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This document provides information on 10 different pharmaceutical preparations including emulsions, mucilages, liniments, gels, magmas, and lotions. It describes the procedures and formulas for each preparation. The cod liver emulsion is made using cod liver oil, acacia, and water. The acacia mucilage is made by dissolving acacia and benzoic acid in water. The efficascient oil liniment contains camphor, menthol, eucalyptus oil, methyl salicylate, and turpentine oil dissolved in mineral oil.

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Gabreille Rullamas Chavez
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1K views4 pages

For Practicalssss

This document provides information on 10 different pharmaceutical preparations including emulsions, mucilages, liniments, gels, magmas, and lotions. It describes the procedures and formulas for each preparation. The cod liver emulsion is made using cod liver oil, acacia, and water. The acacia mucilage is made by dissolving acacia and benzoic acid in water. The efficascient oil liniment contains camphor, menthol, eucalyptus oil, methyl salicylate, and turpentine oil dissolved in mineral oil.

Uploaded by

Gabreille Rullamas Chavez
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as DOCX, PDF, TXT or read online on Scribd
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EXPERIMENT 8- DISPERSE SYSTEMS (EMULSIONS)

1. COD LIVER EMULSION (ENGLISH METHOD/ WET GUM METHOD/ 4:2:1 METHOD*)
 PROCEDURE
 Triturate gum with water in a mortar to form a mucilage.
 Oil is added slowly in portions and then the mixture is triturated
 After adding the oil, thoroughly mix for several minutes to form the primary emulsion
 Once the primary emulsions have been formed, the remaining quantity of water is added to make the final
emulsion
 FORMULA
 Cod liver oil 60 ml
 Acacia 15 g
 Purified water q.s

To make 120 ml

2. TURPENTINE OIL EMULSION (CONTINENTAL METHOD/ DRY GUM METHOD/ 4:2:1 METHOD)
 PROCEDURE
 The gum is triturated with the oil in a dry mortar until thoroughly mixed.
 Two parts of water are added all at once and the mixture is triturated rapidly until the primary emulsion is
creamy white and produces a crackling sound to the movement of the pestle
 FORMULA
 Turpentine oil 60 ml
 Acacia 15 g
 Purified water q.s

To make 120 ml

3. METHYL SALICYLATE EMULSION (FORBES BOTTLE METHOD/ 2:2:1 METHOD)


 PROCEDURE
 Oil or water is first shaken thoroughly and vigorously with the computed amount of gum
 once this emulsified completely, the second liquid (either oil or water) is then added all at once
 the bottle is shaken vigorously to form the primary emulsion
 more of water is added in small portions with constant agitation after each addition to produce the final
volume
 FORMULA
 Methyl Salicylate 60 ml
 Acacia 15 g
 Purified water q.s

To make 120 ml
EXPERIMENT 9- MUCILAGE

4. ACACIA MUCILAGE
 PROCEDURE
 Dissolve the benzoic acid in 400 ml ( ) of purified water with the aid of heat
 Add the solution to 350 g ( ) of acacia in a mortar, triturating until the acacia is dissolved
 Add sufficient quantity of purified water to make 1000 ml ( ) strain if necessary
 FORMULA
 Acacia in small fragments 350 g
 Benzoic acid 2g
 Purified water q.s

To make 1000ml

5. TRAGACANTH MUCILAGE
 PROCEDURE
 Mix 75 ml ( ) of purified water with the glycerin in a tared vessel, heat to boiling
 Discontinue application of heat
 Add the tragacanth and the benzoic acid acid and macerate during 24 hours, stirring occasionally
 Add sufficient quantity of purified water to make the mucilage weigh 100 g ( )
 Stir actively until of uniform consistency and strain through muslin
 FORMULA
 Tragacanth 6g
 Benzoic acid 0.2 g
 Glycerin 18 g
 Purified water q.s

To make 100 g

EXPERIMENT 10- LINIMENTS

6. EFFICASCENT OIL LINIMENT


 PROCEDURE
 Place 20 ml of mineral oil in a flask
 Add camphor and stopper
 Heat gently over a steam bath until camphor dissolves
 Remove from heat and then add menthol. Agitate until dissolved
 Add methyl salicylate, eucalyptol oil, and add turpentine oil and mix
 Add q.s mineral oil to make 100 ml
 Add a drop of colorant if desired.
 FORMULA
 Camphor 7.5 g
 Menthol 6.5 g
 Eucalyptus oil 2 ml
 Methyl salicylate 14 ml
 Turpentine oil 5 ml
 Colorant 1 drop
 Mineral oil q.s

To make 100 ml

EXPERIMENT 11- COLLOIDAL DISPERSIONS (GELS AND MAGMAS)

7. ALUMINUM HYDOXUDE GEL, USP


 PROCEDURE
 Dissolve the sodium carbonate in 4000 ml of hot water and filter
 Dissolve ammonium alum in 2000 ml of hot water and filter into the carbonate solution with constant
stirring
 Then add 4000 ml of hot water and remove all gas
 Dilute to 80000 ml of cold water
 Collect and wash the ppt and suspend it in 2000 ml of purified water flavored with 0.01% peppermint and
preserve with 0.1% of sodium benzoate.
 Homogenize the resulting gel
 FORMULA
 Ammonium alum 800 g
 Sodium carbonate 1000 g
 Purified water q.s

To make 2000 ml

8. BENTONITE MAGMA, USP


 PROCEDURE
 To 800 ml of heated purified water, sprinkle upon it the bentonite, in portions allowing each portion to
become thoroughly wetted without stirring
 Allow to stand with occasionally stirring for 24 hours
 Stir until a uniform magma is obtained.
 Add sufficient quantity of purified water to make 1000 ml and mix
 FORMULA
 Bentonite 50 g
 Purified water q.s

To make 1000 ml
EXPERIMENT 12- LOTIONS

9. CALAMINE LOTION
 PROCEDURE
 Dilute the bentonite magma with an equal volume of calcium hydroxide soln
 Mix the powders intimately with the glycerin and about 100 ml of the diluted magma, triturating until a
smooth, uniform paste is formed
 Gradually incorporate the remainder of the diluted magma
 Finally add enough calcium hydroxide solution to make 1000 ml and shake well
 FORMULA
 Calamine 80 g
 Zinc oxide 80 g
 Glycerin 2o ml
 Bentonite magma 250 ml
 Calcium hydroxide solution q.s

To make 1000 ml

10. PHENOLATED CALAMINE LOTION


 PROCEDURE
 Mix the ingredients thoroughly
 FORMULA
 Liquefied Phenol 10 ml
 Calamine lotion 990 ml

To make 1000 ml

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