Cryogenic Air Separation

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The document discusses the process and equipment used in an on-site cryogenic air separation plant to produce high purity oxygen gas.

The plant uses cryogenic separation techniques to fractionate air into its components in liquid form. Part of the air is expanded in a turbine to produce refrigeration for liquefying the remaining air in the separation column.

The main steps described are air filtration/compression, cooling, dewatering/decarbonation using PSA, cryogenic separation in distillation columns, oxygen extraction and storage.

Cryogenic air separation plant

HPO oxygen production

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Supervision system graphic page
„ here enclosed is shown as example a graphic page of
skid1-skid2

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Introduction
„ Our company has developed on site HPO
(high pressure oxygen) oxygen production
plant skids mounted achieving a purity more
than 99.6 % by vol.

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Process description
„ Our oxygen generator is based on air fractioning to separate the gas on liquid form from the air.
The main steps of the process are as follows
1. Air filtration and compression till to 10 bar
2. AIr cooling till to 7-10°C with a condensate separation using a chiller unit
3. Air dewatering and decarbonation using a PSA unit using activated alumina for water and molecular
sieves for CO2
4. Cryogenic separation. Part of inlet air after a cooling in the Main Exchanger is expanded using a
turbine to produce the frigories need for LOX production.
The other part of air feed is partialy liquefied in the Main exchanger and is totaly liquefied in the
bottom reboiler of the column. The liquid air is sub cooled using the top stream of the column and
,after a lamination ,will be fed into the fractioning column. The liquid oxygen will be extracted from
the bottom of the column. To avoid the danger of the concentration of the hydrocarbon in the
bottom of the column ands adsorbent vessel will be installed on the column.
The gaseous stream of the top of the column and the stream coming from expansion turbine will be
collected to the Main exchanger for frigories recovery. A air coming from the turbine will be collected
on compressor suction.
5. The stream of the poore oxygen air is partially used for the rigeneration of PSA using an electrical
resistance for incresing the temperature.
6. The liquid oxygen is collected into a storage tank , pumped till to 200 bar, vaporized using an
atmospheric high pressure vaporizer and fed into the cylinders

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Process flow sheet
„ Here enclosed is shown the process flow
sheet

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Plant photos
„ 1. Cold Box

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Plant photos
„ 2 Cold box

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Plant photos
„ 3.Cold box

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Plant photos
„ 4 Cold box

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Plant photos
„ 5. PSA and chiller skid

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Plant photos
„ 6. PSA and chiller skid

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P&ID’s
„ 1.0 Here it is enclosed the Air purification P&ID as example
for the documentation

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Lay out
„ Here it is enclosed one example of HPO plant lay
out

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