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This Study Resource Was: Data Sheet Experiment 3 Synthesis of Potassium Tris (Oxalato) Ferrate (III) Trihydrate

This document summarizes an experiment on the synthesis of potassium tris(oxalato)ferrate(III) trihydrate. The student used 5.0144 grams of Fe(NH4)2(SO4)2.6H2O and obtained 4.9632 grams of K3[Fe(C2O4)3].3H2O. Calculations show the theoretical yield was 6.2879 grams. The percent yield was determined to be 78.93%.

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797 views3 pages

This Study Resource Was: Data Sheet Experiment 3 Synthesis of Potassium Tris (Oxalato) Ferrate (III) Trihydrate

This document summarizes an experiment on the synthesis of potassium tris(oxalato)ferrate(III) trihydrate. The student used 5.0144 grams of Fe(NH4)2(SO4)2.6H2O and obtained 4.9632 grams of K3[Fe(C2O4)3].3H2O. Calculations show the theoretical yield was 6.2879 grams. The percent yield was determined to be 78.93%.

Uploaded by

Solutions Master
Copyright
© © All Rights Reserved
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DATA SHEET

EXPERIMENT 3

Synthesis of Potassium tris(oxalato)ferrate(III) trihydrate

Name : KHAIRIN NABILAH BINTI MOHAMAD


YELSOP
Student ID : 2017404078
Date of Experiment : 8/6/2020

RESULTS

m
e r as
co
1. Mass of Fe(NH4)2(SO4)2.6H2O used = 5.0144 g

eH w
o.
2. Moles of Fe(NH4)2(SO4)2.6H2O used = 0.0128 mol
rs e
3. Mass of K3[Fe(C2O4)3].3H2O obtained = 4.9632 g
ou urc
4. Theoretical yield of K3[Fe(C2O4)3].3H2O (moles) =0.0128 𝑚𝑜𝑙𝑒
o

5. Theoretical yield of K3[Fe(C2O4)3].3H2O (mass) =6.2879 g


aC s
v i y re

6. Percent yield of K3[Fe(C2O4)3].3H2O =78.93%


ed d
ar stu

Calculations

Show all your calculations.


sh is

2. Moles of Fe(NH4)2(SO4)2.6H2O used =


Th

mass
NO. OF MOLES =
RMM
5.0144
=
392.13

= 0.0128 g/mol

https://www.coursehero.com/file/67865065/DATA-SHEET-EXP-36pdf/
4. Mole Fe(NH4)2(SO4)2.6H2O = Fe(OH)3
Mole of Fe(OH)3 =0.0128 g/mol

Mass of K2C2O4=
1 × 1000
= 50 𝑔
20
Mole K2C2O4=
50
= 0.3008 𝑚𝑜𝑙
166.22
Mass of H2C2O4=

m
e r as
0.5 × 1000
= 10 𝑔

co
50

eH w
Mole of H2C2O4=

o.
rs e 10
ou urc
= 0.1111 𝑚𝑜𝑙
90
From the overall equation:
o
aC s

3 mole of K2C2O4≡ 2 mole K3[Fe(C2O4)3].3H2O


v i y re

0.3008
× 2 = 0.2005 𝑚𝑜𝑙𝑒
3
ed d
ar stu

3 mole H2C2O4 ≡ 2 mole K3[Fe(C2O4)3].3H2O


0.1111
sh is

× 2 = 0.0741 𝑚𝑜𝑙𝑒
3
Th

2 mol of Fe(OH)3 ≡ 2 mole K3[Fe(C2O4)3].3H2O


0.0128
× 2 = 0.0128 𝑚𝑜𝑙𝑒
2

The limiting reactant is Fe(OH)3


Therefore, the theoretical mole of K3[Fe(C2O4)3].3H2O = 0.0128 𝑚𝑜𝑙𝑒

https://www.coursehero.com/file/67865065/DATA-SHEET-EXP-36pdf/
5. The theoretical yield of K3[Fe(C2O4)3].3H2O (mass)
0.0128 𝑚𝑜𝑙𝑒 × 491.24 𝑔/𝑚𝑜𝑙 =6.2879 g
6. Percent yield of K3[Fe(C2O4)3].3H2O =

4.9632
× 100% = 78.93%
6.2879

m
e r as
co
eH w
o.
rs e
ou urc
o
aC s
v i y re
ed d
ar stu
sh is
Th

https://www.coursehero.com/file/67865065/DATA-SHEET-EXP-36pdf/

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