Topic 0 Drying
Topic 0 Drying
Applications
Continuation of Heat and
Mass Transfer
(Topic 0)
Intended Learning Outcomes
By the end of this topic, students must be able to:
LO.1 To demonstrate the basic principles of drying
by:
Defining Drying
Differentiating between Types of Moisture Content
Classifying Batch and Continuous Driers
Explaining terms in the Batch Drying Rate Equation
LO.2 To discuss the principles of batch drying by:
Drying Curves
Drying Time Equations
1. Constant Rate Period (CRP)
2. Falling Rate Period (FRP)
3. Combined CRP and FRP
Constant Drying Rate Equations
LO.3 To solve batch drying applications
Intended Learning Outcomes
LO.4To be able to set up material and enthalpy
balances around a continuous drying system
and to derive the air and solid properties
needed in the analysis of the dryer;
Requirements
Drying Medium (usually hot air or steam)
Moisture Carrier (usually air)
Pharmaceutical
Food
Textile
Superheated
Steam Dryer
Spray
Dryer
Dryer Classification
According to Mode of Heat Transfer
1. Direct (convective)
2. Indirect (conduction)
3. Radiant
Dryer Classification
According to Mode of Operation
1. Batch Drying - also
known as drying under
constant conditions
Air
2. Continuous Drying -
involves continuous flow
of solid and drying
medium, under variable
conditions
*Study pp. 12-40 to 12-48
Basic Terms Related to Drying
1. Total Moisture Content (W): total weight of moisture per weight of
dry solid
2. Free Moisture Content (X): weight of free or removable moisture
per weight of dry solid
3. Equilibrium Moisture Content (X*): weight of equilibrium or
unremovable moisture per weight of dry solid
%W = %WW/(100- %WW)
Basic Terms Related to Drying
4. Drying Rate (R): weight of moisture removed per time per drying
area
5. Drying Area (A): area in direct contact with the drying medium
7. : drying time
Q - dX
Basic Rate Equation: R =
A d
Other Terms Unbound Moisture - liquid in excess of the
equilibrium moisture content; on the surface
exerts a vapor pressure equivalent to that
of the free liquid
Bound Moisture - retained in a manner that
exerts a vapor pressure less than that of the
free liquid at the given temperature
Liquid may become bound to the solid
by retention in small capillaries
by solution in cells or fiber walls
by homogeneous solution throughout
the solid
by chemical or physical adsorption on
solid surfaces.
Classification of Solids
Nonhygroscopic capillary-porous media
- recognizable pore space
- the pore space is filled with liquid if the capillary
porous medium is completely saturated and is
filled with air when the medium is completely dry
- bound moisture is negligible
- medium does not shrink during drying
-examples: sand, crushed minerals, some ceramics
Classification of Solids
Hygroscopic-porous media
- recognizable pore space
- has large amount of bound moisture
- shrinkage often occurs in the initial stage of
drying
-examples: clay, wood, textile
Classification of Solids
Colloidal (nonporous) media
- no pore space
- evaporation can take place only at the
surface
- all liquid is physically bound
-examples: soap, glue, nylons
Batch Drying Principles
Ideal Batch Drying Process:
1. Transient Period: adjustment, short period
2. Constant Rate Period (CRP): removal of
unbound moisture, partial pressure i = vapor
pressure
3. Falling Rate Period (FRP): removal of bound
moisture, partial pressure i < vapor pressure
4. Critical Free Moisture (Xc): boundary moisture
between CRP and FRP
X1
X CRP
Xc
FRP
c
©UST Ch.E. Department
Batch Drying Curves
Drying Rate Versus Free Moisture
Rc
R CRP
FRP
Xc X1
X
©UST Ch.E. Department
Batch Drying Time Equations
Q - dX
Drying Rate Equation: R=
A d
General Equation for Drying Time:
Q X1 dX
=
A X2 R
A. Constant Rate Period Only (X2 Xc; R = Rc)
Integrating,
Q
= (X1 – X2)
ARc
Q Xc X1
= ln
A Rc X2
Q
= (X1-X2) RLM = (R1- R2)/ ln(R1/R2)
A RLM
Case 3: Given Experimental Data of R and X
X1
Q dX
=
A X2 R
G uG G 1 H
G
VH
2. Air flow perpendicular to solid
h 24.2G 0.37
©UST Ch.E. Department
Batch Drying Examples
1. A wet solid is dried from 20% to 8% moisture in a tray drier
in 6 hours. Critical moisture is 10% and equilibrium
moisture is 2%. All the given % moisture are on dry basis.
a) How long will it take to dry from 8% to 5% moisture?
b) How long did it take to dry from 15% to 10% moisture?
c) How long did it take to dry from 15% to 8% moisture?
Wet slab wt, kg 9.1 7.2 5.3 4.2 3.3 2.9 2.7
Rate, kg/m3-hr 4.9 4.9 4.4 3.9 3.4 2.0 1.0
Drying is from one face. How long will it take to dry the slab to
15% moisture?
• θ?
• X1 Q
[ (0.18 – 0.08) + 0.08 ln (0.08/0.06)]
6=
• Xc ARc
• X2
Batch Drying Examples: Solution
1. A wet solid is dried from 20% to 8% moisture in a tray drier in 6 hours. Critical moisture is 10%
and equilibrium moisture is 2%. All the given % moisture are on dry basis.
a) How long will it take to dry from 8% to 5% moisture?
b) How long did it take to dry from 15% to 10% moisture?
c) How long did it take to dry from 15% to 8% moisture?
b.) Xb1 = 0.15 – 0.02 = 0.13
Q
= 48.7747 CRP
ARc Xb2 = 0.10 – 0.02 = 0.08
t1 w t2
w
H1 H2
F X1 F X2
tS1 tS2
Nomenclature:
F = dry solids rate
Fw = wet solids rate
X = free moisture content
ts = solids temperature
w = dry air rate
H = air humidity
t = air temperature (dry bulb)
Calculation of Air and Heat Requirements
%RHa = 30
Pw1
H1 P1 & tw2 P2 Pa
Tw1 ta = 30oC
𝑃1 18
𝐻1 = × We know that: We know that:
𝑃 − 𝑃1 29
tw2=tw1 H2 = Ha
? but
𝑃2 = 𝑃𝑤2 − 6.5 × 10−4 (1 + 0.000944𝑡𝑤2 ))𝑃(𝑡2 − 𝑡𝑤2 ) 𝑃𝑥 18
𝐻𝑥 = ×
𝑃 − 𝑃𝑥 29
Then, P2 = Pa
Continuous Drying Example
Solution: 𝑃1 18
• Solve H1 𝐻1 = ×
• Solve 𝑷𝒂 𝑃 − 𝑃1 29
𝑃𝑎? 3.642877305 𝑘𝑃𝑎 18
%𝑅𝐻 = 𝐻1 = ×
𝑃𝑠𝑎 101.325 𝑘𝑃𝑎 − 3.642877305 𝑘𝑃𝑎 29
𝐻1 = 0.023149
Vapor Pressure
when ta = 30oC
= 4.247 kPa
• Solve 𝑷𝒂
𝑃2 = 𝑃𝑤2 − 6.5 × 10−4 (1 + 0.000944𝑡𝑤2 ))𝑃(𝑡2 − 𝑡𝑤2 )
• Solve 𝑷1
𝑃1 = 𝑃𝑤1 − 6.5 × 10−4 (1 + 0.000944𝑡𝑤1 ))𝑃(𝑡1 − 𝑡𝑤1 )
𝑃1 = 3.642877305 𝑘𝑃𝑎
Continuous Drying Example
𝑤 𝐻𝑎 − 𝐻1 = 𝐹(𝑊2 − 𝑊1 ) 𝑃𝑎 18 1.2741 18
b.) 𝐻𝑎 = × = × = 0.00790418
𝑃 − 𝑃𝑎 29 101.325 − 1.2741 29
𝐹 = 𝐹𝑤 (1 − 𝑊𝑤 ) = 500(1 − 0.15) = 485 kg/hr
w 𝑊𝑤2 0.05
𝑊2 = =
qw 1 − 𝑊𝑤2 1 − 0.05
0.15
𝑊𝑤1
𝑊1 = =
1 − 𝑊𝑤1 1 − 0.15
𝑞𝑤 = 𝑤𝑉𝐻2
VH2 H2 = Ha = 0.00790418
𝑅𝑇2 1 𝐻2
𝑉𝐻2 = [ + ]
𝑃 29 18
] = 0.982931 m /kg
(0.08206)(70+273) 1 0.00790418 3
𝑉𝐻2 = [ +
1 29 18
𝑘𝑔 𝑘𝐽 1 ℎ𝑟
𝑄𝐻 = 3452.4246 (91.16 − 50.37) ×
ℎ𝑟 𝑘𝑔 3600 𝑠
𝑄𝐻 = 39.12 𝑘𝑊
Continuous Drying Example ©UST Ch.E. Department
2. A rotary drum dryer shall produce 1500 kg/hr of dried solids with 4% Moisture at 35oC from a feed at
30oC and containing 20% Moisture. Specific heat of dry solids is 2.5kJ/kg-K.
Hot air at 85oC with a dew point of 25oC enters the dryer and then leaves it at 45oC with 60%
humidity. Part of this air is recycled and mixed with fresh air at 30oC dry bulb and 15oC wet bulb before
entering the preheater.
The dryer is 12 m long and has 1.5 m diameter, 5 cm wall thickness. It is not insulated and the
convective and radiative heat transfer coefficient to the surroundings may be taken as 25 W/m2-K.
Assume that the outside surface temperature of the dryer is the same as the hot air temperature inside
the dryer. Determine:
a) Volumetric rates of air entering and leaving the dryer (m3/min) to2 = t2
b) Volumetric rates of the fresh and recycled air to the preheater
c) kW of heat supplied to the preheater to1 = t1
d) kW heat loss by dryer to the surroundings
e) kW external heat requirement to the dryer
QL
wR
QL
wR
w = 15868.81777 kg/hr ?
b.) 𝑞𝑎 = 𝑤𝑎 𝑉𝐻𝑎 𝑞𝑅 = 𝑤𝑅?𝑉𝐻𝑅
• Solve for VH1: 𝑉𝐻1 = 𝑅𝑇1 [ 1 + 𝐻1] • Use additional balances to solve for wa & wR
𝑃 29 18
𝑤 = 𝑤𝑎 + 𝑤𝑅 But:
(0.08206)(45+273) 1 0.03895
𝑉𝐻1 = [ + ] = 0.9563 m3/kg 𝐻1′ = 𝐻2
1 29 18 𝑤𝐻1′ = 𝑤𝑎 𝐻𝑎 + 𝑤𝑅 𝐻𝑅 𝐻𝑅 = 𝐻1
𝑅𝑇2 1 𝐻2
• Solve for VH2: 𝑉𝐻2 = [ + ] • Solve for Ha:
𝑃 29 18
𝑉𝐻2 =
(0.08206)(85+273) 1
[ +
0.020045
]= 1.0457 m3/kg 𝑃𝑎 = 𝑃𝑤𝑎 − 6.5 × 10−4 (1 + 0.000944𝑡𝑤𝑎 ))𝑃(𝑡𝑎 − 𝑡𝑤𝑎 )
1 29 18
ℎ𝑠 = [𝐶𝑝𝑠 + 4.184𝑊]𝑡𝑠
ℎ𝑠2 = 93.60167 𝑘𝐽/𝑘𝑔
ℎ𝑠1 = 106.38 𝑘𝐽/𝑘𝑔
𝑘𝐽 1ℎ𝑟
𝑄𝐷 = 15868.81777 145.941 − 138.768 + 1440 93.60167 − 106.38 + 46.42 𝑘𝑊
ℎ𝑟 3600𝑠
𝑄𝐷 = 72.929 kW