AMS 5545E

AEROSPACE
MATERIAL Issued JAN 1961
SPECIFICATION Revised
Reaffirmed
MAR 2002
OCT 2006

Superseding AMS 5545D

Nickel Alloy, Corrosion and Heat-Resistant, Sheet, Strip, and Plate

54Ni - 19Cr - 11Co - 9.8Mo - 3.2Ti - 1.5Al - 0.006B
Vacuum Induction and Consumable Electrode Melted, Solution Heat Treatable
Precipitation Heat Treated
(Composition similar to UNS N07041)
RATIONALE

This document has been reaffirmed to comply with the SAE 5-year Review policy.
1. SCOPE:

1.1 Form:

This specification covers a corrosion and heat-resistant nickel alloy in the form of sheet, strip, and
plate.

1.2 Application:

These products have been used typically for parts requiring high strength up to 1600 °F (871 °C)
and oxidation resistance up to 1800 °F (982 °C), but usage is not limited to such applications.

2. APPLICABLE DOCUMENTS:

The issue of the following documents in effect on the date of the purchase order forms a part of this
specification to the extent specified herein. The supplier may work to a subsequent revision of a
document unless a specific document issue is specified. When the referenced document has been
canceled and no superseding document has been specified, the last published issue of that document
shall apply.

2.1 SAE Publications:

Available from SAE, 400 Commonwealth Drive, Warrendale, PA 15096-0001 or www.sae.org.

AMS 2262 Tolerances, Nickel, Nickel Alloy, and Cobalt Alloy Sheet, Strip, and Plate
MAM 2262 Tolerances, Metric, Nickel, Nickel Alloy, and Cobalt Alloy Sheet, Strip, and Plate
AMS 2269 Chemical Check Analysis Limits, Nickel, Nickel Alloys and Cobalt Alloys
AMS 2371 Quality Assurance Sampling and Testing, Corrosion and Heat-Resistant Steels and
Alloys, Wrought Products and Forging Stock
AMS 2750 Pyrometry
SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is
entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising therefrom, is the sole responsibility of the user.”
SAE reviews each technical report at least every five years at which time it may be reaffirmed, revised, or cancelled. SAE invites your written comments and suggestions.
Copyright © 2006 SAE International
All rights reserved. No part of this publication may be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical,
photocopying, recording, or otherwise, without the prior written permission of SAE.
TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada)
Tel: 724-776-4970 (outside USA)
Fax: 724-776-0790
Email: [email protected]
SAE WEB ADDRESS: http://www.sae.org
 AMS 5545E SAE AMS 5545E

2.1 (Continued):

AMS 2807 Identification, Carbon and Low-Alloy Steels, Corrosion and Heat-Resistant Steels and
Alloys, Sheet, Strip, Plate, and Aircraft Tubing

AS4194 Sheet and Strip Surface Finish Nomenclature

2.2 ASTM Publications:

Available from ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959 or
www.astm.org.

ASTM A 480/A 480M Flat-Rolled Stainless and Heat-Resisting Steel Plate, Sheet, and Strip
ASTM E 8 Tension Testing of Metallic Materials
ASTM E 8M Tension Testing of Metallic Materials (Metric)
ASTM E 18 Rockwell Hardness and Rockwell Superficial Hardness of Metallic Materials
ASTM E 21 Elevated Temperature Tension Tests of Metallic Materials
ASTM E 112 Determining Average Grain Size
ASTM E 290 Semi-Guided Bend Test for Ductility of Metallic Materials
ASTM E 354 Chemical Analysis of High-Temperature, Electrical, Magnetic, and Other
Similar Iron, Nickel, and Cobalt Alloys
ASTM E 384 Microindentation Hardness of Materials

3. TECHNICAL REQUIREMENTS:

3.1 Composition:

Shall conform to the percentages by weight, shown in Table 1, determined by wet chemical methods
in accordance with ASTM E 354, by spectrochemical methods, or by other analytical methods
acceptable to purchaser:

TABLE 1 - Composition
Element min max
Carbon -- 0.12
Manganese -- 0.10
Silicon -- 0.50
Sulfur -- 0.015
Chromium 18.00 20.00
Cobalt 10.00 12.00
Molybdenum 9.00 10.50
Titanium 3.00 3.30
Aluminum 1.40 1.60
Boron (3.1.1) 0.0030 0.010
Iron -- 5.00
Copper -- 0.50
Nickel remainder

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3.1.1 Boron may be less than 0.0030% by weight, determined on sheet and strip under 0.050 inch (1.27
mm) in nominal thickness, provided the specified requirement is met on stock prior to rolling into
sheet or strip.

3.1.2 Check Analysis: Composition variations shall meet the applicable requirements of AMS 2269.

3.2 Melting Practice:

Alloy shall be multiple melted using vacuum induction followed by consumable electrode practice in
the remelt cycle.

3.3 Condition:

The product shall be supplied in the following condition:

3.3.1 Sheet and Strip: Hot or cold rolled, solution heat treated, and, unless solution heat treatment is
performed in an atmosphere yielding a bright finish, descaled having a surface appearance in
accordance with ASTM A 480/A 480M and AS4194 comparable to 3.3.1.1 or 3.3.1.2 as applicable.

3.3.1.1 Sheet: No. 2D finish.

3.3.1.2 Strip: No. 1 strip finish.

3.3.2 Plate: Hot rolled, solution heat treated, and descaled.

3.4 Solution Heat Treatment:

The product shall be solution heat treated by heating in a suitable atmosphere to 1975 °F ± 25 (1079
°C ± 14), holding at heat for not less than 60 minutes per inch (25 mm) of nominal thickness, and
cooling at a rate equivalent to a rapid air cool or faster. Pyrometry shall be in accordance with AMS
2750.

3.5 Properties:

The product shall conform to the following requirements:

3.5.1 As Solution Heat Treated:

3.5.1.1 Tensile Properties: Shall be as shown in Table 2, determined in accordance with ASTM E 8 or
ASTM E 8M.

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TABLE 2A - Tensile Properties, Inch/Pound Units

Tensile Yield Strength Elongation in
Nominal Thickness Strength at 0.2% Offset 2 Inches or 4D
Inches ksi, max ksi, max %, min
Up to 0.015, incl 170 100 20
Over 0.015 to 0.115, incl 170 100 30
Over 0.115 to 0.1874, incl 180 115 30
Over 0.1874 195 140 30

TABLE 2B - Tensile Properties, SI Units

Tensile Yield Strength Elongation in
Nominal Thickness Strength at 0.2% Offset 50.8 mm or 4D
Millimeters MPa, max MPa, max %, min
Up to 0.38, incl 1172 689 20
Over 0.38 to 2.92, incl 1172 689 30
Over 2.92 to 4.760, incl 1241 793 30
Over 4.760 1344 965 30

3.5.1.2 Hardness: Shall be not higher than shown in Table 3, or equivalent (See 8.2), determined in
accordance with ASTM E 18; for thin gages, where superficial hardness testing is impractical,
microhardness testing in accordance with ASTM E 384 may be used. Product shall not be
rejected on the basis of hardness if the tensile property requirements of 3.5.1.1 are acceptable,
determined on specimens taken from the same sample as that with nonconforming hardness or
from another sample with similar nonconforming hardness.

TABLE 3 - Maximum Hardness Requirement

Nominal Thickness Nominal Thickness
Inch Millimeters Hardness
Up to 0.040, incl Up to 1.02, incl 75 HR15N
Over 0.040 to 0.070, incl Over 1.02 to 1.78, incl 64 HRA
Over 0.070 to 0.1874, incl Over 1.78 to 4.760, incl 30 HRC

3.5.1.3 Bending: Product shall withstand, without cracking, bending in accordance with ASTM E 290
through an angle of 180 degrees around a diameter equal to the bend factor shown in Table 4
times the nominal thickness of the product, with axis of bend parallel to the direction of rolling.

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TABLE 4 - Bending Parameters

Nominal Thickness Nominal Thickness Bend
Inch Millimeters Factor
Up to 0.062, incl Up to 1.57, incl 2
Over 0.062 to 0.125, incl Over 1.57 to 3.18, incl 2.5
Over 0.125 to 0.1874, incl Over 3.18 to 4.760, incl 3

3.5.1.4 Average Grain Size: Shall be ASTM No. 3 or finer, determined in accordance with ASTM E 112.

3.5.1.5 Microstructure: Metallographic examination shall disclose no significant alloy-depleted layer or

other undesirable surface condition. Standards for acceptance shall be as agreed upon by
purchaser and vendor.

3.5.2 After Precipitation Heat Treatment: The product shall have the following properties after being
precipitation heat treated by heating to 1400 °F ± 15 (760 °C ± 8), holding at heat for not less than
16 hours, and cooling at a rate equivalent to cooling in air.

3.5.2.1 Tensile Properties:

3.5.2.1.1 At Room Temperature: Shall be as shown in Table 5, determined in accordance with ASTM E 8
or ASTM E 8M.

TABLE 5A - Minimum Room Temperature Tensile Properties, Inch/Pound Units

Tensile Yield Strength Elongation in
Nominal Thickness Strength at 0.2% Offset 2 Inches or 4D
Inches ksi ksi %
Up to 0.020, incl 160 120 6
Over 0.020 170 130 10

TABLE 5B - Minimum Room Temperature Tensile Properties, SI Units

Tensile Yield Strength Elongation in
Nominal Thickness Strength at 0.2% Offset 50.8 mm or 4D
Millimeters MPa MPa %
Up to 0.51, incl 1103 827 6
Over 0.51 1172 896 10

3.5.2.1.2 At 1400 °F (760 °C): Shall be as specified in Table 6, determined in accordance with ASTM E
21 on specimens heated to 1400 °F ± 10 (760 °C ± 6), held at heat for not less than 20 minutes
before testing, and tested at 1400 °F ± 10 (760 °C ± 6).

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TABLE 6A - Minimum 1400 °F Tensile Properties, Inch/Pound Units

Tensile Yield Strength Elongation in
Nominal Thickness Strength at 0.2% Offset 2 Inches or 4D
Inches ksi ksi %
Up to 0.020, incl 130 110 3
Over 0.020 140 110 3

TABLE 6B - Minimum 760 °C Tensile Properties, SI Units

Tensile Yield Strength Elongation in
Nominal Thickness Strength at 0.2% Offset 50.8 mm or 4D
Millimeters MPa MPa %
Up to 0.51, incl 896 758 3
Over 0.51 965 758 3

3.5.2.2 Hardness: Shall be not lower than 35 HRC, or equivalent (See 8.2), determined in accordance
with ASTM E 18; for thin gages where superficial hardness testing is impractical, microhardness
testing in accordance with ASTM 384 may be used. Product shall not be rejected on the basis of
hardness if the tensile property requirements of 3.5.2.1.1 are acceptable, determined on
specimens taken from the same sample as that with nonconforming hardness or from another
sample with similar nonconforming hardness.

3.6 Quality:

The product, as received by purchaser, shall be uniform in quality and condition, sound, and free
from foreign materials and from imperfections detrimental to usage of the product.

3.7 Tolerances:

Shall conform to all applicable requirements of AMS 2262 or MAM 2262.

4. QUALITY ASSURANCE PROVISIONS:

4.1 Responsibility for Inspection:

The vendor of the product shall supply all samples for vendor's tests and shall be responsible for the
performance of all required tests. Purchaser reserves the right to sample and to perform any
confirmatory testing deemed necessary to ensure that the product conforms to specified
requirements.

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4.2 Classification of Tests:

All technical requirements are acceptance tests and shall be performed on each heat or lot as
applicable.

4.3 Sampling and Testing:

Shall be in accordance with AMS 2371.

4.4 Reports:

The vendor of the product shall furnish with each shipment a report showing the following results of
tests and relevant information:

4.4.1 For Each Heat:

Composition.

4.4.2 For Each Lot:

Tensile properties solution heat treated

Bending properties
Average grain size
Microstructure
Tensile properties precipitation heat treated, room temperature and at 1400 °F (760 °C)
Hardness precipitation heat treated.

4.4.3 A statement that the product conforms to the other technical requirements.

4.4.4 Purchase order number

Heat and lot numbers
AMS 5545E
Size
Quantity.

4.5 Resampling and Retesting:

Shall be in accordance with AMS 2371.

5. PREPARATION FOR DELIVERY:

5.1 Identification:

Shall be in accordance with AMS 2807.

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5.2 Packaging:

The product shall be prepared for shipment in accordance with commercial practice and in
compliance with applicable rules and regulations pertaining to the handling, packaging, and
transportation of the product to ensure carrier acceptance and safe delivery.

6. ACKNOWLEDGMENT:

A vendor shall mention this specification number and its revision letter in all quotations and when
acknowledging purchase orders.

7. REJECTIONS:

Product not conforming to this specification, or to modifications authorized by purchaser, will be

subject to rejection.

8. NOTES:

8.1 A change bar ( l ) located in the left margin is for the convenience of the user in locating areas where
technical revisions, not editorial changes, have been made to the previous issue of this specification.
An (R) symbol to the left of the document title indicates a complete revision of the specification,
including technical revisions. Change bars and (R) are not used in original publications, nor in
specifications that contain editorial changes only.

8.2 Hardness conversion tables for metals are presented in ASTM E 140.

8.3 Terms used in AMS are clarified in ARP1917.

8.4 Dimensions and properties in inch/pound units and the Fahrenheit temperatures are primary;
dimensions and properties in SI units and the Celsius temperatures are shown as the approximate
equivalents of the primary units and are presented only for information.

8.5 Purchase documents should specify not less than the following:

AMS 5545E
Form and size of product desired
Quantity of product desired
Acceptance standards for microstructure (See 3.5.1.5).

PREPARED UNDER THE JURISDICTION OF AMS COMMITTEE "F"

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