Cryogenic Air Separation
Cryogenic Air Separation
Cryogenic Air Separation
16/01/2006 1
Supervision system graphic page
here enclosed is shown as example a graphic page of
skid1-skid2
16/01/2006 2
Introduction
Our company has developed on site HPO
(high pressure oxygen) oxygen production
plant skids mounted achieving a purity more
than 99.6 % by vol.
16/01/2006 3
Process description
Our oxygen generator is based on air fractioning to separate the gas on liquid form from the air.
The main steps of the process are as follows
1. Air filtration and compression till to 10 bar
2. AIr cooling till to 7-10°C with a condensate separation using a chiller unit
3. Air dewatering and decarbonation using a PSA unit using activated alumina for water and molecular
sieves for CO2
4. Cryogenic separation. Part of inlet air after a cooling in the Main Exchanger is expanded using a
turbine to produce the frigories need for LOX production.
The other part of air feed is partialy liquefied in the Main exchanger and is totaly liquefied in the
bottom reboiler of the column. The liquid air is sub cooled using the top stream of the column and
,after a lamination ,will be fed into the fractioning column. The liquid oxygen will be extracted from
the bottom of the column. To avoid the danger of the concentration of the hydrocarbon in the
bottom of the column ands adsorbent vessel will be installed on the column.
The gaseous stream of the top of the column and the stream coming from expansion turbine will be
collected to the Main exchanger for frigories recovery. A air coming from the turbine will be collected
on compressor suction.
5. The stream of the poore oxygen air is partially used for the rigeneration of PSA using an electrical
resistance for incresing the temperature.
6. The liquid oxygen is collected into a storage tank , pumped till to 200 bar, vaporized using an
atmospheric high pressure vaporizer and fed into the cylinders
16/01/2006 4
Process flow sheet
Here enclosed is shown the process flow
sheet
16/01/2006 5
Plant photos
1. Cold Box
16/01/2006 6
Plant photos
2 Cold box
16/01/2006 7
Plant photos
3.Cold box
16/01/2006 8
Plant photos
4 Cold box
16/01/2006 9
Plant photos
5. PSA and chiller skid
16/01/2006 10
Plant photos
6. PSA and chiller skid
16/01/2006 11
P&ID’s
1.0 Here it is enclosed the Air purification P&ID as example
for the documentation
16/01/2006 12
Lay out
Here it is enclosed one example of HPO plant lay
out
16/01/2006 13