Translation of the Original Instructions

FOUNDRY-MASTER Smart

Version: 1.0GB/2016-02-03
Document number: : 6000000186

Oxford Instruments Analytical GmbH

Wellesweg 31 · 47589 Uedem / Germany
Phone: +49 (0) 2825 9383-0
Fax: +49 (0) 2825 9383-100
[email protected] · www.oxford-instruments.com
All rights reserved

This document may only be used by the recipient for the intended purpose. It shall not be reproduced in whole
or in part or translated into another language without prior written consent.

Right to technical changes reserved.

© 2015 Oxford Instruments Analytical GmbH

 Preface FOUNDRY-MASTER Smart

Preface

To ensure smooth operation, we have drawn up these practical operating instructions.

We explicitly point out that Oxford Instruments Analytical GmbH does not assume
responsibility for damage or losses resulting from the disregard of these operating
instructions or the misuse of the products described herein.

These operating instructions are protected by copyright.

They can also be supplied on CD (Acrobat® Reader 7.0).

Our products are subject to continuous further development — technical changes are
reserved.

Uedem, November 2015

Version: 1.0GB/2016-02-03 © 2015 Oxford Instruments Analytical GmbH

 Table of contents FOUNDRY-MASTER Smart

Table of contents

1 Notes regarding the use of these operating instructions.................................................................... 1

1.1 Validity of the operating instructions .......................................................................................... 1
1.2 Pictograms and signal words ..................................................................................................... 2
1.2.1 Hazard symbols .......................................................................................................... 2
1.2.2 Symbols for personal protective equipment................................................................ 2
1.2.3 Information symbol ..................................................................................................... 2

2 Intended use and misuse ....................................................................................................................... 3

3 General safety instructions .................................................................................................................... 5

3.1 Safety instructions for work on the electrical system ................................................................. 7
3.2 Personnel qualification ............................................................................................................... 8

4 Description of the instrument .............................................................................................................. 11

4.1 Function ................................................................................................................................... 11
4.2 Components and operating controls ........................................................................................ 12
4.2.1 Spectrometer components........................................................................................ 13
4.2.2 Operating controls, displays and ports of the spectrometer ..................................... 14
4.3 Technical data.......................................................................................................................... 15

5 Scope of delivery, transport, set-up and installation......................................................................... 17

5.1 Scope of delivery...................................................................................................................... 17
5.2 Transport.................................................................................................................................. 17
5.3 Set-up....................................................................................................................................... 18
5.4 Installation ................................................................................................................................ 20

6 Putting into service ............................................................................................................................... 21

7 Quick start.............................................................................................................................................. 25
7.1 Analysing in spark mode (argon) ............................................................................................. 25
7.2 Flowcharts for analysis and recalibration ................................................................................. 28
7.2.1 Start and sequence of a check measurement in spark mode................................... 28
7.2.2 Recalibrating "Full" ................................................................................................... 29
7.2.3 Recalibrating "Type" ................................................................................................. 30
7.2.4 Performing an analysis ............................................................................................. 31

8 Removal from service ........................................................................................................................... 33

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FOUNDRY-MASTER Smart Table of contents

9 Maintenance........................................................................................................................................... 35
9.1 Safety instructions for maintenance and repair........................................................................ 35
9.2 Maintenance table.................................................................................................................... 36
9.3 Disassembling and cleaning the spark stand........................................................................... 37
9.4 Maintenance of the electrode................................................................................................... 39
9.4.1 Replacing the electrode ............................................................................................ 39
9.4.2 Adjusting the electrode ............................................................................................. 41
9.4.3 Cleaning the electrode with the electrode brush....................................................... 42
9.5 Replacing filters........................................................................................................................ 43
9.6 Cleaning and filling the wash bottle.......................................................................................... 43
9.7 Replacing the argon bottle(s) ................................................................................................... 44
9.8 Cleaning the instrument ........................................................................................................... 44
9.9 Measuring adapters ................................................................................................................. 45

10 Faults ...................................................................................................................................................... 47
10.1 Information regarding WINDOWS™ installation ...................................................................... 47
10.1.1 WINDOWS™ CD-ROM ............................................................................................ 47
10.1.2 Installing the printer .................................................................................................. 47
10.1.3 Power options ........................................................................................................... 47
10.2 General faults........................................................................................................................... 48
10.3 Faults of FOUNDRY-MASTER Smart...................................................................................... 49

11 Reshipment and disposal ..................................................................................................................... 51

11.1 Declaration of Decontamination ............................................................................................... 51
11.2 Disposal ................................................................................................................................... 51

12 Annex ..................................................................................................................................................... 53
12.1 Service ..................................................................................................................................... 55
12.2 Glossary ................................................................................................................................... 57
12.3 Standard accessory case, packed ........................................................................................... 59
12.4 Forms ....................................................................................................................................... 61
12.4.1 Declaration of Conformity ......................................................................................... 61
12.4.2 Declaration of Decontamination................................................................................ 61

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 Table of figures FOUNDRY-MASTER Smart

Table of figures

4 Description of the instrument

Fig. 4-1 Instrument components ..................................................................................................... 13
Fig. 4-2 Operating controls and ports of the instrument.................................................................. 14

5 Scope of delivery, transport, set-up and installation

Fig. 5-1 Workstation at the spectrometer ........................................................................................ 18
Fig. 5-2 Ports on the instrument...................................................................................................... 20

6 Putting into service

Fig. 6-1 On/off switch ...................................................................................................................... 21
Fig. 6-2 Display of the requested recalibration sample ................................................................... 21
Fig. 6-3 Instrument front.................................................................................................................. 22

7 Quick start
Fig. 7-1 Positioning the sample (example) ...................................................................................... 26

9 Maintenance
Fig. 9-1 Reminder to clean the spark stand .................................................................................... 37
Fig. 9-2 Opening the spark stand plate ........................................................................................... 37
Fig. 9-3 O-ring spark stand plate..................................................................................................... 37
Fig. 9-4 Screwing out the spacer .................................................................................................... 39
Fig. 9-5 Installing the electrode ....................................................................................................... 40
Fig. 9-6 Screwing out the spacer .................................................................................................... 41
Fig. 9-7 Installing the electrode ....................................................................................................... 41
Fig. 9-8 Spark stand........................................................................................................................ 42
Fig. 9-9 Wash bottles ...................................................................................................................... 43
Fig. 9-10 Argon bottle (example)....................................................................................................... 44
Fig. 9-11 Adjustment aid and boron nitride collimator (example) ...................................................... 45
Fig. 9-12 "side-on" wire adapter on spark stand plate (example)...................................................... 46
Fig. 9-13 "face-on" wire adapter on spark stand plate (example) ..................................................... 46

10 Faults
Fig. 10-1 Power options (Windows) .................................................................................................. 47

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1 Notes regarding the use of these operating instructions FOUNDRY-MASTER Smart

1 Notes regarding the use of these operating instructions

This chapter contains information regarding these operating instructions as well as

general safety instructions for handling the instrument.

Note! Due to the customer-specific configuration of all spectrometers, the matrices and/or
grades displayed on your screen can deviate from the illustrations and descriptions in
this manual and in the software manual.

If not indicated otherwise, we assume that the user has already started the
WINDOWS™ operating system. Basic knowledge as to handling software under
WINDOWS™ is assumed as given.

1.1 Validity of the operating instructions

These operating instructions are valid for FOUNDRY-MASTER Smart stationary optical
emission spectrometers.
These operating instructions are only valid in combination with the "WasLab" software
manual.

Observe these operating instructions for all work. If the instrument is not used according
to these operating instructions, your safety as well as the instrument function can be
affected.
To maintain product reliability, enhance the life cycle and avoid downtimes, do in any
case observe the instructions herein.

Furthermore observe the current valid regulations for accident prevention and
environmental protection as well as the recognised technical rules for safe working
according to good professional practice.

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FOUNDRY-MASTER Smart 1 Notes regarding the use of these operating instructions

1.2 Pictograms and signal words

Important information in these operating instructions and on the instrument is marked

with the following pictograms.

1.2.1 Hazard symbols

Danger!
This sign indicates an immediate risk of death or injury.

Danger!
Hazardous electric current!
This sign indicates hazardous electric current.

Warning!
Crush hazard!
This sign indicates hazardous situations with limb crush hazard.

Warning!
Hot surfaces!
This sign indicates hot surfaces of the instrument.

1.2.2 Symbols for personal protective equipment

Wear eye protection!

Wear ear protection!

Wear protective gloves!

1.2.3 Information symbol

Note! Tips and information are marked with the word "Note!" in bold print.

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2 Intended use and misuse FOUNDRY-MASTER Smart

2 Intended use and misuse

The stationary optical emission spectrometer (OES) is exclusively intended for

qualitative and quantitative element analysis of alloys.

The instrument may only be used in dry rooms.

The instrument may only be operated with the protective covers installed.

The intended use also includes

• the observance of all information and regulations in these operating instructions,
• the observance of the software manual,
• the observance of the technical data and
• the adherence to the periods for inspection and maintenance work prescribed
or contained in these operating instructions.

Misuse The use in hazardous areas is not permitted.

The employment of insufficiently qualified personnel is regarded as misuse.

Measurements without correctly positioned samples is regarded as misuse.

Unauthorised structural modifications, attachments to or conversions of the instrument,

modifications of and interference with the instrument program as well as unauthorised
updates of the operating system and the software are prohibited. Improper interference
with the instrument or the software by the customer will void any warranty.

The manufacturer is not liable for damage resulting from misuse.

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3 General safety instructions FOUNDRY-MASTER Smart

3 General safety instructions

Observe the following safety instructions for the operation of the instrument:

• Only operate the instrument if free from defects and under observance of these
operating instructions.
• Prior to starting work, read these operating instructions. This applies particularly
to personnel who only occasionally work with the instrument, such as
maintenance personnel.
• Observe all safety and information signs on the instrument and maintain legible.
• Check the instrument for external visible damage. Report any visible damage
and only put the instrument into service after remediation of damage.
• Protect the instrument from influences which can cause corrosion or affect the
function of components.
• Do not place any liquids on top of the instrument.
• No not excessively load the hood of the instrument (>10 kg).
• Internal or external safety devices of the instrument shall in no case be made
inoperative.
• Maintenance and repair may only be carried out by qualified specialised
personnel.
• In the event of malfunctions, remove the instrument from service. Have faults
immediately remedied by an electrically skilled person.
• Never open the housing! There are no user-relevant elements inside the
housing.
• Have defective parts of the instrument immediately replaced.
• Spare parts must comply with the technical requirements specified by Oxford
Instruments Analytical GmbH. This is always the case if you use original spare
parts.
• For inspection or repair work, attach a warning sign against restart to the
external de-energizing device.
• The safety instructions must be supplemented with national accident prevention
regulations.
• During measurement, electromagnetic waves may disturb other devices.
Please observe the information in chapter 5.3, page 19.
• In the event of an emergency, press the stop switch on the front side to abort
the measurement and switch the instrument off at the main switch.
• Always use the sample clamp (hold-down device). The hold-down device
establishes the electrical connection between sample and electrode. When the
hold-down device is positioned next to the spark stand plate, measurement is
not possible.
• The sample weight shall not exceed the admissible load of the spark stand (see
chapter 4.3, page 16).
• The instrument must not be exposed to the following:
• extreme temperatures or temperature changes;
• heavy shock or vibration (particularly when the transport lock has been
removed);
• moisture and condensing humidity;
• metal dust and large quantities of dust in general.

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FOUNDRY-MASTER Smart 3 General safety instructions

Danger!
During work with the spectrometer, hazards may arise from electric current / volt-
age. Observe the following safety instructions to avoid the risk of an electric
shock:
• If you touch the instrument and electrically conducting parts, such as machines
or devices, simultaneously, voltage can be generated from possible potential
differences which is perceptible but non-hazardous.
• Never spark wet or moist surfaces, since there is a risk of a short circuit!
• Never spark without a clamped sample!
• When the excitation source is switched on, avoid any contact with the spark
electrode!
• When working at the spark stand, e.g. for changing the electrode, do in any case
switch off the excitation source.
• Do not touch the sample during measurement!
• During sparking, do not, under any circumstances, introduce a conducting
object into the proximity of the spark stand hole!
• During sparking, do not, under any circumstances, remove a conducting
object from the spark stand hole!
• With the spark stand hole open during sparking, do not, under any
circumstances, bring a part of your body into its immediate vicinity!

Warning! Hot surface!

Small and/or thin samples can become hot during sparking. During measurement of
small or thin samples, wear protective gloves!

Warning!
During the analysis of samples that do not cover the hole in the spark stand plate (e.g.
wires), spark light can emerge. Your eyes can be blinded by the light and the high-
energy UV radiation can damage your eyes. Never look into the arc! Wear suitable eye
protection during work.

Warning!
During the analysis of samples that do not cover the hole in the spark stand plate (e.g.
wires), the sound generated upon sparking (measuring) exits through the gap. Wear ear
protection when sparking samples that do not cover the hole.

Danger!
When measuring hazardous substances, there is a hazard from escaping gases or
vapours.
• The operator must know what substances he is working with.
• The operating company must provide for suitable protective measures (e.g.
exhaustion). (Metal dusts are primarily released. Those are usually washed in
the washing bottle and do not escape.)

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3 General safety instructions FOUNDRY-MASTER Smart

3.1 Safety instructions for work on the electrical system

Observe the following safety instructions for work on the electrical system:

• Only electrically skilled persons may carry out work on the electrical system.
• Do not carry out any work at live parts of the electrical system.
Observe the following safety rules when working on the electrical system:

1. De-energise.
2. Secure against restart.
3. Verify de-energised state.
4. Shield live parts.
5. Earth and short-circuit.

• In the event of faults of the electrical energy supply, immediately switch off the
instrument.
• An interruption in the energy supply of > 20 ms requires restarting the software.
• In the event of a short circuit, there is a risk of spark generation or the break-out
of a fire. Only use original fuses with specified amperage and tripping
characteristic! When a fuse must be replaced, first identify the corresponding
cause and remedy the error before you replace the fuse.
• If work on live parts is required, only use insulated tools.

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FOUNDRY-MASTER Smart 3 General safety instructions

3.2 Personnel qualification

All persons entrusted with work at the instrument commit themselves to the following
before starting work:
• to observing the basic regulations related to occupational safety and accident
prevention;
• to reading the safety instructions and warnings in these operating instructions
and to confirming with their signature that they have understood them;
• to wearing or using personal protective clothing and accessories or workstation-
related personal protective clothing and accessories serving occupational
safety as required for reasons of safety during work.

Only personnel who have read and understood these operating instructions may work
with the instrument.
Personnel to be trained or instructed or personnel in training shall only work with the
instrument under constant supervision of an experienced person.
Only personnel who are at least 18 years of age may be entrusted with independent
work with the instrument.
The individual activities at the instrument require different personnel qualifications listed
in table 3-1, page 9.

The various qualifications comprise the following abilities and knowledge:

• Instructed persons must be able to operate the instrument and identify possible
damage and hazards related to the instrument.
• Electrically skilled persons must be able to read and understand electric circuit
diagrams, to put electrical machines/devices into service, to maintain them, to
wire control cabinets, to install control software, to ensure the functionality of
electrical components and to identify possible hazards from handling electrical
and electronic systems.
• Trained pneumatic specialists must be able to read and understand pneumatic
circuit diagrams, to put pneumatic systems into service and to maintain them, to
remove and install pneumatic hoses, to ensure the functionality of pneumatic
components, to evaluate the work on the pneumatic system they have been
entrusted with and to identify possible hazards.

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3 General safety instructions FOUNDRY-MASTER Smart

Table 3-1 Overview of minimum required personnel qualifications

Skilled workersb with

Instructed the qualification of an Electrically
Pneumatic
Activities "industrial mechanic" skilled per-
personsa specialists
or "mechatronics sons
engineer"
Transport X
Putting into service, operation,
X
removal from service
Cleaning X
Mechanical work:
troubleshooting, repair and X X
maintenance
Work on the electrical system:
troubleshooting, repair and X
maintenance
Work on the pneumatic system:
troubleshooting, repair and X
maintenance
Disposal X

a. Instructed persons are persons trained in handling the instrument by Oxford Instruments
Analytical GmbH. For instruments delivered with a PC user interface, PC knowledge is required.
b. A skilled worker is who, due to his professional training, his knowledge and experience as well
as due to his knowledge of relevant regulations, is able to judge the work assigned to him as
well as to identify possible hazards.

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4 Description of the instrument FOUNDRY-MASTER Smart

4 Description of the instrument

4.1 Function

FOUNDRY-MASTER Smart is a laboratory spectrometer for qualitative and quantitative

analysis of metal grades.
The metal sample to be analysed is positioned at the spark stand and clamped with a
hold-down device. The sample is sparked with an electrically generated arc at the
surface. Upon discharging, an area of the sample surface is melted and evaporated by
the spark. From the high energy in the spark, a plasma results. This plasma emits light
which is spectrally analysed and measured by means of CCDs (charge coupled devices,
light-sensitive semiconductor chips). A certain area of the measured spectrum can be
assigned to every element.
The instrument is operated via control keys using a supplied software which displays the
analysis result on the screen of the connected computer. The analysis result can be
stored in the internal database or exported. Through comparison with stored grade data
it can be determined immediately whether or with what deviations the analysed grade
fulfils the required specifications. Certificates can be easily designed and printed.

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FOUNDRY-MASTER Smart 4 Description of the instrument

4.2 Components and operating controls

The instrument consists of three important assemblies:

Excitation Source A digitally controlled excitation source generates a strong electric discharge between
sample and electrode in the argon-purged spark stand melting a small part of the sample
material out of the surface, evaporating it and exciting it to glow in a plasma. The argon
atmosphere avoids oxidation on the sample surface and changes the discharge
conditions insofar as practically all discharge energy is converted at the sample
connected as a cathode. The characteristic blue light (common in ferrous metal)
contains the spectral information about the elements and their contents in the sample.

Optics The light generated in the spark stand is mapped on a diffraction grating and spread out
into its spectral components. Light with longer wavelengths is deflected ("diffracted")
stronger than light with shorter wavelengths. This produces an emission spectrum of the
sample which can be evaluated using light-sensitive detectors. FOUNDRY-
MASTER Smart uses the latest generation of CCD line sensors featuring high sensitivity
and long life. The complete optical system operates in an argon atmosphere so that
emission wavelengths shorter than approx. 200 nm are not absorbed by air.
FOUNDRY-MASTER Smart has one light path through which the light reaches the
optical system. This light path is an argon-purged tube ("direct light path").

Readout system Recording a complete spectrum requires a fast readout system to process large
amounts of data fast. Light intensities obtained from the emission spectrum are
converted to contents using the calibration curves stored in the instrument.
The contents are displayed on the screen and further processed (quality detection,
monitoring of limit values for process control, etc.). FOUNDRY-MASTER Smart uses a
special processor which allows the simultaneous evaluation of up to 18 individual CCD
sensors. That permits very precise analysis by means of DIA (Dynamic Integration
Algorithm).

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4 Description of the instrument FOUNDRY-MASTER Smart

4.2.1 Spectrometer components

FOUNDRY-MASTER Smart consists of the following components (see fig. 4-1):

• housing (1)
• hold-down device (2)
• spark stand (3) with removable spark stand plate
• operating elements on the front (4)
• fan/filter (5)
• operating elements and connection on the rear (6)
• washing bottle to clean off-gases from the spark stand (no picture)
• computer with monitor and mouse (not depicted)

1 2 3 4 1 5 6 5

Fig. 4-1 Instrument components

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FOUNDRY-MASTER Smart 4 Description of the instrument

4.2.2 Operating controls, displays and ports of the spectrometer

There are the following operating controls, display elements and ports on FOUNDRY-
MASTER Smart (see fig. 4-2):
• hold-down device (1) for sample
• rotary knob (2) to switch on the excitation source
• stop button (3)
• start button (4)
• fuses (5)
• socket (6) for power plug
• on/off switch (7)
• port (8) for argon
• exhaust hose for washing bottle (9)
• USB port (10) to connect the computer
• computer monitor (not depicted)
• computer keyboard (not depicted)
• computer mouse (not depicted)

3
4
1

5 6 7 8 9 10
Fig. 4-2 Operating controls and ports of the instrument

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4 Description of the instrument FOUNDRY-MASTER Smart

4.3 Technical data

Table 4-1 Technical data of FOUNDRY-MASTER Smart

Parameter Value
Designation FOUNDRY-MASTER Smart

Dimensions width x height x depth 415 mm x 280 mm x 665 mm

Weights instrument approx. 35 kg

max. sample weight 10 kg

Electrical system voltage 90-250 VAC, 50–60 Hz

fuse 2 x 6 A slow, 5 x 20 mm

power consumption, max. 700 VA

power consumption in idle state 100 VA; source switched on

(without PC)
50 VA; source switched off

protection class IP20

optical system multi-CCD optics with Paschen-Runge mounting

focal length 300 mm

number of grid lines 1774/mm

wavelength range 174-419 nm

Excitation source sparking high-energy pre-spark (HEPS)

parameters
frequency 80–500 Hz

voltage 250–500 V

Ambient conditions temperature 40 °C max.

air humidity 10–90 %, non-condensing

System requirements for Operating system: The current Microsoft® Windows™ version at the
external PC time of printing or the Microsoft® Windows™ version officially
designated by Oxford Instruments Analytical GmbH at the time of
ordering/delivery or its successor version.

Intel® Pentium® 4, AMD Athlon™ 64 or better

1 GB RAM or more
100 MB available space
mouse
screen resolution: 1024 x 768
1 x free USB 2.0 port
DVD drive
Options wire adapter set
sample preparation devices
accessories set
consumables set

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5 Scope of delivery, transport, set-up and installation FOUNDRY-MASTER Smart

5 Scope of delivery, transport, set-up and installation

5.1 Scope of delivery

The following objects are included in the scope of delivery:

• FM Smart basic instrument incl. optical system
• set of recalibration samples
• tungsten electrode with cleaning brush
• standard accessory case, packed (chapter 12.3, page 59)
• copper tube for argon connection
• washing bottle for off-gases incl. off-gas hose
• pressure reducer

Optional • transport case

Unpack the instrument and check the delivered contents for completeness.
Should any parts be missing or damaged, please immediately contact our local Oxford
Instruments Analytical GmbH partner.

5.2 Transport

Note! Observe the following for transport:

• In general, the instrument must be lifted and transported with greatest care.
• During transport, make sure the instrument is in horizontal position!

For short-distance transport (e.g. within the same room), the instrument can be lifted and
transported by two people.

For transport over longer distances use the optional transport case supplied.

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FOUNDRY-MASTER Smart 5 Scope of delivery, transport, set-up and installation

5.3 Set-up

Warning!
When the instrument is placed on the working surface, there is a crush hazard between
the instrument and the surface the instrument is placed on.
Make sure the surface is horizontal and level.
Check if the feet of the instrument are sufficiently screwed out.
Wear protective gloves.

• Place the instrument on a horizontal, level and sufficiently stable working

surface at ergonomically suitable height (workbench or work table).
Indications regarding the instrument weight are given in the technical data in
chapter 4.3, page 16.
• Make sure there is sufficient distance to the wall (> 15 cm) on the rear side so
that power cord, Ar line and exhaust hose to the washing bottle are not kinked.
• Straightly align the instrument. For improved accessibility for larger samples,
the spark stand should protrude.
• Set up the instrument so that the operator can operate the instrument on the
front (1, fig. 5-1) without restrictions to his freedom of movement. The
instrument is operated at the computer screen, at the spark stand (3) and at the
buttons (2) on the front.

Fig. 5-1 Workstation at the spectrometer

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5 Scope of delivery, transport, set-up and installation FOUNDRY-MASTER Smart

Note! In spark mode, the instrument emits electromagnetic waves. This radiation can cause
radio interference. To minimise emitted interference, the instrument must be set up and
operated as specified in this manual. In the event of electromagnetic incompatibility, the
operating company may have to take additional measures.
The following procedures may contribute to minimising interference:
• enlarging the distance to the "receivers" (power and signal/telecommunications
lines as well as radio receivers);
• specific coordination with respect to other systems;
• additional filtering for the power supply;
• low-inductive earthing of the sample to be analysed;
• and in special cases shielding of the entire instrument.

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FOUNDRY-MASTER Smart 5 Scope of delivery, transport, set-up and installation

5.4 Installation

Note! The spectrometer may only be installed by a person authorised by Oxford Instruments
Analytical GmbH.

Note! A software licence key is required for the operation of the instrument. It must be
requested and installed 180 days after delivery or 90 days after initial start-up of the
instrument at the latest, whichever comes first. Further information can be obtained from
the customer service of Oxford Instruments Analytical GmbH (chapter 13.1, page 71).

If you connect the mains voltage, the PC and the argon to the device yourself, proceed
as follows:

1. Connect the PC to the instrument (1, fig. 5-2) using the supplied USB cable. Do
not use a USB cable longer than 2 m.
Should the original USB cable be replaced, provide the new cable with a type
"Würth 742 727 33" ferrite.
2. Connect keyboard, mouse and printer to the computer.
3. Connect the power cable to the PC.
4. Insert the exhaust hose (2) into the water-filled washing bottle.
5. Connect the power cable to the spectrometer (4).
The instrument may only be operated on mains with protective conductors.
6. Use the supplied copper pipe to connect the device's argon connection (3) to
the argon container or supply.

4 3 2 1

Fig. 5-2 Ports on the instrument

Note! Only use 4.8 argon suitable for spectrometry (99.998 % or above). Other gases in the
argon (e.g. nitrogen) can affect precision.

7. Ensure that the supply pressure is always in the range of 3.0–5.0 bar.

To avoid condensation inside the instrument, prior to putting it into service, leave the
instrument to acclimatise to the ambient temperature.

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6 Putting into service FOUNDRY-MASTER Smart

6 Putting into service

The initial start-up of the instrument is carried out by customer service employees of
Oxford Instruments Analytical GmbH or an authorised representative and includes a
complete functional test of the instrument as well as operator training.

Should you put the instrument into service yourself, proceed as follows:

Note! The following description of putting into service assumes that you are familiar with
operating the software and the instrument.

Prerequisite • The installation of the instrument has been carried out as described in
chapter 5.4, page 20.
• A known (analysed or certified) sample of similar chemical composition as the
probe you want to analyse is available.

Recalibration 1. Switch on the computer and wait until WINDOWS™ has been completely
started up.
2. Open the WASLab spectrometer software double-clicking the WASLab
icon . The start screen is displayed.

3. Switch on the spectrometer at the on/off switch (1, fig. 6-1).

Fig. 6-1 On/off switch

4. In the start screen, select "Analysis" mode.

5. Select a matrix and analysis program and confirm your selection with "OK". The
analysis screen is displayed.
6. Click "Recal." to recalibrate the instrument. The selection window for the
recalibration method is displayed.
7. Select the "Full" option. The name of the first recalibration sample (e.g. RE12)
is displayed in the centre of the screen.

Fig. 6-2 Display of the requested recalibration sample

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FOUNDRY-MASTER Smart 6 Putting into service

8. Place the displayed recalibration sample on the spark stand (1, fig. 6-3) and fix
it with the hold-down device (2).
9. Switch on the excitation source at the rotary knob (3) on the front of the
instrument.

Fig. 6-3 Instrument front

10. Spark this well prepared (freshly ground, fat-free) sample at least 3 times by
pressing the start button (4) or clicking the "Start" button in the analysis screen.

Note! Avoid sparking the same point twice. The RSD value in the left column (RSD: Relative
Standard Deviation) is displayed after the third sparking and should be less than or
equal to 10 %.
• If that is the case, carry out further sparkings.
• The results of sparking with the greatest deviations from the average value
are deleted (average value display in the right column). To delete individual
sparkings, highlight the column by double-clicking and click the "Delete"
button. Caution: Deletion cannot be undone!

11. Clean the electrode tip.

12. In the upper left of the screen click "Next" to spark the next recalibration sample.

Note! For the other samples, the RSD value in the left column should be less than or equal to
3 %.

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6 Putting into service FOUNDRY-MASTER Smart

Checking the results After recalibration is completed ("Recalibration successful" note), proceed as follows to
check the recalibration factors:

1. From the "Mode" menu bar and, in the following window, from the picklist, select
"Recalibration factors".
2. Confirm your selection with "OK". The analysis window with the recalibration
factors is displayed. All values in the "Factor" column should range between 0.5
and 2.0, ideally near 1.
3. The "offset.dat" file is in the program directory. Open the file (e.g. with the
editor).
With an ambient temperature of about 20 °C, the values in the last line should
range between -10 and +10.
Values marked with an asterisk (*) can be ignored.

Note! If factors and/or offset values are outside these ranges, please contact our local Oxford
Instruments Analytical GmbH service partner.

After putting into service and recalibration, back up the whole "Master" program
directory so that all relevant data can be recovered if required.
The customer is responsible for regular data backup. Oxford Instruments Analytical
GmbH cannot be called to account in the event of data loss. Data loss can be caused
by a failed hard disk, computer viruses, etc.

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7 Quick start FOUNDRY-MASTER Smart

7 Quick start

7.1 Analysing in spark mode (argon)

Argon quality If the instrument has not been used during a prolonged period of time, the argon system
must be sufficiently purged with argon to avoid contamination. Used argon must contain
less than 5 ppm of O2 and H2O (4.8 argon; 99.998 % or above). Analysis of some
elements such as carbon is heavily affected by impurified argon. With an argon quality
of 4.6 (99.996 %), analysis may not be possible any more.
During measurement breaks, the spark stand hole should always be covered with a
sample.

Sample preparation The most critical part of spark analysis is the preparation of the sample.
The importance of sample preparation is often underestimated, although quality and
reliability of the analysis directly depend on it.
Since the spark discharge only evaporates material on the sample surface and does not
penetrate deep into the material, you also measure all impurities on the surface.
Dirt, oils, oxides and even fingerprints can disturb analysis and even prevent the
formation of plasma. In that case, you obtain a poor burn spot with very low luminous
efficacy ("white focal spot"). The result is a faulty analysis, that means the analysed
sample composition does not correspond to the actual composition.

Note! Observe the following information before analysing the sample:

• Freshly ground and clean sample surfaces are a basic requirement for precise
analyses!
• Replace the abrasive paper as soon as you change the matrix (e.g. from Cu to
Fe) or as soon as the paper does not grind very well any more.
In general, one set of recalibration samples can be prepared with the same
abrasive disk, always starting with the pure sample which is the sample with the
smallest number in the stamped designation (e.g. "RA10" for Al matrix).
• Do not use silicon carbide paper (SiC), since the silicon and carbon content
adulterates the analysis of those elements. Oxford Instruments Analytical
GmbH recommends the use of aluminium oxide paper (corundum) or zirconium
oxide paper. Use paper of grain size 60.
• The spark stand must be cleaned after 300 sparkings at the latest (chapter 9,
page 35).
• The electrode must be cleaned upon every change of sample using the
electrode brush (brass handle; chapter 9, page 35).
• When you change the matrix (e.g. from iron to aluminium), replace the electrode
and brush (chapter 9, page 35). Otherwise, analysis can be adulterated by a
contamination on the electrode or brush. Therefore, there are a separate
tungsten electrode and brush for every matrix.
• The spacing between electrode tip and sample surface must be set with the
electrode setting gauge (chapter 9, page 35).
• For measuring samples with a diameter of < 6 mm use the measuring adapters
and the boron nitride collimator (chapter 9.9, page 45).

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FOUNDRY-MASTER Smart 7 Quick start

Prerequisites for • The instrument has been put into service as described in chapter 6, page 23.
analysis • The sample to be analysed has been prepared.
• All other required settings have been made (see chapter 8.3, page 45).

1. To spark a sample (1, fig. 7-1), place it on the spark stand (2) with the prepared
side down which is as even as possible so that the hole (3) in the spark stand
plate above the electrode is completely covered, if possible.
To facilitate sample adjustment, you can install an optional prism (5) on the
spark stand.

4
3

2 1

Fig. 7-1 Positioning the sample (example)

Note! Choose the point of support of the hold-down device on the sample so that the sample
closes the spark stand hole as tightly as possible. This is mainly the case if the point of
support is in the centre above the electrode.

2. Press on the sample using the rotatable and height-adjustable hold-down

device (4) attached to the left of the spark stand.

Note! If the sample is not placed correctly, there is a gap between sample and spark stand
plate so that air from outside can enter the argon-purged analysis volume (between
electrode and sample) and adulterate analysis. At the same time, the sound generated
during sparking (measurement) exits through the gap more easily. A sparking noise as
low as possible is therefore a good criterion for an optimally placed sample.

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7 Quick start FOUNDRY-MASTER Smart

Warning!
During the analysis of samples that do not cover the hole in the spark stand plate (e.g.
wires), spark light can emerge. Your eyes can be blinded by the light and the high-
energy UV radiation can damage your eyes. Never look into the arc! Wear suitable eye
protection during work.

Warning!
During the analysis of samples that do not cover the hole in the spark stand plate (e.g.
wires), the sound generated upon sparking (measuring) exits through the gap. Wear ear
protection when sparking samples that do not cover the hole.

Danger!
Risk of electric shock!
During sparking, do not, under any circumstances, introduce a conducting object into
the proximity of the spark stand hole!
During sparking, do not, under any circumstances, remove a conducting object from
the spark stand hole!
With the spark stand hole open during sparking, do not, under any circumstances,
bring a part of your body into its immediate vicinity!

Note! The measurement can only be started if there is a sample clamped in the hold-down
device, or if the hold-down device is swung outwards (90° to spark stand) and engages
at the bottom.
If the hold-down device is at the bottom parallel to the spark stand, no measurement is
possible.
Prior to starting sparking, make sure the hold-down device presses down the sample at
the correct position.

3. In the start screen of the WASLab program, select "Analysis".

4. In the "Select analytical program" window, select the subprogram and confirm
your selection with "OK".
5. Switch on the excitation source at the rotary knob on the front of the instrument.
6. Start analysis of the placed sample by clicking "Start" or pressing the green start
button on the front of the instrument.

The flowcharts in the following chapter illustrate the sequence of analysis and
recalibration.

Further information on how to use the software can be found in the software manual.

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FOUNDRY-MASTER Smart 7 Quick start

7.2 Flowcharts for analysis and recalibration

7.2.1 Start and sequence of a check measurement in spark mode

Start and sequence of a check

measurement

setting argon supply to 3 bar chapter 5.4, page 20

Connect power supply

switching on computer

waiting until WINDOWS™ has

completely started up

switching on spectrometer

starting spectrometer software

Select "Analysis" and subprogram

Select "Mode" menu item;

Click "Argon purging" button;
purge for 1 minute, click button
again to complete purging

Measure control sample

not OK Recalibration: Select recalibration

Check result
method "FULL" or "TYPE"

chapter 7.2.2, page 29

OK
or
chapter 7.2.3, page 30
Continue with "Analysing"

chapter 7.2.4, page 31

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7 Quick start FOUNDRY-MASTER Smart

7.2.2 Recalibrating "Full"

Recalibrate "Full"

Select "Recal" in analysis window

Select "Full" option

Should one sparking

deviate excessively:
remove by double- Spark shown sample
clicking the column 3 to 4 times minimum
and clicking (avoid sparking the same burn
"Delete". spot)

not
RSD within the OK Check samples
specification?

OK

Continue, until all

recalibration samples
for that matrix have
been sparked.
Continue with "Next".

all sparked,
"Recalibration successful" message

Continue with "Analysing"

chapter 7.2.4, page 31

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FOUNDRY-MASTER Smart 7 Quick start

7.2.3 Recalibrating "Type"

Recalibrate "Type"

Select "Recal" in analysis window

Select "Type" option

Should one sparking

deviate excessively:
remove by double- Spark desired sample
clicking the column 3 to 4 times minimum
and clicking (avoid sparking the same burn
"Delete". spot)

Check results

OK

Confirm result

Continue with "Analysing"

chapter 7.2.4, page 31

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7 Quick start FOUNDRY-MASTER Smart

7.2.4 Performing an analysis

Analyse

Select "New" in analysis window

Enter sample name/number

Should one sparking

deviate excessively:
remove by double- Spark desired sample
clicking the column 3 to 4 times minimum
and clicking (avoid sparking the same burn
"Delete". spot)

Verify analysis

OK

If 3 values are
consistent Continue with
next sample

Select "Store",
"Print"?

Complete analysis

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8 Removal from service FOUNDRY-MASTER Smart

8 Removal from service

Proceed as follows to remove the instrument from service:

1. Switch off the excitation source at the rotary knob on the front.
2. Terminate the WASLab software (Alt+Q), shut down the operating system and
switch off the PC.
3. Switch off the instrument at the on/off switch on the rear.
4. Shut off argon supply at the pressure regulating valve of the bottle.

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9 Maintenance FOUNDRY-MASTER Smart

9 Maintenance

9.1 Safety instructions for maintenance and repair

Maintenance and repair may only be carried out by qualified specialised personnel.

Switching off the Prior to beginning maintenance or repair work, switch off the instrument:
instrument • Switch off the excitation source at the rotary knob.
• Exit the WASLab software and shut down the operating system.
• Switch off the instrument at the on/off switch on the rear.
• Secure the instrument against restart and attach a warning "Caution —
Maintenance!".

Warning!
There is a crush hazard when opening or closing the holding clamps on the flap of the
spark stand.
• If necessary, use a tool to open the holding clamps.
• Close the holding clamps from above.

Since the software is subject to continuous further development, Oxford Instruments

Analytical GmbH recommends regular maintenance. This is to ensure the use of the
respective current version for the device and to allow the customer to benefit from the
enhanced scope of functions.

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FOUNDRY-MASTER Smart 9 Maintenance

9.2 Maintenance table

In the following table,

the abbreviation means that the maintenance activity must be

performed
OH .............................................after x operating hours
m ...............................................after x months
y.................................................after x years
.

Table 9-1 Maintenance intervals FOUNDRY-MASTER Smart

Maintenance interval
Assembly Maintenance activity Further information
m y OH
entire instrument replacement of all loaded parts and analytical
1 to be performed by customer service
check of the instrument

check of filters and replacement, if required 3 chapter 9.5, page 43

cleaning of instrument 1 chapter 9.8, page 44

Clean and fill wash bottle when dirty or filled to a low level chapter 9.6, page 43

Replace argon bottle as necessary chapter 9.7, page 44

spark stand
replacement of electrode at every change of matrix chapter 9.4.1, page 39

adjustment of the electrode after every change of electrode chapter 9.4.2, page 41

after every measurement and at

cleaning of electrode with brush chapter 9.4.3, page 42
every change of the sample
after 300 sparkings each; upon
cleaning of spark stand notification; chapter 9.3, page 37
at every change of matrix

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9 Maintenance FOUNDRY-MASTER Smart

9.3 Disassembling and cleaning the spark stand

When the spark stand must be cleaned, the following message is displayed on the
screen:

Fig. 9-1 Reminder to clean the spark stand

Note! We recommend the immediate cleaning of the spark stand when this message is
displayed.
You could skip the message clicking "Remind later", however, that is not recommended.
The cleaning interval can be set in the "Options" window (see software manual).

Proceed as follows:

1. Switch off the instrument as described in chapter 9.1, page 35.

Opening the spark 2. Loosen the 4 holding clamps (1, fig. 9-2) on the spark stand plate (2).
stand
3. Lift the front of the spark stand plate about 45° and take it out toward the front.

Fig. 9-2 Opening the spark stand plate

Note! Make sure that the O-ring (1, fig. 9-3) on the rear of the spark stand plate does not get
lost.

Fig. 9-3 O-ring spark stand plate

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FOUNDRY-MASTER Smart 9 Maintenance

Cleaning the spark 4. Brush the condensate off the surface below the spark stand plate and around
stand the electrode using the brush from the accessory case.

Warning!
There is a crush hazard when closing the holding clamps on the spark stand plate.
Close the holding clamps from above.

5. Replace the spark stand plate on the spark stand and close the holding clamps.

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9 Maintenance FOUNDRY-MASTER Smart

9.4 Maintenance of the electrode

9.4.1 Replacing the electrode

When you change the matrix (e.g. from iron to aluminium), electrode and brush should
be replaced. Otherwise, analysis can be adulterated by contamination of the electrode
or brush.
There are a separate electrode and brush for every matrix.

To replace the electrode, proceed as follows:

1. Switch off the instrument as described in chapter 9.1, page 35.

2. Screw out the spacer (1, fig. 9-4) on the right side of the spark stand.
3. Loosen the inner grub screw (2) on the electrode clamp using a 2 mm Allen key
(3).
The electrode (4) is pushed out of the spark stand toward the top by a spring.

Fig. 9-4 Screwing out the spacer

4. Completely remove the electrode and replace it with a new one.

5. Insert the new electrode from above.

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FOUNDRY-MASTER Smart 9 Maintenance

6. Completely press down the electrode with the head (1, fig. 9-5) of the spacer to
adjust the correct distance to the sample. Simultaneously fasten the grub screw
to the electrode clamp.

Fig. 9-5 Installing the electrode

7. Screw the spacer back into the side of the spark stand finger-tightly.

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9 Maintenance FOUNDRY-MASTER Smart

9.4.2 Adjusting the electrode

The spacing between electrode and sample is adjusted on the side of the spark stand
using the spacer. Proceed as follows:

1. Switch off the instrument as described in chapter 9.1, page 35.

2. Screw out the spacer (1, fig. 9-6) on the right side of the spark stand.
3. Loosen the inner grub screw (2) on the electrode clamp using a 2 mm Allen
key (3).
The electrode (4) is pushed out of the spark stand toward the top by a spring.

Fig. 9-6 Screwing out the spacer

4. Completely press down the electrode with the head (1, fig. 9-7) of the spacer to
adjust the correct distance to the sample. Simultaneously fasten the grub screw
to the electrode clamp again.

Fig. 9-7 Installing the electrode

5. Screw the spacer back into the side of the spark stand finger-tightly.

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FOUNDRY-MASTER Smart 9 Maintenance

9.4.3 Cleaning the electrode with the electrode brush

Note! Too much combustion residue on the electrode can result in a short circuit between
electrode tip and sample.
The short circuit is detected by the instrument and indicated with an error message.
Strongly varying measurements can also indicate that there is too much combustion
residue on the electrode.
The electrode must be cleaned with the electrode brush after every measurement.

To clean the electrode using the electrode brush (brass handle), proceed as follows:

1. Switch off the excitation source at the rotary knob on the front of the instrument.
2. Brush the tungsten electrode through the hole (1, fig. 9-8) in the spark stand
plate using the electrode brush from the accessory case.
3. Switch the excitation source back on.

Fig. 9-8 Spark stand

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9 Maintenance FOUNDRY-MASTER Smart

9.5 Replacing filters

Check the filter mats in the fan and in the outlet filter on the rear of the housing for
contamination. Replace the filter mats if required.

9.6 Cleaning and filling the wash bottle

The washing bottle filled with tap water serves to collect the off-gases from sparking so
that they are not released into the air.
From time to time, check the wash bottle is correctly filled. Clean and fill it if the fill level
is not correct or cannot be easily seen.

1 3

2
4

max. 60 mm
min. 40 mm

Fig. 9-9 Wash bottles

Note! The empty bottle (1, fig. 9-9) prevents water being sucked into the exhaust hose. For
that reason, no water should be filled into the empty bottle (1)!

To clean and fill the wash bottle (3), proceed as follows:

• Unscrew the lid of the wash bottle.
• Empty the wash bottle.
• Rinse any dirt out with tap water.
• Fill up the wash bottle with tap water.
• The wash bottle's tube (4) must be below the water level.
• The fill level in the wash bottle must not exceed 60 mm high and should be
at least 40 mm high.
• Screw the lid back onto the wash bottle. Make sure that the lid is well positioned.

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FOUNDRY-MASTER Smart 9 Maintenance

9.7 Replacing the argon bottle(s)

When replacing the Ar bottle(s), air might enter part of the Ar supply segment.
There are three possible ways to then remove it from the system again:

• One possibility is to purge the Ar system after replacement. For that, activate purging
under "Mode", "Argon purging". That method is quite time-consuming, since it may
take several hours until the supply lines have been purged sufficiently so as to
ensure the analysis is not affected any more.
• A more effective, but also more expensive possibility is the use of purchasable
fittings, with a purging device on the delivery side. That is the safest method.
• As a third possibility, the following procedure can be performed:

1. Regulate the control valve (1, fig. 9-10) from 3 bar to 0. By that, the section from
the pressure regulator / manometer to the spectrometer is isolated.
2. Close the bottle valve (2).
3. Screw the pressure regulator / manometer off the bottle.
4. Replace the bottle.
5. Screw the pressure regulator / manometer onto the new bottle.
6. Open the bottle valve and immediately close it. The primary manometer should
now indicate the bottle pressure (usually 200 bar).
7. Loosen the union nut (3) to the extent that the pressure between bottle and
pressure regulator / manometer can drop to 0.
8. Repeat steps 6 and 7 four to five times.
9. Adjust the control valve to 3 bar.
10. Let purging go on for about 2 min.

2 3

Fig. 9-10 Argon bottle (example)

9.8 Cleaning the instrument

Use a soft, dry or slightly damp cloth to clean the spectrometer on the outside. DO NOT
use any solvents!
No water may penetrate into the instrument!

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9 Maintenance FOUNDRY-MASTER Smart

9.9 Measuring adapters

For measuring wire samples and tubes with a diameter of < 6 mm, the diameter of the
spark stand hole in the spark stand plate must be reduced in order to increase
measuring accuracy.
For this purpose, a boron nitride collimator and two different wire adapters are available.
• The boron nitride collimator reduces the diameter of the spark stand hole from
10 mm to 5 mm.
• The wire adapters retain the wire on the spark stand plate.
• Using the adapters, you can measure samples with a diameter of < 3 mm with
sufficient precision.
• Generally, it is preferable to use the "face-on" adapter in order to achieve more
consistent measuring results and avoid surface effects.

Note! Even if the constant argon flow reduces the negative effects of an open spark stand
hole, it is indispensable to shield the measuring spot from ambient air for the precise
determination of carbon (C) and phosphorus (P).
A disadvantage of boron nitride is that the boron contained therein is also contained in
steel. During sparking, a contamination with boron can therefore not be excluded, and
a recognition of boron concentrations in steel of < 30 ppm cannot be guaranteed.

Risk of electric shock!

The boron nitride collimator is non-conductive. Small parts measured using the
collimator do not have earthing contact with the instrument, thus there is a risk of electric
shock!
• Do not touch the sample during measurement!
• Should the hold-down device shift or any other inadvertent event occur during a
measurement, always switch off the excitation source before remedying the
error.

Boron nitride Install the measuring adapters as follows:

collimator

Note! Touch the boron nitride collimator carefully so that it does not break.

1. Place the adjustment aid (1, fig. 9-11) for the wire adapter onto the spark stand
plate and fix the adjustment aid using the knurled screw (2).
2. Insert the boron nitride collimator (3) into the spark stand hole.

2
1
3

Fig. 9-11 Adjustment aid and boron nitride collimator (example)

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FOUNDRY-MASTER Smart 9 Maintenance

Wire adapters For analysing wire samples, please use the optional wire adapters.
There is an adapter for analysing the lateral wire surface ("side-on") and an adapter for
analysing the front wire surface ("face-on").

3. Fix the wire to be measured with the wire adapter.

The following illustrations show the two adapters and their positions on the spark stand
plate.

Fig. 9-12 "side-on" wire adapter on spark stand plate (example)

Fig. 9-13 "face-on" wire adapter on spark stand plate (example)

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10 Faults FOUNDRY-MASTER Smart

10 Faults

10.1 Information regarding WINDOWS™ installation

10.1.1 WINDOWS™ CD-ROM

WINDOWS™ CD data are provided on the hard disk in the C:\Windows directory.

10.1.2 Installing the printer

Printer drivers are provided on the CD-ROM of the printer. You can also download
current printer drivers from the Internet. Use a CD-ROM drive with a USB port or copy
the drive onto a USB stick to transfer.

10.1.3 Power options

If Windows suddenly switches to sleep mode, the WASLab software may change to an
undefined state.

Important! To avoid this, you must set the Windows power options to "Balanced".
The following figure (fig. 10-1) illustrates this setting:

Fig. 10-1 Power options (Windows)

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FOUNDRY-MASTER Smart 10 Faults

10.2 General faults

Note! An anti-virus software or other software installed on the computer which is not specified
by Oxford Instruments Analytical GmbH may cause system faults.

You can recognise any instrument faults e.g. from error messages displayed on the
screen. Try to remedy the error using the following table and the information in the
software manual.
Should you have any problems remedying the error, feel free to contact our customer
service for support.
Our contact data are provided under "Service" (chapter 13.1, page 71).

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10 Faults FOUNDRY-MASTER Smart

10.3 Faults of FOUNDRY-MASTER Smart

Table 10-1 Possible faults and remedies (FOUNDRY-MASTER Smart)

Fault Information Remedy/explanation

no communication between PC and Error message: Follow the instructions in the error message.
instrument No spectrometer connected! Possible reasons: ...
Measurement cannot be started. Red bar at the bottom of the analysis window of
the instrument:
1. Switch on the excitation source on the
1. No source instrument.
2. No sample 2. Place the hold-down device prior to
3. No argon D measurement.
3. Is argon pressure 3 bar?
Instrument cannot be switched on. no visible reaction at the instrument 1. Mains voltage? yes/no
2. Check fuses at the power input.
measurements extremely loud loud measurement 1. Position the sample correctly.
2. Connect the off-gas hose to the washing
bottle.
3. Check the water level in the washing
bottle.
Intensity in the direct light path Error message: 1. Incorrect analysis program selected?
decreases or has completely ceased. Reference beyond tolerance 2. Poor burn spot?
3. Optics sufficiently purged?
Measuring results deviate from usual (See fault) 1. Check the electrode spacing and
values, precision decreases, spark- readjust, if required.
overs in the spark stand. 2. Clean the spark stand.
Message: Message: Wrong analysis program selected — start in
e.g. Cr > 6 % Admissible calibration range exceeded. orientation program.
Message: Message: The content of the corresponding element in
e.g. C < 0.001 Detection limits fallen below of. the measured sample is too low.

Note! If none of the above named faults can be identified or the fault cannot be remedied
applying the methods indicated under "Remedy", please contact the service (see
chapter 13.1, page 71).

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12 Reshipment and disposal FOUNDRY-MASTER Smart

12 Reshipment and disposal

12.1 Declaration of Decontamination

Due to legal regulations and to ensure safety of our employees, Oxford Instruments
Analytical GmbH requires a signed Declaration of Decontamination prior to processing
your reshipment.
Enclose this form signed with the shipping documents and attach it on the outside of the
packaging. Reshipments that have been exposed to hazardous substances and which
have not been decontaminated according to good professional practice, are not
processed and returned at your expense.

Note! The instrument must not be shipped without the transport lock installed. Previous to that,
contact our customer service.

The Declaration of Decontamination as well as the contact information are provided in

the Annex.

12.2 Disposal

The PC includes a battery containing contaminants. That must not be disposed of with
the domestic waste.
After the life has expired, disposal may only be executed through the customer service
of Oxford Instruments Analytical GmbH or a suitable collection point.

The operating company is obliged to dispose of the instrument after the completion of
its use at his/her own expense according to the legal requirements and to exempt us
from the take-back obligation and related claims of third parties.

Disassemble the instrument for disposal into the individual material groups:
• plastics
• non-ferrous metals (e.g. copper scrap)
• aluminium
• electronic scrap
• steel.

Dispose of the materials according to national legislation!

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12 Annex FOUNDRY-MASTER Smart

12 Annex

This chapter contains

• service address
• glossary
• list of components in the standard accessory case
• Declaration of Conformity
• Declaration of Decontamination

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13 Annex FOUNDRY-MASTER Smart

13.1 Service

If you need any help handling this product, please contact your service partner of Oxford
Instruments Analytical GmbH or call us at the Service Centre:

Oxford Instruments Analytical GmbH

Abt. Service
Wellesweg 31
47589 Uedem
Germany

Phone: +49 (0)2825 9383-421

Fax: +49 (0)2825 9383-100
E-mail: [email protected]

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12 Annex FOUNDRY-MASTER Smart

12.2 Glossary

AES Short for Atomic Emission Spectrometry:

Arc mode here: Using an arc probe or a combined probe with the arc adapter. The sparking occurs
in an air atmosphere without argon. Thus, the measurement is less precise but can be
carried out faster and is less complicated.

CCD Short for Charge Coupled Device.

CCDs are light-sensitive semiconductor chips used to measure the wavelength of a
source. In a spectrometer, the source is the plasma generated during sparking.

CE value Carbon equivalent value:

CRM Short for Certified Reference Material:

designation for samples whose precise composition is known. Used for spectrometer
recalibration.

DIA short for Dynamic Integration Algorithm.

Spark mode In spark mode, the sparking takes place in argon atmospheres in the spark stand for
stationary instruments and in the spark adapter of the combined probe or in the head of
the UVPro probe and the spark probe for mobile instruments.

ICP short for Inductively Coupled Plasma

PMI short for "Positive Material Identification"

plasma A plasma is a material state in which so far neutral atoms or molecules of the material
are split into their charged fragments (ions and electrons) at very high temperatures.
Those fragments emit rays of a specific wavelength. That wavelength is measured in the
spectrometer and assigned to the corresponding element in the software.

Recalibration periodic remeasuring of a measuring/test device (here spectrometer and recalibration

sample) to monitor its accuracy

standard deviation The standard deviation is a measure for the deviation of measured values around their
average value. A distinction is made between relative standard deviation (RSD) and
absolute standard deviation (SD).

white burn spot Poor burn spot with very low luminous efficacy. It results from contamination on the
sparked surface.

XRF short for X-ray fluorescence analysis

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12.3 Standard accessory case, packed

Table 12-1 Standard accessory case, packed

Quan-
Part number Designation
tity
6000000173 Service Flyer (English) 1
7000000322 assortment case 1
0000000339 power cable cold appliances, 2 m 2
5200000141 premium USB cable A-B, 1.8 m, with snap ferrite 2
3520000194 premium USB cable A-B, 2.0 m 1
3510000040 snap ferrite 1
0000000869 electrode cleaning brush 1
0000002103 assembly extraction tool ceramic insert 1
0000002101 palm grip M6 1
4000000104 clamping screw extractor ceramic 1
1010000032 brass pin 1
0000002209 cleaning brush 1
0000001996 hexagon screwdriver with T-handle SW 2 1
3510000036 snap ferrite toroidal core 2
0000001325 fuse 6.3 A, 20 mm T 10
0000000028 tungsten electrode 1
0000000287 electrode cleaning brush, round 2
0000002045 Swagelok union nut 2
0000002046 Swagelok locking ring set (front + rear) 3
0000001272 M4x4 galvanised Allen set screw 5
0000000029 compression spring 2
0000000521 O-ring 8 x 1 mm 5
0000003589 rubber bump stop 3
7000000162 angle Allen key SW 2 1
3800000040 mouse, 3 buttons, USB port 1
0000003102 Rittal spare filter mat 2
0000000337 Allen key SW 2.5 1

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12.4 Forms

12.4.1 Declaration of Conformity

12.4.2 Declaration of Decontamination

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 Declaration of Decontamination
Dekontaminationserklärung
Because of legal regulations and for the safety of our employees Oxford Instruments Analytical GmbH needs a signed
“declaration of decontamination” before your return can be handled.
This signed declaration must be included with the shipping documents on the outside of the packaging. Any returns which were
exposed to hazardous substances and were not professionally decontaminated are not accepted and will be sent back on your
cost.
Aufgrund gesetzlicher Bestimmungen und um die Sicherheit unserer Mitarbeiter zu gewährleisten benötigt die Oxford
Instruments Analytical GmbH eine unterschriebene Dekontaminationserklärung, bevor Ihre Rücksendung bearbeitet werden
kann. Legen Sie dieses unterschriebene Formular den Versandpapieren bei und bringen Sie es außen an der Verpackung an.
Rücksendungen, welche gefährlichen Stoffen ausgesetzt waren und nicht fachgerecht dekontaminiert wurden, werden nicht
bearbeitet und auf Ihre Kosten zurückgeschickt.

Name / Name Address / Adresse

Serial number / Seriennummer

Order number / Auftragsnummer Phone / Telefon Email / E-Mail

Notes / Bemerkungen

1. Equipment has been in contact with hazardous substances.

Das Gerät ist mit gefährlichen Stoffen in Berührung gekommen.
No / Nein Yes / Ja = Please list the hazardous substances. / Bitte benennen Sie die gefährlichen Stoffe.

Substance / Stoff Danger Class / Gefahrenklasse Safety precautions / Sicherheitsvorkehrungen

1

2. Equipment has been decontaminated professionally. / Das Gerät wurde fachgerecht dekontaminiert.
No / Nein Yes / Ja = Cleaning agent / Reinigungsmittel:
-------------------------------------------------------------------------------------

3. Legally binding declaration / Rechtsverbindliche Erklärung

Herewith I confirm that the returned instruments were cleaned and decontaminated according to the industry standards and all
appropriate regulations. The instruments are free of hazardous substances.
Hiermit bestätige ich, dass die zurückgesendeten Geräte nach industriellen und gesetzlichen Bestimmungen gereinigt und
dekontaminiert sind. Die Geräte sind frei von gefährlichen Stoffen.

------------------------------------------ ---------------------------------------------------------------------------------------
Location / Ort Company stamp and legally binding signature
Firmenstempel und rechtsverbindliche Unterschrift

------------------------------------------ ---------------------------------------------------------------------------------------
Date / Datum Name of signatory in block letters
Name des Unterzeichnenden in Druckbuchstaben
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