IJRET: International Journal of Research in Engineering and Technology eISSN: 2319-1163 | pISSN: 2321-7308

FABRICATION AND MECHANICAL PROPERTIES OF STIR CAST

AL-SI12CU/B4C COMPOSITES
T.Raviteja1, N.Radhika2, R.Raghu3
1
Mtech Student, Department of Mechanical Engineering, Amrita Vishwa Vidyapeetham, Tamilnadu, India
2
Assistant Professor, Department of Mechanical Engineering, Amrita Vishwa Vidyapeetham, Tamilnadu, India
3
Research Scholar, Department of Mechanical Engineering, Amrita Vishwa Vidyapeetham, Tamilnadu, India

Abstract
The present study was made to understand the fabrication and mechanical properties of Al-Si12Cu/B4C Metal Matrix Composites.
The composites were fabricated by reinforcing B4C particles with varying wt % of 2, 4, 6, 8 and 10, using stir casting process. The
performance of the composites was compared with the alloy to study the improvement in mechanical properties that has been
imparted by the reinforcement particles to the composites. The microstructure was examined on the composite specimens using
optical microscope to confirm the homogeneous dispersion of reinforcement particles in the matrix. Mechanical properties such
as hardness and tensile strength were tested on the composite using Brinell hardness tester and computerized Universal Testing
Machine respectively. The results revealed that the B4C particles were homogeneously distributed in the composite. The hardness
and tensile test results showed that, by increasing wt % of reinforcement particles in the matrix, hardness and tensile strength of
the composites was improved to 6.97 % and 33 % respectively compare to base alloy.

Key Words: Metal Matrix Composite, Stir casting, Microstructure, Mechanical properties, Hardness and Tensile
strength.
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1. INTRODUCTION strength as well as the hardness of the aluminium

composites [5].
Metal Matrix composites (MMCs) are the combination of Hardness of the Aluminium Nitride (AlN) reinforced stir
two or more distinct phases that has improved properties cast aluminium composite is tested and concluded that,
than the monolithic alloy. Aluminium MMCs are greatly overall hardness of the composites increased with increasing
developing in the recent years due to their low cost and light the wt % of AlN particles, as this is due to the hardness of
weight, which replaces the high cost bronze and cast alloys the AlN particles that has been embedded uniformly in the
in several applications [1]. Due to its unique combination of composite [6]. Effect of Alumina (Al2O3) particles on the
properties such as high specific strength, high corrosive tensile strength of the aluminium composite is investigated
resistance, high elastic modulus, good thermal stability, high and interpreted that the Al2O3 particles increases tensile
hardness, high wear resistance, superior strength to weight strength of the composite up to 10% [7].
ratio and light weight, its usage increased drastically in the There are numerous studies found out on mechanical
automobile, aerospace and defense sectors [2]. behaviour of particles reinforced MMCs but very few
Stir casting process is employed to fabricate aluminium studies only have been explored on the mechanical
composites with varying wt% (5, 10, 15, 20, 25, and 30) of properties of B4C particles reinforced MMCs. Thus the
Silicon Carbide (SiC) particles and inferred that uniform present study deals with the fabrication of Al-Si12Cu alloy
dispersion of reinforcement particles is successfully attained reinforced with B4C particles with varying wt % of 2, 4, 6, 8
through this method, and also stated this method as the low and 10, and analyzing its microstructure and mechanical
cost effective method for fabrication of MMCs among behaviour.
various conventional casting techniques [3]. Microstructural
observation is done on the stir cast aluminium composites 2. MATERIAL SELECTION
and interpreted that wettability is important factor in
achieving uniform dispersion of the reinforcement particles The materials chosen for the fabrication of the composite are
in the matrix without agglomeration, which helps in Al-Si12Cu alloy as base matrix and B4C particle as
improvement of mechanical properties of the composites reinforcement. This alloy is chosen because of its
[4]. Selection of type of reinforcement also contributes in applications in pistons, pulleys, sheaves and bearings. The
increasing the mechanical properties such as hardness and B4C particle is selected for reinforcing with the composite
tensile strength of the composites. Soft reinforcements due to its high hardness. The density of the alloy and B 4C
increase the tensile strength and decrease the hardness of the particles are 2.71 g/cm3 and 2.51 g/cm3 respectively. B4C
composite, whereas hard reinforcements increase the tensile particles with size of 33 microns are added as particulate to
the composite for the varying wt % of 2, 4, 6, 8, and 10. The

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chemical composition of Al-Si12Cu aluminium alloy is 3. MICROSTRUCTURE EXAMINATION

shown in Table 1.
The specimens for microstructure examination are machined
Table -1: Chemical composition of Al-Si12Cu aluminium from the cylindrical cast specimens. Initially, the samples
alloy are grinded in bench grinding machine to remove the burs
and polished in belt grinder for the rough surface finish.
Chemical % Then the specimen is polished with emery sheets of grade
composition 1/0 and 2/0. Finally it is polished using disc polisher with
diluted Al2O3 to remove all the scratches on the surface to
Al 83.39
get good surface finish. The polished specimens are etched
Si 10.9
with general aluminium agent prior to examination using
Fe 0.527
Zeiss Axiovert 25 CA Inverted Metallurgical Microscope.
Cu 1.31 The microstructural examination is done for various
Mn 0.113 magnifications on all the composite specimens (2, 4, 6, 8,
Mg 1.05 and 10 wt %) for observing the homogeneous distribution of
Cr 0.0065 the reinforcement particles in the composite.
Ni 2.32
Zn 0.275 4. HARDNESS TEST
Sn 0.0590
Ti 0.340 Macro hardness test is performed on alloy and all the
Pb 0.00 composite with different compositions (2, 4, 6, 8 and 10 wt
Ca 0.065 %) by using the Brinell hardness tester. The specimens are
grinded and polished using emery sheets. The tester is
equipped with hardened steel ball having diameter of 10 mm
2. FABRICATION OF COMPOSITES for producing indentation on the specimen surface. The
specimen is placed on the test platform and the indenter is
Al-Si12Cu/B4C MMCs with varying wt % of 2, 4, 6, 8 and allowed to touch the specimen surface. A minor load of 10
10 are fabricated by using stir cast process. Aluminium kgf is applied on the specimen surface by operating the lever
billets are loaded in the graphite crucible and placed in an to locate the position for producing indentation. Then the
open hearth furnace. Coal is charged around the crucible in major load of 1000 kgf is applied on the located point of the
the furnace which produces heat on burning. This allows the specimen for 30 seconds. Then the load is released and the
aluminium billets to melt. One side of the furnace is specimen is removed from the machine. The hardness is
connected with an electrically operated blower which sucks tested at four different places on the surface of all the
the air from the atmosphere and sends to the furnace for the composites specimens and the diameter of the indentation is
continuous generation of heat. Once attaining the molten measured by microscopic screw gauge. The Brinell
metal condition of the alloy, the preheated B4C particles are Hardness Number (BHN) is calculated and the average
added to the molten metal and the stirring action is done value is taken as the hardness value of the specimen.
simultaneously for 5 min to achieve the homogeneous
distribution of the reinforcement particles in the composite.
5. TENSILE TEST
Then the molten metal is poured at 800 ºC into the
cylindrical sand moulds having dimensions of diameter 25 The specimens (Figure 2) are machined as per ASTM (E8-
mm and length 150 mm. After pouring the molten metal into 04) standard from the composites specimens. The machined
the moulds, it kept for some time to solidify. After specimens are fixed in between the jaws of the computerized
solidification, composite specimens are withdrawn from the Universal Testing Machine (UTM). Input data of the
mould. The same procedure is followed for all composites specimens is fed into the UTM software. The load is applied
with varying wt %. The schematic illustration of the gradually on the two ends of the specimen by pulling. The
fabrication process is shown in Figure 1. specimen gets broken after the formation of neck. Then the
specimen is removed from the machine. The test results are
obtained through the software in the graphical form. The
specimen before and after tensile test is shown in Figure 3
(a) and (b).

Fig -1: Schematic illustration of fabrication process Fig -2: Specimen prepared for tensile test

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IJRET: International Journal of Research in Engineering and Technology eISSN: 2319-1163 | pISSN: 2321-7308

Fig -3: Specimen (a) before test and (b) after test

6. RESULTS & DISCUSSIONS

The microstructure evaluation and the mechanical properties
of the composites are detailed in the further sections.
Fig -4: Microstructure of the Al-Si12Cu/B4C composites (a)
2 wt % (b) 4 wt % and (c) 10 wt %
6.1 Microstructure evaluation
6.2 Mechanical properties
The microstructure is evaluated on the Al-Si12Cu/ B4C (2,
4, 10 wt %) composites and shown in Figure 4(a), (b) and The mechanical properties such as hardness and tensile
(c). The homogeneous distribution of the reinforcement strength of the Al-Si12Cu/B4C composites is discussed
particles in the composite is observed due to the greater briefly in the following sections
wettability of the B4C particles with the aluminium alloy.
This greater wettability of B4C with the aluminium alloy 6.2.1 Hardness of the composites
might be due to the formation of liquid B 2O3 layer on the
B4C particles. This liquid layer forms above certain The hardness results of the Al-Si12Cu alloy and Al-Si12Cu/
temperature on the surface of B4C and the wettability gets B4C (2, 4, 6, 8 and 10 wt %) composites are shown in Chart
increased as there is a liquid–liquid reaction, whereas the 1. Hardness value is increased by increasing the wt % of
same pattern is resulted [8]. From the microstructure (Figure B4C reinforcement particles in the composites. By adding
4 (c)), it is observed that white area is aluminium matrix and the reinforcement particles to the composites, surface area of
remaining dark grey area are the B4C reinforcement the reinforcement gets increased and grain sizes of the
particles. The better interfacial bonding between the matrix matrix get decreased. The presence of such hard
and reinforcement particles is observed because of less reinforcement particles on the surface resists the plastic
porosity, whereas same behaviour is observed [9]. deformation of the material. The strength of the grain
boundaries increases to maximum level and dislocation of
atoms are decreased by increasing the wt % of
reinforcement, which gives strength to the matrix and
thereby hardness of the composite gets increased. The same
phenomenon is observed [10]. The 10 wt % of B4C
reinforced composite yields better hardness than
unreinforced alloy by 6.97 %.

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IJRET: International Journal of Research in Engineering and Technology eISSN: 2319-1163 | pISSN: 2321-7308

wt % of reinforcement and after that level of increasing in

tensile strength gets reduced due to the clustering of
reinforcement particles. The results obtained from this study
can be used effectively for development of the structural and
automotive components that requires better mechanical
properties.

REFERENCES
[1]. U.B. Gopala Krishna, K.V. Sreenivas Rao and B.
Vasudeva, “Effect of boron carbide reinforcement on
aluminum matrix composites”, International Journal Of
Metallurgical & Materials Science And Engineering, Vol. 3,
Chart -1: Hardness of Al-Si12Cu alloy and Al-Si12Cu/B4C No. 1, pp 41-48, 2013.
composites [2]. S.Rama Rao and G. Padmanaban, “Fabrication and
mechanical properties of aluminium boron carbide
6.2.2 Tensile strength of the composites composites”, International Journal of Materials and
The tensile strength of the Al-Si12Cu alloy and Al-Si12Cu/ Biomaterials Applications, Vol. 2, No. 3, pp.15-18, 2012.
B4C composites is shown in Chart 2. From Chart 2, it is [3]. Manoj Singla, D. Deepak Dwivedi, Lakhvir Singh and
observed that ultimate tensile strength is increased by Vikas Chawla, “Development of aluminium based silicon
increasing the percentage of B4C particles in the composite. carbide particulate metal matrix composite”, Journal of
This is due to the better interfacial bonding between the Minerals & Materials Characterization & Engineering, Vol
matrix and the reinforcement which transfers and distributes 8, No 6, pp. 455-467, 2009.
the load from the matrix to the reinforcement. Therefore the [4]. Ankush Sachdeva, Ram Narayan and R.D. Gupta,
reinforcement particle tends to bear the entire load that has “Evaluation & comparison of mechanical properties of
been acted upon the matrix. The tensile strength is observed aluminium alloy 5052 reinforced with silicon carbide,
to get increased drastically up to 8 wt % of reinforcement graphite and fly ash hybrid metal matrix composites”,
and after that amount of increase in tensile strength gets International Journal of Engineering Science and
reduced as this might due to the of formation of clustering in Technology, Vol. 5, No.10 pp.1780-1787, 2013.
a matrix, same pattern is resulted [11]. The tensile strength [5]. S. Rajanna, Evaluation of mechanical response of
of 10 wt % of B4C particles reinforced composite shows an graphite reinforced metal matrix composite, Journal of
increase of 33 % more than the Al-Si12Cu alloy. Harmonized Research, Vol. 1, No. 1, pp. 39-44, 2013.
[6]. M. N. Wahab, A. R. Daud and M. J. Ghazali,
“Preparation and characterization of stir cast-aluminum
nitride reinforced aluminum metal matrix composites”,
International Journal of Mechanical and Materials
Engineering, Vol. 4, No. 2, 115-117, 2009.
[7]. Muhammad Hayat Jokhio, Muhammad Ibrahim
Panhwar and Mukhtiar Ali Unar, Manufacturing of
aluminum composite material using stir casting process,
Mehran University Research Journal of Engineering &
Technology, Vol. 30, No. 1, pp.53-64, 2011.
[8]. P.K. Jayashree, M.C. Gowri Shankar, Achutha Kini,
S.S. Sharma and Raviraj Shetty, Review on effect of silicon
carbide (SiC) on stir cast aluminium metal matrix
composites International Journal of Current Engineering and
Chart -2: Tensile strength of Al-Si12Cu alloy and Technology, Vol. 3, No. 3, pp. 1061-1071, 2013.
Al-Si12Cu/B4C composites [9]. K.M. Shorowordi, T. Laoui, A.S.M.A. Haseeb, J.P.
Celis and L. Froyen, “Microstructure and interface
7. CONCLUSION characteristics of B4C, SiC and Al2O3 reinforced Al matrix
composites: a comparative study” Journal of Materials
Al-Si12Cu/B4C metal matrix composites with varying wt % Processing Technology, Vol. 142, pp. 738–743, 2003
of 2, 4, 6, 8 and 10 are successfully fabricated using stir [10]. K. Kalaiselvan, N. Murugan and Siva Parameswaran,
casting process. The homogeneous distribution of the
“Production and characterization of AA6061–B4C stir cast
reinforcement particles in the composite is attained due to
the greater wettability of the B4C particles with the composite”, Materials and Design, Vol. 32, 4004–4009,
aluminium alloy. By increasing the wt % of B4C particles in 2011.
the aluminium matrix, hardness of the composites gets [11]. M.C. Gowri Shankar, P.K. Jayashree, Raviraj Shetty,
increased than the alloy due to the resistance offered by the Achutha Kinia and S.S. Sharma “Individual and combined
reinforcement particles to the plastic deformation. The effect of reinforcements on stir cast aluminium metal matrix
tensile strength of the composites increases greatly up to 8 composites-a review”, International Journal of Current

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IJRET: International Journal of Research in Engineering and Technology eISSN: 2319-1163 | pISSN: 2321-7308

Engineering and Technology, Vol. 3, No. 3, pp.922-934,

2013.

BIOGRAPHIES

T.Raviteja completed his

Bachelor’s degree in Mechanical
Engineering and currently pursuing
M.Tech in Mechanical Engineering
at Amrita Vishwa Vidyapeetham.

Dr.N.Radhika completed her

Bachelor’s degree and Master’s
degree in Mechanical Engineering.
She completed her Ph.D on
Materials Science and currently
working at Amrita Vishwa
Vidyapeetham.

R.Raghu completed his Bachelor’s

degree in Mechanical Engineering
and currently working as Junior
Research Fellow at Amrita Vishwa
Vidyapeetham.

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