Sr No Activity Time Required Hr.

Remarks
8
1 Line up and Inertisation of following systems 8
Reactor 1/2 feed system no 429-PA-03. 8
Reactor/ Settler train-1 system no 429-PA-07 8
Alkylate flushing oil distribution system no 429-FL-03 8
Refrigerant compressor-1 system no. 429-PA-15 8
Refrigerant compressor-2 system no. 429-PA-16 8
Refrigerant Vapor common header 429-PA-27 8
Reactor product Caustic/ Water wash system no 429-PA-18 8
Fresh Acid make up system no 429-VA-01 8
Spent Acid/ Pump out system no 429-VA-02 8
Caustic drain system no. 429-CD-01 8
Acidic drain drain system no. 429-VD-01 8
Acid flare system no. 429-BA-03 8
Wash water system 429-WW-01 8
Isobutane common system 429-PA-24 8
Liquid refrigeration Distribution -1 system 429-PA-25 8
Liquid refrigeration Distribution -2 system 429-PA-26 8
.Reactor product Caustic / Water wash system429-PA-18 8
HP isobutane flushing oil distribution 429-FL-01 8
.LP isobutane flushing oil distribution 429-FL-02 8
Filling feed preparation train-1with HTLN. Starting at d/s of XV-014 via a start up line from run
2
down line. 2
3 Filling HTLN to R101 2
4 Testing Reactor mixers on HTLN 2
5 Filling HTLN to V101 via Pump out header 2
6 Filling P103A/B/C and Testing them on HTLN
2
7 Filling P104A/B and testing on HTLN
8 Transferring HTLN to V121/V221 using P104A/B 4
Washing of refrigeration section including Economisers, Economiser liquid pumps, Chiller shell
9 side. 4
10 Test and send HTLN from chiller shell side to R101 via P101A/B
4
11 Testing P121A/B on HTLN
12 Testing Compressor KO drum pumps with HTLN 2
13 Pumping Reactor/ Settler HTLN to slop oil system. 8
14 Draining of Water and HTLN from Reactor/ Settler and from all low drain point including chiller 4
15 Draining of Water and HTLN from Refrigeration section low drain points. 4
16 Testing P19A/B and emptying V14 to slop oil system 2
17 Filling settler accumulator with HTLN from run down line via start up line 4
18 Testing P102A/B on HTLN 2
Acid filling

1 Fill up of Acid in V101 8

2 Fill up of Acid in R101 using P103A/B/C 8

Isobutane Filling Up
1 Filling iC4 from DIB overhead to Feed preparation Train-1 4
2 Filling of iC4 in R101 8
3 Filling of iC4 in V101 8
4 isobutane filling to refrigeration section -1 8
5 Compressor start up C-120 24
Product wash section
1 Filling of Caustic in caustic Accumulator 8
2 Filling of Water in Wash water accumulator 8
3 Starting Caustic to caustic wash mixer 2
4 Starting water to water mixers 2
5 Sampling and Product out to storage 48
6 Line up of washed water to purge water stripper 8
7 Starting Refrigeration purge to DP column via DP feed pump. 4

Cooling Down Reactor and Olefin Feed cut in

1 Line up of Refrigerant from Refrigeration section to Reactor 2
2 Line up of iC4 from DIB overhead to Reactor via Feed preparation unit. 2
3 Starting Recycle Acid Flow. 2
Considering reduction in temp. from ambient (Appx. 32oC) to
4 Cooing down Reactor up to 12oC from ambient temperature. 8
12 oC at the rate 3oC/hr
5 Start Olefin Feed to the Reactor and stabilisation 8
Purge wash section
1 Starting Caustic to purge caustic wash mixer 2
2 Starting water to purge water mixers 2
3 line up refrigeration purge to DP column feed 4
 Start up of Alkylation Reactor R201

Sr No Activity

1 Line up and Inertisation Reactor/ Settler train-2 system no 429-PA-08

2 Filling HTLN to R201starting at d/s of FV-040

3 Testing Reactor mixers on HTLN
4 Filling HTLN to V201 via Pump out header
5 Filling P203A/B/C and Testing them on HTLN
6 Filling P204A/B and testing on HTLN
9 Pumping Reactor/ Settler HTLN to slop oil system.
10 Draining of Water and HTLN from Reactor/ Settler and from all low drain point including chiller
12 Filling settler accumulator with HTLN from run down line via start up line
13 Testing P202A/B on HTLN
Acid filling
1 Fill up of Acid in V201
2 Fill up of Acid in R201 using P203A/B/C
Isobutane Filling Up
2 Filling of iC4 in R201
3 Filling of iC4 in V201
Cooling Down Reactor and Olefin Feed cut in
1 Line up of Refrigerant from Refrigeration section to Reactor
2 Line up of iC4 to R201.
3 Starting Recycle Acid Flow.
4 Cooing down Reactor up to 12oC from ambient temperature.
5 Start Olefin Feed to the Reactor and stabilisation
Time Required In Hr

2
2
2
2
8
4
4
2

8
8

8
8

2
2
2
8
8
1

3
4
5
6
7
8
9
10
11

1
2

1
2

1
2
3
4
5
 Start up of Alkylation Reactor R301

Line up and Inertisation Reactor/ Settler train-3 system no 429-PA-09

Reactor 3/4 feed system no 429-PA-04.

Filling Alkylate to R301

Testing Reactor mixers on Alkylate
Filling Alkylate to V301 via Pump out header
Filling P303A/B/C and Testing them on Alkylate
Filling P304A/B and testing on Alkylate
Pumping Reactor/ Settler Alkylate to slop oil system.
Draining of Water and Alkylate from Reactor/ Settler and from all low drain point including chiller
Filling settler accumulator with Alkylate from run down line via start up line
Testing P302A/B on Alkylate
Acid filling
Fill up of Acid in V301
Fill up of Acid in R301 using P303A/B/C
Isobutane Filling Up
Filling of iC4 in R301
Filling of iC4 in V301
Cooling Down Reactor and Olefin Feed cut in
Line up of Refrigerant from Refrigeration section to Reactor
Line up of iC4 to R301.
Starting Recycle Acid Flow.
Cooing down Reactor up to 12oC from ambient temperature.
Start Olefin Feed to the Reactor and stabilisation
8

2
2
2
2
8
4
4
2

8
8

8
8

2
2
2
8
8
 Start up of Alkylation Reactor R401

Sr No Activity

1 Line up and Inertisation Reactor/ Settler train-4 system no 429-PA-10

3 Filling Alkylate to R401

4 Testing Reactor mixers on Alkylate
5 Filling Alkylate to V401 via Pump out header
6 Filling P403A/B/C and Testing them on Alkylate
7 Filling P304A/B and testing on Alkylate
8 Pumping Reactor/ Settler Alkylate to slop oil system.
9 Draining of Water and Alkylate from Reactor/ Settler and from all low drain point.
10 Filling settler accumulator with Alkylate from run down line via start up line
11 Testing P402A/B on Alkylate
Acid filling
1 Fill up of Acid in V401
2 Fill up of Acid in R401 using P403A/B/C
Isobutane Filling Up
1 Filling of iC4 in R401
2 Filling of iC4 in V401
Cooling Down Reactor and Olefin Feed cut in
1 Line up of Refrigerant from Refrigeration section to Reactor
2 Line up of iC4 to R401.
3 Starting Recycle Acid Flow.
4 Cooing down Reactor up to 12oC from ambient temperature.
5 Start Olefin Feed to the Reactor and stabilisation
Time Required In Hr

2
2
2
2
8
4
4
2

8
8

8
8

2
2
2
8
8
Sr No
1
2
3
4
5
6
7
8
9
10
11

1
2

1
2
3
4
5

1
2
3
4
5
 Start up of Alkylation Reactor R501

Activity
Line up and Inertisation Reactor/ Settler train-5 system no 429-PA-11
Reactor 5/6 feed system no 429-PA-05.
Filling Alkylate to R501
Testing Reactor mixers on Alkylate
Filling Alkylate to V501 via Pump out header
Filling P503A/B/C and Testing them on Alkylate
Filling P504A/B and testing on Alkylate
Pumping Reactor/ Settler Alkylate to slop oil system.
Draining of Water and Alkylate from Reactor/ Settler and from all low drain point including chiller
Filling settler accumulator with Alkylate from run down line via start up line
Testing P502A/B on Alkylate
Acid filling
Fill up of Acid in V501
Fill up of Acid in R501 using P503A/B/C
Isobutane Filling Up
Filling iC4 from DIB overhead to Feed preparation Train-3
Filling of iC4 in R501
Filling of iC4 in V501
isobutane filling to refrigeration section -2
Compressor start up C-220
Cooling Down Reactor and Olefin Feed cut in
Line up of Refrigerant from Refrigeration section to Reactor
Line up of iC4 to R501.
Starting Recycle Acid Flow.
Cooing down Reactor up to 12oC from ambient temperature.
Start Olefin Feed to the Reactor and stabilisation
Time Required In Hr
8

2
2
2
2
8
4
4
2

8
8

4
8
8
8
24

2
2
2
8
8
 Start up of Alkylation Reactor R601

Sr No Activity

1 Line up and Inertisation Reactor/ Settler train-6 system no 429-PA-12

2 Filling Alkylate to R601starting at Feed coalescer downstream

3 Testing Reactor mixers on Alkylate
4 Filling Alkylate to V601 via Pump out header
5 Filling P603A/B/C and Testing them on Alkylate
6 Filling P604A/B and testing on Alkylate
9 Pumping Reactor/ Settler Alkylate to slop oil system.
10 Draining of Water and Alkylate from Reactor/ Settler and from all low drain point.
12 Filling settler accumulator with Alkylate from run down line via start up line
13 Testing P602A/B on Alkylate
Acid filling
1 Fill up of Acid in V601
2 Fill up of Acid in R601 using P603A/B/C
Isobutane Filling Up
2 Filling of iC4 in R601
3 Filling of iC4 in V601
Cooling Down Reactor and Olefin Feed cut in
1 Line up of Refrigerant from Refrigeration section to Reactor
2 Line up of iC4 to R601.
3 Starting Recycle Acid Flow.
4 Cooing down Reactor up to 12oC from ambient temperature.
5 Start Olefin Feed to the Reactor and stabilisation
Time Required In Hr

2
2
2
2
8
4
4
2

8
8

8
8

2
2
2
8
8
1

3
4
5
6
7
8
9
10
11

1
2

1
2

1
2
3
4
5
 Start up of Alkylation Reactor R701

Line up and Inertisation Reactor/ Settler train-7 system no 429-PA-13

Reactor 7/8 feed system no 429-PA-06

Filling Alkylate to R701

Testing Reactor mixers on Alkylate
Filling Alkylate to V701 via Pump out header
Filling P703A/B/C and Testing them on Alkylate
Filling P704A/B and testing on Alkylate
Pumping Reactor/ Settler Alkylate to slop oil system.
Draining of Water and Alkylate from Reactor/ Settler and from all low drain point including chiller
Filling settler accumulator with Alkylate from run down line via start up line
Testing P702A/B on Alkylate
Acid filling
Fill up of Acid in V701
Fill up of Acid in R701 using P703A/B/C
Isobutane Filling Up
Filling of iC4 in R701
Filling of iC4 in V701
Cooling Down Reactor and Olefin Feed cut in
Line up of Refrigerant from Refrigeration section to Reactor
Line up of iC4 to R701.
Starting Recycle Acid Flow.
Cooing down Reactor up to 12oC from ambient temperature.
Start Olefin Feed to the Reactor and stabilisation
8

2
2
2
2
8
4
4
2

8
8

8
8

2
2
2
8
8
 Start up of Alkylation Reactor R801

Sr No Activity

1 Line up and Inertisation Reactor/ Settler train-8 system no 429-PA-14

2 Filling Alkylate to R801starting at Feed coalescer downstream

3 Testing Reactor mixers on Alkylate
4 Filling Alkylate to V801 via Pump out header
5 Filling P803A/B/C and Testing them on Alkylate
6 Filling P804A/B and testing on Alkylate
9 Pumping Reactor/ Settler Alkylate to slop oil system.
10 Draining of Water and Alkylate from Reactor/ Settler and from all low drain point.
12 Filling settler accumulator with Alkylate from run down line via start up line
13 Testing P802A/B on Alkylate
Acid filling
1 Fill up of Acid in V801
2 Fill up of Acid in R801 using P803A/B/C
Isobutane Filling Up
2 Filling of iC4 in R801
3 Filling of iC4 in V801
Cooling Down Reactor and Olefin Feed cut in
1 Line up of Refrigerant from Refrigeration section to Reactor
2 Line up of iC4 to R801.
3 Starting Recycle Acid Flow.
4 Cooing down Reactor up to 12oC from ambient temperature.
5 Start Olefin Feed to the Reactor and stabilisation
Time Required In Hr

2
2
2
2
8
4
4
2

8
8

8
8

2
2
2
8
8
 Start up of Alkylation Reactor R101

1 Systems Required

2 Hydrotest of the system completed

3 Flushing of the system completed
4 Leak test, Line up and Inertisation completed

Activity

5 HTLN wash
5a. HTLN wash of R101
5b. HTLN wash of V101
5c. HTLN wash of Refrigeration section-1 via spent acid pump
5d. HTLN wash of Refrigeration section-2 via spent acid pump
Total
6 Acid fill up
6a. Acid filling in R101
6b. Acid filling in V101
Total
7 Isobutane fill up
7a.Isobutane fill up in R101
7b.Isobutane fill up in V101
Total

8 Cooling down R101

9 Olefin feed cut in R101

Punch Point List

Draining of Water and HTLN from low point drains (List is
1
provided in SOP)
429-PA-03,429-PA-07,429-FL-03,429-PA-15,429-PA-
16,429-PA-27, 429-PA-18, 429-VA-01, 429-VA-02, 429-
CD-01,429-VD-01,429-BA-03

Approximate Time Required, Hrs Remarks

8
8
4
4
24

6
6
12

4
4
8
Considering reduction in temp. from
8 ambient (Appx. 32oC) to 12 oC at the rate
3oC/hr
12