Thermal Isolation of Encapsulated MEMS Resonators: Journal of Microelectromechanical Systems March 2008
Thermal Isolation of Encapsulated MEMS Resonators: Journal of Microelectromechanical Systems March 2008
Thermal Isolation of Encapsulated MEMS Resonators: Journal of Microelectromechanical Systems March 2008
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N OMENCLATURE
I. I NTRODUCTION
k Thermal conductivity, W m−1 K−1 .
Surface emissivity, 0 ≤ ε ≤ 1.
ε
σ
ρ
Stefan–Boltzmann constant,5.67×10−8W m−2 K−4.
Density, kg m−3 .
T HE CMOS-compatible microelectromechanical-system
(MEMS) resonators are becoming an interesting and vi-
able technology [1]–[7] as a replacement for quartz crystals
cp Specific heat capacity at constant pressure, [8]–[13] for timing- and frequency-reference applications. Cur-
J kg−1 K−1 . rently, oven-controlled quartz resonators are used to generate
high-precision frequency references suitable for high-end in-
Manuscript received February 21, 2007; revised June 10, 2007. This work
dustry and military standards [10]–[13]. In this method, the
was supported in part by DARPA HERMIT under Grant ONRN66001-03- resonator is held at a fixed temperature to compensate for the
1-8942, in part by the Robert Bosch Corporation, Palo Alto Research and temperature dependence of the resonator frequency. The extent
Technology Center, in part by a CIS Seed Grant, in part by The National
Nanofabrication Users Network facilities funded by the National Science
to which the resonator is heated depends on the difference
Foundation under Award ECS-9731294, and in part by The National Science between the set point and the ambient temperature. For an
Foundation Instrumentation for Materials Research Program under Grant DMR ovenized resonator that is required to operate within a tem-
9504099. Subject Editor D. DeVoe.
C. M. Jha, M. A. Hopcroft, S. A. Chandorkar, J. C. Salvia, M. Agarwal, perature range of −40 ◦ C to 85 ◦ C, the heating has to cover
R. Melamud, B. Kim, and T. W. Kenny are with the Department of Mechanical a range of 125 ◦ C. Due to the large volume of a conventional
and Electrical Engineering, Stanford University, Stanford, CA 94305 USA quartz-crystal oscillators, which can be up to 1000 mm3 [14],
(e-mail: [email protected]).
R. N. Candler was with Stanford University, Stanford, CA 94305 USA. He is the power consumption for heating can be as much as 10 W
now with the Robert Bosch Corporation Research and Technology Center, Palo with a warm-up time of approximately 30 min [13]–[15].
Alto, CA 94304 USA. MEMS technology offers miniaturization to submillime-
Color versions of one or more of the figures in this paper are available online
at http://ieeexplore.ieee.org. ter scales, which can provide substantial power reduction
Digital Object Identifier 10.1109/JMEMS.2007.904332 [1], [16]–[18].
l
Rth = . (1)
kAc
Fig. 3. Thermal equivalent circuit. Package is assumed to be at ambient Fig. 4. Thermal equivalent circuit when there is radiative heat loss from the
temperature. Unit of thermal resistances shown above is in Kelvin per watt. bottom of the chip Rradbot in the absence of the adhesive. Unit of thermal
resistances shown above is in Kelvin per watt.
Radiative and convective thermal loss can be found by
1 is shown in Fig. 4, and the total effective thermal isolation is
Rrad =
hrad As estimated to be approximately 3000 K/W—an improvement by
1 a factor of five.
Rconv = (3) This method of improving thermal resistance is effective but
hconv As
not robust and may lead to packaging problems. Furthermore,
where hrad = εσ(Ts + Tsurr )(Ts2 + Tsurr 2
) is the linearized since the heat transfer from the heater to the resonator takes
radiation-heat-transfer coefficient [22]. Ts is the surface tem- place in the device layer, the device layer gets heated which
perature, and Tsurr is the surrounding temperature. The hconv is leads to unwanted heating up of the entire chip because of
the convective-heat-transfer coefficient. Fig. 3 shows the equiv- the lack of thermal isolation between the device layer and
alent thermal-resistance circuit, where P is the input power. the substrate. The thermal mass of a typical resonator chip is
Approximate values for the material constants are taken from approximately 1200 times larger than that of a single DETF,
the literature [24]–[27]. and hence, heating of the entire chip leads to longer thermal
In this design configuration of the MEMS chip, the ther- time constant and more heat loss resulting in increased input
mal resistance calculated for the device layer and the chip power.
(∼20 K/W) is very small as compared to that of wire bond and
adhesive. It is therefore assumed that the entire chip, including
the resonator, is approximately at a constant temperature. It is B. Heating Resonator Alone With Local Thermal Isolation
also assumed that the package acts as a heat sink, and hence, its
Therefore, it is desired to have an alternative technique to
temperature is the same as the ambient temperature. The total
increase the heating efficiency by heating only the resonator
effective thermal isolation Reff is estimated to be approximately
and simultaneously providing large thermal isolation between
600 K/W.
the resonator and its immediate vicinity in the device layer. This
The power required to achieve a ∆T rise in temperature of
calls for a local heat delivery and thermal-isolation mechanism.
the resonator can be found by
This can be achieved by designing a resonator coupled with
V2 ∆T an in-built heater and restricting the heat loss to the ends of the
P = = . (4) heaters. The in-built heater, in this configuration, serves the dual
Re Reff
purpose of heating, as well as thermally isolating, the DETF.
To obtain ∆T of 125 ◦ C, the input power is approximately To design a resonator for good thermal isolation, it is nec-
200 mW. The thermal time constant can be estimated by (5) essary to study various heat-loss mechanisms in the structure.
and is approximately 500 ms. The resonator is encapsulated, and the atmosphere inside the
encapsulation consists mainly of hydrogen gas at a low pressure
τ = Reff Cth . (5) of approximately 1 Pa [19]. The three modes of heat transfer
considered here are as follows:
One method to improve thermal isolation is to release the chip
from the package by removing the adhesive and keep it floating 1) convection due to hydrogen molecules in the cavity;
in air, thus reducing the heat loss from substrate to the package. 2) radiation from the resonator;
The chip, in this case, is supported from the top by six wire 3) conduction through the silicon beams of the in-built
bonds. The equivalent thermal circuit for the released device heater.
178 JOURNAL OF MICROELECTROMECHANICAL SYSTEMS, VOL. 17, NO. 1, FEBRUARY 2008
Fig. 5. Temperature profile along the length of a current-carrying resistive heater having thermal resistance of Rth and electrical resistance of Re and its
equivalent lumped model.
Fig. 6. Resonator design with local thermal isolation. The heater is in-built to the DETF, such that, the resonant structure is attached at the center of the heater.
The entire structure is released except at the four anchors.
Convection due to hydrogen molecules can be analyzed by simplification, it is also assumed that the heat loss due to
using microscopic-particle-based kinetic theory of heat diffu- radiation is relatively small and can be neglected.
sion [28]. Thermal conductivity of molecular-energy carriers It is, therefore, the conductive heat transfer through the sili-
can be evaluated as con beams which is the dominant heat-loss mechanism in this
encapsulated MEMS resonator. If a current-carrying resistive
1 heater of constant cross section is analyzed, the temperature
CνΛ
kh = (6)
3 profile along the length of the heater, in the absence of con-
vection and radiation heat loss, is given by (7) [22], [23] and
where C = (3/2)kB nM , and ν = 8kB T /πm. shown in Fig. 5
It is assumed that the mean free path Λ is equal to the
2
gap width of the cavity (1.5 µm) because of low pressure. ql 4x2
The thermal conductivity due to the hydrogen molecules kh is Tx = 1− 2 + Ts (7)
8k l
estimated to be around 1 × 10−6 W/m/K at room temperature,
resulting in an effective thermal resistance of the order of where x varies from −l/2 to +l/2, and Ts is the end surface
1 × 107 K/W and, hence, can be assumed that the heat loss temperature of the heater (Fig. 5).
due to molecular conduction is negligible as compared to other The maximum temperature occurs at the center of the heater
modes. (at x = 0) and is given by
The thermal resistance due to radiation for a DETF structure, 2
assumed to be at a maximum heating temperature of 425 K, ql
Tc = + Ts . (8)
is estimated to be approximately 1 × 106 K/W. Hence, for 8k
JHA et al.: THERMAL ISOLATION OF ENCAPSULATED MEMS RESONATORS 179
Fig. 8. Equivalent thermal circuit schematic for the resonator with in-built
heater.
Fig. 10. (a) Optical image of the top view of the fabricated device before the deposition of the encapsulation layer. (b) SEM cross section of a resonator beam
after the deposition of the encapsulation layer.
Fig. 11. Isometric view of device layer schematic showing the DETF with Fig. 12. Schematic of the test setup for frequency measurement.
the in-built heater. A stimulus signal is applied to the input electrode. Heating
voltages V1 and V2 are controlled using a feedback control loop to maintain a
constant bias for the resonator. A finite-element simulation was done to examine the tem-
perature distribution along the length of the in-built heater
as opposed to the entire silicon die described in Section II-A. and the DETF, as shown in Fig. 9. From the simulation, a
This means that there will be rapid heating and cooling of the power consumption of approximately 12 mW was required
resonator over and above the slower thermal response of the for a temperature increase of 125 ◦ C. The time constant and
chip. A 1-D equivalent thermal-circuit model of the in-built heating power consumption of the three designs are compared
heater is shown in Fig. 8. As with temperature, the thermal in Table I. Clearly, the in-built heater can be very effective, both
time constant of the resonator cannot be calculated precisely in terms of reducing power consumption and dynamic thermal
by a simple lumped-element model because of the complex response.
temperature profile through the device, but we can make an
estimate using the effective resistance of the heaters and the
total thermal capacitance of the heaters and the resonator, as III. F ABRICATION
shown in
One of the biggest advantages of this technique is with
respect to fabrication. A CMOS compatible “epi-seal” encap-
τ = Reff (Cresonator + Cheaters ) (11)
sulation process [19], [20] is used to fabricate this device. The
τchip ≈ Reff _ext Cchip . (12) structure of the fabricated device is shown in Fig. 1(a). The
device layer is insulated from the encapsulation layer by a
For the thermally isolated DETF, τ is estimated to be ap- thin sacrificial oxide, and openings for electrical contacts are
proximately 15 ms. The actual dynamic behavior of the device made through the encapsulation layer over the anchors. Since
is characterized by multiple time constants from the nonheated the in-built heaters are in the device layer with the resonator,
resistor, the silicon die, and the resonator. Finite-element sim- no changes to the fabrication process are required to create
ulations indicate that the temperature change of the resonator the thermally isolated DETF. This process ensures a vacuum
itself may be up to 50% slower than the heaters. inside the encapsulation with a pressure of < 1 Pa. Long term
JHA et al.: THERMAL ISOLATION OF ENCAPSULATED MEMS RESONATORS 181
Fig. 13. Variation of resonator frequency due to joule heating of the in-built heater. The decrease in frequency (right y-axis) corresponds to a temperature rise
(left y-axis) with increasing input power. Experimental results are compared with theoretical estimates. The analytical expression (10) estimates the temperature
at the center of the in-built heater, while the FEM results are for the temperature at the center of the resonator.
Fig. 15. Drop test resulted in a temporary change in frequency at the time of drop.
It is also necessary to check the influence of the in-built heating pulse of 4.5 V was used, and the voltage was maintained
heater suspension on the mechanical quality factor (Q) of the at 0.5 V during the cooling period in order to observe the change
resonator. Since the heater suspension is on both sides of the in voltage during cooling.
DETF, there is a linear temperature gradient across the length The measured time constants of several resonators varied
of the resonator beam. This gradient in temperature affects the between 7 and 10 ms. A typical measurement is shown in
Q. It has been shown [32] that the Q for a resonator with a Fig. 14. We expect the measurement to understate the time
linear temperature gradient and average temperature TA will be constant, because the measurement indicates the average tem-
slightly higher than the Q of a resonator with no temperature perature of the heater, not the temperature of the resonator itself.
gradient and uniform temperature TA . However, the tempera- It is to be noted that the thermal capacitance of the DETF is
ture gradient has a minimal effect on the frequency–temperature approximately equal to that of an in-built heater, and so, there is
calibration of the resonator. potential in reducing the thermal time constant in future designs
by reducing the thermal mass of the resonator itself.
A. Power Consumption
C. Impact Resistance of Mechanical Suspension
The DETF was heated using the in-built heater, and its
frequency was measured as a function of input power. As shown The thermal resistance of the resistive heater directly depends
in Fig. 13, the frequency decreases with the increase in input on the length of the beam and is inversely proportional to its
power as the temperature rises. The temperature rise was evalu- cross-sectional area. Design of a large thermal resistance is
ated using the calibration data of frequency versus oven temper- limited by the reduction of mechanical stiffness of the structure.
ature. It has been observed that there is a rise in temperature of However, miniaturization allows a stiffer design of the heater
approximately 125 ◦ C with total power consumption of around having relatively higher thermal resistance. To investigate the
12 mW. The experimental output is observed to be slightly stiffness of the thermally isolated DETF structure, a drop test
nonlinear as compared to the simulation results. This can be was carried out. The chip was soldered to an oscillator circuit
attributed to the fact that the material properties, including ther- board, which was rigidly bolted to a heating chuck (Fig. 15)
mal conductivity and electrical resistivity of silicon, vary with maintained at a constant temperature of 70 ◦ C. The chuck was
temperature but were considered constant for the calculation. dropped from a height of 1.0 cm onto a rigid platform, and the
response of the resonator frequency was measured, as shown in
Fig. 15. At the time of impact, the oscillator frequency changed
B. Thermal Time Constant
by approximately −45 000 ppm. The resonator immediately
The thermal time constant of the micro-ovenized resonator returned to normal operation. The change in frequency before
is an important parameter for temperature control. The thermal and after the impact is within the noise of the frequency fluc-
response was evaluated using a transient electrical-resistance tuation of the uncompensated resonator due to small variation
measurement. A voltage pulse was applied to the heater, which in the chuck temperature, as shown in Fig. 15. Furthermore,
caused its resistance to increase as it heated up. After the the resonators survived the 5000-rpm rotation (up to ∼1400 g
pulse ended, the heater resistance decreased as it cooled. A of acceleration) during the photoresist spin-coating steps of the
wheatstone bridge was used to measure the change in heater fabrication process. The spin duration was approximately 1 min
resistance during this cycle (Fig. 14). For the measurement, a and was repeated six to eight times during the fabrication.
JHA et al.: THERMAL ISOLATION OF ENCAPSULATED MEMS RESONATORS 183
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pensated crystal oscillator,” in Proc. 43rd Annu. Freq. Control Symp., mechanical engineering from the Birla Institute of
1989, pp. 8–15. Technology, Mesra, India, in 1996 and the M.S.
[10] J. R. Vig, “Temperature stable crystal oscillator,” IEEE Trans. Ultrason., degree in mechanical engineering from Stanford
Ferroelectr., Freq. Control, vol. 42, no. 4, pp. 797–799, Jul. 1995. University, Stanford, CA, in 2006. He is currently
[11] A. Ballato and J. R. Vig, “Static and dynamic frequency-temperature working toward the Ph.D. degree in the Department
behavior of singly and doubly rotated, oven-controlled quartz resonators,” of Mechanical Engineering and the Department of
in Proc. 32nd FCS, 1978, pp. 180–188. AD-A955 718. Electrical Engineering, Stanford University.
[12] I. Balaz and M. Minarik, “Towards an OCXO with infrared heater,” in From 1996 to 1997, he was with LML Ltd.,
Proc. IEEE Int. FCS, 1996, pp. 674–680. India, as an Engineer. From 1997 to 2004, he was
[13] M. Vaish, “A high precision quartz oscillator with performance compa- with Bhabha Atomic Research Centre as a Scientific
rable to rubidium oscillators in many respects,” in Proc. IEEE Int. FCS, Officer, working on design and development of mechanical systems for harsh
1996, pp. 752–760. environments. His current research is focused on the design and optimization
[14] Vectron International, C4550 OCXO. [Online]. Available: http://www. of micro-oven-based MEMS resonators for low power and high-temperature
vectron.com stability.
[15] M. E. Frerking, Crystal Oscillator Design and Temperature Compensa- Mr. Jha is a Student Member of the American Society of Mechanical
tion. New York: Van Nostrand, 1978. Engineers (ASME).
184 JOURNAL OF MICROELECTROMECHANICAL SYSTEMS, VOL. 17, NO. 1, FEBRUARY 2008
Matthew A. Hopcroft received the B.Sc. degree in Rob N. Candler (S’98–M’00) received the B.S.
computer engineering from the George Washington degree in electrical engineering from Auburn
University, Washington, D.C., in 1998, the M.Phil. University, Auburn, AL, in 2000 and the M.S.
degree from Cambridge University, Cambridge, and Ph.D. degrees in electrical engineering from
England, in 2002, and the Ph.D. degree in mechan- Stanford University, as a National Defense Science
ical engineering from Stanford University, Stanford, and Engineering Graduate Fellow, in 2002 and 2006,
CA, in 2007. respectively.
He is currently a Research Specialist with the He was a Consulting Assistant Professor with the
Berkeley Micromechanical Analysis and Design Department of Electrical Engineering and the De-
Group and the Berkeley Sensor and Actuator Cen- partment of Mechanical Engineering, Stanford Uni-
ter, University of California, Berkeley. His research versity. He is currently a Senior Research Engineer
interests include MEMS material property measurements, microscale and with Bosch Research and Technology Center, Palo Alto, CA, working on
portable power systems, and micromechanical resonators. MEMS-based sensors for automotive and commercial markets. He also directs
Bosch’s involvement in the DARPA Science and Technology Fundamentals
program. His research interests include RF MEMS, wafer-scale sensor pack-
aging, and sensor reliability.
Saurabh A. Chandorkar received the B.Tech. Renata Melamud received the B.S. degree in me-
degree in mechanical engineering from the Indian chanical engineering from Carnegie Mellon Univer-
Institute of Technology, Mumbai, India, in 2003 sity, Pittsburgh, PA, in 2003 and the M.S. degree
and the M.S. degree in mechanical engineering in mechanical engineering from Stanford University,
from Stanford University, Stanford, CA, in 2005. Stanford, CA, in 2006. She is currently working
He is currently working toward the Ph.D. degree at toward the Ph.D. degree in the Department of Me-
Stanford University. chanical Engineering and the Department of Elec-
His current research interests include the study trical Engineering, Stanford University, wherein she
of energy loss mechanisms, namely, thermoelastic is supported by the Gabilan Stanford Graduate Fel-
dissipation, Akhieser effect loss and clamping loss, lowship for her research on passive compensation
and micromechanical resonators. techniques to reduce the temperature dependence of
frequency in silicon resonators.