Tubular Rust Directions
Tubular Rust Directions
Tubular Rust Directions
In this experiment, you will determine the fraction of air that is made up of oxygen (“the % oxygen in air”). We will take
advantage of the fact that steel rusts in air as it reacts with the oxygen in the air. Steel is mostly (99%) iron, and the as
the oxygen and iron react, we will form iron oxide. As the oxygen is removed from the air, the volume of air will change.
From this change you can figure out what percentage of the air was made up of oxygen.
Procedure:
1. Create a data table with two columns – “time in minutes” and “height of water in mm.”
2. Attach a small centimeter ruler to the test tube using a rubber band. Make sure the 0mm mark is toward the open
end of the test tube.
3. Measure about 1 gram of steel wool. Record the exact mass of the steel wool you use. Pull it apart to increase its
surface area. To promote rusting, dip the wool into some vinegar. Shake off the excess vinegar into the sink.
4. Push the steel wool halfway up the test tube using a pencil. Make sure you keep the wool packed very loosely.
6. Turn the test tube so it is upside down, and clamp the test tube to a ring stand. Adjust the height of
the test tube so it is in the water, and so the water level inside the test tube is lower than the water level in the
beaker.
7. Adjust the ruler so it is even with the water level inside the test tube.
Water level
Ruler inside test
tube
8. Observe what happens to the level of the water in the test tube as the steel wool rusts. Record your results in your
lab notebook.
9. In your data table, record where the water level is along the ruler in the test tube, not the beaker, every 5 minutes.
10. As the level changes, keep adjusting the height of the test tube so that the water level inside the test tube remains
below the water level in the beaker. Be sure not to change the position of the ruler!
11. Once the water level has not changed for at least 10 minutes, you may stop collecting data.
12. Discuss with your group a method of calculating the fraction of air that is composed of oxygen. Write down your
method and calculate the % of oxygen in the air.
13. Please answer the following questions (on a separate sheet of paper!):
a. What changes did you observe take place? (List at least 3) For each change you observed, indicate
whether this was a chemical or physical change.
b. Why does the level of water in the test tube change?
c. What method did you use to calculate the % oxygen in air? Show your calculation(s) for the
% oxygen in air and how that number compares to your hypothesis.
d. Do you think it would take a shorter or longer time for this experiment to run if it was packed tightly?
Explain.
e. What questions do you have after doing this experiment that you would like to explore?