Scribd
Upload
345 views1 page

A TitrationChart

This document provides a titration chart for analyzing mud samples. It lists various chemical tests that can be performed on mud filtrate and mud samples, including tests for pH, total hardness, calcium, magnesium, chloride, and excess lime or gypsum. For each test, it indicates the sample needed, indicator used, titrant, and color change point to determine the test result and related calculations. The goal is to analyze mud properties through titration and calculate relevant values like hardness, calcium, magnesium and excess lime/gypsum levels.

Uploaded by

Christian Ivan Acosta Zavala
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
345 views1 page

A TitrationChart

This document provides a titration chart for analyzing mud samples. It lists various chemical tests that can be performed on mud filtrate and mud samples, including tests for pH, total hardness, calcium, magnesium, chloride, and excess lime or gypsum. For each test, it indicates the sample needed, indicator used, titrant, and color change point to determine the test result and related calculations. The goal is to analyze mud properties through titration and calculate relevant values like hardness, calcium, magnesium and excess lime/gypsum levels.

Uploaded by

Christian Ivan Acosta Zavala
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
You are on page 1/ 1

BASIC MUD SCHOOL TITRATION CHART

TEST AMOUNT OF SAMPLE INDICATOR TITRATE WITH COLOR CHANGE MULTIPLIER


NEEDED
1 ml FILTRATE Phenolphthalein 0.02 N H2SO4 (N50) Pink to Clear (pH 8.3) ml of 0.02 N H2SO4
Pf {2 - 3 drops} OR color of original filtrate
Sulfuric Acid
(Take the Red out)
1 ml FILTRATE Methyl Orange Brom Cresol Green 0.02 N H2SO4 (N50) Green/Blue to Orange/Yellow ml of 0.02 N H2SO4
Mf {4 - 6 drops} (pH 4.3)
Sulfuric Acid (Take the Green out)
1 ml MUD + Phenolphthalein 0.02 N H2SO4 (N50) Pink to Original mud color ml of 0.02 N H2SO4
Pm 5 - 10 ml of Distilled water {3 - 4 drops} or (pH 8.3) or
0.1 N H2SO4 (N10) ml of 0.1 N H2SO4 x (5)
Sulfuric Acid
1 ml MUD + Versenate hardness Buffer solution Versenate Hardness ml of Versenate Hardness Titrating
5 - 10 ml of Distilled water {20 drops} Titrating Solution Take The Redness Out Solution x (400) = mg/l
Vm Versenate hardness indicator (20 EPM) (“C”) x (400) = mg/l Ca2+, Mg2+
solution – {4 - 6 drops}
(1 ml = 400 mg/l Ca2+) Total Hardness Of The Mud
Use same 1 ml sample from ml of 0.0282 AgNO3 x (1000) = Mg/l Cl-
Cl- which the Pf was determined
Potassium Chromate
{4 - 6 drops}
0.0282 N AgNO3
or
Yellow to First permanent Red
or OR
0.282 N AgNO3 ml of 0.282 AgNO3 x (10,000) = Mg/l Cl-
Reddish color
Silver Nitrate

Total 1 ml FILTRATE Versenate hardness Buffer solution Versenate Hardness Wine Red to Blue/Gray ml of Versenate Hardness Titrating Solution
{20 drops} Titrating Solution or gray/green
Hardness (“A”) x (400) = mg/l Ca2+, Mg2+
(Ca
2+ 2+
and Mg ) Versenate hardness indicator EDTA (20 EPM) (Take the Redness out)
solution – {4 - 6 drops} Total Hardness Of The Filtrate
2+
(1 ml = 400 mg/l Ca )

8-N NaOH – { 20 drops,}


Ca2+ 1 ml FILTRATE
Distilled water – {20 ml}
Versenate Hardness
Titrating Solution
Wine Red to Blue ml of Versenate Hardness Titrating Solution
(Take the Redness out) (“B”) x (400) = mg/l Ca2+ Soluble Calcium
CALCON or CALVER ll.-
(20 EPM)
{1-porcelain/brass spoonful}
2+
(1 ml = 400 mg/l Ca )

(Mg2+) mg/l = (“A”-“B”) x (243) PPB Excess Lime: Unweighted Muds = (Pm – Pr) ÷ 4 PPB Excess Gyp = (“C” – “A”) ÷ 2
Weighted Muds = 0.26 [ Pm – (Pf x Fw)]

You might also like