Cold Molding
Cold Molding
Lab Report # 3
Cold Mounting
ACRYLIC RESINS:
Acrylics are easy-to-use resins with short curing times, very limited shrinkage, and excellent
mounting properties. They are well-suited for both serials mounting of irregularly shaped specimens
and for routine work or single specimens. Acrylics are available with and without a mineral filler. Dye
can be used if color coding is needed. When mixing acrylic resins, it is recommended to add powder
to the liquid (hardener) – this will result in the most uniform resin mixture.
EPOXY RESINS:
Epoxy resins are suitable for mounting of all types of materials and are especially recommended for
vacuum impregnation. Epoxies have the lowest shrinkage of all cold-mounting resins. The curing
time is relatively long, but adhesion to most materials is excellent. They polymerize through a
chemical reaction after being mixed in the correct proportions. The hardened epoxy is duroplastic,
and not affected by moderate heat or chemicals. Struers' epoxy systems consist of two components:
a resin and a curing agent/hardener. Properties such as low vapor pressure, transparency, good
adhesion, low viscosity, and no shrinkage are all specific to epoxies. As the stoichiometric resin:
hardener ratio is critical; both parts should be weighed to obtain the best mounting result. If it is
only possible to measure the amount by volume, use syringes to measure the quantities of resin and
curing agent/hardener.
Polyester resins:
Polyester belongs to the catalyzed system, like acrylics. Curing times are relatively short and the
hardened specimen is duroplastic.
Procedure:
To prepare the sample we first poured the acrylic resin in a container. Then six drops of
binder and three drops of activator were added. This mixture was thoroughly mixed with a
small spatula. After that our metal specimens were placed in molds which in our case were
PET bottle caps. Then the resin mixture was carefully added in each mold. The molds were
left overnight for resin to harden. After almost 24 hours, the resin had hardened, and the
molds were cut open using blades. We finally had our cold molded metallography samples.
Sources of error:
The problems that occur while cold mounting are:
Improper mixing of the hardener, activator which can produce flaws in our mount.
Formation of bubbles of air inside the mount.
Precautions:
Wear personal protection equipment(PPE).
Do not touch or smell the chemicals it can hazardous.
Conclusion:
The purpose of cold mounting is to provide better grip while metallography processes such as
grinding as the metal samples are very small so handling such small pieces on machine becomes a
difficult task. So it provides ease in doing such a difficult process.
References
[1] "Miley D.V., Calabra A.E. (1974) A Review of Specimen Mounting Methods for Metallography. In:
McCall J.L., Mueller W.M. (eds) Metallographic Specimen Preparation. Springer, Boston, MA".