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    PEAK 1: Area and Migration Time Peak 2: Area and Migration Time

    Uploaded by

    Angela Mora
    This document contains information from calibration tests and measurements of an instrument. It includes data tables showing area and migration time measurements from two peaks across six replicates, with average, standard deviation, and relative standard deviation calculations. It also includes voltage calibration measurements at different levels, temperature calibration measurements and coefficients for the capillary and sample storage, temperature stability tests, forward and reverse pressure calibration measurements, and notes on performing low and high pressure calibrations.

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    © All Rights Reserved
    Download as XLSX, PDF, TXT or read online from Scribd

    PEAK 1: Area and Migration Time Peak 2: Area and Migration Time

    Uploaded by

    Angela Mora
    33 views7 pages
    This document contains information from calibration tests and measurements of an instrument. It includes data tables showing area and migration time measurements from two peaks across six replicates, with average, standard deviation, and relative standard deviation calculations. It also includes voltage calibration measurements at different levels, temperature calibration measurements and coefficients for the capillary and sample storage, temperature stability tests, forward and reverse pressure calibration measurements, and notes on performing low and high pressure calibrations.

    Original Title

    Calculations

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    © © All Rights Reserved

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    This document contains information from calibration tests and measurements of an instrument. It includes data tables showing area and migration time measurements from two peaks across six replicates, with average, standard deviation, and relative standard deviation calculations. It also includes voltage calibration measurements at different levels, temperature calibration measurements and coefficients for the capillary and sample storage, temperature stability tests, forward and reverse pressure calibration measurements, and notes on performing low and high pressure calibrations.

    Copyright:

    © All Rights Reserved
    Download as XLSX, PDF, TXT or read online from Scribd
    Download as xlsx, pdf, or txt
    33 views7 pages

    PEAK 1: Area and Migration Time Peak 2: Area and Migration Time

    Uploaded by

    Angela Mora
    This document contains information from calibration tests and measurements of an instrument. It includes data tables showing area and migration time measurements from two peaks across six replicates, with average, standard deviation, and relative standard deviation calculations. It also includes voltage calibration measurements at different levels, temperature calibration measurements and coefficients for the capillary and sample storage, temperature stability tests, forward and reverse pressure calibration measurements, and notes on performing low and high pressure calibrations.

    Copyright:

    © All Rights Reserved
    Download as XLSX, PDF, TXT or read online from Scribd
    Download as xlsx, pdf, or txt
    of 7

    PEAK 1: Area and Migration Time Peak 2: Area and Migration time

    Area Migration Time Area Migration Time


    Rep1 466581 3.820 114461 3.600000
    Rep2 467498 3.800 114863 3.591667
    Rep3 464999 3.790 115842 3.587500
    Rep4 468469 3.780 116024 3.587500
    Rep5 467325 3.760 115546 3.587500
    Rep6 469863 3.740 117509 3.579167

    467456 3.78166666666667 AVERAGE 115708 3.588889


    1652 0.02857738033247 STANDARD DEVIATION 1064 0.006804
    0.0035335 0.00755682159519 RSD 0.009193 0.001896

    0.353% 0.756% %RSD 0.919% 0.190%


    on time
    Voltage

    3.0 KV 15.0 KV 30.0 KV 3.0 KV


    Measurement 1 2.99 15.1 30.3 3.1
    Measurement 2 2.97 15.2 30.3 3.09
    Measurement 3 2.98 15.2 30.3 3.09
    Measurement 4 2.99 15.2 30.3 3.07
    Measurement 5 2.99 15.2 30.3 3.07
    Measurement 6 2.99 15.2 30.3 3.08

    AVERAGE 2.99 15 30 3
    STANDARD DEVIATION 0.008367 0 0 0
    RSD 0.002803 0.002689 0.000000 0.003928

    %RSD 0.28% 0.27% 0.00% 0.39%


    oltage

    15.0 KV 30.0 KV
    15.2 30.3
    15.2 30.3
    15.2 30.3
    15.2 30.3
    15.2 30.3
    15.2 30.3

    15 30
    0 0
    0.000000 0.000000

    0.00% 0.00%
    Capillary and Sample Storage temperature calibration

    Check temperature
    Capillary Temperature
    TD 15 25 50
    TM 14.6 51.48

    New coefficients
    A= 1.05
    B= -1.21

    Sample Storage Temperature


    D
    T 7 25 60
    TM 3.5 62.2

    New coefficients
    A= 1.11
    B= -4.25 -2.54 -6.79

    Note: replace coefficient A, and add on coefficient B to existing value.

    Input in EEPROM

    Capillary Cooler [30] & [31]


    Sample Storage [32] & [33]

    EETEMPUPDATE

    Then Test temperatures again


    Capillary Temperature Stability
    0 minutes 24.9
    2 minutes 25.0
    4 minutes 24.9
    6 minutes 25.0
    8 minutes 25.1
    10 minutes 25.1
    Mean= 25.0

    Sample Cooler Temperature Stability


    0 minutes 24.6
    2 minutes 24.6
    4 minutes 24.7
    6 minutes 24.7
    8 minutes 24.7
    10 minutes 24.7
    Mean= 24.7
    Forward Pressure Test
    0.50 1.00 7.50 20.0 50.0 80.0
    Measurement 1
    Measurement 2
    Measurement 3
    Mean #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!

    Reverse Pressure Test


    0.50 1.00 7.50 20.0 50.0 80.0
    Measurement 1
    Measurement 2
    Measurement 3
    Mean #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0!

    Vacuum Test
    -0.50 -1.00 -5.00
    Measurement 1
    Measurement 2
    Measurement 3
    Mean #DIV/0! #DIV/0! #DIV/0!

    Low Pressure Calibration


    Note: Attatch Pressure Vial and Meter to calibrate

    Debug 0_1

    clop *will apply 7.0 psi

    inlo XX.x *should store to eeprom

    High Pressure Calibration


    Debug 0_1

    chip *will apply 70 psi

    inhi XX.x

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