/min]
Standard Mode
ACCURACY
Model Minimum scale MID. LO
0.001 % 0.01 %/min 0.02 %/min 0.05 %/min
MS-70 0.01 % 0.02 %/min 0.05 %/min 0.10 %/min
0.1 % 0.10 %/min 0.20 %/min 0.50 %/min
0.01 % 0.02 %/min 0.05 %/min 0.10 %/min
Preset MX-50
0.1 % 0.10 %/min 0.20 %/min
Termination
value 0.05 % 0.05 %/min 0.10 %/min
MF-50 0.1 %
0.50 %/min
1%
0.10 %/min 0.20 %/min
0.1 %
ML-50
1%
Sample quantity 10 g 5g 1g
Use Precise result « Quick measurement
Quick Mode
ACCURACY
Model Minimum scale MID. LO
0.001 % 0.02 %/min 0.05 %/min 0.05 %/min
MS-70 0.01 % 0.05 %/min 0.10 %/min 0.20 %/min
0.1 % 0.10 %/min 0.20 %/min 0.50 %/min
0.01 % 0.05 %/min 0.10 %/min 0.20 %/min
Preset MX-50
0.1 % 0.10 %/min 0.20 %/min 0.50 %/min
Termination
value 0.05 %
MF-50 0.1 % 0.10 %/min 0.20 %/min 0.50 %/min
1%
0.1 %
ML-50 0.20 %/min 0.50 %/min 1.00 %/min
1%
Sample quantity 5g 2g 1g
Use Precise result « Quick measurement
Temperature Temperature
Ramp drying -
Time Time2Time1
Temperature2 Temperature2
Step drying Temperature1 Temperature1 -
Time Time1 Time2
Stage 1 Stage 2 Stage 1 Stage 2
200°C
Quick drying - - 3 min.
Temperature
"Temperature 1" can be set higher than "temperature 2" in step drying.
ML-50, can select standard drying and quick drying only, does not display heating pattern.
Temperature Time1
Heating pattern
Temperature Temperature2
Ti m e Time2
Heating pattern Heating pattern
Measurement unit
Minimum scale value during measurement . 0.01 %
Minimum scale value of gram display...........0.001 g
Sample quantity.............................................Approximately 5 g
Data memory function...................................Not used
Timer mode
Set the Analysis Time for the Timer Mode Analysis Time
10. Select time with the SELECT key.
Select 10.0 [min] with the J or T key. "1"0."0 0.000
Standard mode
min g
Manual mode
0.000g
Gram display of
weighing mode
This explanation uses the following parameters and sample displays of MX-50.
Common Items
Program number..........................................3 ( PROG 3 )
Drying program Heating pattern...................Ramp drying ( )
Final drying temperature...160°C
Ramp time.........................5.0 minutes
% MOIST
Measurement Unit.........................................Moisture content /W
Minimum scale value during measurement . 0.01 %
Minimum scale value of gram display...........0.001 g
Sample quantity.............................................Approximately 5 g
Data memory function...................................Not used
end
PROG 3 0.000g
Caution If the data memory function is active, the data
memory number (MEM) is displayed in place of the
program number (PROG).
ACCURACY
Set ACCURACY for Standard Mode ACCURACY
0. Select ACCURACY with the SELECT key. MID.
Ramp time
Set the Ramp Time
8. Set 5.0 minutes with the J or T key. 5.0 min nu.nu
nunug
Automatic
mode
Set the Preset Termination Value for Automatic Mode
0. Select preset termination value with the SELECT
Preset termination value "0."0"
key. Select 0.05 [%/min] with the J or T key. 5
Standard mode
Manual mode
Set the Measurement Unit
0. Select measurement unit with the SELECT key.
Select a moisture content (based on a wet Measurement unit "%"M"O"I
"S"T "/"W
sample ) with the J or T key.
.........................................
4 Timer mode (Symbol: U-t
.........................................
Heating pattern................ Ramp drying ( )
Final drying temperature 160°C )%
Ramp time....................... 5.0 minutes
Drying time...................... 10.0 minutes
MOIST /
.............. Moisture content W
Refer to page 33 for
Standard Mode,
Automatic Mode or
Manual Mode
Common Items
Program
number
Analysis
mode
.....................
Drying
program
Measurement
unit
Minimum
scale value
during
measuremen
t ......................................
0.01 %
Minimum
scale value
of gram
display.............................
0.001 g
Sample
quantity...........................
Approximatel
y5g
Data memory
function...........................
Not used
end
PROG 4 0.000g
Select an Analysis Mode
5. Press the SELECT key to select a symbol, it Analysis mode
will blink. Select IJ-E of the timer mode with
the J or T key. (Press these keys to select it) "IJ"-"E nu.nununug
"1"6"0°C
nu.nununug
Set the Ramp Time
8. Set 5.0 minutes with the J or T key. Ramp Time
"5."0 min
1
"1"0."0 min
This explanation uses the following parameters and sample displays of MX-50.
Drying temperature 2
Drying temperature 1
Time
Stage 1 Stage 2
"Temperature 1" can be set higher than "temperature 2" in step drying.
Common Items
Program number 5 ( PROG 5 )
Drying program Heating pattern................. Step drying ( )
Drying temperature 1 .......120°C
Drying temperature 2........160°C
Time.................................. 5.0 minutes
% MOIST /
Measurement Unit Moisture content W
Minimum scale value during measurement . 0.01 %
Minimum scale value of gram display...........0.001 g
Sample quantity.............................................Approximately 5 g
Data memory function...................................Not used
Drying temperature 1
Set Drying Temperature 1
8. Set 120°C to drying temperature 1 with
the J or T key. "1"2"0 1
°C
Automatic
Set the Preset Termination Value for Automatic Mode mod
e
11. Select a preset termination value with the
SELECT key. Select 0.05 [%/min] with Preset termination value "0."0"
the J or T key. Standard mode
5
Manual mode
Drying temperature 2
Drying temperature 1
Time 1 Time 2
Stage 1 Stage 2
"temperature 2" in step drying.
Common Items
Program number............... 6 ( PROG 6 )
Analysis mode Timer mode (Symbol: U-t
Drying program Heating pattern................. Step drying ( )
Drying temperature 1 ....... 160°C
Drying temperature 2........ 120°C )%
Time 1............................... 5.0 minutes
Time 2............................... 10.0 minutes
MOIST
Measurement unit............. Moisture content /W
Minimum scale value during
measurement
................................................................
0.01 %
Minimum scale value of the gram
display
................................................................
0.001 g
Sample quantity
................................................................
Approximately 5 g
Data memory function
................................................................
Not used
key and press the J or
Program number
T key to select a program number.
PROG "6
3. Press the ENTER key to use the number.
Drying Temperature 1
Set Drying Temperature 1
7. Set 120°C with the J or T key.
"1"2"0 1
°C
Set Time 1
8. Select time 1 with the SELECT key.
Time 1
Set 5.0 minutes with the J or T key.
"5."0min
1
Drying Temperature 2
Set Drying Temperature 2
9. Select Drying Temperature 2 with the SELECT key.
Set 160°C with the J or T key.
"1"6"0 2
°C
Set Time 2
10. Select time 2 with the SELECT key.
Time 2
Set 10.0 minutes with the J or T key.
"1"0."0
min 2
Set the Measurement Unit
11. Select measurement unit with the SELECT key.
To cancel the new parameters and return to the
Measurement unit "%"M"O
"I"S"T
SELECT key. "/"W
Caution
Do not put flammable matter near the analyzer.
Do not put anything on the heater cover.
8.1.1. Operation
Caution A hot sample pan may cause an error. Allow the pan to cool before the
next test.
Measurement
1. Enter the following parameters.
Analysis mode.........................................................Standard mode (Symbol: 5td )
2. Pre-heating process.
Put a sample pan, instead of a sample, on the pan. Press the Pre-heating process
START key to heat it. The analyzer temperature becomes
equilibrium.
Connect to RS-232C
interface of the analyzer.
Accessory cable
of AD-8121B
9.1. Print samples
9.1.1. Example To Print The Whole Data At One Time
This example is printed items of "analyzer information", "measurement program",
"measurement data" and "signature space" at one time.
Prepa
Device Parameter Description
Prt 0 1 When pressing the ENTER key, the result is outputted.
Prt 1 Data is outputted after measurement automatically.
Analyzer 5-d 0 1 Result is outputted only.
PO5E 1 1 Approx. two seconds interval in each line.
inFo 1 To print items at one time.
AD-8121B MODE 3 Dump print (Received data is printed as it is)
1: Factory settings
How To Print
Select a parameter to print "Measurement data". Refer to "13. Function Table"
Prt 0 When pressing the ENTER key, the result is outputted.
Prt Data is outputted after measurement automatically.
Print Example
A&D Factory
M O D E L M X .....5 0 Product
S/NP1234567 Serial number Analyzer information
I D L A B .......1 2 3 ID number. 2
PROGRAMNo.1 PROG No.
} MODESTANDARD Analysis mode. Refer to9.1.3
Measurement
} MID.DRYINGSTANDARD
1 6 0 C
Drying program. Refer to 9.1.3 program
UNITMOIST/W Measurement Unit
} Wet weight
} Dried weight
} IGTH4.567gRESULTMOIST/W19
Remarks. Refer to 9.1.3
.57%ANALYSISTIME
2: ID number can be changed. Refer to "12.1. Identification Number (ID No.)"
Prepa
Parameter
Description
prt 0 1
When pressing the ENTER key, the result is outputted.
prt 1 Data is outputted after measurement automatically.
Analyzer 5-d 0 1 Result is outputted only.
pU5e 1 1 Approx. two seconds interval in each line.
info 2 To print specified item.
AD-8121B MODE 3 Dump print (Received data is printed as it is)
1: Factory settings
0.000g
Print
0.000g
INITIALWEIGHT5.432gFINAL
} Wet weight
} Dried weight
WEIGTH
} Measurement Result
Measurement data
4.321g
RESULTMOIST/W
} Analysis time
5.4min
DATE2004/09/30
TIME13:24:57 } Date. Refer to 9.1.3
REMARKS
} Remarks. Refer to 9.1.3
*1: ID number can be changed. Refer to "12.1. Identification Number (ID No.)"
MS-70 / MX-50 / MF-50 / ML-50 47
9.1.3. Explanation for Print Item
"Analyzer information" and "Measurement program"
Analysis Mode A Part of Print and Description
Standard mode
Standard mode MODESTANDARD
ACCURACY
5td HI
HI、 MID. or LO
Quick mode
Quick mode MODEQUICK
HI ACCURACY
quc HI、 MID. or LO
Automatic mode
Automatic mode MODEAUTOMATIC
0.10%/min Analyzing mode to finish
U-a measurement
"Heating pattern"
Heating pattern A Part of Print and Description
Standard drying
Standard drying
DRYINGSTANDARD140C
Drying temperature
Ramp drying
Ramp drying DRYINGRAMP
15.0min110C Final drying temperature
Ramp time
Step drying
DRYINGSTEP
Step drying 8.0min180C Drying temperature of stage 1
95C
Drying temperature of stage 2
Time 1
of stage
Quick drying
Quick drying DRYINGQUICK
130C Drying temperature
:I..... ... ,
W-D x100 % MOIST
Moisture content is based
on W /W
W % RATIO
Ratio 2 x 100
D /W/D
Gram value - g
10. Connecting to a
Computer side D- Computer
Sub 9 pins
Female connector
Inch screw thread
Analyzer side D-
.........................
. . . .Sub
. . ..............
........... . . . 25
Male. . . . pins
.................. .....
.............
connector Metric
screw thread
.......
.... .. .
. ........... ..
.... ...... ......
The MS-70 and MX-50 have the standard accessory software "WinCT-Moisture" for
Windows. It has the function to make graphs of the change of moisture content in realtime
and has an optimum temperature search program that judges heating at an appropriate
.............
temperature setting.. Refer to "English Readme.txt" on the CD-ROM for the details.
The MF-50 has the standard accessory software " WinCT" for Windows. It can
The
transmit data to a computer and can be used to monitor data and to check the
analyz
measurement condition.
er can
be
There is the accessory AX-MX-42 of the software " WinCT" for Windows.
connec
ted to
person
al
compu
ter
using
the
RS-
232C
interfa
50 MS-70 / MX-50 / MF-50 / ML-50
10.1. RS-232C Serial Interface
RS-232C Serial Interface
Transmission system EIA RS-232C
Transmission form Asynchronous, bi-directional, half duplex
Data format Baud rate 2400bps
Data bits 7bits
Parity EVEN
Stop bit 1bit
Code ASCII
Terminator CR LF (CR: 0Dh, LF: 0Ah)
RS-232C
-5 V to -15 V
+5 V to +15 V
Data bits Stop bit
Start bit Parity bit
Pin Connections
Bit format 2.6mm, metric screw thread
MX-50 and MF-50 (DCE) Computer (DTE)
Direction
Pin No. Signal Name 2 Description Signal Name
1 FG Frame ground - FG
2 RXD Receive data ¬ TXD
3 TXD Transmit data ® RXD
4 RTS Ready to send 3 ¬ RTS
5 CTS Clear to send 3 ® CTS
6 DSR Data set ready ® DSR
7 SG Signal ground - SG
16, 18, 19,
Internal use Do not connect
21, 23
Other Not used
1: Normal DOS/V cables do not use these terminals.
2: Signal names of the analyzer side are the same as the DTE side with TXD and RXD
reversed.
3: RTS and CTS control are not used. CTS output is HI always.
10.3. Command
The analyzer can be controlled by the following commands from the
computer.
11.1.1. Preparation
This example selects "store result" at data of the function table.
MEM 0 0.000g
12.1.1. Setting the ID Number 11.1.3. Delete All Data at One Time
1.Turn
1. Display the analyzer.
on the gram unit (of the weighing mode). MEM fUl
0.000
0.000gg
The gram unit (of weighing mode) is displayed. Press and
2. Press and hold the SELECT key to enter the function CL adJ
table. Then CL adJ is displayed.
0. Press the SELECT key to display Id . Id
Press and
2.0. Press
Pressand
the hold the key.
ENTER ENTER key to display out . Clr
out"n"o data
data
4. 3. Press
Press J. or key to display Clr "g"o
thethe SELECT key to display Clr . .
0. Set the ID number using the following keys.
Press ENTER key to enter the mode.
theLab-123
Example:
Clr "g"o data
Clear all SELECT key . Selects a figure. Lab-123
¯, key................Selects a value for the figure.
5. Press the key.
ENTER ENTER keythe
Stores to ID
delete all stored
No. and data.to step 6.
proceeds
Clear data
6. Press the RESET key to return to the weighing mode.
0.000g
56 MS-70 / MX-50 / MF-50 / ML-50
12.2. Calibration of the Weighting Sensor
A standard mass of 20g or 50g can be used for the calibration
A 20g standard mass (AX-MX-41) is recommend.
Caution
Avoid vibration and drafts that affect the calibration. If affected, the analyzer
may be unable to calibrate the weighing sensor.
Use a 20g mass for the calibration, because the height between the weighing
pan and glass-housing is 26 mm. If a tall mass is used, open the glass-housing
and avoid external influence.
12.2.1. Operation
1. Display the gram unit (of the weighing mode). 0.000g
0. Install the weighing pan, pan support and pan handle. Close the
Preparation
heater cover.
1. Press and hold the PROGRAM key to display CH . Press and hold
CH
4. Press the SELECT key to display Cal .
Cal Cal 0 .
5. Press the ENTER key to display
6. If 20g mass is used, .... Press the ENTER key. Cal 0
Proceed to step 8.
If 50g mass is used,..........Press the SELECT key.
Proceed to step 7.
7. Press the ¯ or key to select 50.000g. Press the ENTER key to store it. end , Cal 0
are displayed in order.
end
Standard mass
Remove mass
50.000g
Mass value 20
end
glp
0.000g
Calibration Report Example for the Weighing Sensor Adapted to GLP, GMP and ISO
......Signature
Calibration type
} Calibration mass
58 MS-70 / MX-50 / MF-50 / ML-50
12.3. Calibration of Drying Temperature (for MS-70 and MX-50)
The temperature calibrator (accessory AX-MX-43)
Sensor pan
adjusts the drying temperature on the pan. Put the
sensor on the pan and input measurement data at
100°C and 160°C.
Each adjustment needs fifteen minutes. The buzzer
sounds at the end.
t-Up is displayed after no adjustment for five minutes
during the operation and calibration is stopped. Press
any key to return to weighing mode. Refer to the
instruction manual of the certified temperature
calibrator (accessory AX-MX-43).
Thermometer
12.3.1. Operation
0.000g
Calibration
Report Example
for Temperature
Sensor Adapted
to GLP, GMP and
ISO
Preset the
following
parameters to print
data to AD-8121B
Device Parame
Interval p
Output format
Analyzer
adapted to GLP, o
GMP and ISO
AD-8121B MODE
CALIBRATED . .
TEMPERATUR
ARGETACTU
100C97C
................
100°C
value targe
measureme
1 6 0 C
1 6 2 C
..................
160°C targe
value
..................
measureme
value
SIGNATU
RE
..................
Signature
60 MS-70 /
ML-50
13. Function Table
The function table can store the following parameters to control the analyzer.
Select an Item
3. Select an item using the following keys. Item
Example: Data output mode prt is selected.
SELECT key ....Selects a figure.
prt
ENTER key.........Enters to the selected item. Cl adj
RESET key.........Cancels the operation and
returns to the weighing mode.
¡ prt
"0
New parameter
¡prt "1
ENTER
Cl adj
2. Press the SELECT key to display dp .
dp
1. Press and hold the SELECT key to enter the function table.
14. Maintenance
Caution
Remove power cord before replacement. If the power cord is not removed during
lamp replacement, it may cause receiving an electric shock.
Power cord
Read the power supply voltage label on the back of the heater cover and confirm
Example
that the rated voltage of the halogen lamp is correct for your power supply voltage.
The Rated Voltage of
Voltage Label Accessory number
the Halogen Lamp
100 - 120 V AC 120 V AX-MX-34-120V
200 - 240 V AC 240 V AX-MX-34-240V
Do not drop, throw or crack the halogen lamp. Broken
glass may cause an injury.
Clean the surface of the halogen lamp. If there is a stain
or fingerprint, it may shorten life of the halogen lamp. Do
not touch the lamp directly.
Screw
Dispose of a used halogen lamp that keeps its shape. If it
Screw
is broken, glass may spread and cause injury.
We recommend that you replace the halogen Heater Unit Halogen lamp
lamp, when it exceeds the rated life.
Affix the lamp wire to the hook so that the lamp wire does not touch the
glass-housing and heater cover.
14.3.1. Operation
2.In Case that the Lamp does not Light or it takes Too Long to Reach the Drying Temperature.
The Rated Voltage of
Voltage
Itthe
requires Power
Label six Supply
seconds to Voltage
light the halogen lamp using Accessory number
START key. the Halogen Lamp Halogen lamp
100 - 120 V AC 100 V to AC 120 V AC 120 V AX-MX-34-120V
When the heater cover is opened, power is not
200Vsupplied
- 240 V to AC
the 200V to AC 240 V AC 240 V AX-MX-34-240V
halogen lamp.
Is a fuse
Whenblown? Check has
an overheat the occurred,
fuses after removing
power Power
is not supplied to supply voltage label
the power cord. Check the rated value and
the halogen lamp until the halogen lamp put becomes
new cool. Read rated
fuses into the correct holders. voltage
Check the rated voltage of the halogen lamp that is
Do youprinted
measure a lower
around the drying
holder.temperature after a
high drying temperature? If the lamp is hotter than
Readtemperature,
the drying the power supply voltage label
the measurement canonnot
the back of the heater cover and confirm
that the rated voltage of the halogen lamp is correct for your power supply voltage.
be started.
Check that the sample pan is cool. Fuse, T100mA 250V
Other cases, the halogen lamp may be defective. Fuse, T6.3A 250V
Replace with a new halogen lamp. Refer to "14.2.
Replacement of the Halogen Lamp".
Peripheral equipment
AD-8121B Dot matrix compact printer
Function: Statistical function, interval printing, chart printing,
Character: 5x7 dot, height 2.5mm/01.in., 16 characters/line
Power source: AC adapter or alkaline batteries
adJ ------------------------------------ 61
CL Err ---------------------------------67
Comma-----------------------------------------61 Dust cover--------------------------------------12
Command--------------------------------------53 E --------------------------------------- 67
Continuous measurement------------------17 -E--------------------------------------- 67
CR------------------------------------------------52 Earth terminal --------------------------------15
CTS----------------------------------------------51 ENTER key------------------------------------14
data---------------------------------54, 61 Error0-----------------------------------67
Data bits----------------------------------------51 Error3-----------------------------------67
Data memory----------------------------------54 Error8-----------------------------------67
Data memory function-----------------------61 Error9-----------------------------------67
Data output mode----------------------------61 Factory settings-------------------------------61
Decimal point----------------------------------61 FG------------------------------------------------51
Display------------------------------------------13 FULL -------------------------------54, 67
Display cover----------------------------------12 Fuse-----------------------------------------11, 12
Disposable aluminum foil pan---- 10, 11, 12, Glass fiber sheet------------------------12, 18
15, 69, 70 Glass-housing--------------------7, 11, 12, 64
dmy------------------------------------- 16 gLP----------------------------------57, 60
Dot-----------------------------------------------61 GLP-------------------------------44, 57, 60, 61
dP---------------------------------------61 GMP------------------------------44, 57, 60, 61
Dried sample mass--------------------------29 Gram value------------------------------------29
Dry content-------------------------------------29 Grip-------------------------------------------7, 11
Drying program-----------------------9, 13, 28 Halogen lamp-------6, 9, 11, 12, 15, 64, 66
Drying rate-------------------------------------26 Header------------------------------------------52
Drying temperature------26, 29, 34, 36, 59 Heater cover-----------------------------------11
DSR----------------------------------------------51 HI-------------------------------------- 19, 22, 27
Ht Err-----------------------------------67