BRITISH STANDARD BS EN ISO

1518:2001
BS 3900-E2:1992
Incorporating
Amendment No. 1 to
BS 3900-E2:1992
(renumbers the BS as
BS EN ISO 1518:2001)
Methods of test for

Paints —
Part E2: Scratch test

NOTE It is recommended that this Part be read in conjunction with

BS 3900-0, issued separately.

The European Standard EN ISO 1518:2000 has the status of a

British Standard.

ICS 87.040

NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAW

BS EN ISO 1518:2001

Committees responsible for this

British Standard

The preparation of this British Standard was entrusted by the Pigments,

Paints and Varnishes Standards Policy Committee (PVC/-) to Technical
Committee PVC/10, upon which the following bodies were represented:
British Gas plc
Health and Safety Executive
Institute of Metal Finishing
Ministry of Defence
Oil and Colour Chemists’ Association
Paint Research Association
Paintmakers’ Association of Great Britain Ltd.
Titanium Pigment Manufacturers’ Technical Committee

This British Standard, having

been prepared under the
direction of the Pigments,
Paints and Varnishes
Standards Policy Committee,
was published under the
authority of the Standards
Board and comes into effect on
15 June 1992

© BSI 03-2001

First published 1966

Amendments issued since publication
Second edition June 1969
Third edition June 1992 Amd. No. Date Comments

12091 March Implementation of the European Standard

2001
The following BSI references
relate to the work on this
standard:
Committee reference STI/10
Draft for comment 87/51645 DC

ISBN 0 580 20914 8

 BS EN ISO 1518:2001

Contents

Page
Committees responsible Inside front cover
National foreword ii
1 Scope 3
2 Normative references 3
3 Required supplementary information 3
4 Apparatus 3
5 Sampling 4
6 Test panels 4
7 Procedure 5
8 Precision 5
9 Test report 5
Annex A (normative) Required supplementary information 6
Annex B (informative) Procedure found to be convenient for
manufacture and re-tipping of scratch test needles 7
Annex ZA (normative) Normative references to international publications
with their relevant European publications 9
Figure 1 — Scratch apparatus 4
Figure B.1 — Suitable shank for scratch test tip 8

© BSI 03-2001 i
BS EN ISO 1518:2001

National foreword

This British Standard is the official English language version of

EN ISO 1518:2000. It is identical with ISO 1518:1992.
The UK participation in its preparation was entrusted to Technical Committee
STI/10, Test methods for paints, which has the responsibility to:

— aid enquirers to understand the text;

— present to the responsible international/European committee any
enquiries on the interpretation, or proposals for change, and keep the
UK interests informed;
— monitor related international and European developments and
promulgate them in the UK.
A list of organizations represented on this committee can be obtained on request
to its secretary.
Cross-references
Attention is drawn to the fact that CEN and CENELEC Standards normally
include an annex which lists normative references to international publications
with their corresponding European publications. The British Standards which
implement these international or European publications may be found in the BSI
Standards Catalogue under the section entitled “International Standards
Correspondence Index”, or by using the “Find” facility of the BSI Standards
Electronic Catalogue.
A British Standard does not purport to include all the necessary provisions of a
contract. Users of British Standards are responsible for their correct application.
Compliance with a British Standard does not of itself confer immunity
from legal obligations.

Summary of pages
This document comprises a front cover, an inside front cover, pages i and ii, the
EN ISO title page, the EN ISO foreword page, pages 1 to 9 and a back cover.
The BSI copyright notice displayed in this document indicates when the
document was last issued.

ii © BSI 03-2001
EUROPEAN STANDARD EN ISO 1518
NORME EUROPÉENNE
EUROPÄISCHE NORM March 2000

ICS 87.040

English version

Paints and varnishes — Scratch test

(ISO 1518:1992)

Peintures et vernis — Essai de rayure Beschichtungsstoffe — Ritzprüfung

(ISO 1518:1992) (ISO 1518:1992)

This European Standard was approved by CEN on 18 February 2000.

CEN members are bound to comply with the CEN/CENELEC Internal
Regulations which stipulate the conditions for giving this European Standard
the status of a national standard without any alteration. Up-to-date lists and
bibliographical references concerning such national standards may be obtained
on application to the Central Secretariat or to any CEN member.
This European Standard exists in three official versions (English, French,
German). A version in any other language made by translation under the
responsibility of a CEN member into its own language and notified to the
Central Secretariat has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Czech
Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy,
Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and
United Kingdom.

CEN
European Committee for Standardization
Comité Européen de Normalisation
Europäisches Komitee für Normung

Central Secretariat: rue de Stassart 36, B-1050 Brussels

© 2000 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national
Members.
Ref. No. EN ISO 1518:2000 E
EN ISO 1518:2000

Foreword
The text of the International Standard from
Technical Committee ISO/TC 35, Paints and
varnishes, of the International Organization for
Standardization (ISO) has been taken over as a
European Standard by Technical Committee
CEN/TC 139, Paints and varnishes, the Secretariat
of which is held by DIN.
This European Standard shall be given the status of
a national standard, either by publication of an
identical text or by endorsement, at the latest by
September 2000, and conflicting national standards
shall be withdrawn at the latest by September 2000.
According to the CEN/CENELEC Internal
Regulations, the national standards organizations
of the following countries are bound to implement
this European Standard: Austria, Belgium, Czech
Republic, Denmark, Finland, France, Germany,
Greece, Iceland, Ireland, Italy, Luxembourg,
Netherlands, Norway, Portugal, Spain, Sweden,
Switzerland and the United Kingdom.
NOTE Normative references to International Standards are
listed in Annex ZA (normative).

© BSI 03-2001
 EN ISO 1518:2000

1 Scope 3 Required supplementary

1.1 This International Standard is one of a series of
information
standards dealing with the sampling and testing of For any particular application, the test method
paints, varnishes and related products. specified in this International Standard needs to be
It specifies a test method for determining under completed by supplementary information. The
defined conditions the resistance of a single coating items of supplementary information are given in
or a multi-coat system of paint, varnish or related Annex A.
product to penetration by scratching with a 4 Apparatus
hemispherically tipped needle. Penetration of the
needle is to the substrate, except in the case of a 4.1 Scratch apparatus, the principle of which is
multi-coat system, where the penetration of the illustrated in Figure 1; other arrangements which
needle may be either to the substrate or to an give a similar performance can be used, however.
intermediate coat. This apparatus consists essentially of a horizontally
1.2 The method is intended for application as sliding test panel holder (A) driven by a
constant-speed motor (B) at a rate of 30 mm/s
follows:
to 40 mm/s beneath the point of a scratching needle
a) either as a pass/fail test, by testing with a (C), which is perpendicular to the test panel. The
single specified load applied to the needle to needle is fixed in a chuck, directly above which is a
assess compliance with a particular specification; holder capable of carrying weights up to a mass
b) or by applying increasing loads to the needle to of 2 kg. The maximum load for which the apparatus
determine the minimum load at which the coating is designed shall be marked on the test apparatus.
is penetrated. The apparatus is adjusted so that the needle comes
smoothly into contact with the film, i.e. before the
2 Normative references stop (D) reaches the bottom of the sloping ramp, to
The following standards contain provisions which, form a straight scratch not less than 60 mm in
through reference in this text, constitute provisions length. A ramp with an angle of 10° to 15° to the
of this International Standard. At the time of horizontal has been found to be satisfactory. The
publication, the editions indicated were valid. All panel holder can be designed to allow a lateral
standards are subject to revision, and parties to movement of test pieces so that more than one
agreements based on this International Standard scratch test can be carried out on the same test
are encouraged to investigate the possibility of piece.
applying the most recent editions of the standards NOTE 1 Apparatus is now becoming available which will
indicated below. Members of IEC and ISO maintain permit a scratch test to be conducted under continuously
registers of currently valid International Standards. increasing load.

ISO 1512:1991, Paints and varnishes — Sampling 4.2 Indicating device, based on electrical contact
of products in liquid or paste form. between the needle and the metallic substrate to
show when the paint film has been penetrated.
ISO 1513:—1), Paints and varnishes — Examination
and preparation of samples for testing. NOTE 2 This device is not suitable for paints containing
electrically conducting pigments, or if the substrate is
ISO 1514:—2), Paints and varnishes — Standard non-metallic, or if penetration to an intermediate non-conducting
panels for testing. coat is required.

ISO 2808:1991, Paints and varnishes — 4.3 Needle, having a hard hemispherical tip of 1 mm
Determination of film thickness. diameter. The hemispherical tip shall be firmly
attached and the exposed part shall be free from any
ISO 3270:1984, Paints and varnishes and their raw contaminants.
materials — Temperatures and humidities for
conditioning and testing. NOTE 3 Details about the tip and the needle are given in
Annex B.

1) To be published. (Revision of ISO 1513:1980)

2) To be published. (Revision of ISO 1514:1984)

© BSI 03-2001 3
EN ISO 1518:2000

Figure 1 — Scratch apparatus

5 Sampling 6.2 Preparation and coating

Take a representative sample of the product to be Unless otherwise specified, prepare each test panel
tested (or of each product in the case of a multi-coat in accordance with ISO 1514 and then coat it by the
system), as described in ISO 1512. specified method with the product or system under
test. If the product under test is applied by
Examine and prepare each sample for testing, as brushing, any brush marks shall be parallel to the
described in ISO 1513. direction of the scratch on the panel.
6 Test panels NOTE 4 Poorer precision is often obtained if the coating has
been applied by brush.
6.1 Substrate
6.3 Drying and conditioning
Unless otherwise agreed, the substrate shall comply
Dry (or stove) and age each coated test panel for the
with the requirements of ISO 1514 for burnished
specified time and under the specified conditions.
tinplate, burnished steel or hard aluminium Then condition the coated panels at (23 ± 2) °C and
prepared by acid chromating.
a relative humidity of (50 ± 5)%, unless otherwise
The test panels may be cut to fit the apparatus after agreed (see also ISO 3270), for a minimum period
coating the substrate and drying, provided no of 16 h. Carry out the test procedure as soon as
distortion occurs. possible.
6.4 Thickness of coating
Determine the thickness, in micrometres, of the
dried coating by one of the procedures specified in
ISO 2808.

4 © BSI 03-2001
 EN ISO 1518:2000

7 Procedure 7.3 Procedure for determination of minimum

load to cause penetration
7.1 Test conditions
Carry out the procedure given in 7.2.1, 7.2.2, 7.2.3,
Carry out the test at (23 ± 2) °C and a relative 7.2.4, 7.2.5 and 7.2.6, using a different part of the
humidity of (50 ± 5)%, unless otherwise agreed test panel for each scratch, starting at a load
(see also ISO 3270). somewhat less than that expected to cause
Conduct the test on a bench free from vibrations. penetration of the coating and successively
increasing the mass on the needle by suitable
7.2 Procedure for a single specified load increments (for example masses of 50 g), until the
(“pass/fail” test) coating is penetrated. Record the minimum load at
which the needle penetrates the coating to the
7.2.1 Examine a needle (4.3) under × 30 extent specified. Repeat the procedure on a further
magnification to check that the hard tip is smooth, two panels. Report the lowest result of the three
hemispherical and free from contamination. determinations.
7.2.2 Fix the needle in the chuck so that, when in
position on the test panel, the needle will be
8 Precision
perpendicular to the panel holder. Balance the The repeatability of results by the “pass/fail”
needle holder arm by means of the adjustable test (7.2) will usually be ± 10 % of the load.
counterweight. Ensure that the indicating NOTE 5 The precision of the result is strongly dependent on the
device (4.2), if used, is operational by contacting the (uniformity of the) film thickness of the coating.
needle with the panel holder.
9 Test report
7.2.3 Clamp the test panel, with the coating under
test uppermost, to the panel holder of the The test report shall contain at least the following
apparatus, with the longer side of the panel parallel information:
to the direction in which the scratch will be made. a) all details necessary to identify the product
7.2.4 Place weights on the holder above the needle tested;
to obtain the specified load. b) a reference to this International Standard
(ISO 1518);
7.2.5 Start the motor of the apparatus and allow the
scratch to be made on the coating. Observe the c) the items of supplementary information
indicating device during the test, if appropriate, to referred to in Annex A;
determine whether electrical contact between the
d) a reference to the international or national
needle and the panel occurs. standard, product specification or other document
7.2.6 Remove the panel and examine the scratch to supplying the data referred to in c) above;
see if the coating has been penetrated to the extent e) the results of the test:
specified. If, by agreement between the interested
parties, the scratch is observed under suitable — either, for each determination, whether or
magnification, state the degree of magnification in not the coating was penetrated under the
the test report. specified conditions (pass/fail),
— or the minimum load at which the needle
7.2.7 The sequence of operations shall be carried out penetrated the coating;
three times on each of two test panels. If on none of
the six test surfaces the coating has been penetrated f) any deviation from the test method specified;
beyond the performance required under the g) the date(s) of the test.
specified conditions, report the result as “pass”. If
the coating has been penetrated beyond the
performance required on one or more of the six test
surfaces, report the result as “fail”.

© BSI 03-2001 5
EN ISO 1518:2000

Annex A (normative)
Required supplementary information
The items of supplementary information listed in
this annex shall be supplied as appropriate to
enable the method to be carried out.
The information required should preferably be
agreed between the interested parties and may be
derived, in part or totally, from an international or
national standard or other document related to the
product under test.
a) Material (including thickness) and surface
preparation of the substrate.
b) Method of application of the test coating to the
substrate, including duration and conditions of
drying between coats in the case of a multi-coat
system.
c) Duration and conditions of drying (or stoving)
the coat, and conditions of ageing, if applicable,
before testing.
d) Thickness, in micrometres, of the dry coating
and method of measurement in accordance with
ISO 2808, and whether it is a single coating or a
multi-coat system.
e) Temperature and humidity for the test, if
different from those specified in 7.1
(see ISO 3270).
f) Procedure to be carried out (see 1.2).
g) Specified load to be applied to the needle during
the test, if applicable.
h) Performance required of the test coating in
terms of penetration by the needle (see 1.1).

6 © BSI 03-2001
 EN ISO 1518:2000

Annex B (informative) B.2.3 When the shanks have cooled, proceed as

Procedure found to be convenient for described in B.1.2, B.1.3, B.1.4 and B.1.5.
manufacture and re-tipping of scratch B.3 Guidance on tip material
test needles The following tips are in common use.
B.1 Manufacture of new needles a) Steel balls.
B.1.1 Fix a batch of shanks in the vertical position Depending on the circumstances, this type of tip
with the dimpled end uppermost by inserting them may show signs of early wear. In view of the ease
in a tray made from perforated sheet metal. with which needles with steel balls can be made,
it is recommended that they be used once only and
B.1.2 Place a very small quantity of a suitable then re-tipped.
solder paste on the end of each shank, and then put
b) Tungsten carbide tips.
a steel ball in position, relying on the solder paste to
hold the ball in position at this stage. These tips last much longer than steel tips and
NOTE 6 The amount of solder paste to be used is judged by can be obtained commercially.
experience; insufficient will not make a firm soldered joint and c) Ruby tips.
too much will lead to more or less complete envelopment of the
steel ball. These (ceramic) tips last a very long time. The tips
have to be attached to the shank by glueing rather
B.1.3 Place the tray of shanks in an oven or muffle
than by soldering and can be obtained
furnace adjusted to a temperature
of 210 °C to 220 °C for about 5 min to melt the commercially.
solder and thus secure the ball in the dimple at the In all cases, it is important that a suitable steel
end of the shank. shank is used which will hold the tip securely in the
correct position. An example of a suitable shank is
B.1.4 Remove the needles from the source of heat, given in Figure B.1.
allow to cool, and wipe each ball to remove flux
residues.
B.1.5 Check that the ball is securely fixed and that
there is no solder on the part of the ball which will
be used to make the scratch.
B.2 Re-tipping of needles
B.2.1 Fix the needles in a tray made from
perforated sheet metal as described in B.1.1 above.
B.2.2 Place the tray of needles in an oven or muffle
furnace adjusted to a temperature
of 210 °C to 220 °C and, as soon as the solder has
softened, remove the tray and brush the end of the
needles with a clean brush in order to dislodge the
steel balls.

© BSI 03-2001 7
EN ISO 1518:2000

Figure B.1 — Suitable shank for scratch test tip

8 © BSI 03-2001
 EN ISO 1518:2000

Annex ZA (normative)
Normative references to international publications with their relevant
European publications
This European Standard incorporates by dated or undated reference, provisions from other publications.
These normative references are cited at the appropriate places in the text and the publications are listed
hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply
to this European Standard only when incorporated in it by amendment or revision. For undated references
the latest edition of the publication referred to applies.

Publication Year Title EN Year

ISO 2808 1997 Paints and varnishes — Determination of film EN ISO 2808 1999
thickness
ISO 1512 1991 Paints and varnishes — Sampling of products in EN 21512 1994
liquid or paste form
ISO 3270 1984 Paints and varnishes and their raw materials — EN 23270 1991
Temperatures and humidities for conditioning and
testing
ISO 1513 1992 Paints and varnishes — Examination and EN ISO 1513 1994
preparation of samples for testing
ISO 1514 1993 Paints and varnishes — Standard panels for EN ISO 1514 1997
testing

© BSI 03-2001 9
BS EN ISO
1518:2001
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