Date: 12-Mar-2020

Certificate of Analysis: PA20-00338.008 MOTIVA ENTERPRISES LLC

TWO HOUSTON CENTER
909 FANNIN SUITE 700
PO BOX 4604
HOUSTON
TX
UNITED STATES
77010
The results shown in this test report specifically refer to the sample(s) tested as received unless otherwise stated. All tests have been performed using the latest revision of the methods
indicated, unless specifically marked otherwise on the report. Precision parameters apply in the determination of the above results. Users of analytical results, when establishing conformance
with commercial or regulatory requirements should note the full provisions of ASTM D3244, IP 367 and ISO 4259 in that context, the default confidence level of petroleum testing having been
set at the 95% confidence level. Your attention is specifically drawn to Sections 7.3.6., 7.3.7 and 7.3.8 of ASTM D3244. With respect to the UOP methods listed in the report below the user is
referred to the method and the statement within it specifying that the precision statements were determined using UOP Method 999. This Test Report is issued under the Company’s General
Conditions of Service (copy available upon request or on the company website at https://www.sgs.com/en/terms-and-conditions). Attention is drawn to the limitations of liability, indemnification
and jurisdictional issues defined therein. This report shall not be reproduced except in full, without the written approval of the laboratory.
CLIENT ORDER NUMBER : PRD2020GL0025CTL SGS ORDER NO.: 4599710
CLIENT ID : PRD2020GL0025CTL VESSEL : KRITI EMERALD
LOCATION : Motiva-Port Arthur,TX PRODUCT DESCRIPTION : Diesel - ULSD
SAMPLE SOURCE : Ships Tanks SOURCE ID : VESSEL COMPOSITE
SAMPLE TYPE : After Loading SAMPLED BY : SGS - Port Arthur
SAMPLED : 11-Mar-2020 00:10 RECEIVED 11-Mar-2020 04:46
ANALYSED : 11-Mar-2020 11:40 - 12-Mar-2020 04:52 COMPLETED : 12-Mar-2020 04:52
SGS OG&C makes no representation and assumes no responsibility for the reliability of analysis by a non-SGS Sub-Contract Laboratory. The laboratory analysis
for the Sub-Contract Laboratory tests are provided by:
S34 - Subcontracted to an External Laboratory - Inspectorate
PROPERTY METHOD RESULT UNITS MIN MAX False
API at 60°F ASTM D4052 37.4 °API -- --
Density at 15°C ASTM D4052 0.8375 kg/L -- --
Clear and Bright ASTM D4176 (Procedure 1) C&B --- Clear/Bright --
Free Water and Particulate Contamination ASTM D4176 (Procedure 1) Pass --- -- --
Sediment and Water ASTM D2709 <0.01 % (v/v) -- 0.05
Total Sulfur Content ASTM D2622 6.7 mg/kg -- 15
Ramsbottom Carbon Residue on 10 % ASTM D524 0.09 % (m/m) -- 0.21
Distillation Residue
Carbon Residue (on 10 % Distillation Residue) ASTM D4530 <0.1 % (m/m) -- 0.35
Oxidation Stability of Distillate Fuel Oil ASTM D2274
(Accelerated Method)
Filterable Insolubles 0.0 mg/100mL -- --
Adherent Insolubles 0.0 mg/100mL -- --
Total Insolubles 0.0 mg/100mL -- 1.0
Ash ASTM D482 <0.001 % (m/m) -- 0.01 #
Copper Strip corrosion (3h / 50°C {122°F}) ASTM D130 1A Rating -- 3
Distillation of Petroleum Products at ASTM D86
Atmospheric Pressure (Automated)
Initial boiling point (IBP) 174.4 °C -- --
5 % Recovered at 206.7 °C -- --
10 % Recovered at 221.0 °C -- --
20 % Recovered at 239.0 °C -- --
30 % Recovered at 254.5 °C -- --

# - Result is outside of test method limits and/or analytical range used in method precision study
AUTHORISED SIGNATORY

Cindy Haynes
Lab Tech

1203202004530000088261 Page 1 of 3 OGC-En_report-2014-08-12_v59i

SGS North America Inc. Oil, Gas & Chemicals Services 4575 Jerry Ware Drive, Beaumont, TX 77705, U.S.A Tel: +1-
(409)-727-1035 Fax: +1-(409)-729-1249

Member of the SGS Group ( Société Générale de Surveillance )

 Date: 12-Mar-2020

Certificate of Analysis: PA20-00338.008 MOTIVA ENTERPRISES LLC

TWO HOUSTON CENTER
909 FANNIN SUITE 700
PO BOX 4604
HOUSTON
TX
UNITED STATES
77010
CLIENT ORDER NUMBER : PRD2020GL0025CTL SGS ORDER NO.: 4599710
CLIENT ID : PRD2020GL0025CTL VESSEL : KRITI EMERALD
LOCATION : Motiva-Port Arthur,TX PRODUCT DESCRIPTION : Diesel - ULSD
SAMPLE SOURCE : Ships Tanks SOURCE ID : VESSEL COMPOSITE
SAMPLE TYPE : After Loading SAMPLED BY : SGS - Port Arthur
SAMPLED : 11-Mar-2020 00:10 RECEIVED 11-Mar-2020 04:46
ANALYSED : 11-Mar-2020 11:40 - 12-Mar-2020 04:52 COMPLETED : 12-Mar-2020 04:52
SGS OG&C makes no representation and assumes no responsibility for the reliability of analysis by a non-SGS Sub-Contract Laboratory. The laboratory analysis
for the Sub-Contract Laboratory tests are provided by:
S34 - Subcontracted to an External Laboratory - Inspectorate
PROPERTY METHOD RESULT UNITS MIN MAX False
40 % Recovered at 268.0 °C -- --
50 % Recovered at 279.5 °C -- --
60 % Recovered at 290.7 °C -- --
70 % Recovered at 302.4 °C -- --
80 % Recovered at 315.8 °C -- --
90 % Recovered at 333.5 °C 282 360
95 % Recovered at 346.9 °C -- --
% Recovery 98.0 % (v/v) -- --
Final boiling point (FBP) 355.5 °C -- --
% Residue 1.4 % (v/v) -- --
% Loss 0.6 % (v/v) -- --
Cloud Point ASTM D2500 -9 °C -- --
Flash Point by PMCC ASTM D93 (Procedure A) 157 °F -- --
Flash Point by PMCC ASTM D93 (Procedure A) 69.5 °C 52 --
Cold Filter Plugging Point (CFPP) ASTM D6371 -10 °C -- --
Kinematic Viscosity at 40°C ASTM D445 3.248 cSt 2.4 4.1
ASTM Colour ASTM D1500 <0.5 --- -- 1.5
Wear scar diameter at 60°C ASTM D6079 390 µm -- 520
S34 - Cetane Number ASTM D613 51.5 Rating 45 --
Conductivity ASTM D2624 110 pS/m 25 --
Cetane Index ASTM D976 53.9 Rating 40 --
Pour Point ASTM D97 -15 °C -- 4.0
Pour Point ASTM D97 5 °F -- --
Total Volume of the Sample Filtered ASTM D6217 300 mL -- --
Particulate Content ASTM D6217 0.0 mg/L -- --
Aromatic Hydrocarbon Types in Middle EN 12916
Distillates by HPLC
Mono Aromatic Hydrocarbons (Procedure A) 29.7 % (m/m) -- --

This document is only valid in its entirety and your attention is drawn to the Terms and Conditions on Page 1 of this report
AUTHORISED SIGNATORY

Cindy Haynes
Lab Tech

1203202004530000088261 Page 2 of 3 OGC-En_report-2014-08-12_v59i

SGS North America Inc. Oil, Gas & Chemicals Services 4575 Jerry Ware Drive, Beaumont, TX 77705, U.S.A Tel: +1-
(409)-727-1035 Fax: +1-(409)-729-1249

Member of the SGS Group ( Société Générale de Surveillance )

 Date: 12-Mar-2020

Certificate of Analysis: PA20-00338.008 MOTIVA ENTERPRISES LLC

TWO HOUSTON CENTER
909 FANNIN SUITE 700
PO BOX 4604
HOUSTON
TX
UNITED STATES
77010
CLIENT ORDER NUMBER : PRD2020GL0025CTL SGS ORDER NO.: 4599710
CLIENT ID : PRD2020GL0025CTL VESSEL : KRITI EMERALD
LOCATION : Motiva-Port Arthur,TX PRODUCT DESCRIPTION : Diesel - ULSD
SAMPLE SOURCE : Ships Tanks SOURCE ID : VESSEL COMPOSITE
SAMPLE TYPE : After Loading SAMPLED BY : SGS - Port Arthur
SAMPLED : 11-Mar-2020 00:10 RECEIVED 11-Mar-2020 04:46
ANALYSED : 11-Mar-2020 11:40 - 12-Mar-2020 04:52 COMPLETED : 12-Mar-2020 04:52
SGS OG&C makes no representation and assumes no responsibility for the reliability of analysis by a non-SGS Sub-Contract Laboratory. The laboratory analysis
for the Sub-Contract Laboratory tests are provided by:
S34 - Subcontracted to an External Laboratory - Inspectorate
PROPERTY METHOD RESULT UNITS MIN MAX False
Di Aromatic Hydrocarbons (Procedure A) 2.4 % (m/m) -- --
Tri+ - Aromatic Hydrocarbons (Procedure A) 0.2 % (m/m) -- --
Poly Aromatic Hydrocarbons (Procedure A) 2.6 % (m/m) -- --
Total Aromatic Hydrocarbons (Procedure A) 32.3 % (m/m) -- --
** End of Analytical Results **

This document is only valid in its entirety and your attention is drawn to the Terms and Conditions on Page 1 of this report
AUTHORISED SIGNATORY

Cindy Haynes
Lab Tech

1203202004530000088261 Page 3 of 3 OGC-En_report-2014-08-12_v59i

SGS North America Inc. Oil, Gas & Chemicals Services 4575 Jerry Ware Drive, Beaumont, TX 77705, U.S.A Tel: +1-
(409)-727-1035 Fax: +1-(409)-729-1249

Member of the SGS Group ( Société Générale de Surveillance )