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Lab Report #4

The student performed an experiment to standardize a NaOH solution. They found: 1) The molarity of their KHP standard solution was 0.04766M. 2) They titrated 7mL of 10M NaOH solution with 700mL water. 3) By titrating the KHP solution with the NaOH solution, they calculated an average volume of NaOH used of 12.12mL with a standard deviation of 0.1560. 4) From this, they determined the molarity of their NaOH solution to be 0.09835M.

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Mad Basbla
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25 views

Lab Report #4

The student performed an experiment to standardize a NaOH solution. They found: 1) The molarity of their KHP standard solution was 0.04766M. 2) They titrated 7mL of 10M NaOH solution with 700mL water. 3) By titrating the KHP solution with the NaOH solution, they calculated an average volume of NaOH used of 12.12mL with a standard deviation of 0.1560. 4) From this, they determined the molarity of their NaOH solution to be 0.09835M.

Uploaded by

Mad Basbla
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Experiment 4 Lab report – Standardization of NaOH solution

Procedure

Procedure can be seen in my lab manual on page 10. One change was that we used 7ml of NaOH instead
of 6ml also and we added 100ml more water.

Part A –Experimental Data

Mass of weighing tray 2.327g


Mass of weighing tray + KHP 4.760g
Volume of Solution 250.00ml

Part A- Calculated Results

Mass of KHP 2.433g


Molarity of KHP solution 0.04766M

Part A – Sample calculations

mKHP =mW +KHP −mW =4.760 g−2.327 g=2.433 g

m KHP 2.433 g
n M 204.2 g /mol
M KHP = KHP = = =0.0476 5 91577 M
V V 1L
250.00 ml x
1000 ml
Part B- Experimental Data

Volume of 10M NaOH 7.00ml


Volume of water 700.00ml

Part C – Experimental Data

My data:

Trial 1 Trial 2 Trial 3


Initial Buret Reading 0.21ml 0.28ml 0.59ml
Initial Buret Reading 12.41ml 12.52ml 12.90ml
My Lab partners Data

Trial 1 Trial 2 Trial 3


Initial Buret Reading 0.28ml 0.68ml 0.61ml
Initial Buret Reading 12.31ml 12.60ml 12.60ml

Part C- Calculated results

Trial 1 Trial 2 Trial 3


Used NaOH solution 12.20ml 12.24ml 12.31ml
(Mine)
Used NaOH 12.03ml 11.92ml 11.99ml
solution(My Lab
Partners)
Average Volume 12.12ml
Standard deviation 0.1560
Molarity of NaOH 0.09835M
solution

Part C – Sample calculations

Trial 1: V NaOH =V F−V I =12.31 ml−0.21 ml=12.20 ml


V 1+V 2+V 3+ V 4+V 5+V 6 12.20 ml+12.24 ml +12.31 ml+12.03 ml+11.92 ml +11.99 ml
Average Volume= = =1
6 6
2 2 2 2 2 2

√
2
( V́ −V 1) + ( V́ −V 2 ) + ( V́ −V 3 ) + ( V́ −V 4 ) + ( V́ −V 5 ) + ( V́ −V 6 ) ( 12.115 ml−12.20 ml ) + ( 12.11
Std .deviation=
6−1
=
√
1L
Moles of Acid∈ Flask =V KHP x M KHP =25.00 mlx x 0. 04766 M =0.0011915 mol
1000 ml
Moles of Acid = Moles of Base
n NaOH 0.0011915 mol
M NaOH = = =0.0983 4 91539 M
V NaOH 1L
12.115 mlx
1000 ml
Discussion/Questions
1. My results were very close together which means that they were precise but they were
not as accurate as they are all bit off from the theoretical value. Errors could be due to
NaOH reacting to CO2 in the atmosphere.
2. There was no bad data.

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