Gas Turbine Blade Superalloy Material Property Handbook PDF
Gas Turbine Blade Superalloy Material Property Handbook PDF
Gas Turbine Blade Superalloy Material Property Handbook PDF
Property Handbook
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Technical Report
11089116
11089116
Gas Turbine Blade Superalloy
Material Property Handbook
1004652
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DISCLAIMER OF WARRANTIES AND LIMITATION OF LIABILITIES
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CITATIONS
Principal Investigators
J. H. Feiger
V. P. Swaminathan
The report is a corporate document that should be cited in the literature in the following manner:
Gas Turbine Blade Superalloy Material Property Handbook, EPRI, Palo Alto, CA: 2001.
1004652.
iii
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REPORT SUMMARY
Published material property data on superalloy bucket (blade) materials used in land-based
combustion turbines is meager and widely scattered in literature. This handbook provides a
comprehensive resource of all available material property data for superalloys used in
combustion turbine buckets. Such data are critical for use in remaining life assessment
calculations, failure analysis, comparison of various alloys, and alloy selection. The material data
presented in this handbook were developed from experimental alloys and actual turbine
components.
Background
Under EPRI direction, Southwest Research Institute (SwRI™) created a material property
database for superalloys used in rotating blades of industrial gas turbines. SwRI consolidated the
material property data from many sources in a computerized relational database. In the early
1990s, dBase IV software was widely used for this purpose, and the subject database was
developed using this software. However, due to rapid changes in software architecture and
variability in computer operating systems, users found it difficult to take full advantage of the
database. EPRI initiated this project to compile and update in a single handbook all available
data for the nickel-base superalloys used in hot section blade applications in land-based gas
turbines.
Objective
To provide combustion turbine (CT) owners with a ready reference handbook of material
property data on superalloy bucket materials.
Approach
Included in the handbook are tables of raw data as well as several plots and tables from the
original database references. Users may scan plots using a digitizer for further processing and
comparative plotting. For each subject alloy, the handbook describes the alloy property
represented, and where available, lists codes for heat treatment, chemical composition,
refurbishment identification, and coating identification. The handbook provides separate tabs for
original database references, chemical composition, and heat treatment details. Rather than
relying on a computerized database, EPRI decided to present all available data in a loose-leaf
notebook format for ease of access, use, and update as new data becomes available.
Results
The superalloy material property handbook provides data for the following alloys—Inconel 700,
Inconel 939, Inconel X-750, Inconel 738, Inconel 738 LC, Inconel 792, MAR-M002, MAR-
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M200, MAR-M247, Nimonic 115, Rene 80, Udimet 500, Udimet 520, Udimet 700, Udimet 710,
Udimet 720, GTD 111 DS, and GTD 111 EA. The handbook cites physical properties such as
density, dynamic and static moduli of elasticity, and coefficient of thermal expansion for each
alloy. It also presents mechanical properties—including tensile, stress rupture, creep, and
thermal-mechanical fatigue properties—as well as high-cycle fatigue, low-cycle fatigue, and
impact strength in graphical and tabular format. Limited data that became available following in-
service degradation of some of the base alloys are included in the handbook. Finally, where
possible, the handbook lists property variation as a function of temperature.
EPRI Perspective
CT owners must make informed decisions about reuse, repair, or replacement of hot section
components. Most often, original equipment manufacturer recommendations are conservative,
allowing valuable, unused remaining life of the components to go untapped due to premature
replacement. CT operators who wish to make remaining life assessments require material
property data. This handbook serves as a one-step ready reference for CT bucket material
properties and is expected to prove valuable in remaining life assessment calculations, alloy
comparisons, and materials selection. The ring binder format permits easy addition of new data,
as they become available. EPRI hopes that in future years, the handbook will be expanded to
include nozzle, combustor, transition piece, and other hot section components.
Keywords
Combustion turbines
Blades
Alloys
Material properties
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In the current competitive and deregulated environment, turbine users are forced to explore ways
of reducing the cost of maintenance and operation of their engines. They need to make informed
decisions about reuse, repair, or replacement of the hot section components. Most often, the
recommendations of the original equipment manufacturers are conservative. Very valuable and
unused remaining life of the components may go untapped when the components are
prematurely replaced. The gas turbine operators with these alloy buckets have a need for the
material data to conduct condition and remaining life assessment of their buckets and to make
independent decisions about their gas turbine components.
Southwest Research Institute (SwRI™) created a material property database for EPRI under
project RP2775-6 for superalloys used in rotating blades of industrial gas turbines. Various
material properties were gathered from many sources and consolidated in a computerized
relational database. In the early 1990’s dBase IV software was widely used for this purpose and
the subject database was created using this software. However, due to rapid changes in the
software architecture and variability in the computer operating systems, users found it difficult to
take full advantage of this database. Thus, EPRI initiated this project to compile and update all
the available data for the nickel base superalloys used in hot section blading application in land-
based gas turbines. Instead of computer software, it was decided to present all of the available
data in a format similar to that used in the Aerospace Structural Metals Handbook for ease of
access and use. Updating of this manual with additional data will be more practical as new data
becomes available.
The database includes physical properties such as density, dynamic and static modulii of
elasticity, and coefficient of thermal expansion. Mechanical properties such as tensile properties,
stress rupture properties, creep properties, impact strength, high-cycle fatigue, low-cycle fatigue
and thermal mechanical fatigue properties are also presented in graphical and tabular format.
Limited data was also available after in-service degradation of some of the base alloys. Property
variation as a function of temperature is presented when available. This database was intended
to provide a good source of data that can be used in remaining life assessment calculations,
comparison of various alloys, and material selection. The material data presented in this
handbook were developed both from experimental alloys and actual turbine components.
Inconel 700, Inconel 939, Inconel X750, Inconel 738, Inconel 738 LC, Inconel 792,
MAR-M002, MAR-M200, MAR-M247, Nimonic 115, Rene 80, Udimet 500, Udimet
520, Udimet 700, Udimet 710, Udimet 720, GTD 111 DS, and GTD 111 EA.
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The data for this handbook was collected, collated and plotted to generate hard copy plots similar
to those published in the Aerospace Structural Metals Handbook. Tables of raw data gathered
whenever available are also printed and included in the manual. Several plots and tables were
directly scanned in from the original references and a new page was created to fit the format of
this handbook. If the user wishes, the plots can be scanned using a digitizer for further
processing and comparative plotting. Each page includes alloy identification, the property
represented, and whenever available, codes for heat treatment, chemical composition,
refurbishment identification, and coating identification. The units on the axes are shown in both
the English and SI units wherever possible. If the plots are directly scanned in from the source,
the units are the same as in the references since no further modifications were made to these
plots. At the end of the handbook, separate tabs are provided for original references, chemical
composition, and heat treatment details.
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CONTENTS
7 MAR-M002........................................................................................................................... 7-1
8 MAR-M200........................................................................................................................... 8-1
9 MAR-M247........................................................................................................................... 9-1
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LIST OF FIGURES
Figure 1-1 Tensile Strength as a Function of Temperature for Inconel 700. ............................ 1-3
Figure 1-2 Tensile Elongation as a Function of Temperature for Inconel 700. ......................... 1-4
Figure 1-3 Larson-Miller Plot for Inconel 700........................................................................... 1-5
Figure 2-1 Tensile Strengths for Inconel 939 at Room Temperature. ...................................... 2-3
Figure 2-2 Tensile Elongation at Room Temperature for Inconel 939...................................... 2-4
Figure 2-3 Reduction in Area (Tensile) at Room Temperature for Inconel 939. ....................... 2-5
Figure 2-4 Tensile Properties of the Alloy as a Function of Temperature. ............................... 2-6
Figure 2-5 Room Temperature Impact Properties After Soakingat Elevated
Temperatures. ................................................................................................................. 2-7
Figure 2-6 Fatigue Crack Growth at R = 0.1 and 0.9 (Room Temperature). ............................ 2-8
Figure 2-7 Elevated Temperature Fatigue Crack Growth at R = 0.3. ....................................... 2-9
Figure 2-8 Elevated Temperature Fatigue Crack Growth at R = 0.1 and 0.3 (Vacuum). ........ 2-10
Figure 2-9 The Stress Rupture Properties at 850°C; Standard Heat Treatment. ................... 2-11
Figure 2-10 The Stress Rupture Properties with Two-Stage Heat Treatment. ....................... 2-12
Figure 2-11 Larson-Miller Plot for Inconel 939....................................................................... 2-13
Figure 2-12 Stress to Rupture vs. Time at Elevated Temperatures. ...................................... 2-14
Figure 2-13 Strain to 1% Creep as a Function of Stress........................................................ 2-15
Figure 2-14 High Cycle Fatigue Properties at 750°C and 850°C. .......................................... 2-16
Figure 2-15 High Cycle Fatigue Properties at 600°C. Results from INCO Europe. ................ 2-17
Figure 2-16 Low Cycle Fatigue Properties of IN939 with Results for IN738LC for
Comparison................................................................................................................... 2-18
Figure 3-1 Specific Heat as a Function of Temperature for Inconel X750................................ 3-3
Figure 3-2 Thermal Conductivity as a Function of Temperature for Inconel X750. .................. 3-4
Figure 3-3 Thermal Expansion as a Function of Temperature................................................. 3-5
Figure 3-4 Yield and Tensile Strengths vs. Temperature for Inconel X750. ............................. 3-6
Figure 3-5 Tensile Elongation vs. Temperature....................................................................... 3-7
Figure 3-6 Dynamic Modulus as a Function of Temperature. .................................................. 3-8
Figure 3-7 100 hr Rupture Strength as a Function of Temperature. ........................................ 3-9
Figure 3-8 Fatigue Crack Growth Behavior at 650°C and 540°C Under Air and Vacuum
Conditions. .................................................................................................................... 3-10
Figure 4-1 Specific Heat as a Function of Temperature. ......................................................... 4-3
Figure 4-2 Thermal Conductivity as a Function of Temperature. ............................................. 4-4
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Figure 4-3 Coefficient of Thermal Expansion as a Function of End Temperature. ................... 4-5
Figure 4-4 Yield and Tensile Strengths as a Function of Temperature. ................................... 4-6
Figure 4-5 Tensile Elongation as a Function of Temperature. ................................................. 4-7
Figure 4-6 Yield and Tensile Strengths as a Function of Temperature. ................................... 4-8
Figure 4-7 Dynamic Modulus as a Function of Temperature. .................................................. 4-9
Figure 4-8 Charpy Impact Energy as a Function of Aging Time............................................. 4-10
Figure 4-9 Charpy Impact Energy as a Function of Aging Temperature. ............................... 4-11
Figure 4-10 Fatigue Crack Growth Behavior at Room Temperature Under Vacuum
Conditions. (Low R). ..................................................................................................... 4-12
Figure 4-11 Fatigue Crack Growth Behavior at R = 0.1 and 0.85 (Room Temperature,
Air). ............................................................................................................................... 4-13
Figure 4-12 Fatigue Crack Growth Behavior at 1562°F. ........................................................ 4-14
Figure 4-13 Fatigue Crack Growth Rate as a Function of ∆K in IN-738 at 927°C in Air
and in Vacuum. ............................................................................................................. 4-15
Figure 4-14 Comparison of Fatigue Crack Growth Rate for Three Alloys. ............................. 4-16
Figure 4-15 Fatigue Crack Growth Rate in Superalloys at 927°C in Vacuum. ....................... 4-17
Figure 4-16 100 hr Rupture Strength as a Function of Temperature. .................................... 4-18
Figure 4-17 1000 hr Rupture Strength as a Function of Temperature.................................... 4-19
Figure 4-18 Larson-Miller Plot for Inconel 738....................................................................... 4-20
Figure 4-19 Stress vs. Rupture Time at Three Elevated Temperatures. ................................ 4-21
Figure 4-20 Stress vs. Strain-Rate at Three Temperatures Including Repeat Runs............... 4-22
Figure 4-21 Multiple Relaxation Runs at 850°C Showing Transient Effects for Low
Stresses. ....................................................................................................................... 4-23
Figure 4-22 Creep Data at 850°C for Various Initial Thermal Treatments.............................. 4-24
Figure 4-23 IN-738 VPS Coated Creep Test Results at 900°C/124 MPa............................... 4-25
Figure 4-24 IN-738 VPS Coated Creep Test Results at 982°C/69 MPa................................. 4-26
Figure 4-25 Strain Rate vs. Stress for IN738LC at 850°C in Tests Containing (i) pp and
pc and (ii) pp and cp. ..................................................................................................... 4-27
Figure 4-26 Influence of Environment on Creep Crack Growth Rate in IN-738 at 927°C
and Comparison with Fatigue Crack Growth Rate Converted to Time Domain. ............. 4-28
Figure 4-27 Total Strain Range vs. Life to Failure. ................................................................ 4-29
Figure 4-28 Total Strain Range vs. Life to Crack Initiation..................................................... 4-30
Figure 4-29 Elastic Strain Range vs. Life to Failure............................................................... 4-31
Figure 4-30 Elastic Strain Range vs. Life to Crack Initiation. ................................................. 4-32
Figure 4-31 Inelastic Strain Range vs. Life to Failure. ........................................................... 4-33
Figure 4-32 Inelastic Strain Range vs. Life to Crack Initiation................................................ 4-34
Figure 4-33 Typical Test Results and Partitioned Strain Ranges........................................... 4-35
Figure 4-34 (HTLCF) Results of IN 738 in the Standard and the Exposed Conditions,
Inelastic Strain Range (∆ε in %) vs. Number of Cycles to Failure (Nf)............................ 4-36
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Figure 4-35 (HTLCF) Results of IN 738 at 1123 K, for the Two Types of Specimens
Tested Under Continuous Strain Cycling and Cycling with Tensile Hold Times,
Inelastic Strain range (∆ε in %) vs. Number of Cycles to Failure (Nf). ............................ 4-37
Figure 4-36 Inelastic Strain Range vs. Cycles to Failure for Cast IN 738 LC (a) pp
components only; 750°C and 850°C, (b) pp and pc components 850°C (c) pp and
cp components; 850°C. ................................................................................................. 4-38
Figure 4-37 Inelastic Strain Range vs. Cycles to Failure for Cast IN 738 at 870°C. ............... 4-39
Figure 4-38 Inelastic Strain Range vs. Cycles to Failure for Cast IN 738 at 870°C, pp and
cp components. ............................................................................................................. 4-40
Figure 4-39 Inelastic Strain Range vs. Cycles to Failure for Cast IN 738 at 870°C, pp and
pc components. ............................................................................................................. 4-41
Figure 4-40 Low Cycle Fatigue at 1600°F with Three Hold Times Investigated (Total
Strain Range). ............................................................................................................... 4-42
Figure 5-1 Tensile Strengths as a Function of Temperature.................................................... 5-3
Figure 5-2 Tensile Elongation as a Function of Temperature. ................................................. 5-4
Figure 5-3 Reduction in Area (Tensile) as a Function of Temperature..................................... 5-5
Figure 5-4 Impact Resistance of IN-738 at Room Temperature and 900°C as a Function
of Aging Time at 950°C. .................................................................................................. 5-6
Figure 5-5 Loss of High Temperature Impact Resistance Correlation in Terms of a Time-
Temperature Parameter Analogous to that of Larson-Miller............................................. 5-7
Figure 5-6 Fatigue Crack Growth Behavior at R = 0 (Room Temperature, Lab Air
Conditions). ..................................................................................................................... 5-8
Figure 5-7 Fatigue Crack Growth Behavior at 1382°F at R = 0.1 (Lab Air). ............................. 5-9
Figure 5-8 Fatigue Crack Growth Behavior at 1562°F for R = 0.25 and 0.3 (Lab Air). ........... 5-10
Figure 5-9 Crack Growth for Nimocast 738 LC and 739 at Cyclic Frequencies Between
60 and 100 Hz and R = 0.1; δ is Crack Tip Opening Displacement................................ 5-11
Figure 5-10 Influence of Environment on Fatigue Crack Growth of Nimocast 738 LC and
739 at 850°C and Cyclic Frequencies Between 10 and 100 Hz and R = 0.1.................. 5-12
Figure 5-11 Larson-Miller Plot for Inconel 738 LC. ................................................................ 5-13
Figure 5-12 Larson-Miller Plot at Two Test Temperatures (Light Oil Conditions)................... 5-14
Figure 5-13 Stress vs. Rupture Time at Two Elevated Temperatures (Light Oil
Conditions). ................................................................................................................... 5-15
Figure 5-14 Larson-Miller Plot (P = T (20 + log t f) x 10-3, where T is in K and tf in hr) of
Cast and Hipped IN-738LC Turbine Blades Showing Unexposed and Service
Exposed Creep-Rupture Properties............................................................................... 5-16
Figure 5-15 Dependence of the Time to Rupture on the Minimum Creep Rate, for IN-
738LC (Monkman-Grant Relationship). ......................................................................... 5-17
Figure 5-16 Dependence of Primary Plus Secondary, Creep Life on the Minimum Creep
Rate for Cast IN-738LC. ................................................................................................ 5-18
Figure 5-17 Time to Rupture Dependence on the Tertiary Life for Cast IN-738LC................. 5-19
Figure 5-18 Low Cycle Fatigue at 1699°F (Total Strain Range). ........................................... 5-20
Figure 5-19 Low Cycle Fatigue Behavior at Two Elevated Temperatures (Total Strain
Range). ......................................................................................................................... 5-21
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Figure 5-20 Low Cycle Initiation and Failure at Four Elevated Temperatures........................ 5-22
Figure 5-21 Strain-Amplitude-Life Relations for IN738LC at 650°C as an Effect of
Casting Process. ........................................................................................................... 5-23
Figure 5-22 Strain-Amplitude-Life Relations for IN738LC at 650°C as an Effect of
Casting Process. ........................................................................................................... 5-24
Figure 5-23 Stress vs. Reversals of IN738LC at 650°C (1202°F) as an Effect of Casting
Process. ........................................................................................................................ 5-25
Figure 5-24 Strain-Amplitude-Life Relations for IN738LC at 850°C as an Effect of
Casting Process. ........................................................................................................... 5-26
Figure 5-25 Stress vs. Reversals of IN738LC at 850°C (1532°F) as an Effect of Casting
Process. ........................................................................................................................ 5-27
Figure 5-26 Strain-Amplitude-Life Relations for IN738LC at 850°C as an Effect of
Casting Process. ........................................................................................................... 5-28
Figure 5-27 Low Cycle Fatigue Behavior for Inconel 738 LC................................................. 5-29
Figure 5-28 Thermal-Mechanical Fatigue Behavior of Inconel 738 LC. ................................. 5-30
Figure 6-1 Tensile Strengths as a Function of Temperature.................................................... 6-3
Figure 6-2 Tensile Elongation as a Function of Temperature. ................................................. 6-4
Figure 6-3 Fatigue Crack Growth Rate as a Function of ∆K in IN-792 at 927°C in Air and
in Vacuum. ...................................................................................................................... 6-5
Figure 6-4 Comparison of Fatigue Crack Growth Rate in Terms for Three Alloys.................... 6-6
Figure 6-5 Fatigue Crack Growth Rate in Superalloys at 927°C in Vacuum. ........................... 6-7
Figure 6-6 100 hr Rupture Strength as a Function of Temperature. ........................................ 6-8
Figure 6-7 1000 hr Rupture Strength as a Function of Temperature. ...................................... 6-9
Figure 6-8 Larson-Miller Plot for Inconel 792......................................................................... 6-10
Figure 6-9 Influence of Environment on Creep Crack Growth Rate in IN-792 at 927°C
and Comparison with Fatigue Crack Growth Rate (Fatigue Crack Growth Rate
Given on a Time Basis). ................................................................................................ 6-11
Figure 7-1 Influence of R on Crack Growth in Directionally Solidified and Single Crystal
Materials at 950°C and a Frequency of 0.1 Hz. ............................................................... 7-3
Figure 7-2 Influence of Grain Structure and R on Crack Growth at 950°C and a
Frequency of 20 Hz. ........................................................................................................ 7-4
Figure 7-3 Effect of Frequency on Crack Growth in Directionally Solidified Alloy at 950°C
and R = 0.1...................................................................................................................... 7-5
Figure 7-4 Effect of Temperature on Crack Growth/Cycle in Directionally Solidified and
Single Crystal Materials at a Frequency of 0.1 Hz and R = 0.1. ....................................... 7-6
Figure 7-5 Effect of Prior Creep Damage on Crack Growth in Directionally Solidified and
Single Crystal Material at 950°C at a Frequency of 20 Hz and R = 0.7. ........................... 7-7
Figure 7-6 Effect of R on Crack Growth Per Cycle in the Threshold Region at 950°C. ............ 7-8
Figure 7-7 Effect of Prior Creep Damage on Crack Growth Per Cycle at 950°C for R =
0.9. .................................................................................................................................. 7-9
Figure 7-8 Crack Growth for MAR-M002 at Cyclic Frequency of 0.25 Hz and R = 0.1........... 7-10
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Figure 7-9 Influence of R on Crack Growth Rate for MAR-M002 at 950°C and 20 Hz,
da/dN versus ∆K............................................................................................................ 7-11
Figure 7-10 Influence of R on Crack Growth Rate for MAR-M002 at 950°C and 20 Hz,
da/dt versus Kmax. ........................................................................................................... 7-12
Figure 7-11 Influence of Grain Structure and Temperature on Creep Crack Growth Rate. .... 7-13
Figure 7-12 Effect of Prior Creep Damage on Creep Crack Growth Rate at 950°C in
Directionally Solidified Material...................................................................................... 7-14
Figure 7-13 Accumulation of Creep Strain at 950°C and a Stress of 256 MPa in
Directionally Solidified and Single Crystal Material. ....................................................... 7-15
Figure 8-1 Comparison of Crack Growth Rates of MAR-M200 Single Crystals at 25 and
982°C. (∆Keff is a Function of Three Nodes of Cracking.) ................................................ 8-3
Figure 8-2 Fatigue Crack Growth Rate Results of MAR-M200 Single Crystals Under
Uniaxially Applied Cyclic Loading at 982°C. (∆Keff is a Function of Three Nodes of
Cracking.)........................................................................................................................ 8-4
Figure 8-3 Comparison of Theoretical and Experimental Thermal Fatigue Lives of MAR
M200 and MAR M200DS Double Wedges (0.6 and 1.0 mm Radius Edge, Heating
and Cooling in Fluidized Beds at 320 and 1090°C).......................................................... 8-5
Figure 9-1 Prediction of Isothermal Fatigue Data at 500°C...................................................... 9-3
Figure 9-2 Prediction of 871°C Isothermal Fatigue Test Results. ............................................ 9-4
Figure 9-3 Prediction of Out-of-Phase TMF (500°C–871°C) Test Results. .............................. 9-5
Figure 9-4 Prediction of In-Phase TMF (500°C–871°C) Test Results. ..................................... 9-6
Figure 9-5 Prediction of Diamond Shape (Nonproportional) Strain-Temperature History......... 9-7
Figure 9-6 Mechanical Strain Range Versus Life for Out-of-Phase and In-Phase TMF
Experiments, = 5 x 10-5 s-1 .............................................................................................. 9-8
Figure 10-1 Thermal Conductivity as a Function of Temperature. ......................................... 10-3
Figure 10-2 Coefficient of Thermal Expansion as a Function of Temperature. ...................... 10-4
Figure 10-3 Tensile Strengths as a Function of Temperature................................................ 10-5
Figure 10-4 Tensile Elongation as a Function of Temperature. ............................................. 10-6
Figure 10-5 Dynamic Modulus as a Function of Temperature. .............................................. 10-7
Figure 10-6 100 hr Rupture Strength as a Function of Temperature. .................................... 10-8
Figure 10-7 1000 hr Rupture Strength as a Function of Temperature.................................... 10-9
Figure 10-8 Partial Larson-Miller Plot for Nimonic 115. ....................................................... 10-10
Figure 11-1 Temperature Dependence of Yield Strength (σy) of Unused and Used
Coatings and Substrates in Comparison with Tensile Test Data of Unused
Substrate....................................................................................................................... 11-3
Figure 11-2 Temperature Dependence of Ductility (ε f) Obtained from SP Tests on
Unused and Used Coatings and Substrates, Compared with Tensile Test Data of
Unused Substrate.......................................................................................................... 11-4
Figure 11-3 Temperature Dependence of Strength and Ductility of the Rene 80 Alloy
Specimens. ................................................................................................................... 11-5
Figure 11-4 Fatigue Crack Growth Rate as a Function of ∆K in Rene 80 at 927°C in Air
and in Vacuum. ............................................................................................................. 11-6
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Figure 11-5 Comparison of Fatigue Crack Growth Rate for Three Alloys. ............................. 11-7
Figure 11-6 Fatigue Crack Growth Rate in Superalloys at 927°C in Vacuum. ....................... 11-8
Figure 11-7 Influence of Environment on Creep Crack Growth Rate in Rene 80 at 927°C
and Comparison with Fatigue Crack Growth Rate. (Fatigue Crack Growth Rate
Give on a Time Basis.) .................................................................................................. 11-9
Figure 11-8 A Larson Miller Plot Comparing the GTD111 Alloy Test Points with Rene 80
Data from the Literature and the GTD111 Larson Miller Curve Published by General
Electric. ....................................................................................................................... 11-10
Figure 12-1 Thermal Conductivity as a Function of Temperature. ......................................... 12-3
Figure 12-2 Coefficient of Thermal Expansion as a Function of Final Temperature............... 12-4
Figure 12-3 Tensile Strengths as a Function of Temperature................................................ 12-5
Figure 12-4 Tensile Elongation as a Function of Temperature. ............................................. 12-6
Figure 12-5 Dynamic Modulus as a Function of Temperature. .............................................. 12-7
Figure 12-6 100 hr Rupture Strength as a Function of Temperature. .................................... 12-8
Figure 12-7 1000 hr Rupture Strength as a Function of Temperature.................................... 12-9
Figure 12-8 Larson-Miller Plot for Udimet 500. .................................................................... 12-10
Figure 13-1 Tensile Strengths as a Function of Temperature................................................ 13-3
Figure 13-2 Tensile Elongation as a Function of Temperature. ............................................. 13-4
Figure 13-3 100 hr Rupture Strength as a Function of Temperature. .................................... 13-5
Figure 13-4 1000 hr Rupture Strength as a Function of Temperature.................................... 13-6
Figure 13-5 Larson-Miller Plot for Udimet 520. ...................................................................... 13-7
Figure 14-1 Specific Heat as a Function of Temperature....................................................... 14-3
Figure 14-2 Thermal Conductivity as a Function of Temperature. ......................................... 14-4
Figure 14-3 Coefficient of Thermal Expansion as a Function of Temperature. ...................... 14-5
Figure 14-4 Tensile Strengths as a Function of Temperature................................................ 14-6
Figure 14-5 Tensile Elongation as a Function of Temperature. ............................................. 14-7
Figure 14-6 Dynamic Modulus as a Function of Temperature. .............................................. 14-8
Figure 14-7 Fatigue Crack Growth Behavior at R = 0, 0.05, 0.24, and 0.53 (Lab Air,
Room Temperature). ..................................................................................................... 14-9
Figure 14-8 Fatigue Crack Growth Behavior Under Vacuum Conditions (Room
Temperature)............................................................................................................... 14-10
Figure 14-9 Elevated Temperature Fatigue Crack Growth Behavior at R = 0. ..................... 14-11
Figure 14-10 Elevated Fatigue Crack Growth Behavior Under Vacuum Conditions............. 14-12
Figure 14-11 Crack Growth for Udimet 700 at 850°C, R = 0.05, and Cyclic Frequency of
0.17 Hz........................................................................................................................ 14-13
Figure 14-12 The Effect of the Environment on the Creep Crack Growth in Udimet 700 at
Ì
850°C: o , 14.2 kN, vacuum, batch 2; , 16.0 kN, vacuum, batch 2; —— air, batch
1; ——, air, batch 2. .................................................................................................... 14-14
Figure 14-13 100 hr Rupture Strength as a Function of Temperature.................................. 14-15
Figure 14-14 1000 hr Rupture Strength as a Function of Temperature................................ 14-16
xvi
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EPRI Licensed Material
xvii
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EPRI Licensed Material
Figure 16-18 Relationship Between Strain Range and Number of Cycles to Failure
Obtained During the Low Cycle Fatigue Testing of Udimet 710 and Coated and
Uncoated Udimet 720 at 1350°F (732°C) at 1 cpm...................................................... 16-20
Figure 16-19 Relationship Between the Strain Range Components and Number of
Cycles to Failure Obtained During the Low Cycle Fatigue Testing of Udimet 720 at
1350°F (732°C) as a Function of Hold Time and Test Environment............................. 16-21
Figure 16-20 Relationship Between the Strain Range Components and Number of
Cycles to Failure Obtained During the Low Cycle Fatigue Testing of RT-22 Coated
Udimet 720 at 1350°F (732°C) at 1 cpm as a Function of Hold Time and Test
Environment. ............................................................................................................... 16-22
Figure 16-21 Low-Cycle Fatigue Results for Udimet 720 at 1350°F (732°C) and 1 cpm...... 16-23
Figure 16-22 Low-Cycle Fatigue Results for RT-22 Coated Udimet 720 Tested at 1350°F
(732°C) and 1 cpm. ..................................................................................................... 16-24
Figure 17-1 Tensile Properties and Hardness in the Service Aged Condition........................ 17-3
Figure 17-2 Tensile and Hardness Properties after Refurbishment. ...................................... 17-4
Figure 17-3 Bucket to Bucket Variation of Yield and Tensile Strengths of GTD-111 DS
(Undegraded). ............................................................................................................... 17-5
Figure 17-4 Bucket to Bucket Variation of Percent Elongation and Reduction of Area
(Undegraded). ............................................................................................................... 17-6
Figure 17-5 Variation of Yield Strength of the Longitudinal and Transverse Specimens........ 17-7
Figure 17-6 Variation of Tensile Strength for the Longitudinal and Transverse
Specimens. ................................................................................................................... 17-8
Figure 17-7 Variation of Tensile Ductility of Longitudinal and Transverse Specimens as a
Function of Temperature. .............................................................................................. 17-9
Figure 17-8 Airfoil Stress Rupture Data for IN-738, GTD-111EA and GTD-111DS Alloys
Before and After Rejuvenation..................................................................................... 17-10
Figure 17-9 Iso-Stress Creep Rupture Data of Longitudinal Specimens Machined from
the Shank Section (Unaged)........................................................................................ 17-11
Figure 17-10 Iso-Stress Creep Rupture Data of Transverse Specimens Machined from
the Shank Section. ...................................................................................................... 17-12
Figure 17-11 LMP Plot of GTD-111 DS and IN-738 LC Creep Data. ................................... 17-13
Figure 17-12 Larson-Miller Plot of Longitudinal Shank (Undegraded) Creep Data............... 17-14
Figure 17-13 LMP Plot of Transverse Specimen Data from Undegraded Shank Location. .. 17-15
Figure 17-14 Influence of Specimen Orientation on Creep Rupture Strength of Unaged
(Shank) Material. ......................................................................................................... 17-16
Figure 18-1 Tensile Properties and Hardness in the Service Aged Condition........................ 18-3
Figure 18-2 Tensile and Hardness Properties after Refurbishment. ...................................... 18-4
Figure 18-3 Tensile Strengths as a Function of Temperature................................................ 18-5
Figure 18-4 Tensile Strengths as a Function of Temperature................................................ 18-6
Figure 18-5 Tensile Properties for Root and Airfoil Material at 70°F and 1600°F................... 18-7
Figure 18-6 Tensile Properties for Root and Airfoil Material at 70°F and 1600°F................... 18-8
Figure 18-7 Tensile Elongation as a Function of Temperature. ............................................. 18-9
xviii
11089116
EPRI Licensed Material
Figure 18-8 Tensile Elongation and Reduction in Area as a Function of Temperature. ....... 18-10
Figure 18-9 Stress vs. Rupture Time for Two Material Conditions....................................... 18-11
Figure 18-10 Stress-Rupture Results for Root and Airfoil Material. ..................................... 18-12
Figure 18-11 Stress-Rupture Data for GTD-111 EA and DS Compared to IN-738............... 18-13
Figure 18-12 Stress-Rupture Results for Root and Airfoil Material. ..................................... 18-14
Figure 18-13 Larson-Miller Plot of GTD-111 EA (Standard Heat Treat and Thermally
Exposed). .................................................................................................................... 18-15
Figure 18-14 Larson-Miller Plot for GTD-111 EA................................................................. 18-16
Figure 18-15 Larson-Miller Plot for GTD-111 for Different Exposure Conditions.................. 18-17
Figure 18-16 Larson-Miller Plot for GTD-111 EA................................................................. 18-18
Figure 18-17 A Larson Miller Plot Comparing the GTD111 Alloy Test Points with Rene
80 Data from the Literature and the GTD111 Larson Miller Curve Published by
General Electric........................................................................................................... 18-19
Figure 18-18 A Least Squares Regression Model (Y = β 0 + β 1 X + e ) Fitted to the
GTD111 Creep Rupture Data Illustrating the Fit. The 95% Confidence Intervals
About the Mean and the 95% Prediction Interval for an Individual Observation. Test
Data from the Thermally Exposed GTD111 Material and Select Service Exposed
GTD111 Data Points are Plotted. ................................................................................ 18-20
Figure 18-19 A Plot of Percent Creep Deformation (Strain) Versus Time for the Creep
Rupture Samples in the Standard Heat Treated Condition and After Thermal
Exposures at 816°C and 899°C................................................................................... 18-21
Figure 18-20 A Plot of Percent Creep Deformation (Strain) Versus Time for the Creep
Rupture Samples in the Standard Heat Treated Condition and After Thermal
Exposures at 816°C and 899°C................................................................................... 18-22
Figure 18-21 A Plot of Percent Creep Deformation (Strain) Versus Time for the Creep
Rupture Samples in the Standard Heat Treated Condition and After Thermal
Exposures at 816°C and 899°C................................................................................... 18-23
Figure 18-22 A Plot of Percent Creep Deformation (Strain) Versus Time for the Creep
Rupture Samples in the Standard Heat Treated Condition and After Thermal
Exposures at 816°C and 899°C................................................................................... 18-24
Figure 18-23 A Plot of Percent Creep Deformation (Strain) Versus Time for the Creep
Rupture Samples in the Standard Heat Treated Condition and After Thermal
Exposures at 816°C and 899°C................................................................................... 18-25
xix
11089116
11089116
EPRI Licensed Material
1
INCONEL 700
1-1
11089116
EPRI Licensed Material
Inconel 700
1-2
11089116
EPRI Licensed Material
Inconel 700
160 1100
1000
strength (MPa)
140
strength (ksi)
900
120
800
100 700
600
80
500
60 400
40 300
200
20 Inconel 700 100
test environment: air
0 0
0 300 600 900 1200 1500 1800 2100
Page 1 of 3
Figure 1-1
Tensile Strength as a Function of Temperature for Inconel 700.
1-3
11089116
EPRI Licensed Material
Inconel 700
35
30
% elongation
25
20
15
10
0
0 400 800 1200 1600 2000
Page 2 of 3
Figure 1-2
Tensile Elongation as a Function of Temperature for Inconel 700.
1-4
11089116
EPRI Licensed Material
Inconel 700
1000
stress (MPa)
stress (ksi)
1000
100
LMP (°R-hr)
(460+°F)(C+log t)
Page 3 of 3
Figure 1-3
Larson-Miller Plot for Inconel 700.
1-5
11089116
11089116
EPRI Licensed Material
2
INCONEL 939
2-1
11089116
EPRI Licensed Material
Inconel 939
2-2
11089116
EPRI Licensed Material
Inconel 939
180
1200
160
1000
strength (MPa)
140
strength (ksi)
120
800
100
600
80
60 400
40
200
20 Inconel 939
test environment: air
0 0
50 60 70 80 90 100
Page 1 of 16
Figure 2-1
Tensile Strengths for Inconel 939 at Room Temperature.
2-3
11089116
EPRI Licensed Material
Inconel 939
12.5
10.0
% elongation
7.5
5.0
2.5
0.0
50 60 70 80 90 100
Page 2 of 16
Figure 2-2
Tensile Elongation at Room Temperature for Inconel 939.
2-4
11089116
EPRI Licensed Material
Inconel 939
20
reduction in area (%)
15
10
0
50 60 70 80 90 100
Page 3 of 16
Figure 2-3
Reduction in Area (Tensile) at Room Temperature for Inconel 939.
2-5
11089116
EPRI Licensed Material
Inconel 939
Page 4 of 16
Figure 2-4
Tensile Properties of the Alloy as a Function of Temperature.
2-6
11089116
EPRI Licensed Material
Inconel 939
Page 5 of 16
Figure 2-5
Room Temperature Impact Properties After Soakingat Elevated Temperatures.
2-7
11089116
EPRI Licensed Material
Inconel 939
∆K (MPa√m)
10 100
10-4
Inconel 939
test temperature: 75°F (24°C) 10-3
test environment: air
10-5
10-4
10-6
da/dN (mm/cycle)
da/dN (in/cycle)
10-5
10-7
10-6
10-8
10-7
10-9
R= 0.1 10-8
R= 0.9
10-10
10 100
∆K (ksi√in)
Page 6 of 16
Figure 2-6
Fatigue Crack Growth at R = 0.1 and 0.9 (Room Temperature).
2-8
11089116
EPRI Licensed Material
Inconel 939
∆K (MPa√m)
10 100
10-3
Inconel 939
test temperature: 1562°F (850°C) 10-2
test environment: air
10-4
10-3
10-5
da/dN (mm/cycle)
da/dN (in/cycle)
10-4
10-6
10-5
10-7
10-6
10-8
10-7
R= 0.3
10-9
10 100
∆K (ksi√in)
Page 7 of 16
Figure 2-7
Elevated Temperature Fatigue Crack Growth at R = 0.3.
2-9
11089116
EPRI Licensed Material
Inconel 939
∆K (MPa√m)
10 100
10-3
Inconel 939
test temperature: 1562°F (850°C) 10-2
test environment: vacuum
10-4
10-3
da/dN (mm/cycle)
10-5
da/dN (in/cycle)
10-4
10-6
10-5
10-7
10-6
10-8
R= 0.1 10-7
R= 0.3
10-9
10 100
∆K (ksi√in)
Page 8 of 16
Figure 2-8
Elevated Temperature Fatigue Crack Growth at R = 0.1 and 0.3 (Vacuum).
2-10
11089116
EPRI Licensed Material
Inconel 939
Page 9 of 16
Figure 2-9
The Stress Rupture Properties at 850°C; Standard Heat Treatment.
2-11
11089116
EPRI Licensed Material
Inconel 939
Page 10 of 16
Figure 2-10
The Stress Rupture Properties with Two-Stage Heat Treatment.
2-12
11089116
EPRI Licensed Material
Inconel 939
LMP (K-hr)
(T(K))(C + log tr)
20 22 24 26 28
1000
100
stress (MPa)
stress (ksi)
100
10
Inconel 939
test environment: air
36 38 40 42 44 46 48 50 52 54
LMP (°R-hr)
(460+°F)(C + log tr)
Page 11 of 16
Figure 2-11
Larson-Miller Plot for Inconel 939.
2-13
11089116
EPRI Licensed Material
Inconel 939
1000
1292 °F (700 °C) 6500
900 1400 °F (760 °C)
1500 °F (816 °C) 6000
1600 °F (870 °C)
800 5500
1650 °F (900 °C)
1700 °F (927 °C) 5000
700
4500
stress (MPa)
stress (ksi)
600
4000
500 3500
3000
400
2500
300 2000
1500
200
1000
100
Inconel 939 500
test environment: air
0 0
101 102 103 104
Page 12 of 16
Figure 2-12
Stress to Rupture vs. Time at Elevated Temperatures.
2-14
11089116
EPRI Licensed Material
Inconel 939
Page 13 of 16
Figure 2-13
Strain to 1% Creep as a Function of Stress.
2-15
11089116
EPRI Licensed Material
Inconel 939
Page 14 of 16
Figure 2-14
High Cycle Fatigue Properties at 750°C and 850°C.
2-16
11089116
EPRI Licensed Material
Inconel 939
Page 15 of 16
Figure 2-15
High Cycle Fatigue Properties at 600°C. Results from INCO Europe.
2-17
11089116
EPRI Licensed Material
Inconel 939
Page 16 of 16
Figure 2-16
Low Cycle Fatigue Properties of IN939 with Results for IN738LC for Comparison.
2-18
11089116
EPRI Licensed Material
3
INCONEL X750
3-1
11089116
EPRI Licensed Material
Inconel X750
3-2
11089116
EPRI Licensed Material
Inconel X750
temperature (°C)
0 200 400 600 800 1000 1200
0.20
Inconel X750
product form: wrought 0.80
0.18 0.75
specific heat (btu/lb/°F)
0.70
0.60
0.14
0.55
0.12 0.50
0.45
0.10
0.40
0.35
0.08
0 400 800 1200 1600 2000
temperature (°F)
Page 1 of 8
Figure 3-1
Specific Heat as a Function of Temperature for Inconel X750.
3-3
11089116
EPRI Licensed Material
Inconel X750
temperature (°C)
0 200 400 600 800 1000 1200
220
Inconel X750
product form: wrought 30
200
thermal conductivity (btu/ft /in/hr/°F)
160
140 20
120
15
100
80
10
60
40
0 400 800 1200 1600 2000
temperature (°F)
Page 2 of 8
Figure 3-2
Thermal Conductivity as a Function of Temperature for Inconel X750.
3-4
11089116
EPRI Licensed Material
Inconel X750
temperature (°C)
0 200 400 600 800 1000 1200
12.0
11.5
Inconel X750
product form: wrought
21 a
α [×10 ], 70°F to temperature (in/in/°F)
-6
10.5 19
10.0 18
9.5 17
9.0
16
8.5
15
8.0
14
7.5
-6
13
7.0
12
6.5
11
6.0
0 400 800 1200 1600 2000
temperature (°F)
Page 3 of 8
Figure 3-3
Thermal Expansion as a Function of Temperature.
3-5
11089116
EPRI Licensed Material
Inconel X750
160 1100
1000
140
strength (MPa)
strength (ksi)
900
120
800
100 700
600
80
500
60 400
300
40
Inconel X750
test environment: air 200
20
0 300 600 900 1200 1500 1800 2100
Page 4 of 8
Figure 3-4
Yield and Tensile Strengths vs. Temperature for Inconel X750.
3-6
11089116
EPRI Licensed Material
Inconel X750
34 Inconel X750
test environment: air
32
30
28
26
% elongation
24
22
20
18
16
14
12
10
8
0 400 800 1200 1600 2000
Page 5 of 8
Figure 3-5
Tensile Elongation vs. Temperature.
3-7
11089116
EPRI Licensed Material
Inconel X750
210
30
dynamic modulus (10 ksi)
28
190
26 180
170
24
160
22 150
140
20
130
18
120
16
0 400 800 1200 1600 2000
Page 6 of 8
Figure 3-6
Dynamic Modulus as a Function of Temperature.
3-8
11089116
EPRI Licensed Material
Inconel X750
80
500
70
60
400
50
300
40
30 200
20
100
10
0 0
1000 1200 1400 1600 1800 2000
Page 7 of 8
Figure 3-7
100 hr Rupture Strength as a Function of Temperature.
3-9
11089116
EPRI Licensed Material
Inconel X750
Page 8 of 8
Figure 3-8
Fatigue Crack Growth Behavior at 650°C and 540°C Under Air and Vacuum Conditions.
3-10
11089116
EPRI Licensed Material
4
INCONEL 738
4-1
11089116
EPRI Licensed Material
Inconel 738
4-2
11089116
EPRI Licensed Material
Inconel 738
temperature (°C)
0 200 400 600 800 1000 1200
0.20
Inconel 738
product form: cast 0.80
0.18 0.75
specific heat (Btu/lb/°F)
0.60
0.14
0.55
0.12 0.50
0.45
0.10
0.40
0.35
0.08
0 400 800 1200 1600 2000
temperature (°F)
Page 1 of 40
Figure 4-1
Specific Heat as a Function of Temperature.
4-3
11089116
EPRI Licensed Material
Inconel 738
temperature (°C)
0 200 400 600 800 1000 1200
220
Inconel 738
product form: cast 30.0
200
thermal conductivity (Btu/ft /in/hr/°F)
27.5
160
22.5
140 20.0
120 17.5
15.0
100
12.5
80
10.0
60
7.5
40
0 400 800 1200 1600 2000
temperature (°F)
Page 2 of 40
Figure 4-2
Thermal Conductivity as a Function of Temperature.
4-4
11089116
EPRI Licensed Material
Inconel 738
temperature (°C)
0 200 400 600 800 1000 1200
10.0 18
Inconel 738
product form: cast
9.0
16
8.5
15
8.0
14
7.5
13
7.0
12
6.5
11
6.0
5.5 10
5.0 9
0 400 800 1200 1600 2000
temperature (°F)
Page 3 of 40
Figure 4-3
Coefficient of Thermal Expansion as a Function of End Temperature.
4-5
11089116
EPRI Licensed Material
Inconel 738
160 1100
1000
140
strength (MPa)
strength (ksi)
900
120
800
100 700
600
80
500
60 400
300
40
Inconel 738
test environment: air 200
20
0 300 600 900 1200 1500 1800 2100
Page 4 of 40
Figure 4-4
Yield and Tensile Strengths as a Function of Temperature.
4-6
11089116
EPRI Licensed Material
Inconel 738
12
10
% elongation
0
0 400 800 1200 1600 2000
Page 5 of 40
Figure 4-5
Tensile Elongation as a Function of Temperature.
4-7
11089116
EPRI Licensed Material
Inconel 738
Page 6 of 40
Figure 4-6
Yield and Tensile Strengths as a Function of Temperature.
4-8
11089116
EPRI Licensed Material
Inconel 738
30
dynamic modulus (10 ksi)
28
26 180
24
160
22
140
20
18
120
16
0 400 800 1200 1600 2000
Page 7 of 40
Figure 4-7
Dynamic Modulus as a Function of Temperature.
4-9
11089116
EPRI Licensed Material
Inconel 738
12
16
Inconel 738
test temperature: 1652°F (900°C)
11 environment: air 15
14
10
13
9
12
8 11
10
7
9
6 8
7
5
6
4
5
3
0 2000 4000 6000 8000 10000 12000
Page 8 of 40
Figure 4-8
Charpy Impact Energy as a Function of Aging Time.
4-10
11089116
EPRI Licensed Material
Inconel 738
11
10
7
9
6 8
7
5
6
4
5
3
0 300 600 900 1200 1500 1800
Page 9 of 40
Figure 4-9
Charpy Impact Energy as a Function of Aging Temperature.
4-11
11089116
EPRI Licensed Material
Inconel 738
∆K (MPa√m)
10 100
10-2
Inconel 738 10-1
test temperature: 75°F (24°C)
environment: vacuum
10-3
10-2
10-4
10-3
da/dN (mm/cycle)
da/dN (in/cycle)
10-5
10-4
10-6
10-5
10-7
10-6
10-8
10-7
10-9
R= 0 (479113)
10-8
R= 0.1 (818660)
10-10
10 100
∆K (ksi√in)
Page 10 of 40
Figure 4-10
Fatigue Crack Growth Behavior at Room Temperature Under Vacuum Conditions. (Low R).
4-12
11089116
EPRI Licensed Material
Inconel 738
∆K (MPa√m)
10 100
10-3
Inconel 738 10-2
test temperature: 75°F (24°C)
10-4 environment: air
10-3
10-5
10-4
da/dN (mm/cycle)
da/dN (in/cycle)
10-6
10-5
10-7
10-6
10-8
10-7
10-9
10-8
10-10
R= 0.1 (C= 7e-14 in/cycle, n= 5.29) 10-9
R= 0.85 (C= 4.9e-12 in/cycle, n= 5.79)
10-11
1 10 100
∆K (ksi√in)
Page 11 of 40
Figure 4-11
Fatigue Crack Growth Behavior at R = 0.1 and 0.85 (Room Temperature, Air).
4-13
11089116
EPRI Licensed Material
Inconel 738
∆K (MPa√m)
10 100
10-2
Inconel 738 10-1
test temperature:1562°F (850°C)
10-3 environment: vacuum
10-2
10-4
10-3
10-5
da/dN (mm/cycle)
da/dN (in/cycle)
10-4
10-6
10-5
10-7
10-6
10-8
10-7
10-9
10-8
R= 0.1
10-10 R= 0.3 (C= 2.4e-10 in/cycle, n= 3.62)
R= 0.9 10-9
10-11
1 10 100
∆K (ksi√in)
Page 12 of 40
Figure 4-12
Fatigue Crack Growth Behavior at 1562°F.
4-14
11089116
EPRI Licensed Material
Inconel 738
Page 13 of 40
Figure 4-13
Fatigue Crack Growth Rate as a Function of •K in IN-738 at 927°C in Air and in Vacuum.
4-15
11089116
EPRI Licensed Material
Inconel 738
√ ∆ J • E OR ∆K
Page 14 of 40
Figure 4-14
Comparison of Fatigue Crack Growth Rate for Three Alloys.
4-16
11089116
EPRI Licensed Material
Inconel 738
Page 15 of 40
Figure 4-15
Fatigue Crack Growth Rate in Superalloys at 927°C in Vacuum.
4-17
11089116
EPRI Licensed Material
Inconel 738
80
500
70
60
400
50
300
40
30 200
20
100
10
0 0
1200 1400 1600 1800 2000
Page 16 of 40
Figure 4-16
100 hr Rupture Strength as a Function of Temperature.
4-18
11089116
EPRI Licensed Material
Inconel 738
500
70
60
400
50
300
40
30 200
20
100
10
0 0
1200 1400 1600 1800 2000
Page 17 of 40
Figure 4-17
1000 hr Rupture Strength as a Function of Temperature.
4-19
11089116
EPRI Licensed Material
Inconel 738
stress (MPa)
stress (ksi)
Inconel 738
test environment: air
10
36 38 40 42 44 46 48 50 52
3
LMP (°R-hr)×10
(460+°F)(C+log tr)
Page 18 of 40
Figure 4-18
Larson-Miller Plot for Inconel 738.
4-20
11089116
EPRI Licensed Material
Inconel 738
1000
Inconel 738
100 test environment: air
stress (MPa)
stress (ksi)
10
Page 19 of 40
Figure 4-19
Stress vs. Rupture Time at Three Elevated Temperatures.
4-21
11089116
EPRI Licensed Material
Inconel 738
Page 20 of 40
Figure 4-20
Stress vs. Strain-Rate at Three Temperatures Including Repeat Runs.
4-22
11089116
EPRI Licensed Material
Inconel 738
Page 21 of 40
Figure 4-21
Multiple Relaxation Runs at 850°C Showing Transient Effects for Low Stresses.
4-23
11089116
EPRI Licensed Material
Inconel 738
Page 22 of 40
Figure 4-22
Creep Data at 850°C for Various Initial Thermal Treatments.
4-24
11089116
EPRI Licensed Material
Inconel 738
900°C
124 MPa
Page 23 of 40
Figure 4-23
IN-738 VPS Coated Creep Test Results at 900°C/124 MPa.
4-25
11089116
EPRI Licensed Material
Inconel 738
982°C
69 MPa
Page 24 of 40
Figure 4-24
IN-738 VPS Coated Creep Test Results at 982°C/69 MPa.
4-26
11089116
EPRI Licensed Material
Inconel 738
Temperature: 850°C
Page 25 of 40
Figure 4-25
Strain Rate vs. Stress for IN738LC at 850°C in Tests Containing (i) pp and pc and (ii) pp
and cp.
4-27
11089116
EPRI Licensed Material
Inconel 738
Page 26 of 40
Figure 4-26
Influence of Environment on Creep Crack Growth Rate in IN-738 at 927°C and Comparison
with Fatigue Crack Growth Rate Converted to Time Domain.
4-28
11089116
EPRI Licensed Material
Inconel 738
Page 27 of 40
Figure 4-27
Total Strain Range vs. Life to Failure.
4-29
11089116
EPRI Licensed Material
Inconel 738
Page 28 of 40
Figure 4-28
Total Strain Range vs. Life to Crack Initiation.
4-30
11089116
EPRI Licensed Material
Inconel 738
Page 29 of 40
Figure 4-29
Elastic Strain Range vs. Life to Failure.
4-31
11089116
EPRI Licensed Material
Inconel 738
Page 30 of 40
Figure 4-30
Elastic Strain Range vs. Life to Crack Initiation.
4-32
11089116
EPRI Licensed Material
Inconel 738
Page 31 of 40
Figure 4-31
Inelastic Strain Range vs. Life to Failure.
4-33
11089116
EPRI Licensed Material
Inconel 738
Page 32 of 40
Figure 4-32
Inelastic Strain Range vs. Life to Crack Initiation.
4-34
11089116
EPRI Licensed Material
Inconel 738
Page 33 of 40
Figure 4-33
Typical Test Results and Partitioned Strain Ranges.
4-35
11089116
EPRI Licensed Material
Inconel 738
Page 34 of 40
Figure 4-34
(HTLCF) Results of IN 738 in the Standard and the Exposed Conditions, Inelastic Strain
Range (∆ε in %) vs. Number of Cycles to Failure (Nf).
4-36
11089116
EPRI Licensed Material
Inconel 738
Page 35 of 40
Figure 4-35
(HTLCF) Results of IN 738 at 1123 K, for the Two Types of Specimens Tested Under
Continuous Strain Cycling and Cycling with Tensile Hold Times, Inelastic Strain range (∆ε
in %) vs. Number of Cycles to Failure (Nf).
4-37
11089116
EPRI Licensed Material
Inconel 738
Page 36 of 40
Figure 4-36
Inelastic Strain Range vs. Cycles to Failure for Cast IN 738 LC (a) pp components only;
750°C and 850°C, (b) pp and pc components 850°C (c) pp and cp components; 850°C.
4-38
11089116
EPRI Licensed Material
Inconel 738
Page 37 of 40
Figure 4-37
Inelastic Strain Range vs. Cycles to Failure for Cast IN 738 at 870°C.
4-39
11089116
EPRI Licensed Material
Inconel 738
Page 38 of 40
Figure 4-38
Inelastic Strain Range vs. Cycles to Failure for Cast IN 738 at 870°C, pp and cp
components.
4-40
11089116
EPRI Licensed Material
Inconel 738
Page 39 of 40
Figure 4-39
Inelastic Strain Range vs. Cycles to Failure for Cast IN 738 at 870°C, pp and pc
components.
4-41
11089116
EPRI Licensed Material
Inconel 738
1.2
Inconel 738
1.1 test temperature: 1600°F (871°C)
environment: air
1.0
0.9
0.8
0.7
∆εt
0.6
0.5
0.4
0.3
0.2
hold time: 0
hold time: 120 sec
0.1
hold time: 600 sec
0.0
101 102 103 104 105 106
Nf (cycles)
Page 40 of 40
Figure 4-40
Low Cycle Fatigue at 1600°F with Three Hold Times Investigated (Total Strain Range).
4-42
11089116
EPRI Licensed Material
5
INCONEL 738 LC
5-1
11089116
EPRI Licensed Material
Inconel 738 LC
5-2
11089116
EPRI Licensed Material
Inconel 738 LC
180
1200
160
1000
strength (MPa)
140
strength (ksi)
120
800
100
600
80
60 400
40
200
20 Inconel 738 LC
test environment: air
0 0
0 400 800 1200 1600 2000
Page 1 of 28
Figure 5-1
Tensile Strengths as a Function of Temperature.
5-3
11089116
EPRI Licensed Material
Inconel 738 LC
30
25
% elongation
20
15
10
0
0 400 800 1200 1600 2000
Page 2 of 28
Figure 5-2
Tensile Elongation as a Function of Temperature.
5-4
11089116
EPRI Licensed Material
Inconel 738 LC
60
Inconel 738 LC
55 test environment: air
50
45
reduction in area (%)
40
35
30
25
20
15
10
0
0 400 800 1200 1600 2000
Page 3 of 28
Figure 5-3
Reduction in Area (Tensile) as a Function of Temperature.
5-5
11089116
EPRI Licensed Material
Inconel 738 LC
Page 4 of 28
Figure 5-4
Impact Resistance of IN-738 at Room Temperature and 900°C as a Function of Aging Time
at 950°C.
5-6
11089116
EPRI Licensed Material
Inconel 738 LC
Page 5 of 28
Figure 5-5
Loss of High Temperature Impact Resistance Correlation in Terms of a Time-Temperature
Parameter Analogous to that of Larson-Miller.
5-7
11089116
EPRI Licensed Material
Inconel 738 LC
∆K (MPa√m)
10 100
10-2
Inconel 738 LC 10-1
test temperature: 75°F (24°C)
10-3 test environment: air
10-2
10-4
10-3
da/dN (mm/cycle)
da/dN (in/cycle)
10-5
10-4
10-6
10-5
10-7
10-6
10-8
10-7
10-9
10-10
10 100
∆K (ksi√in)
Page 6 of 28
Figure 5-6
Fatigue Crack Growth Behavior at R = 0 (Room Temperature, Lab Air Conditions).
5-8
11089116
EPRI Licensed Material
Inconel 738 LC
∆K (MPa√m)
10-4
Inconel 738 LC
test temperature: 1382°F (750°C)
test environment: air
10-3
10-5
da/dN (mm/cycle)
da/dN (in/cycle)
10-4
10-6
10-5
∆K (ksi√in)
Page 7 of 28
Figure 5-7
Fatigue Crack Growth Behavior at 1382°F at R = 0.1 (Lab Air).
5-9
11089116
EPRI Licensed Material
Inconel 738 LC
∆K (MPa√m)
10 100
10-2
Inconel 738 LC 10-1
test temperature:1562°F (850°C)
air
10-3
10-2
10-4
da/dN (mm/cycle)
10-3
da/dN (in/cycle)
10-5
10-4
10-6
10-5
10-7
10-6
10-8
R= 0.25 (C=2.7e-14 in/cycle, n= 6.1) 10-7
R= 0.3 (C= 1.6e-10 in/cycle, n= 3.74)
10-9
1 10 100
∆K (ksi√in)
Page 8 of 28
Figure 5-8
Fatigue Crack Growth Behavior at 1562°F for R = 0.25 and 0.3 (Lab Air).
5-10
11089116
EPRI Licensed Material
Inconel 738 LC
Page 9 of 28
Figure 5-9
Crack Growth for Nimocast 738 LC and 739 at Cyclic Frequencies Between 60 and 100 Hz
and R = 0.1; δ is Crack Tip Opening Displacement.
5-11
11089116
EPRI Licensed Material
Inconel 738 LC
Page 10 of 28
Figure 5-10
Influence of Environment on Fatigue Crack Growth of Nimocast 738 LC and 739 at 850°C
and Cyclic Frequencies Between 10 and 100 Hz and R = 0.1.
5-12
11089116
EPRI Licensed Material
Inconel 738 LC
3
LMP (K-hr)×10
(T(K))(C+tr)
20 21 22 23 24 25 26 27 28 29 30
100
stress (MPa)
stress (ksi)
100
10
Inconel 738 LC
test environment: air
36 38 40 42 44 46 48 50 52 54 56
3
LMP (°R-hr)×10
(460+°F)(C + log tr)
Page 11 of 28
Figure 5-11
Larson-Miller Plot for Inconel 738 LC.
5-13
11089116
EPRI Licensed Material
Inconel 738 LC
LMP (K-hr)×103
(T(K))(C+log tr)
21 22 23 24
Inconel 738 LC
test environment: light oil (ASTM grade #2)
1000
100
stress (MPa)
stress (ksi)
test temperature
100
1292°F (700°C)
1562°F (850°C)
10
37 38 39 40 41 42 43 44
3
LMP (°R-hr)×10
(460+°F)(C + log tr)
Page 12 of 28
Figure 5-12
Larson-Miller Plot at Two Test Temperatures (Light Oil Conditions).
5-14
11089116
EPRI Licensed Material
Inconel 738 LC
120
test temperature 800
1292°F (700°C)
1562°F (850°C)
100 700
600
80
stress (MPa)
500
stress (ksi)
60 400
300
40
200
20
100
Inconel 738 LC
test environment: light oil (ASTM grade #2)
0 0
100 1000 10000
tr (hr)
Page 13 of 28
Figure 5-13
Stress vs. Rupture Time at Two Elevated Temperatures (Light Oil Conditions).
5-15
11089116
EPRI Licensed Material
Inconel 738 LC
Page 14 of 28
Figure 5-14
-3
Larson-Miller Plot (P = T (20 + log t f) x 10 , where T is in K and tf in hr) of Cast and Hipped
IN-738LC Turbine Blades Showing Unexposed and Service Exposed Creep-Rupture
Properties.
5-16
11089116
EPRI Licensed Material
Inconel 738 LC
Page 15 of 28
Figure 5-15
Dependence of the Time to Rupture on the Minimum Creep Rate, for IN-738LC (Monkman-
Grant Relationship).
5-17
11089116
EPRI Licensed Material
Inconel 738 LC
Page 16 of 28
Figure 5-16
Dependence of Primary Plus Secondary, Creep Life on the Minimum Creep Rate for Cast
IN-738LC.
5-18
11089116
EPRI Licensed Material
Inconel 738 LC
TIME TO RUPTURE ( t r ) , s
Page 17 of 28
Figure 5-17
Time to Rupture Dependence on the Tertiary Life for Cast IN-738LC.
5-19
11089116
EPRI Licensed Material
Inconel 738 LC
10
Inconel 738 LC failure
test temperature: 1699 °F
test environment: air
∆εt
0.1
101 102 103 104 105
Nf (cycles)
Page 18 of 28
Figure 5-18
Low Cycle Fatigue at 1699°F (Total Strain Range).
5-20
11089116
EPRI Licensed Material
Inconel 738 LC
10
Inconel 738 LC
test environment: air 1112°F
1382°F
∆εt
0.1
102 103 104 105
Nf (cycles)
Page 19 of 28
Figure 5-19
Low Cycle Fatigue Behavior at Two Elevated Temperatures (Total Strain Range).
5-21
11089116
EPRI Licensed Material
Inconel 738 LC
10
800°F- initiation
800°F- failure
1400°F- initiation
1400°F- failure
1600°F- initiation
1600°F- failure
1800°F- initiation
1800°F- failure
∆εt
Inconel 738 LC
test environment: air
0.1
102 103 104 105
N (cycles)
Page 20 of 28
Figure 5-20
Low Cycle Initiation and Failure at Four Elevated Temperatures.
5-22
11089116
EPRI Licensed Material
Inconel 738 LC
Page 21 of 28
Figure 5-21
Strain-Amplitude-Life Relations for IN738LC at 650°C as an Effect of Casting Process.
5-23
11089116
EPRI Licensed Material
Inconel 738 LC
Page 22 of 28
Figure 5-22
Strain-Amplitude-Life Relations for IN738LC at 650°C as an Effect of Casting Process.
5-24
11089116
EPRI Licensed Material
Inconel 738 LC
Page 23 of 28
Figure 5-23
Stress vs. Reversals of IN738LC at 650°C (1202°F) as an Effect of Casting Process.
5-25
11089116
EPRI Licensed Material
Inconel 738 LC
Page 24 of 28
Figure 5-24
Strain-Amplitude-Life Relations for IN738LC at 850°C as an Effect of Casting Process.
5-26
11089116
EPRI Licensed Material
Inconel 738 LC
Page 25 of 28
Figure 5-25
Stress vs. Reversals of IN738LC at 850°C (1532°F) as an Effect of Casting Process.
5-27
11089116
EPRI Licensed Material
Inconel 738 LC
Page 26 of 28
Figure 5-26
Strain-Amplitude-Life Relations for IN738LC at 850°C as an Effect of Casting Process.
5-28
11089116
EPRI Licensed Material
Inconel 738 LC
0.9
Inconel 738 LC
initiation
test environment: air
failure
0.8
0.7
0.6
∆εt
0.5
0.4
0.3
0.2
101 102 103 104 105 106
N (cycles)
Page 27 of 28
Figure 5-27
Low Cycle Fatigue Behavior for Inconel 738 LC.
5-29
11089116
EPRI Licensed Material
Inconel 738 LC
120
800
initiation
failure
100 700
80
500
60
400
300
40
Inconel 738 LC
200
test environment: air
max temperature: 1600°F
20
101 102 103 104 105 106
N (cycles)
Page 28 of 28
Figure 5-28
Thermal-Mechanical Fatigue Behavior of Inconel 738 LC.
5-30
11089116
EPRI Licensed Material
6
INCONEL 792
6-1
11089116
EPRI Licensed Material
Inconel 792
6-2
11089116
EPRI Licensed Material
Inconel 792
160 1100
1000
140
strength (MPa)
strength (ksi)
900
120
800
100 700
600
80
500
60 400
300
40
Inconel 792
test environment: air 200
20
0 300 600 900 1200 1500 1800 2100
Page 1 of 9
Figure 6-1
Tensile Strengths as a Function of Temperature.
6-3
11089116
EPRI Licensed Material
Inconel 792
12
10
% elongation
0
0 400 800 1200 1600 2000
Page 2 of 9
Figure 6-2
Tensile Elongation as a Function of Temperature.
6-4
11089116
EPRI Licensed Material
Inconel 792
Page 3 of 9
Figure 6-3
Fatigue Crack Growth Rate as a Function of ∆K in IN-792 at 927°C in Air and in Vacuum.
6-5
11089116
EPRI Licensed Material
Inconel 792
Page 4 of 9
Figure 6-4
Comparison of Fatigue Crack Growth Rate in Terms for Three Alloys.
6-6
11089116
EPRI Licensed Material
Inconel 792
Page 5 of 9
Figure 6-5
Fatigue Crack Growth Rate in Superalloys at 927°C in Vacuum.
6-7
11089116
EPRI Licensed Material
Inconel 792
90
600
80
500
70
60
400
50
300
40
30 200
20
100
10
0 0
1200 1400 1600 1800 2000
Page 6 of 9
Figure 6-6
100 hr Rupture Strength as a Function of Temperature.
6-8
11089116
EPRI Licensed Material
Inconel 792
500
70
60
400
50
300
40
30 200
20
100
10
0 0
1200 1400 1600 1800 2000
Page 7 of 9
Figure 6-7
1000 hr Rupture Strength as a Function of Temperature.
6-9
11089116
EPRI Licensed Material
Inconel 792
3
LMP (K-hr)×10
(T(K))(C+log tr)
30.00 29.75 29.50 29.25 29.00 28.75
1000
100
stress (MPa)
stress (ksi)
100
Inconel 792
test environment: air
10
38 40 42 44 46 48 50 52
3
LMP (°R-hr)×10
(460+°F)(C+log tr)
Page 8 of 9
Figure 6-8
Larson-Miller Plot for Inconel 792.
6-10
11089116
EPRI Licensed Material
Inconel 792
Page 9 of 9
Figure 6-9
Influence of Environment on Creep Crack Growth Rate in IN-792 at 927°C and Comparison
with Fatigue Crack Growth Rate (Fatigue Crack Growth Rate Given on a Time Basis).
6-11
11089116
11089116
EPRI Licensed Material
7
MAR-M002
7-1
11089116
EPRI Licensed Material
MAR-M002
7-2
11089116
EPRI Licensed Material
MAR-M002
Page 1 of 13
Figure 7-1
Influence of R on Crack Growth in Directionally Solidified and Single Crystal Materials at
950°C and a Frequency of 0.1 Hz.
7-3
11089116
EPRI Licensed Material
MAR-M002
Page 2 of 13
Figure 7-2
Influence of Grain Structure and R on Crack Growth at 950°C and a Frequency of 20 Hz.
7-4
11089116
EPRI Licensed Material
MAR-M002
Page 3 of 13
Figure 7-3
Effect of Frequency on Crack Growth in Directionally Solidified Alloy at 950°C and R = 0.1.
7-5
11089116
EPRI Licensed Material
MAR-M002
Page 4 of 13
Figure 7-4
Effect of Temperature on Crack Growth/Cycle in Directionally Solidified and Single Crystal
Materials at a Frequency of 0.1 Hz and R = 0.1.
7-6
11089116
EPRI Licensed Material
MAR-M002
Page 5 of 13
Figure 7-5
Effect of Prior Creep Damage on Crack Growth in Directionally Solidified and Single
Crystal Material at 950°C at a Frequency of 20 Hz and R = 0.7.
7-7
11089116
EPRI Licensed Material
MAR-M002
Page 6 of 13
Figure 7-6
Effect of R on Crack Growth Per Cycle in the Threshold Region at 950°C.
7-8
11089116
EPRI Licensed Material
MAR-M002
Page 7 of 13
Figure 7-7
Effect of Prior Creep Damage on Crack Growth Per Cycle at 950°C for R = 0.9.
7-9
11089116
EPRI Licensed Material
MAR-M002
R = 0.1
frequency: 20 Hz
Page 8 of 13
Figure 7-8
Crack Growth for MAR-M002 at Cyclic Frequency of 0.25 Hz and R = 0.1.
7-10
11089116
EPRI Licensed Material
MAR-M002
Page 9 of 13
Figure 7-9
Influence of R on Crack Growth Rate for MAR-M002 at 950°C and 20 Hz, da/dN versus ∆K.
7-11
11089116
EPRI Licensed Material
MAR-M002
Page 10 of 13
Figure 7-10
Influence of R on Crack Growth Rate for MAR-M002 at 950°C and 20 Hz, da/dt versus Kmax.
7-12
11089116
EPRI Licensed Material
MAR-M002
Page 11 of 13
Figure 7-11
Influence of Grain Structure and Temperature on Creep Crack Growth Rate.
7-13
11089116
EPRI Licensed Material
MAR-M002
Temperature: 950°C
Page 12 of 13
Figure 7-12
Effect of Prior Creep Damage on Creep Crack Growth Rate at 950°C in Directionally
Solidified Material.
7-14
11089116
EPRI Licensed Material
MAR-M002
Page 13 of 13
Figure 7-13
Accumulation of Creep Strain at 950°C and a Stress of 256 MPa in Directionally Solidified
and Single Crystal Material.
7-15
11089116
11089116
EPRI Licensed Material
8
MAR-M200
8-1
11089116
EPRI Licensed Material
MAR-M200
8-2
11089116
EPRI Licensed Material
MAR-M200
Page 1 of 3
Figure 8-1
Comparison of Crack Growth Rates of MAR-M200 Single Crystals at 25 and 982°C. (∆Keff is
a Function of Three Nodes of Cracking.)
8-3
11089116
EPRI Licensed Material
MAR-M200
Page 2 of 3
Figure 8-2
Fatigue Crack Growth Rate Results of MAR-M200 Single Crystals Under Uniaxially Applied
Cyclic Loading at 982°C. (∆Keff is a Function of Three Nodes of Cracking.)
8-4
11089116
EPRI Licensed Material
MAR-M200
Page 3 of 3
Figure 8-3
Comparison of Theoretical and Experimental Thermal Fatigue Lives of MAR M200 and
MAR M200DS Double Wedges (0.6 and 1.0 mm Radius Edge, Heating and Cooling in
Fluidized Beds at 320 and 1090°C).
8-5
11089116
11089116
EPRI Licensed Material
9
MAR-M247
9-1
11089116
EPRI Licensed Material
MAR-M247
9-2
11089116
EPRI Licensed Material
MAR-M247
Page 1 of 6
Figure 9-1
Prediction of Isothermal Fatigue Data at 500°C.
9-3
11089116
EPRI Licensed Material
MAR-M247
Page 2 of 6
Figure 9-2
Prediction of 871°C Isothermal Fatigue Test Results.
9-4
11089116
EPRI Licensed Material
MAR-M247
Page 3 of 6
Figure 9-3
Prediction of Out-of-Phase TMF (500°C–871°C) Test Results.
9-5
11089116
EPRI Licensed Material
MAR-M247
Page 4 of 6
Figure 9-4
Prediction of In-Phase TMF (500°C–871°C) Test Results.
9-6
11089116
EPRI Licensed Material
MAR-M247
Page 5 of 6
Figure 9-5
Prediction of Diamond Shape (Nonproportional) Strain-Temperature History.
9-7
11089116
EPRI Licensed Material
MAR-M247
Page 6 of 6
Figure 9-6
Mechanical Strain Range Versus Life for Out-of-Phase and In-Phase TMF Experiments,
ε = 5 x 10-5 s-1
9-8
11089116
EPRI Licensed Material
10
NIMONIC 115
10-1
11089116
EPRI Licensed Material
Nimonic 115
10-2
11089116
EPRI Licensed Material
Nimonic 115
temperature (°C)
0 200 400 600 800 1000 1200
220
Nimonic 115
product form: wrought 30
200
28
thermal conductivity (btu/ft /in/hr/°F)
26
24
2
160
22
140 20
18
120
16
100
14
12
80
10
60
8
40 6
0 400 800 1200 1600 2000
temperature (°F)
Page 1 of 8
Figure 10-1
Thermal Conductivity as a Function of Temperature.
10-3
11089116
EPRI Licensed Material
Nimonic 115
temperature (°C)
0 200 400 600 800 1000 1200
11
Nimonic 115
10 18
17
9
16
15
8
14
-6
13
7
12
11
6
0 400 800 1200 1600 2000
temperature (°F)
Page 2 of 8
Figure 10-2
Coefficient of Thermal Expansion as a Function of Temperature.
10-4
11089116
EPRI Licensed Material
Nimonic 115
160 1100
1000
140
strength (MPa)
strength (ksi)
900
120
800
100 700
600
80
500
60 400
300
40
Nimonic 115
test environment: air 200
20
0 300 600 900 1200 1500 1800 2100
Page 3 of 8
Figure 10-3
Tensile Strengths as a Function of Temperature.
10-5
11089116
EPRI Licensed Material
Nimonic 115
26
24
% elongation
22
20
18
16
14
0 400 800 1200 1600 2000
Page 4 of 8
Figure 10-4
Tensile Elongation as a Function of Temperature.
10-6
11089116
EPRI Licensed Material
Nimonic 115
32 220
210
30
200
28
190
26 180
170
24
160
22 150
140
20
0 400 800 1200 1600 2000
Page 5 of 8
Figure 10-5
Dynamic Modulus as a Function of Temperature.
10-7
11089116
EPRI Licensed Material
Nimonic 115
80
500
70
60
400
50
300
40
30 200
20
100
10
0 0
1200 1400 1600 1800 2000
Page 6 of 8
Figure 10-6
100 hr Rupture Strength as a Function of Temperature.
10-8
11089116
EPRI Licensed Material
Nimonic 115
80
500
70
60
400
50
300
40
30 200
20
100
10
0 0
1200 1400 1600 1800 2000
Page 7 of 8
Figure 10-7
1000 hr Rupture Strength as a Function of Temperature.
10-9
11089116
EPRI Licensed Material
Nimonic 115
LMP (K-hr)
(T(K))(C+log tr)
21.5 22.0 22.5 23.0 23.5 24.0 24.5
1000
100
stress (MPa)
stress (ksi)
100
Nimonic 115
test environment: air
10
39 40 41 42 43 44 45
LMP (°R-hr)
(460+°F)(C+log tr)
Page 8 of 8
Figure 10-8
Partial Larson-Miller Plot for Nimonic 115.
10-10
11089116
EPRI Licensed Material
11
RENE 80
11-1
11089116
EPRI Licensed Material
Rene 80
11-2
11089116
lEPRI Licensed Material
Rene 80
Page 1 of 8
Figure 11-1
Temperature Dependence of Yield Strength (σy) of Unused and Used Coatings and
Substrates in Comparison with Tensile Test Data of Unused Substrate.
11-3
11089116
EPRI Licensed Material
Rene 80
Page 2 of 8
Figure 11-2
Temperature Dependence of Ductility (ε f) Obtained from SP Tests on Unused and Used
Coatings and Substrates, Compared with Tensile Test Data of Unused Substrate.
11-4
11089116
lEPRI Licensed Material
Rene 80
Page 3 of 8
Figure 11-3
Temperature Dependence of Strength and Ductility of the Rene 80 Alloy Specimens.
11-5
11089116
EPRI Licensed Material
Rene 80
Page 4 of 8
Figure 11-4
Fatigue Crack Growth Rate as a Function of ∆K in Rene 80 at 927°C in Air and in Vacuum.
11-6
11089116
lEPRI Licensed Material
Rene 80
√ ∆ J • E OR ∆K
Page 5 of 8
Figure 11-5
Comparison of Fatigue Crack Growth Rate for Three Alloys.
11-7
11089116
EPRI Licensed Material
Rene 80
Page 6 of 8
Figure 11-6
Fatigue Crack Growth Rate in Superalloys at 927°C in Vacuum.
11-8
11089116
lEPRI Licensed Material
Rene 80
Page 7 of 8
Figure 11-7
Influence of Environment on Creep Crack Growth Rate in Rene 80 at 927°C and
Comparison with Fatigue Crack Growth Rate. (Fatigue Crack Growth Rate Give on a Time
Basis.)
11-9
11089116
EPRI Licensed Material
Rene 80
Page 8 of 8
Figure 11-8
A Larson Miller Plot Comparing the GTD111 Alloy Test Points with Rene 80 Data from the
Literature and the GTD111 Larson Miller Curve Published by General Electric.
11-10
11089116
EPRI Licensed Material
12
UDIMET 500
12-1
11089116
EPRI Licensed Material
Udimet 500
12-2
11089116
EPRI Licensed Material
Udimet 500
24
2
160
22
140 20
18
120
16
100 14
12
80
10
60
8
40 6
0 400 800 1200 1600 2000
temperature (°F)
Page 1 of 8
Figure 12-1
Thermal Conductivity as a Function of Temperature.
12-3
11089116
EPRI Licensed Material
Udimet 500
9.0
-6
16
8.5
15
8.0
14
7.5
13
7.0
12
6.5
-6
11
6.0
5.5 10
5.0 9
0 400 800 1200 1600 2000
temperature (°F)
Page 2 of 8
Figure 12-2
Coefficient of Thermal Expansion as a Function of Final Temperature.
12-4
11089116
EPRI Licensed Material
Udimet 500
1300
180
1200
160 1100
strength (MPa)
1000
strength (ksi)
140
900
120
800
100 700
600
80
500
60 400
300
40
Udimet 500
test environment: air 200
20
0 300 600 900 1200 1500 1800 2100
Page 3 of 8
Figure 12-3
Tensile Strengths as a Function of Temperature.
12-5
11089116
EPRI Licensed Material
Udimet 500
40
35
% elongation
30
25
20
15
0 400 800 1200 1600 2000
Page 4 of 8
Figure 12-4
Tensile Elongation as a Function of Temperature.
12-6
11089116
EPRI Licensed Material
Udimet 500
36 Udimet 500
product form: wrought
240
34
32
dynamic modulus (10 ksi)
220
30
200
28
26 180
24
160
22
20 140
18
120
16
0 400 800 1200 1600 2000
Page 5 of 8
Figure 12-5
Dynamic Modulus as a Function of Temperature.
12-7
11089116
EPRI Licensed Material
Udimet 500
120
110
100 700
90
600
80
500
70
60 400
50
300
40
30 200
20
100
10
0 0
1000 1200 1400 1600 1800 2000
Page 6 of 8
Figure 12-6
100 hr Rupture Strength as a Function of Temperature.
12-8
11089116
EPRI Licensed Material
Udimet 500
100 700
90
600
80
500
70
60 400
50
300
40
30 200
20
100
10
0 0
1000 1200 1400 1600 1800 2000
Page 7 of 8
Figure 12-7
1000 hr Rupture Strength as a Function of Temperature.
12-9
11089116
EPRI Licensed Material
Udimet 500
LMP (K-hr)
(T(K))(C+log tr)
18 20 22 24 26 28 30
1000
100
stress (MPa)
stress (ksi)
100
10
Udimet 500
10
test environment: air
1
32 34 36 38 40 42 44 46 48 50 52 54
LMP (°R-hr)
(460+°F)(C+log tr)
Page 8 of 8
Figure 12-8
Larson-Miller Plot for Udimet 500.
12-10
11089116
EPRI Licensed Material
13
UDIMET 520
13-1
11089116
EPRI Licensed Material
Udimet 520
13-2
11089116
EPRI Licensed Material
Udimet 520
1300
180
1200
160 1100
strength (MPa)
1000
strength (ksi)
140
900
120
800
100 700
600
80
500
60 400
300
40
Udimet 520
test environment: air 200
20
0 300 600 900 1200 1500 1800 2100
Page 1 of 5
Figure 13-1
Tensile Strengths as a Function of Temperature.
13-3
11089116
EPRI Licensed Material
Udimet 520
25
% elongation
20
15
10
0
0 400 800 1200 1600 2000
Page 2 of 5
Figure 13-2
Tensile Elongation as a Function of Temperature.
13-4
11089116
EPRI Licensed Material
Udimet 520
120
110
100 700
90
600
80
500
70
60 400
50
300
40
30 200
20
100
10
0 0
1000 1200 1400 1600 1800 2000
Page 3 of 5
Figure 13-3
100 hr Rupture Strength as a Function of Temperature.
13-5
11089116
EPRI Licensed Material
Udimet 520
100 700
90
600
80
500
70
60 400
50
300
40
30 200
20
100
10
0 0
1000 1200 1400 1600 1800 2000
Page 4 of 5
Figure 13-4
1000 hr Rupture Strength as a Function of Temperature.
13-6
11089116
EPRI Licensed Material
Udimet 520
LMP (K-hr)
(T(K))(C+log tr)
21 22 23 24 25 26 27 28
1000
100
stress (MPa)
stress (ksi)
100
10
Udimet 520
10
test environment: air
1
38 40 42 44 46 48 50 52
LMP (°R-hr)
(460+°F)(C+log tr)
Page 5 of 5
Figure 13-5
Larson-Miller Plot for Udimet 520.
13-7
11089116
11089116
EPRI Licensed Material
14
UDIMET 700
14-1
11089116
EPRI Licensed Material
Udimet 700
14-2
11089116
EPRI Licensed Material
Udimet 700
temperature (°C)
0 200 400 600 800 1000 1200
0.20
Udimet 700
product form: wrought 0.80
0.18 0.75
specific heat (Btu/lb/°F)
0.70
0.60
0.14
0.55
0.12 0.50
0.45
0.10
0.40
0.35
0.08
0 400 800 1200 1600 2000
temperature (°F)
Page 1 of 17
Figure 14-1
Specific Heat as a Function of Temperature.
14-3
11089116
EPRI Licensed Material
Udimet 700
temperature (°C)
0 200 400 600 800 1000 1200
260
Udimet 700
product form: wrought 36
240
thermal conductivity (btu/ft /in/hr/°F)
34
30
200
28
180 26
24
160
22
140 20
18
120
0 400 800 1200 1600 2000
temperature (°F)
Page 2 of 17
Figure 14-2
Thermal Conductivity as a Function of Temperature.
14-4
11089116
EPRI Licensed Material
Udimet 700
temperature (°C)
0 200 400 600 800 1000 1200
10.0 18.0
Udimet 700
product form: wrought
9.5
17.0
16.5
9.0
16.0
15.5
8.5
15.0
14.5
8.0
14.0
7.5 13.5
13.0
7.0
0 400 800 1200 1600 2000
temperature (°F)
Page 3 of 17
Figure 14-3
Coefficient of Thermal Expansion as a Function of Temperature.
14-5
11089116
EPRI Licensed Material
Udimet 700
200 1400
180
1200
strength (MPa)
160
strength (ksi)
1000
140
120
800
100
600
80
60 400
40 Udimet 700
test environment: air 200
20
0 300 600 900 1200 1500 1800 2100
Page 4 of 17
Figure 14-4
Tensile Strengths as a Function of Temperature.
14-6
11089116
EPRI Licensed Material
Udimet 700
30
28
% elongation
26
24
22
20
18
16
14
0 400 800 1200 1600 2000
Page 5 of 17
Figure 14-5
Tensile Elongation as a Function of Temperature.
14-7
11089116
EPRI Licensed Material
Udimet 700
32 220
210
30
200
28
190
26 180
170
24
160
22 150
140
20
0 400 800 1200 1600 2000
Page 6 of 17
Figure 14-6
Dynamic Modulus as a Function of Temperature.
14-8
11089116
EPRI Licensed Material
Udimet 700
∆K (MPa√m)
10 100
10-2
Udimet 700 10-1
test temperature: 75°F (24°C)
10-3 air
10-2
10-4
10-3
da/dN (mm/cycle)
da/dN (in/cycle)
10-5
10-4
10-6
10-5
10-7
10-6
10-8
10-7
R= 0 (C= 9.12e-16 in/cycle, n= 6.3)
10-9 R= 0.05 (C= 2.1e-11 in/cycle, n= 0.65)
R= 0.24 (C= 1.4e-12 in/cycle, n= 4.21)
10-8
R= 0.53 (C= 3.7e-12 in/cycle, n= 3.5)
10-10
10 100
∆K (ksi√in)
Page 7 of 17
Figure 14-7
Fatigue Crack Growth Behavior at R = 0, 0.05, 0.24, and 0.53 (Lab Air, Room Temperature).
14-9
11089116
EPRI Licensed Material
Udimet 700
∆K (MPa√m)
100
10-1
Udimet 700
test temperature: 75°F (24°C) 100
vacuum
10-2
10-1
da/dN (mm/cycle)
10-3
da/dN (in/cycle)
10-2
10-4
10-3
10-5
10-4
10-6
10-5
R= 0 (C= 2e-18 in/cycle, n= 7.7)
10-7
100
∆K (ksi√in)
Page 8 of 17
Figure 14-8
Fatigue Crack Growth Behavior Under Vacuum Conditions (Room Temperature).
14-10
11089116
EPRI Licensed Material
Udimet 700
∆K (MPa√m)
10 100
10-1
Udimet 700
test temperature: 1562°F (850°C) 100
air
10-2
10-1
da/dN (mm/cycle)
10-3
da/dN (in/cycle)
10-2
10-4
10-3
10-5
10-4
10-6
10-5
R= 0 (C= 6.3e-13 in/cycle, n= 5.4)
10-7
10 100
∆K (ksi√in)
Page 9 of 17
Figure 14-9
Elevated Temperature Fatigue Crack Growth Behavior at R = 0.
14-11
11089116
EPRI Licensed Material
Udimet 700
∆K (MPa√m)
10 100
10-1
Udimet 700
test temperature: 1562°F (850°C) 100
vacuum
10-2
10-1
da/dN (mm/cycle)
10-3
da/dN (in/cycle)
10-2
10-4
10-3
10-5
10-4
10-6
10-5
R= 0 (C= 1.1e-9 in/cycle, n= 3.02)
10-7
10 100
∆K (ksi√in)
Page 10 of 17
Figure 14-10
Elevated Fatigue Crack Growth Behavior Under Vacuum Conditions.
14-12
11089116
EPRI Licensed Material
Udimet 700
Page 11 of 17
Figure 14-11
Crack Growth for Udimet 700 at 850°C, R = 0.05, and Cyclic Frequency of 0.17 Hz.
14-13
11089116
EPRI Licensed Material
Udimet 700
Temperature: 850°C
Page 12 of 17
Figure 14-12
The Effect of the Environment on the Creep Crack Growth in Udimet 700 at 850°C: o , 14.2
Ì
kN, vacuum, batch 2; , 16.0 kN, vacuum, batch 2; —— air, batch 1; ——, air, batch 2.
14-14
11089116
EPRI Licensed Material
Udimet 700
100 700
90
600
80
500
70
60 400
50
300
40
30 200
20
100
10
0 0
1200 1400 1600 1800 2000
Page 13 of 17
Figure 14-13
100 hr Rupture Strength as a Function of Temperature.
14-15
11089116
EPRI Licensed Material
Udimet 700
100 700
90
600
80
500
70
60 400
50
300
40
30 200
20
100
10
0 0
1000 1200 1400 1600 1800 2000
Page 14 of 17
Figure 14-14
1000 hr Rupture Strength as a Function of Temperature.
14-16
11089116
EPRI Licensed Material
Udimet 700
LMP (K-hr)
(T(K))(C+log tr)
21 22 23 24 25 26 27 28 29 30
1000
100
stress (MPa)
stress (ksi)
100
10
Udimet 700
test environment: air
38 40 42 44 46 48 50 52 54
LMP (°R-hr)
(460+°F)(C+log tr)
Page 15 of 17
Figure 14-15
Larson-Miller Plot for Udimet 700.
14-17
11089116
EPRI Licensed Material
Udimet 700
10
Udimet 700
test temperature: 1400°F (760°C)
test environment: air
∆εt
0.1
101 102 103 104
Nf (cycles)
Page 16 of 17
Figure 14-16
Low-Cycle Fatigue at 1400°F (Total Strain Range).
14-18
11089116
EPRI Licensed Material
Udimet 700
480
Udimet 700
68 test environment: air
test temperature: 1500°F (815°C) 460
64 440
420
60
400
∆σ (MPa)
∆σ (ksi)
56
380
52 360
340
48
320
44
300
Nf (cycles)
Page 17 of 17
Figure 14-17
High-Cycle Fatigue Behavior at 1500°F (Fully Reversed Loading).
14-19
11089116
11089116
EPRI Licensed Material
15
UDIMET 710
15-1
11089116
EPRI Licensed Material
Udimet 710
15-2
11089116
EPRI Licensed Material
Udimet 710
temperature (°C)
0 200 400 600 800 1000 1200
220
Udimet 710
30
cast -or- wrought
200
28
thermal conductivity (btu/ft /in/hr/°F)
24
2
160
22
140 20
18
120
16
100 14
12
80
10
60
8
40 6
0 400 800 1200 1600 2000
temperature (°F)
Page 1 of 11
Figure 15-1
Thermal Conductivity as a Function of Temperature.
15-3
11089116
EPRI Licensed Material
Udimet 710
temperature (°C)
0 200 400 600 800 1000 1200
10.0
Udimet 710
9.5 product form: wrought
α [×10 ], 70°F to temperature (in/in/°F)
9.0
8.5
8.0
7.5
7.0
6.5
-6
6.0
5.5
5.0
0 400 800 1200 1600 2000
temperature (°F)
Page 2 of 11
Figure 15-2
Coefficient of Thermal Expansion as a Function of Temperature.
15-4
11089116
EPRI Licensed Material
Udimet 710
160
1000
140
strength (MPa)
strength (ksi)
120
800
100
600
80
60 400
40
Udimet 710
test environment: air 200
20
0 300 600 900 1200 1500 1800 2100
Page 3 of 11
Figure 15-3
Tensile Strengths as a Function of Temperature.
15-5
11089116
EPRI Licensed Material
Udimet 710
30
25
% elongation
20
15
10
5
0 400 800 1200 1600 2000
Page 4 of 11
Figure 15-4
Tensile Elongation as a Function of Temperature.
15-6
11089116
EPRI Licensed Material
Udimet 710
32
dynamic modulus (10 ksi)
30
3
28
26
24
22
20
18
16
0 400 800 1200 1600 2000
Page 5 of 11
Figure 15-5
Dynamic Modulus as a Function of Temperature.
15-7
11089116
EPRI Licensed Material
Udimet 710
16
Udimet 710
test temperature: 1652°F (900°C) 20
14 environment: air
18
12 16
14
10
12
8
10
6 8
6
4
4
2
2
0 0
0 2000 4000 6000 8000 10000 12000
Page 6 of 11
Figure 15-6
Charpy Impact Energy as a Function of Aging Time.
15-8
11089116
EPRI Licensed Material
Udimet 710
8 11
10
9
6 8
6
4
5
3
2
2
0 0
1400 1450 1500 1550 1600 1650 1700
Page 7 of 11
Figure 15-7
Charpy Impact Energy as a Function of Aging Temperature.
15-9
11089116
EPRI Licensed Material
Udimet 710
120
800
100 700
600
80
500
60 400
300
40
200
20
cast 100
wrought
0 0
1000 1200 1400 1600 1800 2000
Page 8 of 11
Figure 15-8
100 hr Rupture Strength as a Function of Temperature.
15-10
11089116
EPRI Licensed Material
Udimet 710
120
800
110
100 700
90
600
80
70 500
60 400
50
300
40
30 200
20
cast 100
10 wrought
0 0
1000 1200 1400 1600 1800 2000
Page 9 of 11
Figure 15-9
1000 hr Rupture Strength as a Function of Temperature.
15-11
11089116
EPRI Licensed Material
Udimet 710
1000
100
stress (MPa)
stress (ksi)
100
10
Udimet 710
test environment: air
36 38 40 42 44 46 48 50 52 54
LMP (°R-hr)
(460+°F)(C+log t)
Page 10 of 11
Figure 15-10
Larson-Miller Plot for Udimet 710.
15-12
11089116
EPRI Licensed Material
Udimet 710
Page 11 of 11
Figure 15-11
Effect of Mean Stress on the Fatigue Strength of Udimet 710. ( A = σALTERNATING / σMEAN ).
15-13
11089116
11089116
EPRI Licensed Material
16
UDIMET 720
16-1
11089116
EPRI Licensed Material
Udimet 720
16-2
11089116
EPRI Licensed Material
Udimet 720
temperature (°C)
0 200 400 600 800 1000 1200
10.0
Udimet 720
9.5 product form: wrought
α [×10 ], 70°F to temperature (in/in/°F)
9.0
8.5
8.0
7.5
7.0
6.5
-6
6.0
5.5
5.0
0 400 800 1200 1600 2000
temperature (°F)
Page 1 of 22
Figure 16-1
Coefficient of Thermal Expansion as a Function of Temperature.
16-3
11089116
EPRI Licensed Material
Udimet 720
1300
180
strength (MPa)
strength (ksi)
1200
160 1100
1000
140
900
120
800
Udimet 720
test environment: air
100 700
0 300 600 900 1200 1500 1800 2100
Page 2 of 22
Figure 16-2
Tensile Strengths as a Function of Temperature.
16-4
11089116
EPRI Licensed Material
Udimet 720
22
20
18
% elongation
16
14
12
10
4
0 400 800 1200 1600 2000
Page 3 of 22
Figure 16-3
Tensile Elongation as a Function of Temperature.
16-5
11089116
EPRI Licensed Material
Udimet 720
Page 4 of 22
Figure 16-4
Crack Growth Rates in Air and in Vacuum for Single Crystal U720.
16-6
11089116
EPRI Licensed Material
Udimet 720
Page 5 of 22
Figure 16-5
Crack Growth Rates in Air and in Vacuum for Polycrystalline U720.
16-7
11089116
EPRI Licensed Material
Udimet 720
Page 6 of 22
Figure 16-6
Graph of da/dN Data for SENB Specimens in Vacuum at 20, 300 and 600°C.
16-8
11089116
EPRI Licensed Material
Udimet 720
Page 7 of 22
Figure 16-7
Showing da/dN Data at R = 0.5 in Air and Vacuum.
16-9
11089116
EPRI Licensed Material
Udimet 720
80
500
70
60
400
50
300
40
30 200
20
100
10
0 0
1200 1400 1600 1800 2000
Page 8 of 22
Figure 16-8
100 hr Rupture Strength as a Function of Temperature.
16-10
11089116
EPRI Licensed Material
Udimet 720
80
500
70
60
400
50
300
40
30 200
20
100
10
0 0
1200 1400 1600 1800 2000
Page 9 of 22
Figure 16-9
100 hr Rupture Strength as a Function of Temperature.
16-11
11089116
EPRI Licensed Material
Udimet 720
80
500
70
60
400
50
300
40
30 200
20
100
10
0 0
1200 1400 1600 1800 2000
Page 10 of 22
Figure 16-10
1000 hr Rupture Strength as a Function of Temperature.
16-12
11089116
EPRI Licensed Material
Udimet 720
100
Udimet 720
stress (MPa)
stress (ksi)
100
10
40 42 44 46 48 50 52 54
LMP (°R-hr)
(460+°F)(C+log t)
Page 11 of 22
Figure 16-11
Larson-Miller Plot for Udimet 720.
16-13
11089116
EPRI Licensed Material
Udimet 720
60
Udimet 720 120
pretemperature aging: 0
test temperature: 1600 °F (870°C)
test environment: air 110
50
100
40
90
∆σ (MPa)
∆σ (ksi)
80
30
70
20 60
50
10
40
saline
air
30
0
103 104 105 106 107 108 109 1010
Nf (cycles)
Page 12 of 22
Figure 16-12
High Cycle Fatigue Behavior at 1600°F in Saline and Air Environments.
16-14
11089116
EPRI Licensed Material
Udimet 720
Page 13 of 22
Figure 16-13
Effects of Environment and Frequency of Cycling on HCF Strength of Udimet 720 at 1300°F
(704°C) and R = 0.2 to 0.3.
16-15
11089116
EPRI Licensed Material
Udimet 720
Page 14 of 22
Figure 16-14
HCF Strength of Udimet 720 in Salt Environment at 1300°F (704°C) for R = -1.0 and 0.6.
16-16
11089116
EPRI Licensed Material
Udimet 720
Temperature: 1300°F
Page 15 of 22
Figure 16-15
Effect of Salt Environment and Low Alternating Stress on Stress Rupture of Udimet 710
and 720 Alloys at 1300°F (704°C).
16-17
11089116
EPRI Licensed Material
Udimet 720
Temperature: 1300°F
Page 16 of 22
Figure 16-16
Effect of Environment on Creep/Fatigue Strength of Udimet 720 at 1300°F (704°C) and
Constant Maximum Stress.
16-18
11089116
EPRI Licensed Material
Udimet 720
Temperature: 1300°F
Page 17 of 22
Figure 16-17
Creep/Fatigue Strength of Udimet 720 in Air and Salt Under Constant Mean Stress at
1300°F (704°C).
16-19
11089116
EPRI Licensed Material
Udimet 720
Temperature: 1350°F
Page 18 of 22
Figure 16-18
Relationship Between Strain Range and Number of Cycles to Failure Obtained During the
Low Cycle Fatigue Testing of Udimet 710 and Coated and Uncoated Udimet 720 at 1350°F
(732°C) at 1 cpm.
16-20
11089116
EPRI Licensed Material
Udimet 720
Temperature: 1350°F
Page 19 of 22
Figure 16-19
Relationship Between the Strain Range Components and Number of Cycles to Failure
Obtained During the Low Cycle Fatigue Testing of Udimet 720 at 1350°F (732°C) as a
Function of Hold Time and Test Environment.
16-21
11089116
EPRI Licensed Material
Udimet 720
Temperature: 1350°F
Page 20 of 22
Figure 16-20
Relationship Between the Strain Range Components and Number of Cycles to Failure
Obtained During the Low Cycle Fatigue Testing of RT-22 Coated Udimet 720 at 1350°F
(732°C) at 1 cpm as a Function of Hold Time and Test Environment.
16-22
11089116
EPRI Licensed Material
Udimet 720
Temperature: 1350°F
Page 21 of 22
Figure 16-21
Low-Cycle Fatigue Results for Udimet 720 at 1350°F (732°C) and 1 cpm.
16-23
11089116
EPRI Licensed Material
Udimet 720
Temperature: 1350°F
Page 22 of 22
Figure 16-22
Low-Cycle Fatigue Results for RT-22 Coated Udimet 720 Tested at 1350°F (732°C) and 1
cpm.
16-24
11089116
EPRI Licensed Material
17
GTD 111 DS
17-1
11089116
EPRI Licensed Material
GTD 111 DS
17-2
11089116
EPRI Licensed Material
GTD 111 DS
Page 1 of 14
Figure 17-1
Tensile Properties and Hardness in the Service Aged Condition.
17-3
11089116
EPRI Licensed Material
GTD 111 DS
Page 2 of 14
Figure 17-2
Tensile and Hardness Properties after Refurbishment.
17-4
11089116
EPRI Licensed Material
GTD 111 DS
Page 3 of 14
Figure 17-3
Bucket to Bucket Variation of Yield and Tensile Strengths of GTD-111 DS (Undegraded).
17-5
11089116
EPRI Licensed Material
GTD 111 DS
Page 4 of 14
Figure 17-4
Bucket to Bucket Variation of Percent Elongation and Reduction of Area (Undegraded).
17-6
11089116
EPRI Licensed Material
GTD 111 DS
160
140
Longitudinal
120
0.2% Offset Yield Strength
Transverse
100
80
60
20
0 200 400 600 800 1000 1200 1400 1600 1800 2000
Temperature, F
Page 5 of 14
Figure 17-5
Variation of Yield Strength of the Longitudinal and Transverse Specimens.
17-7
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EPRI Licensed Material
GTD 111 DS
200
180
Longitudinal
160
Ultimate Tensile Strength, ksi
140
120 Transverse
100
80
Longitudinal(BIRM001665&000963)
60 Transverse (BIUW000039)
40
0 200 400 600 800 1000 1200 1400 1600 1800 2000
Temperature, F
Page 6 of 14
Figure 17-6
Variation of Tensile Strength for the Longitudinal and Transverse Specimens.
17-8
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GTD 111 DS
60
Longitudinal-(%EL)
Longitudinal (%RA) Longitudinal (%RA)
50 Transverse (%EL)
Transverse (%RA)
% Elongation or Reduction of Area
40
Longitudinal
(%EL)
30
20
Transverse (%RA)
10
Transverse
(%EL)
0
0 200 400 600 800 1000 1200 1400 1600 1800 2000
Temperature, F
Page 7 of 14
Figure 17-7
Variation of Tensile Ductility of Longitudinal and Transverse Specimens as a Function of
Temperature.
17-9
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GTD 111 DS
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Figure 17-8
Airfoil Stress Rupture Data for IN-738, GTD-111EA and GTD-111DS Alloys Before and After
Rejuvenation.
17-10
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EPRI Licensed Material
GTD 111 DS
1850
15 ksi
20 ksi
1800
Temperature, T (°F)
1750
1700
1650
15 ksi
log(tr) = 24.398333 - 0.0118 * T
1600 20 ksi
log(tr) = 21.411507 - 0.010506 * T
1550
101 102 103 104 105
Page 9 of 14
Figure 17-9
Iso-Stress Creep Rupture Data of Longitudinal Specimens Machined from the Shank
Section (Unaged).
17-11
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GTD 111 DS
1850
15 ksi
1800 20 ksi
Temperature, T (°F)
1750
1700
1650
15 ksi
log(tr) = 25.1640775356 - 0.01262814 * T
1600 20 ksi
log(tr) = 21.3610045428 - 0.0108205737 * T
1550
101 102 103 104 105
Page 10 of 14
Figure 17-10
Iso-Stress Creep Rupture Data of Transverse Specimens Machined from the Shank
Section.
17-12
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EPRI Licensed Material
GTD 111 DS
100
90
GTD-111DS
80 2
LMP = 53803.23 + 7674.009 * Log(σ) - 7572.44 * Log(σ)
70
60
50
45
40
Stress, ksi
35
30
25
20
15
IN738LC (∆)
2
LMP = 53146.069 + 4823.3177 * Log(σ) - 5985.901 * Log(σ)
10
38000 40000 42000 44000 46000 48000 50000 52000 54000 56000
Page 11 of 14
Figure 17-11
LMP Plot of GTD-111 DS and IN-738 LC Creep Data.
17-13
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GTD 111 DS
100
90
80
70
60
50
45
40
Stress, ksi
35
30
25
20
15
Page 12 of 14
Figure 17-12
Larson-Miller Plot of Longitudinal Shank (Undegraded) Creep Data.
17-14
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EPRI Licensed Material
GTD 111 DS
100
90
80
70
60
2
50 LMP = 54601.11 + 3568.483 * Log(σ) - 5733.02 * Log(σ)
45
40
Stress, ksi
35
30
25
20
15
10
42000 44000 46000 48000 50000 52000 54000 56000
Page 13 of 14
Figure 17-13
LMP Plot of Transverse Specimen Data from Undegraded Shank Location.
17-15
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GTD 111 DS
100
90
80
70
Longitudinal
60
LMP = 53803.23 + 7674.009 * Log(σ) - 7572.44 * Log(σ)2
50
45
40
Stress, ksi
35
30
25
20
15
Transverse
2
LMP = 54601.11 + 3568.483 * Log(σ) - 5733.02 * Log(σ)
10
40000 42000 44000 46000 48000 50000 52000 54000 56000
Page 14 of 14
Figure 17-14
Influence of Specimen Orientation on Creep Rupture Strength of Unaged (Shank) Material.
17-16
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GTD 111 EA
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GTD 111 EA
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Page 1 of 23
Figure 18-1
Tensile Properties and Hardness in the Service Aged Condition.
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GTD 111 EA
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Figure 18-2
Tensile and Hardness Properties after Refurbishment.
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GTD 111 EA
160 1100
1000
140
strength (MPa)
strength (ksi)
900
120
800
100 700
600
80
500
60 400
300
40
GTD 111
test environment: air 200
20
0 300 600 900 1200 1500 1800 2100
Page 3 of 23
Figure 18-3
Tensile Strengths as a Function of Temperature.
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GTD 111 EA
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Figure 18-4
Tensile Strengths as a Function of Temperature.
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GTD 111 EA
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Figure 18-5
Tensile Properties for Root and Airfoil Material at 70°F and 1600°F.
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GTD 111 EA
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Figure 18-6
Tensile Properties for Root and Airfoil Material at 70°F and 1600°F.
18-8
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GTD 111 EA
34 GTD 111
32 test environment: air
30
28
26
24
% elongation
22
20
18
16
14
12
10
Page 7 of 23
Figure 18-7
Tensile Elongation as a Function of Temperature.
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GTD 111 EA
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Figure 18-8
Tensile Elongation and Reduction in Area as a Function of Temperature.
18-10
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GTD 111 EA
1000
100
stress (MPa)
stress (ksi)
10
GTD 111
test environment: air
Page 9 of 23
Figure 18-9
Stress vs. Rupture Time for Two Material Conditions.
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GTD 111 EA
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Figure 18-10
Stress-Rupture Results for Root and Airfoil Material.
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GTD 111 EA
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Figure 18-11
Stress-Rupture Data for GTD-111 EA and DS Compared to IN-738.
18-13
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GTD 111 EA
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Figure 18-12
Stress-Rupture Results for Root and Airfoil Material.
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GTD 111 EA
3
LMP (K-hr)×10
(T(K))(C+log tr)
22 23 24 25 26 27
100
stress (MPa)
stress (ksi)
GTD 111
test environment: air
100
Page 13 of 23
Figure 18-13
Larson-Miller Plot of GTD-111 EA (Standard Heat Treat and Thermally Exposed).
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Figure 18-14
Larson-Miller Plot for GTD-111 EA.
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GTD 111 EA
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Figure 18-15
Larson-Miller Plot for GTD-111 for Different Exposure Conditions.
18-17
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GTD 111 EA
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Figure 18-16
Larson-Miller Plot for GTD-111 EA.
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GTD 111 EA
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Figure 18-17
A Larson Miller Plot Comparing the GTD111 Alloy Test Points with Rene 80 Data from the
Literature and the GTD111 Larson Miller Curve Published by General Electric.
18-19
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GTD 111 EA
Page 18 of 23
Figure 18-18
A Least Squares Regression Model (Y = β 0 + β 1 X + e ) Fitted to the GTD111 Creep Rupture
Data Illustrating the Fit. The 95% Confidence Intervals About the Mean and the 95%
Prediction Interval for an Individual Observation. Test Data from the Thermally Exposed
GTD111 Material and Select Service Exposed GTD111 Data Points are Plotted.
18-20
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Figure 18-19
A Plot of Percent Creep Deformation (Strain) Versus Time for the Creep Rupture Samples
in the Standard Heat Treated Condition and After Thermal Exposures at 816°C and 899°C.
18-21
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Figure 18-20
A Plot of Percent Creep Deformation (Strain) Versus Time for the Creep Rupture Samples
in the Standard Heat Treated Condition and After Thermal Exposures at 816°C and 899°C.
18-22
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GTD 111 EA
Page 21 of 23
Figure 18-21
A Plot of Percent Creep Deformation (Strain) Versus Time for the Creep Rupture Samples
in the Standard Heat Treated Condition and After Thermal Exposures at 816°C and 899°C.
18-23
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GTD 111 EA
Page 22 of 23
Figure 18-22
A Plot of Percent Creep Deformation (Strain) Versus Time for the Creep Rupture Samples
in the Standard Heat Treated Condition and After Thermal Exposures at 816°C and 899°C.
18-24
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GTD 111 EA
Page 23 of 23
Figure 18-23
A Plot of Percent Creep Deformation (Strain) Versus Time for the Creep Rupture Samples
in the Standard Heat Treated Condition and After Thermal Exposures at 816°C and 899°C.
18-25
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19
SOURCE REFERENCES
4. Fax communication from Jim Allen, Consulting Engineer-Gas Turbines, to Vis Viswanathan,
EPRI, Subject IN-792 DS and EA LCF Curves, June 30, 2000.
5. R. Yang and G. A. Webster, “Creep/Fatigue Crack Growth in a Gas Turbine Blade Nickel
Base Superalloy,” presented at the Winter Annual Meeting of the American Society of
Mechanical Engineers, Dallas, TX, November 25-30, 1990, pp. 31-36.
19-1
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EPRI Licensed Material
Source References
11. D. M. Moon and G. P. Sabol, “Effect of Mean Stress on the High-Cycle Fatigue Behavior of
Udimet 710 at 1000 F,” STP 520, American Society for Testing and Materials, Philadelphia,
PA, 1973, pp. 438-450.
14. D. A. Woodford, “Creep Design Analysis for Superalloys Based on Stress Relaxation
Testing,” Sixth International Conference on Creep and Fatigue: Design and Life Assessment
at High Temperature, April 15-17, 1996, C494/090/96, ImechE Conference Transactions,
1996, pp. 61-69.
15. G. A. Webster, “High Temperature Fatigue Crack Growth in Superalloy Blade Materials,”
Materials Science and Technology, Vol. 3, September 1987, pp. 716-725.
18. J. A. Daleo and J. R. Wilson, “GTD111 Alloy Material Study,” 96-GT-520, The American
Society of Mechanical Engineers, 1996, presented at the International Gas Turbine and
Aeroengine Congress & Exhibition, Birmingham, UK, June 10-13, 1996.
19. M. Y. Nazmy, “Effect of Multiple Crack Propagation on the High Temperature Low Cycle
Fatigue of a Cast Nickel-Base Alloy,” Scripta METALLURGICA, Vol. 17, 1983, pp. 491-
494.
21. R. Castillo, A. K. Koul, and E. H. Toscano, “Lifetime Prediction Under Constant Load Creep
Conditions for a Cast Ni-Base Superalloy,” Journal of Engineering for Gas Turbines and
Power, Transactions of the ASME, Vol. 109, January 1987, pp. 99-106.
19-2
11089116
EPRI Licensed Material
Source References
23. J. M. Allen and G. A. Whitlow, “Observations on the Interaction of High Mean Stress and
Type II Hot Corrosion on the Fatigue Behavior of a Nickel Base Superalloy,” Journal of
Engineering for Gas Turbines and Power, Transactions of the ASME, Vol. 107, January
1985, pp. 220-224.
24. M. A. Burke, C. G. Beck, Jr., and E. A. Crombie, “The Influence of Materials Processing on
the High Temperature Low Cycle Fatigue Properties of the Cast Alloy IN-738LC,”
Superalloys 1984, edited by M. Gell, C. S. Kortovich, R. H. Bricknell, W. B. Kent, and J. F.
Radavich, 1984, pp. 63-71.
25. D. A. Spera, “Comparison of Experimental and Theoretical Thermal Fatigue Lives for Five
Nickel-Base Alloys,” STP 520, American Society for Testing and Materials, Philadelphia,
PA, 1973, pp. 648-656.
26. P. Shahinian and K. Sadananda, “Creep and Fatigue Crack Growth Behavior of Some Cast
Nickel-base Alloys,” Materials Science and Engineering, Vol. A108, 1989, pp. 131-140.
27. K. Sadananda and P. Shahinian, “The Effect of Environment on the Creep Crack Growth
Behavior of Several Structural Alloys,” Materials Science and Engineering, Vol. 43, 1980,
pp. 159-168.
28. M. Y. Nazmy, “High Temperature Low Cycle Fatigue of IN 738 and Application of Strain
Range Partitioning,” Metallurgical Transactions A, Volume 14A, March 1983, pp. 449-461.
29. M. Y. Nazmy, “The Effect of Sulfur Containing Environment on the High Temperature Low
Cycle Fatigue of a Cast Ni-Base Alloy,” Scripta METALLURGICA, Vol. 16, 1982, pp. 1329-
1332.
32. V. P. Swaminathan and N. Sastry Cheruvu, “Bucket Alloy Definition and Experience,”
Southwest Research Institute Final Task Report, “Durability and Life Assessment of GTD-
111 Buckets,” August 1997.
19-3
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EPRI Licensed Material
Source References
34. X. D. Wu and P. A. S. Reed, “Mode I and Mixed Mode I/II Fatigue of Ni-Base Single
Crystal Udimet 720 in Air and in Vacuum,” Fatigue ’96, Vol. II, pp. 855-860.
35. M. Loo Morrey and P. A. S. Reed, “Elevated Temperature Behaviour of Udimet 720 – A
Study of Tear Drop Cracking,” Fatigue 96, Vol. II, pp. 867-872.
36. T. B. Gibbons and R. Stickler, “IN939: Metallurgy, Properties and Performance,” COST 50
Report, 1982, pp. 369-393.
19-4
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EPRI Licensed Material
Source References
9999907. Cincotta, G, Final Report from General Electric Co. to EPRI on Contract RP 2421-2,
Feb. 1988.
9999906. High Temperature, High Strength Nickel Base Alloys, The International Nickel Co.
Inc. July 1977.
9999903. u500.
9999899. High Temperature, High Strength Nickel Base Alloys, The International Nickel Co.
Inc. July 1964.
1541028. Pieraggi, B, Effect of Creep or Low Cycle Fatigue on the Oxidation or Hot Corrosion
Behaviour of Nickel-Base Superalloys, First International Symposium on High
Temperature Corrosion of Materials and Coatings for Energy Systems and
Turboengines. II, Marseille, France, 7-11 July 1986, Mater. Sci. Eng. 88, (1-2), 199-
204, Apr. 1987.
988149. Basso, S; Lupinc, V, Particle Coursening and Long Duration Tertiary Creep Nickel-
Base Superalloy IN-939, Strength of Metals and Alloys, vol. 1, Montreal, Canada 12-
16 Aug. 1985 Publ: Pergamon Press Ltd., Headington Hill Hall, Oxford OX3 OBW,
UK, 1985 719-724.
936020. Day, M F; Thomas, G B, Analysis of the Low-Cycle Fatigue Behaviour of Two Ni--
Cr-Base Alloys, Fatigue Fract. Eng. Mater. Struct. 8, (1), 33-48, 1985.
19-5
11089116
EPRI Licensed Material
Source References
928584. Allen, J M; Whitlow, G A, Observations on the Interaction of High Mean Stress and
Type II Hot Corrosion on the Fatigue Behavior of a Nickel Base Superalloy, J. Eng.
Gas Turbines Power (Trans. ASME) 107, (1), 220-224, Jan. 1985.
876647. Nazmy, M Y; Wuthrich, C, Creep Crack Growth in IN 738 and IN 939 Nickel-Base
Superalloys, Mater. Sci. Eng. 61, (2), 119-125, Nov. 1983.
863150. Schneider, K; Gnirss, G, High Cycle Fatigue Properties of Cast Nickel Base
Superalloys IN 738 LC and IN 939, High Temperature Alloys for Gas Turbines 1982,
Liege, Belgium, 4-6 Oct. 1982 Publ: D. Reidel Publishing Co., P.O. Box 17, 3300
AA Dordrecht, The Netherlands, 1982, 319-344.
859757. Osgerby, S; Gibbons, T B, Creep Cavitation in a Cast Ni--Cr Base Alloy, Mater. Sci.
Eng., 59, (2), L11-L14, June 1983.
19-6
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EPRI Licensed Material
Source References
835155. Schmidt, H; Hoffelner, W, High-Cycle Fatigue and Creep of the Cast Nickel-Base
Superalloy IN738LC at 850 deg C, Fracture and the Role of Microstructure, Vol. 2.
Fatigue, Leoben, Austria, 22-24 Sept. 1982 Publ: Engineering Materials Advisory
Services Ltd., 339, Halesowen Rd., Cradley Heath, Warley, West Midlands B64 6PH,
U.K., 1982 701-708.
805217. An Alloy for Stationary Gas Turbines, Diesel Gas Turb. Worldwide 14, (1), 42, Jan.-
Feb. 1982.
792216. Hartnagel, W; Bauer, R; Grunling, H W, Constant Strain Rate Creep Tests With Gas
Turbine Blade Materials Under Hot Corrosion Environmental Conditions, Corrosion
and Mechanical Stress at High Temperatures, Petten, The Netherlands, May 1980,
Publ: Applied Science Publishers, Ltd., Ripple Rd., Barking, Essex, England, 1981,
257-273.
732604. Cutler, C P; Shaw, S W K, The Interrelationship of Gamma Prime Size, Grain Size
and Mechanical Properties in IN-939, a Cast Nickel-Base Superalloy, Strength of
Metals and Alloys, Vol. 2. Fifth International Conference, Aachen, W. Germany, 27-
19-7
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EPRI Licensed Material
Source References
31 Aug. 1979 Publ: Pergamon Press Ltd., Headington Hill Hall, Oxford OX3 OBW,
England, 1980 1357-1362.
719687. Aning, K; Tien, J K, Creep and Stress Rupture Behavior of a Wrought Nickel-Base
Superalloy in Air and Vacuum, Mater. Sci. Eng. 43, (1), 23-33, Mar. 1980.
667215. Shaw, S W K, Datasheet: Properties and Characteristics of IN 939, Met. Prog. 115,
(3), 66-67, Mar. 1979.
465312. Weiss, I; Rosen, A; Brandon, D G, Creep of Udimet 500 During Thermal Cycling. Pt.
2. Time to Failure, Metall Trans A Apr. 1975, 6A, (4), 767-772.
408031. Chaku, P N; McMahon Jr, C J, Effect of an Air Environment on the Creep and
Rupture Behavior of a Ni-Base High-Temperature Alloy, Metall Trans, Feb. 1974, 5,
(2), 441-450.
304709. Coffin Jr, L F, Effect of Frequency on the Cyclic Strain and Low Cycle Fatigue
Behavior of Cast Udimet 500 at Elevated Temperature, Metall Trans, Nov. 1971, 2,
3105-3113.
19-8
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EPRI Licensed Material
Source References
109860. Wells, C H; Sullivan, C P, Low-Cycle Fatigue of Udimet 700 at 1700 f, ASM Trans
Quart mar. 1968, 61, 149-155.
9999904. Properties of Superalloys, American Society for Metals, ASM Metals Handbook
Ninth Edition, p 242-268.
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CHEMICAL COMPOSITION
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Chemical Composition
20-2
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Chemical Composition
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Chemical Composition
ELEMENT (% by weight)
ID MATERIAL NI CR CO MO TI AL C W TA CB ZR B HF V
75 Rene 80 bal 13.800 9.300 3.900 5.000 3.000 0.160 4.000 0.000 0.000 0.000 0.000 0.000 0.000
76 Rene 80 bal 13.800 9.400 3.900 5.000 3.150 0.160 3.800 0.000 0.000 0.040 0.017 0.000 0.000
77 MAR-M002 bal 9.000 10.000 0.250 1.500 5.500 0.150 10.000 2.500 0.000 0.055 0.015 1.250 0.050
78 MAR-M002 bal 9.000 10.000 0.250 1.500 5.500 0.150 10.000 2.500 0.000 0.055 0.015 1.500 0.050
79 MAR-M200 bal 9.000 10.000 0.000 1.700 4.700 <50 ppm12.500 0.000 1.000 0.000 0.000 0.000 0.000
80 MAR-M247 bal 8.400 10.000 0.650 1.050 5.500 0.130 10.000 3.050 0.000 0.055 0.015 1.400 0.000
20-4
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HEAT TREATMENT
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