IFP Materials PDF
IFP Materials PDF
IFP Materials PDF
10.4 Analyzers
One or more components of a liquid or gaseous mixture were analyzed in
refineries for many years by methods requiring largely human involvement, i.e.
in the chemical laboratory.
The development and increasing implementation of industrial analyzers in
refining units became necessary for the following reasons:
the increasing amounts of raw materials and processed products;
the evolving specifications on finished products;
the different ways of eliminating raw material wastage, particularly by
recycling off specification products;
equipment protection and personnel safety;
environmental protection.
An industrial analyzer is an assembly of instruments composing a mea-
surement sequence that can supply qualitative and quantitative data on:
the total or partial composition of the analyzed sample (gas chro-
matographs, H2/02, CO/CO2, SO, and H,O analyzers);
the physical characteristics of distilled and processed products (distilla-
tion curve, vapor pressure, viscosity, specific gravity, cloud point, flash
point, etc.);
water monitoring (H2S, silica and NH, in water, conductivity, pH, dis-
solved 0,);
monitoring of discharges into the atmosphere (0, and opacity of com-
bustion gases, detecting air pollution);
concentrations in explosive or toxic gases and the presence of fire.
The general functional scheme of an industrial analyzer is represented by
a measurement sequence made up of three blocks as indicated in Figure 10.17:
the sampling system, the analytic unit and the signal processing.
The sampling system takes the sample of the fluid being analyzed, condi-
tions it so that it has the pressure, temperature, cleanness, etc. required for
the analytic unit to operate normally. The objectives of the sampling system
-
I
I ,
I
I I
Figure
10.17 Block diagram o f an industrial anaryzer (After “Analyseurs industriels”).
Chapter 10 CONTROL AND MONITORING 655
Figure
Shutter
Capillary
for pressure
compensation Upstream
chamber
Membrane Radiation
capacitor receiver
Amplifier .
Instrument -0
B
Semi-transparent
mirror +
Comparator filter Sample
z!
source
Figure
10.19 A. Optical analyzer (After “Analyseursindustriels”).B. Block diagram of a UV
analyzer.
658 Chapter 10 CONTROL AND MONITORING
A Sample
I
FFTHpH1 Injection Separation Detection ---- f Signal
Simplified sketch of
electric measurement
circuit for isothermally
operating katharometer
C Sample
It
I
.
1 Furnace
GV
*j I t+-+rq +: E j Direct
I......: output
Programming device
Figure
10.20 A . Block diagram of a chromatograph (After "Analyseursindustriels").
B. Katharometer chromatograph. C. Block diagram of an industrial chromato-
660 Chapter 10 CONTROL AND MONlTORlNG
Interferometer
for FTNlR A
L , Flexible swivel
L ,Scanning
Movement
Prism
Beam to
measurement Beam separator with
cell self-compensation
More recently, near infrared systems (NIR) have been developed. By statis-
tical processing of the whole spectrum, they can give information that is diffi-
cult to access by other methods and can be used for controlling the units.
Today this type of device is utilized to control in-line product blending (gaso-
line, diesel oil) and assure compliance with specifications such as the different
octane numbers, the vapor pressure, the cetane number and the pour point
(Espinosa, 1995).
100%LEL
+ Range measured by exploslmeter
2 5% 5% 15% Methane
I I I I I I I
Figure
10.22 Graph showing the explosiuity range (After “Ana1.yseurs industriels”).
The hazardous explosivity range is located between the end of the LEL and
the beginning of the UEL. The graph in Figure 10.22 illustrates these limits.
There are two types of explosimeters:
Those with platinum filaments mounted in a Wheatstone bridge. One fil-
ament is in a reference cell filled with air and the other in a cell swept by
the gas being monitored.
Those with catalyst coated filaments, similar to the first type but more
robust.
In both cases the measurement is made by a primary detection element
positioned locally and by an electronic module connected by a cable, which
allows input and control of thresholds, testing for proper operation or detec-
tion of line failure.
2. Detectors of toxic gas in the ambient air, or toxicity meters. There are
several types:
electrochemical toxicity meters with liquid and solid electrolytes,
calorimetric toxicity meters,
semi-conductor toxicity meters to detect H,S, with high sensitivity and
miniaturization that make them the most commonly used type of detec-
tor.
Chapter 10 CONTROL AND MONITORING 663
ER
P
f
ER
t I
1 Filter 6 Analyzer ER Cooling water
2 and 4 M i n e filter 7 Circulating pump FI Flow rate indicator
3 Cold heat exchanger 8 Check valve PI Pressure indicator
5 Coalescer TI Temperature indicator
Figure
10.23 Principle o f a sampling loop (After “Analyseurs industriels’y.
664 Chaoter 10. AND MONITORING
CONTROL
The analyzer itself can be installed locally near the sample taking point or
in an analyzer shelter together with other analyzers located nearby. This is the
most widespread set up as it allows easier maintenance and sharing of
resources common to several analyzers (carrier gas, utilities, signal grouping,
etc.).
Error detector
Controlled
Set point parameter
Measurement
Sensor
Figure
10.24 Block diagram of a control loop (After “Instrumentationindustrielle ’9).
10.5.1 Level
Here the level can not remain constant by itself (Fig. 10.25A), since to d o so Q1
would have to be equal to Qz all the time. This is impossible because of dis-
turbances. In addition, since control accuracy can not be absolute there will
always be a small difference between Q1 and QZ.
The level is an integration of this difference,i.e. the following equation:
dh
S - = Q1 - QZ S = tank cross-section
dt
or:
A B
10.5.2 Pressure
A variable steam flow rate Q1 enters a drum B, from which a flow rate QZexits,
that is also variable but lower than Q1. The requirement is to keep the pressure
constant in drum B (Fig. 10.26). Disturbances Q1 and Q2, among others, pre-
vent the pressure from being constant. A pressure controller PC must there-
fore be installed that acts on a valve to let the excess vapor escape (control by
overflow).
Chapter 10 CONTROL AND MONITORING 667
-
Figure
10.26 Pressure control (After “Instrumentation industrielle”).
Figure
10.27 Flow rate control (After “Instrumentation industrielle ’9.
10.5.4 Conclusion
Two extreme attitudes must be avoided:
placing control loops all over even if there are no disturbances,
not placing any control anywhere even if there are disturbances.
It can not be over-emphasized that the existence of disturbances is what
makes control necessary.
I I I
point. In both cases the function of the closed loop is to eliminate the differ-
ence. The schematic in Figure 10.28 shows a closed flow rate loop.
The purpose of this loop is to keep the flow rate at a preset value. The flow
rate measurement sequence (orifice plate + differential pressure transmitter)
transmits the signal to the error module which establishes a correction signal
via the control module (P + I or P + 1 + D). Then the signal is sent to the con-
trol valve. Given the valve safety characteristic (closing with lack of air), if the
measurement increases then the output signal decreases and the controller
works reversely.
The controller can have:
analog or digital technology,
continuous or discontinuous operation,
a PI or PID algorithm.
Secondary or Primary or
slave loop master loop
I A I I
I
Figure
10.29 Cascade loop (After “lnstrumentation industrielle ’3.
Chapter 10. CONTROL AND MONITORING 669
located a long way upstream from the process or when the upstream part of
the process is significantly out of phase. This is obtained by adding a fast loop,
which leads to combining two closed loops, a fast internal one and an external
one. This type of control employs two measurement points, two controllers
and one regulating device. An example is given in Figure 10.29.
The chief advantages of cascade control are the following:
The disturbances located in the internal loop are corrected before reach-
ing the controlled variable.
Dephasing in the upstream part of the process is reduced, resulting in
anticipation and increased speed for the main loop.
The gain variations in the secondary loop are corrected directly.
FE
I Feed
Figure
10.30 Open loop (After “Instrumentationindustrielle’?.
670 Chapter 10 CONTROL AND MONITORING
In the schematic of Figure 10.30 a closed loop controls the heating fluid. If
the temperature became too low at constant feed, the valve would open wide,
while on the contrary the heating fluid should have been adapted to the feed.
In contrast, the open loop reacts in the right way. It adapts the heating fluid
flow rate to the feed variations calculated by the calculation module which
orders the flow rate controller to open or shut the valve in accordance with
feed disturbances.
.
- - - - - - ->- - - - - --
- - -*-Bottom product flow rate
1 Figure
10.3 1 Multi-variable loop (After “lnstrumentation industrielle ’9.
normal operation,
normal shutdown,
degraded operation,
emergency shutdown.
These analyses will allow identification of the technical resources required
for project development. The basic project will rule on the technical feasibil-
ity of the project. On the basis of studies from prior stages, preliminary spec-
ifications will set out precisely the qualities and quantities of equipment
required to develop the automation system. Especially included are the fol-
lowing:
detailled specifications (instrumentation and control system),
installation specifications,
standards to be complied with and specific requirements to the project.
These specifications will permit technical call for tender and instrument
and system selection. At the end of this stage the final decision will be made
whether to proceed to the construction phase.
The construction phase recapitulates the basic project study stages but
with a construction objective. This will require a more or less extensive review
of the basic project allowing a detailed approach to the construction tasks:
detailed automation studies (hardware, software and installation);
purchase, manufacture and installation of instrumentation equipment
and systems;
installation, connection and testing of this equipment;
commissioning.
In order to improve the results of future automation projects, it will be nec-
essary to draft a report concerning:
project development,
quality of equipment and software used,
financial results of the project.
+,&
"="-
Optimization * - a Expert
Operator
assistance
Operating
station
I
Monitoring automatic control
Signaling A ---I
InformLtional
automatic control
Set point
Measurement Action
Informational
I Protection automatic control I and decision-making
automatic control
I Measurement Action I
i' Sensors
PROCESS
Actuators t
Instrumentation
I
Figure
10.32 Control and operating system (After "Automatisationdes s y s t h e s
de production '7.
676 Chaioter 10 CONTROL AND MONITORING
Among the tasks that will be assigned to the control system, two types of
complementary processing can be differentiated as shown schematically in
Figure 10.32:
cyclic deterministic processing (automatic control),
exceptional procedural processing (operator assistance).
Two types of automatic control can be distinguished:
the informational type that performs monitoring tasks without issuing
orders to the process;
the decision-making type that accomplishes reflex automatic protection
and control on the basis of combinatorial, sequential or algorithmic logic
processing.
The reflex automatic control assures control and action sequencing func-
tions that relieve the user of tedious, repetitive tasks while letting him retain
control and decision-making power for critical action. By means of the man-
machine interface, h e can access process data, select the operating mode
(automatic or manual), and manually inhibit or intensify the action performed
by automatic control. He can also modify the sequencing of operations and of
automatic control, start-up and shutdown. Operator assistance is the more or
less complex procedural processing whose time performance will be adapted
to the operator reaction time constant. This processing works by exception
(change of state, threshold exceeded, drift, disturbance) but also for shut-
down and start-up sequences for multi-product processes.
10.8.3 Communications
The DCSs communication networks are its throughways and must meet speci-
fications established with the following criteria:
high speed,
system growth,
distance,
reliability,
openness.
L %D,c 9000 SVSUEM ARGHUUE6TMRE
Host
, ; ;m,
Universal supervision/development
Application
trouble-shooting stations
0 0 0
Gauging
system
,In;rfa1 F!f l
DEC/DPS6
computers
50160
Other
c,
5
P
c
Figure
10.33 Distributed control system (DCS) architecture (Honeywell documentation].
Chapter 10 CONTROL AND MONITORING 679
High speed allows the required data flow to be processed owing to trans-
mission speeds (10 MBits/s), a by exception transmission principle, a multi-
addressing process with identification of all subscribers, etc.
System growth has almost become unlimited due to the possibility of con-
necting secondary networks onto the main one. The secondary networks can
also connect subscribers.
The distance between two subscribers can be several kilometers thanks to
the generalized utilization of fiber-optic cables and general-purpose communi-
cation links such as telephone lines or radio links.
Communication reliability is provided by passive security methods:
the use of reinforced communication cables,
redundant cables laid on two different pathways,
specification of fiber-optic cables which are less sensitive to environ-
mental conditions than coaxial cables.
Reliability is also provided by active security on the validity of transmitted
data (self-verification of messages, self-checking of parity, use of efficient
tested protocols, etc.).
Openness is afforded by the use of gateways that allow connection of a
considerable amount of external equipment:
field networks to communicate with smart transmitters,
programmable logic controllers,
computers,
computer networks such as Ethernet, Decnet, etc.
78 79 80
1 2 3 4
- Programs in "LC" language 159 6o
t 160
Programmable functions (,!;"Qb, e.
x (I group or 1 step of n instructions) per second
5 Internal
fv communication
A
CENTRAL RACK
C e n t r a l Unit I/O modules
6 7 8 9 1 0 1 2 3 4 -1
Is' R A C K * I/O
-31
2"dR A C K I/O
-
#....--....-8 ......................... . .........................
I
4+ 4 4 4 4 J r 4 4 J r
1 IlO module = 16 = 16AI NUM. = 8 low level = 32 low level = 8 analog = 8 ElMP = 32 on/off = 16 on/off
high level analog input analog input analog input output input output
40 active I/O modules p e r simple or redundant CU (in 2 central racks)
~1 8 racks maximumfor redundantcentral units, for redundant HL analog 110 modules and/or remote I/O racks via optical fiber
Figure
Block diagram of a multi-function digital controller (Honeywell documenta-
tion).
The tests and checks listed below are also carried out by the processor t o
promote control strategy integrity:
re-reading of outputs,
loop recording,
default mode of configurable outputs,
alarm management.
This equipment is implemented by configuration of standard functions and
by programming in the “Process Control” oriented language. This allows imple-
mentation of strategies more specific to a manufacturing process and the
printing of targeted production reports.
The communication module has two main functions:
t o manage internal communications between input/output modules and
all the function modules and the internal programs;
t o manage external communications with the networks supporting the
architecture equipment, thereby allowing data t o be exchanged between
the processing interfaces and the user-machine interfaces.
The power supply is generally redundant and generates the different inter-
nal voltages for the processing interfaces a s well as the polarizations for the
sensors/actuators connected to the input/output modules.
(115/230V)
selector for
grid voltage
22
e3
Plug for power
voltage
1 Communication
processor
Peripherical modules
' I
Connector for
extension device
b
5
Switches and LED for modes
1 Programming terminal
(RUNKTOP, remanence)
connector
Figure
10.35 Simplified configuration of a programmable logic controller (Siemens documentation).
684 Chapter 10. CONTROL
AND MONITORING
The electric power supply that generates the different voltages required
by the modules.
The communication modules that allow interaction with a programming
terminal, a printer, a supervisor o r another master o r slave PLC.
The software component contains all the logic (AND, OR, NOT etc.) and
mathematical (addition, counting) instructions generated by different meth-
ods (Eioolean, block diagram, relay, computer, sequential). It is loaded and con-
verted into a “machine” language specific to the PLC by means of the pro-
gramming terminal, a genuine communication tool between the man and the
machine.
InpuV
output
I Timers
image
memory
Chapter 10 CONTROL AND MONITORING 685
The operation of the PLC is governed by the program stored in the “pro-
gram” memory. The internal “program” memory is a RAM (Random Access
Memory) that allows reading and writing, so it can be rapidly modified for
example during start up. It is powered by a back-up battery that allows data to
be preserved in the event of a supply voltage failure. After it is energized, the
central processing unit - in communication with the modules comprising the
PLC architecture via the internal bus (Fig. 10.36) - resets to zero all of the
counters, timers, tests etc. flags and the output memory.
The PLC works cyclically. At the beginning of each cycle the central unit
reads all the input signal statuses and stores them in the input image memory.
This is the input acquisition phase. When the program is being executed, the
central unit uses the values of the image memory. In order to execute the pro-
gram, the central unit “reads” the program memory words in succession start-
ing at the beginning. It executes the program instruction by instruction. If the
program or the momentary status of an input, a test, a timer, etc. indicates that
an output must be at “l”,the central unit stores this information in the output
image memory. At the end of a cycle, the central unit transmits the data from
the output image memory to the output modules; this is called “issuing out-
puts”. Another cycle is then begun: acquiring inputs - processing the pro-
gram - issuing outputs.
.
1I Distributed Control and Supervision System (DCS)
Refinery information
Production control
L Data exchange
system
Supervision
sub-systems
Integration and
supervision of
integrated process
equipment
Product distribution
Compressor monitoring,
Accounting Emergency safety Anti-surge system,
systems Start-up and safety
Motor-operated
Environment valve systems Process monitoring,
Integrated production
units,
Others Furnaces/reactors, etc.
network
I Mechanical
measurement systems
Turbine monitoring,
Supervision and
Analyzers optimization
L
Figure
10.38 Table showing systems integrated into the distributed control system DCS
(Honeywell documentation).
690 ChaDfer 10 AND MONIJORING
CONTROL
References
Bhaly (1988) Boucles de re‘gulation. Editions Kirk.
Cerr M. (1980) Instrumentation industrielle. Technique et Documentation.
DesprCs EM. (1991) Automatisation des systgmes de production. Editions Kirk.
Espinosa A., Lambert D., Valleur M. (1995) Use NIR technology to optimize
plant operations. Hydrocarbon Processing, Febr. 1995.
Groussin J.-C. (1988) Analyseurs industriels. Editions Eyrolles.
Grout M. (1988) Instrumentation. Editions Kirk.
Riout J. (1994) Capteurs industriels. Technologie et me‘thode de choix. Editions
Cetim.
Shiskey F.G. (1967 ) Process Control systems. McGraw-Hill Book Co.
Bouteille et al. (1988) Les automates programmables. Editions Cepadues.
Documentations: Honeywell, Masoneilan, Endress + Hauser, Triconex.