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Flores Batch Reactor Virtual Lab Data PDF

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Performance of a Batch Reactor

Virtual Laboratory Raw Data


Elizalde Miguel S. Flores

Table 1. Conductivity meter readings at varying temperature (T=30℃)


Temperature (T)=30℃ NaOH:Ethyl Acetate molar ratio=1:1
Initial NaOH conc (CAO)=0.2 mol/L Initial NaOH Volume (VA)=500 mL
Initial Ethyl Acetate conc (CBO)=0.2 mol/L Initial Ethyl Acetate Volume (VB)=500 mL
Reactor Volume (V)=1 L
Time Conductivity Time Conductivity Time Conductivity Time Conductivity
(s) meter reading (s) meter reading (s) meter reading (s) meter reading
(YT, mS/cm) (YT, mS/cm) (YT, mS/cm) (YT, mS/cm)
15 16.12 465 1.11 915 0.68 1365 0.54
30 10.32 480 1.08 930 0.68 1380 0.53
45 7.62 495 1.05 945 0.67 1395 0.53
60 8.08 510 1.03 960 0.66 1410 0.53
75 5.05 525 1.01 975 0.66 1425 0.52
90 4.33 540 0.99 990 0.65 1440 0.52
105 3.80 555 0.97 1005 0.65 1455 0.52
120 3.40 570 0.95 1020 0.64 1470 0.51
135 3.07 585 0.93 1035 0.63 1485 0.51
150 2.81 600 0.91 1050 0.63 1500 0.51
175 2.59 615 0.90 1065 0.62 1515 0.51
180 2.40 630 0.88 1080 0.61 1530 0.50
195 2.25 645 0.87 1095 0.61 1545 0.50
210 2.11 660 0.85 1110 0.61 1560 0.50
225 1.99 675 0.84 1125 0.60 1575 0.50
240 1.89 690 0.83 1140 0.60 1590 0.49
255 1.79 705 0.81 1155 0.59 1605 0.49
270 1.71 720 0.80 1170 0.59 1620 0.49
285 1.57 735 0.79 1185 0.59 1635 0.49
300 1.57 750 0.78 1200 0.58 1650 0.48
315 1.51 765 0.77 1215 0.57 1665 0.48
330 1.45 780 0.76 1230 0.57 1680 0.48
345 1.40 795 0.75 1245 0.57 1695 0.48
360 1.35 810 0.74 1260 0.56 1710 0.48
375 1.31 825 0.73 1275 0.56 1725 0.47
390 1.27 840 0.72 1290 0.55 1740 0.47
405 1.23 855 0.72 1305 0.55 1755 0.47
420 1.20 870 0.71 1320 0.55 1770 0.47
435 1.18 885 0.70 1335 0.55 1785 0.47
450 1.13 900 0.69 1350 0.54 1800 0.46
Table 2. Conductivity meter readings at varying temperature (T=35℃)
Temperature (T)=35℃ NaOH:Ethyl Acetate molar ratio=1:1
Initial NaOH conc (CAO)=0.2 mol/L Initial NaOH Volume (VA)=500 mL
Initial Ethyl Acetate conc (CBO)=0.2 mol/L Initial Ethyl Acetate Volume (VB)=500 mL
Reactor Volume (V)=1 L
Time Conductivity Time Conductivity Time Conductivity Time Conductivity
(s) meter reading (s) meter reading (s) meter reading (s) meter reading
(YT, mS/cm) (YT, mS/cm) (YT, mS/cm) (YT, mS/cm)
15 12.82 465 0.83 915 0.53 1365 0.43
30 7.76 480 0.81 930 0.53 1380 0.43
45 5.64 495 0.79 945 0.52 1395 0.43
60 4.45 510 0.78 960 0.52 1410 0.42
75 3.69 525 0.76 975 0.51 1425 0.42
90 3.16 540 0.75 990 0.51 1440 0.42
105 2.77 555 0.73 1005 0.50 1455 0.42
120 2.47 570 0.72 1020 0.50 1470 0.42
135 2.23 585 0.71 1035 0.50 1485 0.41
150 2.04 600 0.69 1050 0.50 1500 0.41
175 1.89 615 0.68 1065 0.49 1515 0.41
180 1.75 630 0.67 1080 0.49 1530 0.41
195 1.64 645 0.66 1095 0.48 1545 0.41
210 1.54 660 0.65 1110 0.48 1560 0.40
225 1.46 675 0.64 1125 0.47 1575 0.40
240 1.36 690 0.63 1140 0.47 1590 0.40
255 1.32 705 0.62 1155 0.47 1605 0.40
270 1.26 720 0.62 1170 0.46 1620 0.40
285 1.20 735 0.61 1185 0.46 1635 0.40
300 1.16 750 0.60 1200 0.46 1650 0.39
315 1.11 765 0.59 1215 0.46 1665 0.39
330 1.07 780 0.59 1230 0.45 1680 0.39
345 1.04 795 0.58 1245 0.45 1695 0.39
360 1.00 810 0.57 1260 0.45 1710 0.39
375 0.97 825 0.57 1275 0.44 1725 0.39
390 0.94 840 0.56 1290 0.44 1740 0.39
405 0.92 855 0.55 1305 0.44 1755 0.38
420 0.89 870 0.55 1320 0.44 1770 0.38
435 0.87 885 0.54 1335 0.43 1785 0.38
450 0.85 900 0.54 1350 0.43 1800 0.38

Table 3. Conductivity meter readings at varying temperature (T=40℃)


Temperature (T)=40℃ NaOH:Ethyl Acetate molar ratio=1:1
Initial NaOH conc (CAO)=0.2 mol/L Initial NaOH Volume (VA)=500 mL
Initial Ethyl Acetate conc (CBO)=0.2 mol/L Initial Ethyl Acetate Volume (VB)=500 mL
Reactor Volume (V)=1 L
Time Conductivity Time Conductivity Time Conductivity Time Conductivity
(s) meter reading (s) meter reading (s) meter reading (s) meter reading
(YT, mS/cm) (YT, mS/cm) (YT, mS/cm) (YT, mS/cm)
15 9.81 465 0.64 915 0.43 1365 0.35
30 5.83 480 0.63 930 0.42 1380 0.35
45 4.18 495 0.61 945 0.42 1395 0.35
60 3.28 510 0.60 960 0.42 1410 0.35
75 2.71 525 0.59 975 0.41 1425 0.35
90 2.32 540 0.58 990 0.41 1440 0.35
105 2.04 555 0.57 1005 0.41 1455 0.35
120 1.82 570 0.56 1020 0.40 1470 0.34
135 1.65 585 0.55 1035 0.40 1485 0.34
150 1.51 600 0.54 1050 0.40 1500 0.34
175 1.40 615 0.53 1065 0.40 1515 0.34
180 1.30 630 0.53 1080 0.39 1530 0.34
195 1.22 645 0.52 1095 0.39 1545 0.34
210 1.15 660 0.51 1110 0.39 1560 0.34
225 1.09 675 0.51 1125 0.39 1575 0.34
240 1.03 690 0.50 1140 0.38 1590 0.33
255 0.99 705 0.49 1155 0.38 1605 0.33
270 0.94 720 0.49 1170 0.38 1620 0.33
285 0.91 735 0.48 1185 0.38 1635 0.33
300 0.87 750 0.48 1200 0.38 1650 0.33
315 0.84 765 0.47 1215 0.37 1665 0.33
330 0.81 780 0.47 1230 0.37 1680 0.33
345 0.79 795 0.46 1245 0.37 1695 0.33
360 0.76 810 0.46 1260 0.37 1710 0.33
375 0.74 825 0.45 1275 0.37 1725 0.32
390 0.72 840 0.45 1290 0.36 1740 0.32
405 0.70 855 0.44 1305 0.36 1755 0.32
420 0.68 870 0.44 1320 0.36 1770 0.32
435 0.67 885 0.43 1335 0.36 1785 0.32
450 0.65 900 0.43 1350 0.36 1800 0.32

Table 4. Conductivity meter readings at varying temperature (T=45℃)


Temperature (T)=45℃ NaOH:Ethyl Acetate molar ratio=1:1
Initial NaOH conc (CAO)=0.2 mol/L Initial NaOH Volume (VA)=500 mL
Initial Ethyl Acetate conc (CBO)=0.2 mol/L Initial Ethyl Acetate Volume (VB)=500 mL
Reactor Volume (V)=1 L
Time Conductivity Time Conductivity Time Conductivity Time Conductivity
(s) meter reading (s) meter reading (s) meter reading (s) meter reading
(YT, mS/cm) (YT, mS/cm) (YT, mS/cm) (YT, mS/cm)
15 7.58 465 0.50 915 0.35 1365 0.30
30 4.39 480 0.49 930 0.35 1380 0.30
45 3.12 495 0.49 945 0.35 1395 0.30
60 2.45 510 0.48 960 0.35 1410 0.30
75 2.02 525 0.47 975 0.34 1425 0.30
90 1.73 540 0.46 990 0.34 1440 0.30
105 1.52 555 0.46 1005 0.34 1455 0.30
120 1.36 570 0.45 1020 0.34 1470 0.29
135 1.24 585 0.44 1035 0.33 1485 0.29
150 1.14 600 0.44 1050 0.33 1500 0.29
175 1.06 615 0.43 1065 0.33 1515 0.29
180 0.98 630 0.42 1080 0.33 1530 0.29
195 0.92 645 0.42 1095 0.33 1545 0.29
210 0.87 660 0.41 1110 0.33 1560 0.29
225 0.83 675 0.41 1125 0.32 1575 0.29
240 0.79 690 0.40 1140 0.32 1590 0.29
255 0.76 705 0.40 1155 0.32 1605 0.29
270 0.72 720 0.40 1170 0.32 1620 0.28
285 0.70 735 0.39 1185 0.32 1635 0.28
300 0.67 750 0.39 1200 0.31 1650 0.28
315 0.66 765 0.38 1215 0.31 1665 0.28
330 0.63 780 0.38 1230 0.31 1680 0.28
345 0.61 795 0.38 1245 0.31 1695 0.28
360 0.59 810 0.37 1260 0.31 1710 0.28
375 0.58 825 0.37 1275 0.31 1725 0.28
390 0.56 840 0.37 1290 0.31 1740 0.28
405 0.55 855 0.37 1305 0.31 1755 0.28
420 0.54 870 0.36 1320 0.31 1770 0.28
435 0.53 885 0.36 1335 0.30 1785 0.28
450 0.51 900 0.36 1350 0.30 1800 0.28

Table 5. Conductivity meter readings at varying temperature (T=50℃)


Temperature (T)=50℃ NaOH:Ethyl Acetate molar ratio=1:1
Initial NaOH conc (CAO)=0.2 mol/L Initial NaOH Volume (VA)=500 mL
Initial Ethyl Acetate conc (CBO)=0.2 mol/L Initial Ethyl Acetate Volume (VB)=500 mL
Reactor Volume (V)=1 L
Time Conductivity Time Conductivity Time Conductivity Time Conductivity
(s) meter reading (s) meter reading (s) meter reading (s) meter reading
(YT, mS/cm) (YT, mS/cm) (YT, mS/cm) (YT, mS/cm)
15 5.85 465 0.41 915 0.30 1365 0.26
30 3.32 480 0.40 930 0.30 1380 0.26
45 2.35 495 0.40 945 0.29 1395 0.26
60 1.84 510 0.39 960 0.29 1410 0.26
75 1.52 525 0.38 975 0.29 1425 0.26
90 1.31 540 0.38 990 0.29 1440 0.26
105 1.15 555 0.37 1005 0.29 1455 0.26
120 1.04 570 0.37 1020 0.29 1470 0.26
135 0.94 585 0.36 1035 0.29 1485 0.25
150 0.87 600 0.36 1050 0.28 1500 0.25
175 0.81 615 0.35 1065 0.28 1515 0.25
180 0.76 630 0.35 1080 0.28 1530 0.25
195 0.71 645 0.35 1095 0.28 1545 0.25
210 0.68 660 0.34 1110 0.28 1560 0.25
225 0.64 675 0.34 1125 0.28 1575 0.25
240 0.62 690 0.34 1140 0.28 1590 0.25
255 0.59 705 0.33 1155 0.27 1605 0.25
270 0.57 720 0.33 1170 0.27 1620 0.25
285 0.55 735 0.33 1185 0.27 1635 0.25
300 0.53 750 0.32 1200 0.27 1650 0.25
315 0.51 765 0.32 1215 0.27 1665 0.25
330 0.50 780 0.32 1230 0.27 1680 0.25
345 0.49 795 0.32 1245 0.27 1695 0.25
360 0.47 810 0.31 1260 0.27 1710 0.25
375 0.46 825 0.31 1275 0.27 1725 0.24
390 0.46 840 0.31 1290 0.27 1740 0.24
405 0.45 855 0.31 1305 0.26 1755 0.24
420 0.44 870 0.30 1320 0.26 1770 0.24
435 0.43 885 0.30 1335 0.26 1785 0.24
450 0.43 900 0.30 1350 0.26 1800 0.24

Table 6. Conductivity meter readings at varying NaOH:Ethyl Acetate Ratio (A:B=1.3)


Temperature (T)=30℃ NaOH:Ethyl Acetate molar ratio=1.3:1
Initial NaOH conc (CAO)=0.2 mol/L Initial NaOH Volume (VA)=565 mL
Initial Ethyl Acetate conc (CBO)=0.2 mol/L Initial Ethyl Acetate Volume (VB)=435 mL
Reactor Volume (V)=1 L
Time Conductivity Time Conductivity Time Conductivity Time Conductivity
(s) meter reading (s) meter reading (s) meter reading (s) meter reading
(YT, mS/cm) (YT, mS/cm) (YT, mS/cm) (YT, mS/cm)
15 21.43 465 9.95 915 9.95 1365 9.95
30 15.93 480 9.95 930 9.95 1380 9.95
45 13.51 495 9.95 945 9.95 1395 9.95
60 12.21 510 9.95 960 9.95 1410 9.95
75 11.44 525 9.95 975 9.95 1425 9.95
90 10.95 540 9.95 990 9.95 1440 9.95
105 10.64 555 9.95 1005 9.95 1455 9.95
120 10.42 570 9.95 1020 9.95 1470 9.95
135 10.28 585 9.95 1035 9.95 1485 9.95
150 10.18 600 9.95 1050 9.95 1500 9.95
175 10.11 615 9.95 1065 9.95 1515 9.95
180 10.06 630 9.95 1080 9.95 1530 9.95
195 10.03 645 9.95 1095 9.95 1545 9.95
210 10.01 660 9.95 1110 9.95 1560 9.95
225 9.99 675 9.95 1125 9.95 1575 9.95
240 9.98 690 9.95 1140 9.95 1590 9.95
255 9.97 705 9.95 1155 9.95 1605 9.95
270 9.97 720 9.95 1170 9.95 1620 9.95
285 9.96 735 9.95 1185 9.95 1635 9.95
300 9.96 750 9.95 1200 9.95 1650 9.95
315 9.96 765 9.95 1215 9.95 1665 9.95
330 9.96 780 9.95 1230 9.95 1680 9.95
345 9.96 795 9.95 1245 9.95 1695 9.95
360 9.96 810 9.95 1260 9.95 1710 9.95
375 9.95 825 9.95 1275 9.95 1725 9.95
390 9.95 840 9.95 1290 9.95 1740 9.95
405 9.95 855 9.95 1305 9.95 1755 9.95
420 9.95 870 9.95 1320 9.95 1770 9.95
435 9.95 885 9.95 1335 9.95 1785 9.95
450 9.95 900 9.95 1350 9.95 1800 9.95

Table 7. Conductivity meter readings at varying NaOH:Ethyl Acetate Ratio (A:B=1.5)


Temperature (T)=50℃ NaOH:Ethyl Acetate molar ratio=1.5:1
Initial NaOH conc (CAO)=0.2 mol/L Initial NaOH Volume (VA)=600 mL
Initial Ethyl Acetate conc (CBO)=0.2 mol/L Initial Ethyl Acetate Volume (VB)=400 mL
Reactor Volume (V)=1 L
Time Conductivity Time Conductivity Time Conductivity Time Conductivity
(s) meter reading (s) meter reading (s) meter reading (s) meter reading
(YT, mS/cm) (YT, mS/cm) (YT, mS/cm) (YT, mS/cm)
15 24.66 465 15.19 915 15.19 1365 15.19
30 19.55 480 15.19 930 15.19 1380 15.19
45 17.45 495 15.19 945 15.19 1395 15.19
60 16.42 510 15.19 960 15.19 1410 15.19
75 15.88 525 15.19 975 15.19 1425 15.19
90 15.58 540 15.19 990 15.19 1440 15.19
105 15.42 555 15.19 1005 15.19 1455 15.19
120 15.32 570 15.19 1020 15.19 1470 15.19
135 15.26 585 15.19 1035 15.19 1485 15.19
150 15.23 600 15.19 1050 15.19 1500 15.19
175 15.21 615 15.19 1065 15.19 1515 15.19
180 15.20 630 15.19 1080 15.19 1530 15.19
195 15.20 645 15.19 1095 15.19 1545 15.19
210 15.19 660 15.19 1110 15.19 1560 15.19
225 15.19 675 15.19 1125 15.19 1575 15.19
240 15.19 690 15.19 1140 15.19 1590 15.19
255 15.19 705 15.19 1155 15.19 1605 15.19
270 15.19 720 15.19 1170 15.19 1620 15.19
285 15.19 735 15.19 1185 15.19 1635 15.19
300 15.19 750 15.19 1200 15.19 1650 15.19
315 15.19 765 15.19 1215 15.19 1665 15.19
330 15.19 780 15.19 1230 15.19 1680 15.19
345 15.19 795 15.19 1245 15.19 1695 15.19
360 15.19 810 15.19 1260 15.19 1710 15.19
375 15.19 825 15.19 1275 15.19 1725 15.19
390 15.19 840 15.19 1290 15.19 1740 15.19
405 15.19 855 15.19 1305 15.19 1755 15.19
420 15.19 870 15.19 1320 15.19 1770 15.19
435 15.19 885 15.19 1335 15.19 1785 15.19
450 15.19 900 15.19 1350 15.19 1800 15.19

Table 8. Conductivity meter readings at varying NaOH:Ethyl Acetate Ratio (A:B=1.7)


Temperature (T)=50℃ NaOH:Ethyl Acetate molar ratio=1.7:1
Initial NaOH conc (CAO)=0.2 mol/L Initial NaOH Volume (VA)=630 mL
Initial Ethyl Acetate conc (CBO)=0.2 mol/L Initial Ethyl Acetate Volume (VB)=370 mL
Reactor Volume (V)=1 L
Time Conductivity Time Conductivity Time Conductivity Time Conductivity
(s) meter reading (s) meter reading (s) meter reading (s) meter reading
(YT, mS/cm) (YT, mS/cm) (YT, mS/cm) (YT, mS/cm)
15 27.63 465 19.67 915 19.67 1365 19.67
30 22.94 480 19.67 930 19.67 1380 19.67
45 21.16 495 19.67 945 19.67 1395 19.67
60 20.38 510 19.67 960 19.67 1410 19.67
75 20.02 525 19.67 975 19.67 1425 19.67
90 19.84 540 19.67 990 19.67 1440 19.67
105 19.76 555 19.67 1005 19.67 1455 19.67
120 19.71 570 19.67 1020 19.67 1470 19.67
135 19.69 585 19.67 1035 19.67 1485 19.67
150 19.68 600 19.67 1050 19.67 1500 19.67
175 19.68 615 19.67 1065 19.67 1515 19.67
180 19.67 630 19.67 1080 19.67 1530 19.67
195 19.67 645 19.67 1095 19.67 1545 19.67
210 19.67 660 19.67 1110 19.67 1560 19.67
225 19.67 675 19.67 1125 19.67 1575 19.67
240 19.67 690 19.67 1140 19.67 1590 19.67
255 19.67 705 19.67 1155 19.67 1605 19.67
270 19.67 720 19.67 1170 19.67 1620 19.67
285 19.67 735 19.67 1185 19.67 1635 19.67
300 19.67 750 19.67 1200 19.67 1650 19.67
315 19.67 765 19.67 1215 19.67 1665 19.67
330 19.67 780 19.67 1230 19.67 1680 19.67
345 19.67 795 19.67 1245 19.67 1695 19.67
360 19.67 810 19.67 1260 19.67 1710 19.67
375 19.67 825 19.67 1275 19.67 1725 19.67
390 19.67 840 19.67 1290 19.67 1740 19.67
405 19.67 855 19.67 1305 19.67 1755 19.67
420 19.67 870 19.67 1320 19.67 1770 19.67
435 19.67 885 19.67 1335 19.67 1785 19.67
450 19.67 900 19.67 1350 19.67 1800 19.67

Table 9. Conductivity meter readings at varying NaOH:Ethyl Acetate Ratio (A:B=2.0)


Temperature (T)=50℃ NaOH:Ethyl Acetate molar ratio=2:1
Initial NaOH conc (CAO)=0.2 mol/L Initial NaOH Volume (VA)=500 mL
Initial Ethyl Acetate conc (CBO)=0.2 mol/L Initial Ethyl Acetate Volume (VB)=500 mL
Reactor Volume (V)=1 L
Time Conductivity Time Conductivity Time Conductivity Time Conductivity
(s) meter reading (s) meter reading (s) meter reading (s) meter reading
(YT, mS/cm) (YT, mS/cm) (YT, mS/cm) (YT, mS/cm)
15 31.53 465 25.20 915 25.20 1365 25.20
30 27.43 480 25.20 930 25.20 1380 25.20
45 26.06 495 25.20 945 25.20 1395 25.20
60 25.54 510 25.20 960 25.20 1410 25.20
75 25.34 525 25.20 975 25.20 1425 25.20
90 25.26 540 25.20 990 25.20 1440 25.20
105 25.23 555 25.20 1005 25.20 1455 25.20
120 25.21 570 25.20 1020 25.20 1470 25.20
135 25.21 585 25.20 1035 25.20 1485 25.20
150 25.21 600 25.20 1050 25.20 1500 25.20
175 25.20 615 25.20 1065 25.20 1515 25.20
180 25.20 630 25.20 1080 25.20 1530 25.20
195 25.20 645 25.20 1095 25.20 1545 25.20
210 25.20 660 25.20 1110 25.20 1560 25.20
225 25.20 675 25.20 1125 25.20 1575 25.20
240 25.20 690 25.20 1140 25.20 1590 25.20
255 25.20 705 25.20 1155 25.20 1605 25.20
270 25.20 720 25.20 1170 25.20 1620 25.20
285 25.20 735 25.20 1185 25.20 1635 25.20
300 25.20 750 25.20 1200 25.20 1650 25.20
315 25.20 765 25.20 1215 25.20 1665 25.20
330 25.20 780 25.20 1230 25.20 1680 25.20
345 25.20 795 25.20 1245 25.20 1695 25.20
360 25.20 810 25.20 1260 25.20 1710 25.20
375 25.20 825 25.20 1275 25.20 1725 25.20
390 25.20 840 25.20 1290 25.20 1740 25.20
405 25.20 855 25.20 1305 25.20 1755 25.20
420 25.20 870 25.20 1320 25.20 1770 25.20
435 25.20 885 25.20 1335 25.20 1785 25.20
450 25.20 900 25.20 1350 25.20 1800 25.20

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